CN103352293B - Flame-retardant and fireproof fabric, and processing technology and textile thereof - Google Patents
Flame-retardant and fireproof fabric, and processing technology and textile thereof Download PDFInfo
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Abstract
The invention relates to flame-retardant and fireproof fabric, and a processing technology and textile thereof. Warp yarns adopt wool tops formed by blending flame-retardant acrylic, flame viscose, fine-denier polyester and aramid fiber 1313 fiber; weft yarns adopt wool tops formed by blending alginate fiber, polyphenylene sulfide, polysulfonamide and phenolic fiber; then the warp yarns and the weft yarns form the flame-retardant and fireproof fabric through steps of dyeing, fixation, rinsing, sizing, weaving, desizing, rinsing, drying, baking, full decatizing and the like. The fabric has the characteristics of simple processing technology, good flame-retardant effect and the like, and can be applied to apparel, home textile, sports goods, medical care and fireproof fabric.
Description
Technical field
The present invention relates to a kind of fireproof facing material field, be specifically related to the application on a kind of flame-proof fireproof facing material, processing technology and fabric thereof.
Background technology
Sound along with expanding economy and state legal system, flame retardant textiles apply the attention that will cause the whole society.Abroad to the exploitation of flame-retardant textile and study more, some industrially developed country have just formulated the flame retardant regulation of textiles as far back as 20 century 70s mid-term, and require more and more higher in recent years, specify more and more thinner.In recent years, the research and development of China to flame retardant textiles increase gradually, and have achieved sizable progress.Along with the quickening that urban modernization is built, the development of tourism, transportation, and the increase of export trade textiles demand, flame retardant textiles also exists huge potential market.
As far back as the sixties in 20th century so far, fire retardant market, the world experienced by a flourish stage, existing hundreds of different kinds at present, and BACN kind still emerges in an endless stream, but for the fire-retardant mainly halogen system of PET, phosphorus system and novel flame retardant polyester/inorganic nano composite material.Polyester fiber is the same with other thermoplastic synthetic fiber's materials, melted by heating, decomposition, burning, and has the phenomenon of melting drippage, and the limited oxygen index of polyster fibre is only about 21, does not reach flame-retardant standard requirement.From the beginning of the seventies in last century, along with a large amount of production and the application of polyester fiber, people start to note research and development flame-resistant terylene kind.Such as, du pont company, company of Japanese Japan, German Hirst company etc., successively have flame-resistant terylene commodity and patent to come out.After entering the eighties, external by the large-scale production of flame-resistant terylene kind, but technology used and key assistant---fire retardant externally holds in close confidence, this period, the research paper published, document is few, report with patent form in a large number, Dupont, Celanese, food machinery chemical company, Aksu company, Monsanto Company, the businessman of Japan, east is beautiful, Japan is spun, clock spins, Kuraray, Ai Kesi synthetic fibre, mitsubishi rayon, the Hirst of Germany, BASF, Baeyer, the DMS of Holland, the world-renowned companies such as Italy Snia, all successively apply for fire-retardant patented technology.Countries in the world are very active to the exploitation of the investigation and application of flame retardant polyester, and patent document continues to bring out, and the kind of various flame retardant polyester is also constantly come out, and has researched and developed ten hundreds of various fire retardants, and commercially produce also have tens kinds.But its production technology more complicated always.
Summary of the invention
The technical problem that the present invention mainly solves is to provide a kind of simple, can provide a kind of production technology of high-quality flame-proof fireproof facing material.
For solving the problems of the technologies described above, the technical scheme that the present invention adopts is:
A processing technology for High-flame-retardancfireproof fireproof fabric, comprises the following steps:
(1) functional yams lines are prepared: the wool top that warp thread adopts flame-retardant acrylic fibre, anti-flaming viscose, fine denier polyester, aramid fiber 1313 blending is made into, weft yarn adopts the wool top of alginate fibre, polyphenylene sulfide, PSA fiber, phenolic fibre blending, then warp thread and weft yarn is prepared from through blowing, opener, drafting, rove, spun yarn, winder twisting.
(2) dyeing, fixation, washing: adopt REACTIVE DYES to dye to functional yams lines, first at 40-50 DEG C, pre-treatment 10-15min is carried out, add releasing toner 15-20g/l, after rerunning 8-10 minute, re-use active dye fixing agent KS and do fixation treatment, then hot water wash and cold wash at normal temperatures at 35-45 DEG C respectively.
(3) sizing: warper beam unwinding-starching, temperature is the strand-oven dry of 70 DEG C-hygroscopic water, temperature 85 DEG C-dry leasing-winding, and tension force is 0.26mpa, moisture regain: 12.2%, and slurry therewith is acrylic size;
(4) weave cotton cloth: adopt knitting or weaving that the functional sliver after process is made into cloth.
(5) destarch, washing, oven dry: first bank up cloth in the destarch enzyme BF-7658 of 0.8-1.2G/L 50-60 minute, temperature controls at 40 DEG C-50 DEG C, then use the clear water of 20-30 DEG C to rinse 35-55 minute, finally dry in dryer, temperature controls at 70 DEG C-90 DEG C.
(5) antiflaming finishing agent is flooded: the temperature of dipping controls at about 30 DEG C, and the time is 7-8 hour, rear clean water 20 minutes.
(6) cure, tank steams: at 160-180 DEG C of temperature, cure 50-70s, then utilizes Two-way Cycle method to carry out tank and steams 140s, pressure: 0.9bar in controlling; External pressure: 1.3bar.
(7) finished product sizing.
The application of High-flame-retardancfireproof fireproof fabric in sports goods, health care, fire prevention
Wherein warp thread adopt flame-retardant acrylic fibre, anti-flaming viscose, fine denier polyester, aramid fiber 1313 percentage by weight be 20%:15%:30%:35%.The percentage by weight of the alginate fibre that weft yarn adopts, polyphenylene sulfide, PSA fiber, phenolic fibre is 30%:15%:25%:30%.Described antiflaming finishing agent is APP.Consumption is the 3-10% of fabric weight.
The invention has the beneficial effects as follows:
(1) the present invention adopts the multiple fiber blend with flame retardant effect to be formed by weaving, and flame retardant effect is remarkable.
(2) make fabric lining by warp thread and weft yarn blending, this processing mode makes fabric intensity stronger, and uses alginate fibre in the material used, and human metabolism can be impelled vigorous, make healthy.And aethiops vegetabilis fiber contains mineral matter and can release α ripple, make people's mental state loose and there is comfort.Aethiops vegetabilis fabric lining has insulation and health care double effects, and long-term dress makes human body molecule rub and produces thermal response, promotes health blood circulation, has a kind of effect of heat storing and heat preserving.Aethiops vegetabilis fiber also has insulation, antibacterial and odor-resistant result.
(3) in process, flood APP antiflaming finishing agent makes the flame retardant effect of fabric better.
Detailed description of the invention
Below preferred embodiment of the present invention is described in detail, can be easier to make advantages and features of the invention be readily appreciated by one skilled in the art, thus more explicit defining is made to protection scope of the present invention.
embodiment 1
A processing technology for flame-proof fireproof facing material, comprises the following steps:
(1) functional yams lines are prepared: the wool top that warp thread adopts flame-retardant acrylic fibre, anti-flaming viscose, fine denier polyester, aramid fiber 1313 blending is made into, weft yarn adopts the wool top of alginate fibre, polyphenylene sulfide, PSA fiber, phenolic fibre blending, then warp thread and weft yarn is prepared from through blowing, opener, drafting, rove, spun yarn, winder twisting.The percentage by weight of the flame-retardant acrylic fibre that warp thread adopts, anti-flaming viscose, fine denier polyester, aramid fiber 1313 is 20%:15%:30%:35%.The percentage by weight of the alginate fibre that weft yarn adopts, polyphenylene sulfide, PSA fiber, phenolic fibre is 30%:15%:25%:30%.
(2) dyeing, fixation, washing: adopt REACTIVE DYES to dye to functional yams lines, first at 40 DEG C, pre-treatment 15min is carried out, add releasing toner 15g/l, after rerunning 8 minutes, re-use active dye fixing agent KS and do fixation treatment, then hot water wash and cold wash at normal temperatures at 35 DEG C respectively.
(3) sizing: warper beam unwinding-starching, temperature is the strand-oven dry of 70 DEG C-hygroscopic water, temperature 85 DEG C-dry leasing-winding, and tension force is 0.26mpa, moisture regain: 12.2%, and slurry therewith is acrylic size;
(4) weave cotton cloth: adopt knitting or weaving that the functional sliver after process is made into cloth.
(5) destarch, washing, oven dry: first banked up 50 minutes in the destarch enzyme BF-7658 of 0.8-1.2G/L by cloth, temperature controls at 50 DEG C, then use the clear water of 20 DEG C to rinse 55 minutes, finally dry in dryer, temperature controls at 70 DEG C.
(5) antiflaming finishing agent is flooded: select antiflaming finishing agent to be APP, consumption is 3% of fabric weight;
The temperature of dipping controls at about 30 DEG C, and the time is 8 hours, rear clean water 20 minutes.
(6) cure, tank steams: at 160 DEG C of temperature, cure 70s, then utilizes Two-way Cycle method to carry out tank and steams 140s, pressure: 0.9bar in controlling; External pressure: 1.3bar.
(7) finished product sizing.
embodiment 2
A processing technology for flame-proof fireproof facing material, comprises the following steps:
(1) functional yams lines are prepared: the wool top that warp thread adopts flame-retardant acrylic fibre, anti-flaming viscose, fine denier polyester, aramid fiber 1313 blending is made into, weft yarn adopts the wool top of alginate fibre, polyphenylene sulfide, PSA fiber, phenolic fibre blending, then warp thread and weft yarn is prepared from through blowing, opener, drafting, rove, spun yarn, winder twisting.The percentage by weight of the flame-retardant acrylic fibre that warp thread adopts, anti-flaming viscose, fine denier polyester, aramid fiber 1313 is 20%:15%:30%:35%.The percentage by weight of the alginate fibre that weft yarn adopts, polyphenylene sulfide, PSA fiber, phenolic fibre is 30%:15%:25%:30%.
(2) dyeing, fixation, washing: adopt REACTIVE DYES to dye to functional yams lines, first at 45 DEG C, pre-treatment 13min is carried out, add releasing toner 18g/l, after rerunning 9 minutes, re-use active dye fixing agent KS and do fixation treatment, then hot water wash and cold wash at normal temperatures at 40 DEG C respectively.
(3) sizing: warper beam unwinding-starching, temperature is the strand-oven dry of 70 DEG C-hygroscopic water, temperature 85 DEG C-dry leasing-winding, and tension force is 0.26mpa, moisture regain: 12.2%, and slurry therewith is acrylic size;
(4) weave cotton cloth: adopt knitting or weaving that the functional sliver after process is made into cloth.
(5) destarch, washing, oven dry: first banked up 55 minutes in the destarch enzyme BF-7658 of 0.8-1.2G/L by cloth, temperature controls at 45 DEG C, then use the clear water of 25 DEG C to rinse 45 minutes, finally dry in dryer, temperature controls at 80 DEG C.
(5) antiflaming finishing agent is flooded: select antiflaming finishing agent to be APP, consumption is 6% of fabric weight;
The temperature of dipping controls at about 30 DEG C, and the time is 7.5 hours, rear clean water 20 minutes.
(6) cure, tank steams: at 170 DEG C of temperature, cure 60s, then utilizes Two-way Cycle method to carry out tank and steams 140s, pressure: 0.9bar in controlling; External pressure: 1.3bar.
(7) finished product sizing.
embodiment 3
A processing technology for flame-proof fireproof facing material, comprises the following steps:
(1) functional yams lines are prepared: the wool top that warp thread adopts flame-retardant acrylic fibre, anti-flaming viscose, fine denier polyester, aramid fiber 1313 blending is made into, weft yarn adopts the wool top of alginate fibre, polyphenylene sulfide, PSA fiber, phenolic fibre blending, then warp thread and weft yarn is prepared from through blowing, opener, drafting, rove, spun yarn, winder twisting.The percentage by weight of the flame-retardant acrylic fibre that warp thread adopts, anti-flaming viscose, fine denier polyester, aramid fiber 1313 is 20%:15%:30%:35%.The percentage by weight of the alginate fibre that weft yarn adopts, polyphenylene sulfide, PSA fiber, phenolic fibre is 30%:15%:25%:30%.
(2) dyeing, fixation, washing: adopt REACTIVE DYES to dye to functional yams lines, first at 50 DEG C, pre-treatment 10min is carried out, add releasing toner 18g/l, after rerunning 10 minutes, re-use active dye fixing agent KS and do fixation treatment, then hot water wash and cold wash at normal temperatures at 45 DEG C respectively.
(3) sizing: warper beam unwinding-starching, temperature is the strand-oven dry of 70 DEG C-hygroscopic water, temperature 85 DEG C-dry leasing-winding, and tension force is 0.26mpa, moisture regain: 12.2%, and slurry therewith is acrylic size;
(4) weave cotton cloth: adopt knitting or weaving that the functional sliver after process is made into cloth.
(5) destarch, washing, oven dry: first banked up 60 minutes in the destarch enzyme BF-7658 of 0.8-1.2G/L by cloth, temperature controls at 40 DEG C, then use the clear water of 30 DEG C to rinse 35 minutes, finally dry in dryer, temperature controls at 90 DEG C.
(5) antiflaming finishing agent is flooded: select antiflaming finishing agent to be APP, consumption is 10% of fabric weight;
The temperature of dipping controls at about 30 DEG C, and the time is 8 hours, rear clean water 20 minutes.
(6) cure, tank steams: at 180 DEG C of temperature, cure 50s, then utilizes Two-way Cycle method to carry out tank and steams 140s, pressure: 0.9bar in controlling; External pressure: 1.3bar.
(7) finished product sizing.
Carry out following several test to the finished product fabric in embodiment respectively, result is as shown in table 1:
The technical indicator of flame-proof fireproof facing material test in table 1 the present invention
| Contrast | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| After flame time (s) | 3.5 | 3.4 | 3.3 |
| Char length (mm) | 93 | 94 | 92 |
| Wear-resistant index (level) | 4 | 4 | 4.5 |
| Radial tearing brute force | 67 | 65 | 72 |
| Dimension is to tearing brute force | 62 | 67 | 68 |
| Fabric quality ratio resistance Ω g/cm 2 | 7.2×10 11 | 5.3×10 11 | 5.7×10 11 |
Note: 1, wear-resistant index: fabric is anti-fluffing and anti-pilling grade after 36000 frictions; 2, tearing brute force: size of sample is 81 × 66/time, yams is 32S/3 × 2S/2
Claims (2)
1. a processing technology for High-flame-retardancfireproof fireproof fabric, comprises the following steps:
(1) functional yams lines are prepared: the wool top that warp thread adopts flame-retardant acrylic fibre, anti-flaming viscose, fine denier polyester, aramid fiber 1313 blending is made into, weft yarn adopts the wool top of alginate fibre, polyphenylene sulfide, PSA fiber, phenolic fibre blending, then warp thread and weft yarn is prepared from through blowing, opener, drafting, rove, spun yarn, winder twisting; The percentage by weight of the flame-retardant acrylic fibre that warp thread adopts, anti-flaming viscose, fine denier polyester, aramid fiber 1313 is 20%:15%:30%:35%; The percentage by weight of the alginate fibre that weft yarn adopts, polyphenylene sulfide, PSA fiber, phenolic fibre is 30%:15%:25%:30%;
(2) dyeing, fixation, washing: adopt REACTIVE DYES to dye to functional yams lines, first at 40 DEG C, pre-treatment 15min is carried out, add releasing toner 15g/l, after rerunning 8 minutes, re-use active dye fixing agent KS and do fixation treatment, then hot water wash and cold wash at normal temperatures at 35 DEG C respectively;
(3) sizing: warper beam unwinding-starching, temperature is the strand-oven dry of 70 DEG C-hygroscopic water, temperature 85 DEG C-dry leasing-winding, and tension force is 0.26mpa, moisture regain: 12.2%, and slurry therewith is acrylic size;
(4) weave cotton cloth: adopt knitting or weaving that the functional sliver after process is made into cloth;
(5) destarch, washing, oven dry: first banked up 50 minutes in the destarch enzyme BF-7658 of 0.8-1.2G/L by cloth, temperature controls at 50 DEG C, then use the clear water of 20 DEG C to rinse 55 minutes, finally dry in dryer, temperature controls at 70 DEG C;
(6) antiflaming finishing agent is flooded: select antiflaming finishing agent to be APP, consumption is 3% of fabric weight;
The temperature of dipping controls at 30 DEG C, and the time is 8 hours, rear clean water 20 minutes;
(7) cure, tank steams: at 160 DEG C of temperature, cure 70s, then utilizes Two-way Cycle method to carry out tank and steams 140s, pressure: 0.9bar in controlling; External pressure: 1.3bar;
(8) finished product sizing.
2. the High-flame-retardancfireproof fireproof fabric produced according to claim 1 spins the application in articles for use, sports goods, health care in clothes, family.
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| CN104131393A (en) * | 2014-06-06 | 2014-11-05 | 南通纺科纺织科技有限公司 | Flame-retardant fabric and processing technique thereof |
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Effective date of registration: 20181109 Address after: 201318 No. 638 Jianyun Road, No. 600 Shenmei Road, Pudong New Area, Shanghai, 2 buildings and 4 buildings Patentee after: Shanghai Zanray Industrial Co., Ltd. Address before: No. 72 Hongshan Road, Qingyang Street, Jinjiang City, Quanzhou City, Fujian Province Patentee before: Jinjiang Mingao Textile Science & Technology Co., Ltd. |