CN103288657A - 一种改性醇胺及其制备方法 - Google Patents
一种改性醇胺及其制备方法 Download PDFInfo
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- CN103288657A CN103288657A CN2013102258687A CN201310225868A CN103288657A CN 103288657 A CN103288657 A CN 103288657A CN 2013102258687 A CN2013102258687 A CN 2013102258687A CN 201310225868 A CN201310225868 A CN 201310225868A CN 103288657 A CN103288657 A CN 103288657A
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- diethanolamine
- alcohol amine
- hydramine
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- 238000002360 preparation method Methods 0.000 title claims abstract description 21
- -1 Modified alcohol amine Chemical class 0.000 title abstract 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 31
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 claims abstract description 28
- 239000003054 catalyst Substances 0.000 claims abstract description 10
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims description 38
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 claims description 35
- ZZVUWRFHKOJYTH-UHFFFAOYSA-N diphenhydramine Chemical compound C=1C=CC=CC=1C(OCCN(C)C)C1=CC=CC=C1 ZZVUWRFHKOJYTH-UHFFFAOYSA-N 0.000 claims description 35
- 238000012986 modification Methods 0.000 claims description 27
- 230000004048 modification Effects 0.000 claims description 27
- 238000006243 chemical reaction Methods 0.000 claims description 19
- 239000002253 acid Substances 0.000 claims description 17
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 14
- 239000007787 solid Substances 0.000 claims description 9
- 239000011964 heteropoly acid Substances 0.000 claims description 7
- 229910052757 nitrogen Inorganic materials 0.000 claims description 7
- 239000003729 cation exchange resin Substances 0.000 claims description 6
- 239000007789 gas Substances 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 239000011949 solid catalyst Substances 0.000 claims description 6
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 5
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 4
- 239000003930 superacid Substances 0.000 claims description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 2
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 2
- 229910010413 TiO 2 Inorganic materials 0.000 claims description 2
- 229910052786 argon Inorganic materials 0.000 claims description 2
- 229940023913 cation exchange resins Drugs 0.000 claims description 2
- 239000001307 helium Substances 0.000 claims description 2
- 229910052734 helium Inorganic materials 0.000 claims description 2
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 claims description 2
- 239000001257 hydrogen Substances 0.000 claims description 2
- 229910052739 hydrogen Inorganic materials 0.000 claims description 2
- 238000000227 grinding Methods 0.000 abstract description 15
- 239000004568 cement Substances 0.000 abstract description 10
- 239000002994 raw material Substances 0.000 abstract description 9
- 238000004519 manufacturing process Methods 0.000 abstract description 8
- 238000005265 energy consumption Methods 0.000 abstract description 7
- 238000000034 method Methods 0.000 abstract description 7
- 238000003860 storage Methods 0.000 abstract description 5
- 238000010438 heat treatment Methods 0.000 abstract description 4
- 239000004566 building material Substances 0.000 abstract description 3
- 238000004821 distillation Methods 0.000 abstract description 3
- 230000008901 benefit Effects 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract description 2
- CRVGTESFCCXCTH-UHFFFAOYSA-N methyl diethanolamine Chemical compound OCCN(C)CCO CRVGTESFCCXCTH-UHFFFAOYSA-N 0.000 description 29
- 239000006227 byproduct Substances 0.000 description 10
- 230000000694 effects Effects 0.000 description 8
- 230000000052 comparative effect Effects 0.000 description 7
- NOAAMORLQWOAEL-UHFFFAOYSA-N ethoxy-n,n-di(propan-2-yl)phosphonamidous acid Chemical compound CCOP(O)N(C(C)C)C(C)C NOAAMORLQWOAEL-UHFFFAOYSA-N 0.000 description 7
- 239000000047 product Substances 0.000 description 7
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 6
- 230000009466 transformation Effects 0.000 description 6
- 238000009413 insulation Methods 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 230000036632 reaction speed Effects 0.000 description 5
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 description 4
- SLINHMUFWFWBMU-UHFFFAOYSA-N Triisopropanolamine Chemical compound CC(O)CN(CC(C)O)CC(C)O SLINHMUFWFWBMU-UHFFFAOYSA-N 0.000 description 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 4
- 238000001816 cooling Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000001301 oxygen Substances 0.000 description 4
- 229910052760 oxygen Inorganic materials 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- 239000002826 coolant Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 229960004418 trolamine Drugs 0.000 description 3
- BYACHAOCSIPLCM-UHFFFAOYSA-N 2-[2-[bis(2-hydroxyethyl)amino]ethyl-(2-hydroxyethyl)amino]ethanol Chemical compound OCCN(CCO)CCN(CCO)CCO BYACHAOCSIPLCM-UHFFFAOYSA-N 0.000 description 2
- 229910021529 ammonia Inorganic materials 0.000 description 2
- 230000006835 compression Effects 0.000 description 2
- 238000007906 compression Methods 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 238000004880 explosion Methods 0.000 description 2
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- 238000000926 separation method Methods 0.000 description 2
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- 238000012360 testing method Methods 0.000 description 2
- HXKKHQJGJAFBHI-UHFFFAOYSA-N 1-aminopropan-2-ol Chemical compound CC(O)CN HXKKHQJGJAFBHI-UHFFFAOYSA-N 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 150000004683 dihydrates Chemical class 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 229910052602 gypsum Inorganic materials 0.000 description 1
- 239000010440 gypsum Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- OHMBHFSEKCCCBW-UHFFFAOYSA-N hexane-2,5-diol Chemical compound CC(O)CCC(C)O OHMBHFSEKCCCBW-UHFFFAOYSA-N 0.000 description 1
- 239000011396 hydraulic cement Substances 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
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- 239000003456 ion exchange resin Substances 0.000 description 1
- 229920003303 ion-exchange polymer Polymers 0.000 description 1
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- 239000007788 liquid Substances 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- 239000004570 mortar (masonry) Substances 0.000 description 1
- 150000002924 oxiranes Chemical class 0.000 description 1
- DHRLEVQXOMLTIM-UHFFFAOYSA-N phosphoric acid;trioxomolybdenum Chemical compound O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.OP(O)(O)=O DHRLEVQXOMLTIM-UHFFFAOYSA-N 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- CGFYHILWFSGVJS-UHFFFAOYSA-N silicic acid;trioxotungsten Chemical compound O[Si](O)(O)O.O=[W]1(=O)O[W](=O)(=O)O[W](=O)(=O)O1.O=[W]1(=O)O[W](=O)(=O)O[W](=O)(=O)O1.O=[W]1(=O)O[W](=O)(=O)O[W](=O)(=O)O1.O=[W]1(=O)O[W](=O)(=O)O[W](=O)(=O)O1 CGFYHILWFSGVJS-UHFFFAOYSA-N 0.000 description 1
- 229920005552 sodium lignosulfonate Polymers 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Description
助磨剂 | 掺量;% | 45u筛余百分数;% | 45u筛余减少值;% |
空白 | 15.2 | ||
实施例10 | 0.02 | 11.5 | 3.7 |
实施例11 | 0.02 | 11.6 | 3.6 |
实施例12 | 0.02 | 11.3 | 3.9 |
对比例2 | 0.02 | 12.1 | 3.1 |
对比例3 | 0.03 | 12.5 | 2.7 |
Claims (10)
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Cited By (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104230724A (zh) * | 2014-09-02 | 2014-12-24 | 南京红宝丽醇胺化学有限公司 | 一种二乙醇单异丙醇胺的制备方法 |
CN104710123A (zh) * | 2015-02-03 | 2015-06-17 | 辽宁鑫隆科技有限公司 | 一种改性二乙醇单异丙醇胺盐水泥助磨剂 |
CN105669909A (zh) * | 2015-12-28 | 2016-06-15 | 江苏中铁奥莱特新材料有限公司 | 一种增强型聚丙烯酰胺系水泥助磨剂的制备方法 |
CN106007444A (zh) * | 2016-05-20 | 2016-10-12 | 山东中岩建材科技有限公司 | 一种改性醇胺及其制备方法和应用 |
CN106083617A (zh) * | 2016-06-14 | 2016-11-09 | 青神鑫统领建材有限公司 | 一种生产低色度二乙醇单异丙醇胺的方法 |
CN106220023A (zh) * | 2016-07-22 | 2016-12-14 | 安徽科博建材科技有限公司 | 一种水泥助磨剂配方 |
CN108863781A (zh) * | 2018-06-12 | 2018-11-23 | 威海金泓高分子有限公司 | 一种环保增塑剂己二酸二乙酯的生产方法 |
CN109503025A (zh) * | 2018-12-29 | 2019-03-22 | 东阿东昌天汇科技有限公司 | 延长寿命提升均度陶瓷磨球专用助磨剂及其制造方法 |
CN111689714A (zh) * | 2020-05-13 | 2020-09-22 | 山东中岩建材科技有限公司 | 一种无氯水泥助磨剂及其制备方法 |
CN112028779A (zh) * | 2020-10-10 | 2020-12-04 | 安徽海螺新材料科技有限公司 | 一种以氯丙醇为原料的羟乙基二异丙醇胺的制备方法 |
CN114031510A (zh) * | 2021-11-25 | 2022-02-11 | 万华化学集团股份有限公司 | 一种2-氨基丙醇的制备方法 |
CN115010611A (zh) * | 2022-04-27 | 2022-09-06 | 北京金隅水泥节能科技有限公司 | 一种二乙醇单异丙醇胺的生产工艺 |
WO2023035398A1 (zh) * | 2021-09-10 | 2023-03-16 | 佳化化学科技发展(上海)有限公司 | 一种水泥用助磨剂及其制备方法 |
TWI805686B (zh) * | 2018-02-06 | 2023-06-21 | 德商巴斯夫歐洲公司 | -單烷醇胺之方法 |
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CN101314533A (zh) * | 2008-07-03 | 2008-12-03 | 南京红宝丽股份有限公司 | 连续制备高效水泥助磨剂的方法 |
CN102924301A (zh) * | 2012-11-01 | 2013-02-13 | 史才军 | 一种二乙醇单异丙醇胺的制备方法 |
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2013
- 2013-06-07 CN CN201310225868.7A patent/CN103288657B/zh active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN101314533A (zh) * | 2008-07-03 | 2008-12-03 | 南京红宝丽股份有限公司 | 连续制备高效水泥助磨剂的方法 |
CN102924301A (zh) * | 2012-11-01 | 2013-02-13 | 史才军 | 一种二乙醇单异丙醇胺的制备方法 |
Cited By (22)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104230724B (zh) * | 2014-09-02 | 2016-09-07 | 南京红宝丽醇胺化学有限公司 | 一种二乙醇单异丙醇胺的制备方法 |
CN104230724A (zh) * | 2014-09-02 | 2014-12-24 | 南京红宝丽醇胺化学有限公司 | 一种二乙醇单异丙醇胺的制备方法 |
CN104710123A (zh) * | 2015-02-03 | 2015-06-17 | 辽宁鑫隆科技有限公司 | 一种改性二乙醇单异丙醇胺盐水泥助磨剂 |
CN104710123B (zh) * | 2015-02-03 | 2017-06-06 | 辽宁鑫隆科技有限公司 | 一种改性二乙醇单异丙醇胺盐水泥助磨剂 |
CN105669909A (zh) * | 2015-12-28 | 2016-06-15 | 江苏中铁奥莱特新材料有限公司 | 一种增强型聚丙烯酰胺系水泥助磨剂的制备方法 |
CN105669909B (zh) * | 2015-12-28 | 2018-01-19 | 江苏中铁奥莱特新材料股份有限公司 | 一种增强型聚丙烯酰胺系水泥助磨剂的制备方法 |
CN106007444A (zh) * | 2016-05-20 | 2016-10-12 | 山东中岩建材科技有限公司 | 一种改性醇胺及其制备方法和应用 |
CN106083617A (zh) * | 2016-06-14 | 2016-11-09 | 青神鑫统领建材有限公司 | 一种生产低色度二乙醇单异丙醇胺的方法 |
CN106220023A (zh) * | 2016-07-22 | 2016-12-14 | 安徽科博建材科技有限公司 | 一种水泥助磨剂配方 |
TWI805686B (zh) * | 2018-02-06 | 2023-06-21 | 德商巴斯夫歐洲公司 | -單烷醇胺之方法 |
US11753364B2 (en) | 2018-02-06 | 2023-09-12 | Basf Se | Method for producing C2-C4 mono alkanol amines using an acid cation exchanger as a catalyst |
CN108863781A (zh) * | 2018-06-12 | 2018-11-23 | 威海金泓高分子有限公司 | 一种环保增塑剂己二酸二乙酯的生产方法 |
CN109503025A (zh) * | 2018-12-29 | 2019-03-22 | 东阿东昌天汇科技有限公司 | 延长寿命提升均度陶瓷磨球专用助磨剂及其制造方法 |
CN111689714B (zh) * | 2020-05-13 | 2022-05-24 | 山东中岩建材科技有限公司 | 一种无氯水泥助磨剂及其制备方法 |
CN111689714A (zh) * | 2020-05-13 | 2020-09-22 | 山东中岩建材科技有限公司 | 一种无氯水泥助磨剂及其制备方法 |
CN112028779B (zh) * | 2020-10-10 | 2022-05-24 | 安徽海螺新材料科技有限公司 | 一种以氯丙醇为原料的羟乙基二异丙醇胺的制备方法 |
CN112028779A (zh) * | 2020-10-10 | 2020-12-04 | 安徽海螺新材料科技有限公司 | 一种以氯丙醇为原料的羟乙基二异丙醇胺的制备方法 |
WO2023035398A1 (zh) * | 2021-09-10 | 2023-03-16 | 佳化化学科技发展(上海)有限公司 | 一种水泥用助磨剂及其制备方法 |
CN114031510A (zh) * | 2021-11-25 | 2022-02-11 | 万华化学集团股份有限公司 | 一种2-氨基丙醇的制备方法 |
CN114031510B (zh) * | 2021-11-25 | 2023-05-30 | 万华化学集团股份有限公司 | 一种2-氨基丙醇的制备方法 |
CN115010611A (zh) * | 2022-04-27 | 2022-09-06 | 北京金隅水泥节能科技有限公司 | 一种二乙醇单异丙醇胺的生产工艺 |
CN115010611B (zh) * | 2022-04-27 | 2024-02-20 | 北京金隅节能科技有限公司 | 一种二乙醇单异丙醇胺的生产工艺 |
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Address after: Zheng Zhen new street 620562 benevolence county of Meishan City, Sichuan Province dragon No. 279 Patentee after: XINTONGLING BUILDING MATERIAL GROUP CO.,LTD. Address before: Zheng Zhen new street 620562 benevolence county of Meishan City, Sichuan Province dragon No. 279 Patentee before: SICHUAN XINTONGLING BUILDING MATERIALS TECHNOLOGY CO.,LTD. |
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Effective date of registration: 20190321 Address after: Room 208, No. 1 Building, No. 9 Wanjiang Avenue, Jiangbei Industrial Concentration Area, Wuhu City, Anhui Province Patentee after: Anhui Conch New Materials Technology Co.,Ltd. Address before: 620562 519 New Town Street, Longzheng Town, Renshou County, Meishan, Sichuan Patentee before: SICHUAN XINTONGLING NEW MATERIAL Co.,Ltd. |
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Address after: Room 208, No. 1 Building, No. 9 Wanjiang Avenue, Jiangbei Industrial Concentration Area, Wuhu City, Anhui Province Patentee after: Anhui Conch Material Technology Co.,Ltd. Address before: Room 208, No. 1 Building, No. 9 Wanjiang Avenue, Jiangbei Industrial Concentration Area, Wuhu City, Anhui Province Patentee before: Anhui Conch New Materials Technology Co.,Ltd. |