CN103299985A - Cantharias specimen and making method thereof - Google Patents
Cantharias specimen and making method thereof Download PDFInfo
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- CN103299985A CN103299985A CN2013102016353A CN201310201635A CN103299985A CN 103299985 A CN103299985 A CN 103299985A CN 2013102016353 A CN2013102016353 A CN 2013102016353A CN 201310201635 A CN201310201635 A CN 201310201635A CN 103299985 A CN103299985 A CN 103299985A
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Abstract
The invention discloses a making method of an artificial cantharias specimen which is made by taking urea-formaldehyde resin as a main raw material and sodium hydroxide and glacial acetic acid as auxiliary raw materials. The making method comprises the following steps of: synthesizing a urea-formaldehyde resin raw monomer, pre-treating insects, preparing a ripe monomer, preparing a mould, fixing and embedding an insect sample, demoulding and polishing, wherein the raw monomer is formed by adding sodium hydroxide and glacial acetic acid into formaldehyde and urea as raw materials and then polymerizing, and the proportion of the formaldehyde to the urea is equal to 55:18 to 50:22; the urea-formaldehyde resin has the shrinking percentage of 5-20%, the hardening time of 2-5d and the bubbling number of 0-5; and the ripe monomer is prepared by mixing the liquid urea-formaldehyde glue of the raw monomer and an extension agent, adding glacial acetic acid and stirring, wherein the extension agent is selected from polyethylene glycol 600, DEHP (Di 2-Ethyl Hexyl Phthalate) and DINP (Diisononyl Phthalate). The making method disclosed by the invention is simple and rapid in process, low in cost and the raw materials are easy to purchase; and a sample is high in strength and good in toughness, glossiness and transparency.
Description
Technical field
The present invention relates to a kind of handicraft manufacturing technology, be specifically related to a kind of insect specimen and preparation method thereof.
Background technology
The cantharias sample had both had permanent preservation insect material and also can further be made as simultaneously and wear ornaments, the small-sized handicraft of viewing and admiring, and tourist item has scientific research value and market value concurrently.The manufacture craft horizontal relationship of cantharias sample.The preservation effect of sample, ornamental value and cost of manufacture.Chinese patent CN3134935.8 has put down in writing a kind of ambroid and manufacturing process, and its inventive point is to be mixed into main material with multiple unsaturated-resin, add curing agent, and other auxiliary material make; The forming method of ambroid is the mould molding that overturns fast; Unsaturated-resin is the unsaturated resin that second dihydroxylic alcohols, propane diols form for the raw material condensation.It is main material that CN96111164.X has put down in writing a certain proportion of unsaturated polyester resin, be batching with a certain proportion of cyclohexanone peroxide and cobalt naphthenate, and can add an amount of color paste deployment and become homogenate, be mixed with the embedding body, earlier in mould, pour into the resin for preparing in right amount and make bottom, put into treated natural exsiccata again, bury, form after the parison demoulding technology of ambroid again through repeatedly watering.CN201110409629.8 has put down in writing that " methyl methacrylate, methacrylic acid, methacrylic acid function monomer and initator synthesize high transparent pre-polymerization resin, and initator is a kind of in benzoyl peroxide, dilauroyl peroxide, peroxidized t-butyl perbenzoate and the azo-bis-isobutyl cyanide.High transparent pre-polymerization resin and composite initiator mix, and injection molding, 20-50 ℃ of baking bottoming in 6-24 hour, injection molding again, 6-24 hour fixed preparation of 20-50 ℃ of baking, envelope is buried insect, the demoulding, 60-100 ℃ of heating slaking in 12-36 hour forms " technology.In the above-mentioned technology, be that raw material or unsaturated-resin are that main material is made artificial cantharias sample with methyl methacrylate, its cost of material height, complex manufacturing technology, fabrication cycle is long, has limited the promotion and application of ambroid sample in preparation of specimen of entomology specialized laboratory.The cantharias of making is easy to change, turn white, be out of shape, and has a strong impact on quality and the ornamental value of product.
Summary of the invention
The present invention aims to provide a kind of high strength, transparency is good, color and luster is bright and new ambroid sample, and a kind ofly makes artificial cantharias manufacturing process simple, quick, with low cost.
For achieving the above object, the present invention is by the following technical solutions:
A kind of artificial cantharias sample, main material is Lauxite, also comprises auxiliary material sodium hydroxide, glacial acetic acid and other auxiliary materials.
In the above-mentioned artificial cantharias sample, Lauxite is to be that raw material mixes the back living monomer that generates of polymerization reaction take place by a certain percentage with formaldehyde, urea, and wherein the ratio of formaldehyde and urea is 55: 18～50: 22.
A kind of manufacture method of artificial cantharias comprises the following steps:
(7) the synthetic monomer of giving birth to,
(8) preliminary treatment of insect
(9) prepare ripe monomer by giving birth to monomer,
(10) preparation of mould;
(11) the fixing and embedding of insect specimen;
(12) demoulding and post processing.
In the step (1), the main material of giving birth to monomer is Lauxite, and auxiliary material comprises sodium hydroxide, glacial acetic acid.Wherein, Lauxite is that formaldehyde, urea are the living monomer that polymerizable raw material forms, the formaldehyde that polymerisation is used and urea ratio 50-55: 18-22.
The reaction method of polymerization is the sodium hydroxide 0.1-0.2ml that adds 10-30% in the time of 20-30 ℃, and reaction system PH is 7-8, keeps 0.25 hour; Add glacial acetic acid 0.1-1ml in the time of 70-100 ℃, reaction system is 4-5, keeps 0.3 hour; The end condition of described polymerisation adds in the normal-temperature water for being stained with a reactant liquor, and the phenomenon that hazes stops heating immediately, adds 0.1-0.5ml10-30% sodium hydroxide and stops reaction.
Wherein the shrinkage factor of Lauxite is 5%-20%, and firm time is 2-5d, and the foaming number is 0-5.
In the step (3), the method for preparing ripe monomer is to get above-mentioned living monomer liquid urea-formaldehyde glue 1-5 part for preparing: extension agent 1-5 part; After mixing fully stirring, add the stirring of 10%-15% glacial acetic acid and namely generate ripe monomer.Wherein extension agent is selected from a kind of among Macrogol 600, DEHP and the DINP, preferred Macrogol 600, and the no color or smell thick liquid is to waxy solid.Water-soluble, ethanol and many other organic solvents.Steam forces down.To thermally-stabilised.Inoperative with many chemicals, not hydrolysis is never degenerated.Nontoxic, eyes and skin there are not obvious stimulation.Can be used as plasticizer, softening agent, humidizer, and be used for pharmacy cream and medicine etc.
DEHP, no color or smell liquid.Water insoluble, be dissolved in ether, ethanol, mineral wet goods, this product has good comprehensive performances, good mixing property, the plasticizing efficiency height, volatility is lower, and low-temperature pliability is better, water-fast extraction, the electric property height, warm tolerance and weather resistance are good.But poisonous, sex entanglement, sexual organ are shortened, harm male reproductive function etc.
DINP, oily liquids, water insoluble.Have good anti-migration performance, anti-extraction ability, resistance to elevated temperatures.The at present domestic producer that does not have a family to produce DINP, required INA all comes from import.And long-term a large amount of meeting generation internal secretion interference effect of taking in, reproduction and maldevelopment can be caused, and animal liver cancer can be brought out.
In the step (4), mould is fixed on the wax layer and is poured into a mould primer and make for adopting lucite and slide, cover glass to be produced on.Adopt a complete poly (methyl methacrylate) plate to make base plate, to the candle liquid of its bottom surface shop one deck liquefied petrolatum or thawing, adopt slide and cover glass to be fixed into the mould that varies in size at the wax layer earlier.
In the step (5), earlier the ripe monomer of part is poured into mold bottom, is used for sealed mold and primer and makes, primer thickness 2～5mm, treat colloid solidification after, namely can be used for specimen embedding.
The insect specimen that handle well early stage is put into primer central authorities, but for preventing sample drift fixed preparation.The method of fixed preparation comprise insect needle fix, directly fixing and sticking cemented fixed, preferably directly insert sample with insect needle and be used for fixing sample; Again the content of want embedding is fixed on the position of mould regulation.Gradation pours into the mould envelope with ripe monomer and buries insect, the each cast of control thickness 2～5mm, all want sealed mold after each the feeding in raw material, in 25～37 ℃ of the normal temperature 1-2 hour, allow ripe monomer form the transparent body of toughness, just can descend cast together, continue to pour into ripe monomer again, according to the number of times of the content diverse location of placing and the ripe monomer of quantity decision cast.Up to the thickness that the insect envelope is buried fully and reached regulation.After treating last colloid solidification, rotatable insect needle also takes out pin and removes mould, solidifies fully until sample.
In the step (6), post processing is to adopt sander and polishing machine to carry out last polishing, the post processing of polishing, namely finishes the making engineering of ambroid sample.
The present invention is that the Lauxite that forms with formaldehyde and urea polymerization is main material, adds auxiliary materials such as curing agent and extension agent thereof and makes; Make releasing agent after adopting the liquefaction of paraffin and candle.
Beneficial effect of the present invention mainly contains:
1, this artificial cantharias preparation of specimen technology is simple, fast, and with low cost and raw material is easily purchased;
2, the artificial cantharias specimen samples intensity height of Zhi Zuoing, good toughness, glossiness and transparency are good.
Embodiment
Below technical scheme of the present invention is made further explanation, but do not limit the scope of the invention, the used preparation raw material of the present invention is commercially available.
Embodiment 1
(1) Lauxite is given birth to the synthetic of monomer: formaldehyde and urea (52: 19) are mixed by mass percentage, when formaldehyde dissolves, constantly stir, the sodium hydroxide 0.15ml of adding 20% in the time of 25 ℃, to reaction system PH be 7, keep 0.1h; In the time of 85 ℃, add glacial acetic acid 0.5ml, to reaction system PH be 4, keep 0.1h; Be stained with a reactant liquor and add in the normal-temperature water, the phenomenon that hazes just stops heating, adds 0.25ml20% sodium hydroxide and stops reaction, and synthetic urea-formaldehyde resin is given birth to monomer.
(2) preliminary treatment of insect: insect places the living monomer soaked overnight of Lauxite standby after whole limb, 60 ℃ of oven dry are handled.
(3) preparation of ripe monomer: get 3 parts of the above-mentioned living monomer liquid urea-formaldehyde glues for preparing: 3 parts of Macrogol 600s; After mixing fully stirring, add the stirring of 12% glacial acetic acid and namely generate ripe monomer, i.e. ripe monomer.
(4) preparation of mould: this research adopts a complete poly (methyl methacrylate) plate to make base plate, spread the candle liquid of one deck liquefied petrolatum or thawing earlier to its bottom surface, adopt slide and cover glass to be fixed into the mould that varies in size at the wax layer, a small amount of glue is used for seam and primer is made, after treating colloid solidification, namely can be used for specimen embedding.
(5) embedding of insect specimen: the insect specimen that handle well early stage is put into primer central authorities, can directly insert sample with insect needle and be used for fixing sample for preventing the sample drift, gradation pours into the mould envelope with ripe monomer and buries insect, the each cast of control thickness 2mm, all want sealed mold after each the feeding in raw material, in the normal temperature 1-2 hour, allow ripe monomer form the transparent body of toughness, just can descend cast together, continue to pour into ripe monomer again, according to the number of times of the content diverse location of placing and the ripe monomer of quantity decision cast.Setting temperature is after 30 ℃ of normal temperature are treated last colloid solidification, and rotatable insect needle also takes out pin and removes mould, solidifies fully until sample.
(6) polishing, polishing: adopt sander and polishing machine to carry out last polishing, the post processing of polishing, namely finish the making engineering of ambroid sample.
Embodiment 2.
(1) Lauxite is given birth to the synthetic of monomer: formaldehyde and urea (50: 22) are mixed by mass percentage, when formaldehyde dissolves, constantly stir, the sodium hydroxide 0.1ml of adding 10% in the time of 25 ℃, to reaction system PH be 7, keep 0.25h; In the time of 85 ℃, add glacial acetic acid 1ml, to reaction system PH be 4, keep 0.3h; Be stained with a reactant liquor and add in the normal-temperature water, the phenomenon that hazes just stops heating, adds 0.1ml10% sodium hydroxide and stops reaction, and synthetic urea-formaldehyde resin is given birth to monomer.
(2) preliminary treatment of insect: insect places Lauxite 1 living monomer soaked overnight standby after whole limb, 60 ℃ of oven dry are handled.
(3) preparation of ripe monomer: get 1 part of the above-mentioned living monomer liquid urea-formaldehyde glue for preparing: 3 parts of Macrogol 600s; After mixing fully stirring, add the stirring of 10% glacial acetic acid and namely generate ripe monomer, i.e. ripe monomer.
(4) preparation of mould: this research adopts a complete poly (methyl methacrylate) plate to make base plate, spread the candle liquid of one deck liquefied petrolatum or thawing earlier to its bottom surface, adopt slide and cover glass to be fixed into the mould that varies in size at the wax layer, a small amount of glue is used for seam and primer is made, after treating colloid solidification, namely can be used for specimen embedding.
(5) embedding of insect specimen: the insect specimen that handle well early stage is put into primer central authorities, can directly insert sample with insect needle and be used for fixing sample for preventing the sample drift, gradation pours into the mould envelope with ripe monomer and buries insect, the each cast of control thickness 3.5mm, all want sealed mold after each the feeding in raw material, in the normal temperature 1-2 hour, allow ripe monomer form the transparent body of toughness, just can descend cast together, continue to pour into ripe monomer again, according to the number of times of the content diverse location of placing and the ripe monomer of quantity decision cast.Setting temperature is 25 ℃ of normal temperature.After treating last colloid solidification, rotatable insect needle also takes out pin and removes mould, solidifies fully until sample.
(6) polishing, polishing: adopt sander and polishing machine to carry out last polishing, the post processing of polishing, namely finish the making engineering of ambroid sample.
Embodiment 3
(1) Lauxite is given birth to the synthetic of monomer: formaldehyde and urea (55: 16) are mixed by mass percentage, when formaldehyde dissolves, constantly stir, the sodium hydroxide 0.2ml of adding 30% in the time of 25 ℃, to reaction system PH be 7.5, keep 0.25h; In the time of 85 ℃, add glacial acetic acid 0.1ml, to reaction system PH be 4.5, keep 0.3h; Be stained with a reactant liquor and add in the normal-temperature water, the phenomenon that hazes just stops heating, adds 0.5ml30% sodium hydroxide and stops reaction, and synthetic urea-formaldehyde resin is given birth to monomer.
(2) preliminary treatment of insect: insect places the living monomer soaked overnight of Lauxite standby after whole limb, 60 ℃ of oven dry are handled.
(3) preparation of ripe monomer: get 3 parts of the above-mentioned living monomer liquid urea-formaldehyde glues for preparing: DEHP1 part; After mixing fully stirring, add the stirring of 15% glacial acetic acid and namely generate ripe monomer, i.e. ripe monomer.
(4) preparation of mould: this research adopts a complete poly (methyl methacrylate) plate to make base plate, spread the candle liquid of one deck liquefied petrolatum or thawing earlier to its bottom surface, adopt slide and cover glass to be fixed into the mould that varies in size at the wax layer, a small amount of glue is used for seam and primer is made, after treating colloid solidification, namely can be used for specimen embedding.
(5) embedding of insect specimen: the insect specimen that handle well early stage is put into primer central authorities, can directly insert sample with insect needle and be used for fixing sample for preventing the sample drift, gradation pours into the mould envelope with ripe monomer and buries insect, the each cast of control thickness 5mm, all want sealed mold after each the feeding in raw material, in the normal temperature 1-2 hour, allow ripe monomer form the transparent body of toughness, just can descend cast together, continue to pour into ripe monomer again, according to the number of times of the content diverse location of placing and the ripe monomer of quantity decision cast.Setting temperature is 25 ℃ of normal temperature.After treating last colloid solidification, rotatable insect needle also takes out pin and removes mould, solidifies fully until sample.
(6) polishing, polishing: adopt sander and polishing machine to carry out last polishing, the post processing of polishing, namely finish the making engineering of ambroid sample.
Embodiment 4.
(1) Lauxite is given birth to the synthetic of monomer: formaldehyde and urea (52: 19) are mixed by mass percentage, when formaldehyde dissolves, constantly stir, the sodium hydroxide 0.15ml of adding 20% in the time of 20 ℃, to reaction system PH be 7.5, keep 0.25h; In the time of 70 ℃, add glacial acetic acid 0.5ml, to reaction system PH be 4.5, keep 0.3h; Be stained with a reactant liquor and add in the normal-temperature water, the phenomenon that hazes just stops heating, adds 0.25ml20% sodium hydroxide and stops reaction, and synthetic urea-formaldehyde resin is given birth to monomer.
(2) preliminary treatment of insect: insect places the living monomer soaked overnight of Lauxite standby after whole limb, 60 ℃ of oven dry are handled.
(3) preparation of ripe monomer: get 3 parts of the above-mentioned living monomer liquid urea-formaldehyde glues for preparing: DEHP3 part; After mixing fully stirring, add the stirring of 12% glacial acetic acid and namely generate ripe monomer, i.e. ripe monomer.
(4) preparation of mould: this research adopts a complete poly (methyl methacrylate) plate to make base plate, spread the candle liquid of one deck liquefied petrolatum or thawing earlier to its bottom surface, adopt slide and cover glass to be fixed into the mould that varies in size at the wax layer, a small amount of glue is used for seam and primer is made, after treating colloid solidification, namely can be used for specimen embedding.
(5) embedding of insect specimen: the insect specimen that handle well early stage is put into primer central authorities, can directly insert sample with insect needle and be used for fixing sample for preventing the sample drift, gradation pours into the mould envelope with ripe monomer and buries insect, the each cast of control thickness 3.5mm, all want sealed mold after each the feeding in raw material, in the normal temperature 1-2 hour, allow ripe monomer form the transparent body of toughness, just can descend cast together, continue to pour into ripe monomer again, according to the number of times of the content diverse location of placing and the ripe monomer of quantity decision cast.Setting temperature is after 37 ℃ of normal temperature are treated last colloid solidification, and rotatable insect needle also takes out pin and removes mould, solidifies fully until sample.
(6) polishing, polishing: adopt sander and polishing machine to carry out last polishing, the post processing of polishing, namely finish the making engineering of ambroid sample.
Embodiment 5
(1) Lauxite is given birth to the synthetic of monomer: formaldehyde and urea (52: 19) are mixed by mass percentage, when formaldehyde dissolves, constantly stir, the sodium hydroxide 0.15ml of adding 20% in the time of 30 ℃, to reaction system PH be 8, keep 0.5h; In the time of 100 ℃, add glacial acetic acid 0.5ml, to reaction system PH be 5, keep 0.5h; Be stained with a reactant liquor and add in the normal-temperature water, the phenomenon that hazes just stops heating, adds 0.25ml20% sodium hydroxide and stops reaction, and synthetic urea-formaldehyde resin is given birth to monomer.
(2) preliminary treatment of insect: insect places the living monomer soaked overnight of Lauxite standby after whole limb, 60 ℃ of oven dry are handled.
(3) preparation of ripe monomer: get 3 parts of the above-mentioned living monomer liquid urea-formaldehyde glues for preparing: DINP3 part; After mixing fully stirring, add the stirring of 12% glacial acetic acid and namely generate ripe monomer, i.e. ripe monomer.
(4) preparation of mould: this research adopts a complete poly (methyl methacrylate) plate to make base plate, spread the candle liquid of one deck liquefied petrolatum or thawing earlier to its bottom surface, adopt slide and cover glass to be fixed into the mould that varies in size at the wax layer, a small amount of glue is used for seam and primer is made, after treating colloid solidification, namely can be used for specimen embedding.
(5) embedding of insect specimen: the insect specimen that handle well early stage is put into primer central authorities, can directly insert sample with insect needle and be used for fixing sample for preventing the sample drift, gradation pours into the mould envelope with ripe monomer and buries insect, the each cast of control thickness 4mm, all want sealed mold after each the feeding in raw material, in the normal temperature 1-2 hour, allow ripe monomer form the transparent body of toughness, just can descend cast together, continue to pour into ripe monomer again, according to the number of times of the content diverse location of placing and the ripe monomer of quantity decision cast.Setting temperature is 37 ℃ of normal temperature.After treating last colloid solidification, rotatable insect needle also takes out pin and removes mould, solidifies fully until sample.
(6) polishing, polishing: adopt sander and polishing machine to carry out last polishing, the post processing of polishing, namely finish the making engineering of ambroid sample.
Be enlightenment with above-mentioned foundation desirable embodiment of the present invention, by above-mentioned description, the related work personnel can carry out various change and modification fully in the scope that does not depart from this invention technological thought.The technical scope of this invention is not limited to the content on the specification, must determine its technical scope according to the claim scope.
The present invention is not limited to above-mentioned concrete embodiment, and those of ordinary skill in the art is from above-mentioned design, and without performing creative labour, all conversion of having done all drop within protection scope of the present invention.
Claims (9)
1. artificial cantharias sample, main material is Lauxite, also comprise auxiliary material sodium hydroxide, glacial acetic acid, it is characterized in that, described Lauxite is that formaldehyde, urea are that raw material mixes the living monomer that the back polymerization reaction take place generates by a certain percentage, and the ratio of described formaldehyde and described urea is 55: 18～50: 22.
2. the manufacture method of an artificial cantharias sample comprises step:
(1) the synthetic monomer of giving birth to,
(2) preliminary treatment of insect,
(3) prepare ripe monomer by giving birth to monomer,
(4) preparation of mould,
(5) the fixing and embedding of insect specimen,
(6) demoulding and grinding and buffing;
Described living monomer is main material with the Lauxite, and sodium hydroxide, glacial acetic acid are that auxiliary material is polymerized; It is characterized in that, described Lauxite is that formaldehyde, urea are the living monomer that polymerizable raw material forms, the formaldehyde in the described living monomer and urea ratio 50-55: 18-22, and the shrinkage factor of described Lauxite is 5%-20%, firm time is 2-5d, and the foaming number is 0-5.
3. according to the manufacture method of the artificial cantharias of claim 2, it is characterized in that the reaction method of described polymerization is the sodium hydroxide 0.1-0.2ml that adds 10-30% in the time of 20-30 ℃, reaction system PH is 7-8, keeps 0.25 (0.1-0.5) hour; Add glacial acetic acid 0.1-1ml in the time of 70-100 ℃, reaction system PH is 4-5, keeps 0.3 (0.1-0.5) hour; The end condition of described polymerisation adds in the normal-temperature water for being stained with a reactant liquor, and the phenomenon that hazes stops heating immediately, adds 0.1-0.5ml10-30% sodium hydroxide and stops reaction.
4. according to the manufacture method of the artificial cantharias of claim 2, it is characterized in that, the preparation method of described ripe monomer is for getting living monomer liquid urea-formaldehyde glue 1-5 part that (1) prepares: after extension agent 1-5 part, mixing were fully stirred, adding 10%-15% glacial acetic acid stirred and namely generates ripe monomer.
5. according to the manufacture method of the artificial cantharias of claim 2, it is characterized in that described extension agent is selected from a kind of among Macrogol 600, DEHP and the DINP.
6. according to the manufacture method of the artificial cantharias of claim 2, it is characterized in that the fixing means of described sample is that the insect needle fixed preparation is in mould on the wax layer pedestal; The embedding of described insect specimen adopts gradation processing insect specimen on the primer in the mould to pour into a mould ripe monomer, each cast thickness is 2～5mm, treat to continue cast again after this time cast colloid solidification, the cast number of times need reach can be with the complete embedding of sample, and described setting temperature is 25～60 ℃ of normal temperature.
7. according to the manufacture method of the manufacturing cantharias of claim 2, it is characterized in that the fixing means of described sample is that insect needle is fixed.
8. according to the manufacture method of the artificial cantharias of claim 2, it is characterized in that described mould is made for adopting lucite and slide, cover glass, fixing and cast primer is made at the wax layer.
9. according to the manufacture method of the manufacturing cantharias of claim 2, it is characterized in that the releasing agent that the described demoulding is handled is paraffin and candle liquified mixt, described post processing comprises the polishing of the insect specimen after the demoulding, polishing.
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| CN2013102016353A CN103299985A (en) | 2013-05-21 | 2013-05-21 | Cantharias specimen and making method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103947609A (en) * | 2014-04-18 | 2014-07-30 | 青岛农业大学 | Method for observing wax gland orifices of eriosoma lanigerum |
| CN104041482A (en) * | 2014-04-30 | 2014-09-17 | 大连大学 | Manufacturing method of lepidopteron plastinated specimens |
| CN104041483B (en) * | 2014-04-30 | 2015-05-20 | 大连大学 | Preparation method of miniature marine animal plastinated specimens |
| CN105010302A (en) * | 2015-07-08 | 2015-11-04 | 南宁千年工艺有限公司 | Method for preparing resin-embedded water-containing animal specimen |
| CN106982819A (en) * | 2017-05-10 | 2017-07-28 | 广西柳州中嘉知识产权服务有限公司 | Honeybee Slide processing |
| CN107183002A (en) * | 2017-05-10 | 2017-09-22 | 广西柳州中嘉知识产权服务有限公司 | Butterfly specimen preparation method |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103947609A (en) * | 2014-04-18 | 2014-07-30 | 青岛农业大学 | Method for observing wax gland orifices of eriosoma lanigerum |
| CN103947609B (en) * | 2014-04-18 | 2015-08-12 | 青岛农业大学 | A kind of wooly aphis wax gland hole observational technique |
| CN104041482A (en) * | 2014-04-30 | 2014-09-17 | 大连大学 | Manufacturing method of lepidopteron plastinated specimens |
| CN104041482B (en) * | 2014-04-30 | 2015-05-20 | 大连大学 | Manufacturing method of lepidopteron plastinated specimens |
| CN104041483B (en) * | 2014-04-30 | 2015-05-20 | 大连大学 | Preparation method of miniature marine animal plastinated specimens |
| CN105010302A (en) * | 2015-07-08 | 2015-11-04 | 南宁千年工艺有限公司 | Method for preparing resin-embedded water-containing animal specimen |
| CN105010302B (en) * | 2015-07-08 | 2017-10-10 | 南宁千年工艺股份有限公司 | A kind of preparation method of the aqueous zoological specimens of resin embedding |
| CN106982819A (en) * | 2017-05-10 | 2017-07-28 | 广西柳州中嘉知识产权服务有限公司 | Honeybee Slide processing |
| CN107183002A (en) * | 2017-05-10 | 2017-09-22 | 广西柳州中嘉知识产权服务有限公司 | Butterfly specimen preparation method |
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Application publication date: 20130918 |