CN103360069A - 锆钛酸铅b位铌锑复合取代改性的压电陶瓷及其制备方法 - Google Patents
锆钛酸铅b位铌锑复合取代改性的压电陶瓷及其制备方法 Download PDFInfo
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- CN103360069A CN103360069A CN2013103016488A CN201310301648A CN103360069A CN 103360069 A CN103360069 A CN 103360069A CN 2013103016488 A CN2013103016488 A CN 2013103016488A CN 201310301648 A CN201310301648 A CN 201310301648A CN 103360069 A CN103360069 A CN 103360069A
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- piezoelectric ceramics
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- piezoelectric ceramic
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- 239000000919 ceramic Substances 0.000 title claims abstract description 74
- CYVNAGQFZFNZEZ-UHFFFAOYSA-N [Nb].[Sb] Chemical compound [Nb].[Sb] CYVNAGQFZFNZEZ-UHFFFAOYSA-N 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title abstract description 9
- 239000002131 composite material Substances 0.000 title abstract 5
- 238000006467 substitution reaction Methods 0.000 title abstract 4
- 229910052451 lead zirconate titanate Inorganic materials 0.000 title abstract 3
- HFGPZNIAWCZYJU-UHFFFAOYSA-N lead zirconate titanate Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[Ti+4].[Zr+4].[Pb+2] HFGPZNIAWCZYJU-UHFFFAOYSA-N 0.000 title abstract 2
- 238000012986 modification Methods 0.000 claims abstract description 21
- 230000004048 modification Effects 0.000 claims abstract description 21
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims abstract description 19
- 229910052709 silver Inorganic materials 0.000 claims abstract description 19
- 239000004332 silver Substances 0.000 claims abstract description 19
- 238000005245 sintering Methods 0.000 claims abstract description 13
- 230000010287 polarization Effects 0.000 claims abstract description 8
- 238000002156 mixing Methods 0.000 claims abstract description 6
- 239000010955 niobium Substances 0.000 claims description 37
- 239000000758 substrate Substances 0.000 claims description 26
- 238000000034 method Methods 0.000 claims description 22
- 238000010792 warming Methods 0.000 claims description 17
- 150000001875 compounds Chemical group 0.000 claims description 15
- 239000000843 powder Substances 0.000 claims description 14
- 239000002994 raw material Substances 0.000 claims description 13
- 238000000498 ball milling Methods 0.000 claims description 9
- 238000010304 firing Methods 0.000 claims description 9
- 238000009413 insulation Methods 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 8
- 239000000463 material Substances 0.000 claims description 7
- 238000006243 chemical reaction Methods 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical group O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 239000008367 deionised water Substances 0.000 claims description 5
- 229910021641 deionized water Inorganic materials 0.000 claims description 5
- 229910010413 TiO 2 Inorganic materials 0.000 claims description 4
- 230000005684 electric field Effects 0.000 claims description 4
- 230000008569 process Effects 0.000 claims description 4
- 238000005303 weighing Methods 0.000 claims description 4
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 3
- 238000005266 casting Methods 0.000 claims description 3
- 239000011248 coating agent Substances 0.000 claims description 3
- 238000000576 coating method Methods 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 238000000465 moulding Methods 0.000 claims description 3
- 238000004080 punching Methods 0.000 claims description 3
- 238000007650 screen-printing Methods 0.000 claims description 3
- 238000005406 washing Methods 0.000 claims description 3
- 230000002194 synthesizing effect Effects 0.000 claims 1
- 229920002994 synthetic fiber Polymers 0.000 claims 1
- 238000003786 synthesis reaction Methods 0.000 abstract description 14
- 230000015572 biosynthetic process Effects 0.000 abstract description 10
- 229910010293 ceramic material Inorganic materials 0.000 abstract 1
- 238000009740 moulding (composite fabrication) Methods 0.000 abstract 1
- 230000008878 coupling Effects 0.000 description 13
- 238000010168 coupling process Methods 0.000 description 13
- 238000005859 coupling reaction Methods 0.000 description 13
- 230000000052 comparative effect Effects 0.000 description 12
- 238000012360 testing method Methods 0.000 description 10
- 230000008859 change Effects 0.000 description 8
- 230000003247 decreasing effect Effects 0.000 description 4
- 238000004891 communication Methods 0.000 description 3
- 238000007766 curtain coating Methods 0.000 description 3
- 238000011161 development Methods 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 230000006978 adaptation Effects 0.000 description 1
- 238000012271 agricultural production Methods 0.000 description 1
- 230000003321 amplification Effects 0.000 description 1
- 229910052787 antimony Inorganic materials 0.000 description 1
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910002056 binary alloy Inorganic materials 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000003990 capacitor Substances 0.000 description 1
- 238000013480 data collection Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 239000011812 mixed powder Substances 0.000 description 1
- 229910052758 niobium Inorganic materials 0.000 description 1
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 description 1
- 238000003199 nucleic acid amplification method Methods 0.000 description 1
- 230000008447 perception Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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- Compositions Of Oxide Ceramics (AREA)
Abstract
Description
(Sb1/2Nb1/2)的取代量X | 合成反应温度℃ | |
实施例1-1 | 0.03 | 900 |
实施例1-2 | 0.05 | 900 |
实施例1-3 | 0.06 | 900 |
对比例1 | 0 | 900 |
实施例2-1 | 0.03 | 950 |
实施例2-2 | 0.05 | 950 |
实施例2-3 | 0.06 | 950 |
对比例2 | 0 | 950 |
实施例3-1 | 0.03 | 980 |
实施例3-2 | 0.05 | 980 |
实施例3-3 | 0.06 | 980 |
对比例3 | 0 | 980 |
εT 33/ε0 | d33(pC/N) | KP(%) | tanδ(%) | |
实施例1-1 | 1750 | 332 | 65 | 2.5 |
实施例1-2 | 1920 | 352 | 70 | 2.3 |
实施例1-3 | 1850 | 335 | 64 | 2.4 |
对比例1 | 1580 | 320 | 60 | 2.9 |
实施例2-1 | 1820 | 348 | 68 | 2.3 |
实施例2-2 | 1920 | 360 | 73 | 2.3 |
实施例2-3 | 1880 | 352 | 68 | 2.6 |
对比例2 | 1760 | 335 | 63 | 2.6 |
实施例3-1 | 1780 | 348 | 65 | 2.4 |
实施例3-2 | 1930 | 350 | 70 | 2.3 |
实施例3-3 | 1600 | 330 | 63 | 2.7 |
对比例3 | 1570 | 342 | 62 | 2.7 |
Claims (10)
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CN201310301648.8A CN103360069B (zh) | 2013-07-17 | 2013-07-17 | 锆钛酸铅b位铌锑复合取代改性的压电陶瓷及其制备方法 |
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103787656A (zh) * | 2013-12-26 | 2014-05-14 | 常州波速传感器有限公司 | 高灵敏度压电陶瓷片配方及制备方法 |
CN108104802A (zh) * | 2017-12-08 | 2018-06-01 | 重庆举程科技发展有限公司 | 一种超声波转能器 |
CN114075073A (zh) * | 2020-08-17 | 2022-02-22 | 中国科学院上海硅酸盐研究所 | 一种PZT-Pb(Sb1/2Nb1/2)三元系压电陶瓷材料及其制备方法和应用 |
CN114591082A (zh) * | 2022-04-19 | 2022-06-07 | 东莞理工学院 | 一种pzt-pnn-psn-pmn压电陶瓷及其制备方法 |
CN114619132A (zh) * | 2022-04-20 | 2022-06-14 | 无锡市惠丰电子有限公司 | 大推力驱动片及其制备方法 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103073289A (zh) * | 2013-01-25 | 2013-05-01 | 瑞声声学科技(深圳)有限公司 | 压电陶瓷材料、烧结体、压电陶瓷器件及其制备方法 |
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Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103073289A (zh) * | 2013-01-25 | 2013-05-01 | 瑞声声学科技(深圳)有限公司 | 压电陶瓷材料、烧结体、压电陶瓷器件及其制备方法 |
Non-Patent Citations (1)
Title |
---|
黄新友等: "三方/四方相共存铌锑锆钛酸铅压电陶瓷极化的研究", 《硅酸盐学报》, vol. 29, no. 5, 31 October 2001 (2001-10-31) * |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103787656A (zh) * | 2013-12-26 | 2014-05-14 | 常州波速传感器有限公司 | 高灵敏度压电陶瓷片配方及制备方法 |
CN108104802A (zh) * | 2017-12-08 | 2018-06-01 | 重庆举程科技发展有限公司 | 一种超声波转能器 |
CN114075073A (zh) * | 2020-08-17 | 2022-02-22 | 中国科学院上海硅酸盐研究所 | 一种PZT-Pb(Sb1/2Nb1/2)三元系压电陶瓷材料及其制备方法和应用 |
CN114591082A (zh) * | 2022-04-19 | 2022-06-07 | 东莞理工学院 | 一种pzt-pnn-psn-pmn压电陶瓷及其制备方法 |
CN114619132A (zh) * | 2022-04-20 | 2022-06-14 | 无锡市惠丰电子有限公司 | 大推力驱动片及其制备方法 |
CN114619132B (zh) * | 2022-04-20 | 2024-04-09 | 无锡市惠丰电子有限公司 | 大推力驱动片及其制备方法 |
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Address after: 526060 Guangdong city of Zhaoqing province Donggang Huanggang town Duanzhou District village before the Temple Road South Patentee after: GUANGDONG JC TECHNOLOGICAL INNOVATION ELECTRONICS Co.,Ltd. Address before: 526060 Guangdong city of Zhaoqing province Donggang Huanggang town Duanzhou District village before the Temple Road South Patentee before: Guangdong Jiecheng Kechuang Electronics Co. Address after: 526060 Guangdong city of Zhaoqing province Donggang Huanggang town Duanzhou District village before the Temple Road South Patentee after: Guangdong Jiecheng Kechuang Electronics Co. Address before: 526060 Guangdong city of Zhaoqing province Donggang Huanggang town Duanzhou District village before the Temple Road South Patentee before: JC ELECTRONIC TECHNOLOGY Co.,Ltd. |
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Denomination of invention: Lead zirconate titanate B-site niobium antimony composite substitution modified piezoelectric ceramics and its preparation method Effective date of registration: 20210519 Granted publication date: 20141217 Pledgee: Zhaoqing Rural Commercial Bank Co.,Ltd. Chengxi sub branch Pledgor: GUANGDONG JC TECHNOLOGICAL INNOVATION ELECTRONICS Co.,Ltd. Registration number: Y2021980003778 |
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Date of cancellation: 20230522 Granted publication date: 20141217 Pledgee: Zhaoqing Rural Commercial Bank Co.,Ltd. Chengxi sub branch Pledgor: GUANGDONG JC TECHNOLOGICAL INNOVATION ELECTRONICS Co.,Ltd. Registration number: Y2021980003778 |
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Denomination of invention: Piezoelectric Ceramics Modified by Lead Zirconate Titanate B Site Niobium Antimony Composite Substitution and Its Preparation Method Effective date of registration: 20230524 Granted publication date: 20141217 Pledgee: Zhaoqing Rural Commercial Bank Co.,Ltd. Chengxi sub branch Pledgor: GUANGDONG JC TECHNOLOGICAL INNOVATION ELECTRONICS Co.,Ltd. Registration number: Y2023980041618 |