CN103230352B - Method for preparing plant extract and hydrolyzed pearl-containing toner composition - Google Patents
Method for preparing plant extract and hydrolyzed pearl-containing toner composition Download PDFInfo
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Abstract
The invention relates to a method for preparing a plant extract and hydrolyzed pearl-containing toner composition. The method comprises the following steps: 1, putting a phase 1 into a container to mix, heating to be 80 DEG C and stirring to completely dissolve, wherein the phase 1 comprises glycerol, allantoin, hydroxyethyl cellulose, sodium hyaluronate and the balance of water; 2, cooling to be 50 DEG C, adding a phase 2 and stirring uniformly, wherein the phase 2 comprises appropriate amounts of water-soluble silicon wax, chamomile extract, hydrolyzed pearls, 1,2-hexanediol/caprylyl glycol, coconut/algae extract, panax ginseng root extract, essence, an antiseptic agent, a solubilizer and pigment; and 3, adding a phase 3, quickly stirring for 5 minutes, mixing uniformly and discharging, wherein the phase 3 comprises polyacrylamide/C13-14 isoparaffin/laureth-7. The composition can sufficiently moisturize skins at night, open the deep infiltration channels of the skins, supplement amino acid and strengthen skin reviving capability and smooth breathing.
Description
Present patent application is application for a patent for invention (application number: 201110294793.9 applyings date: 11-09-27, invention and created name: dividing an application a kind of astringent composition and method of making the same that comprises skin conditioning agent and water-soluble silicon wax).
Technical field
The invention belongs to the astringent composition and method of making the same of a kind of stable skin, balance skin Acidity of Aikalinity.
Background technology
Due to the quickening of modern people's rhythm of life, and be subject to various environmental effects, the speed of skin aging is increasing.Too much sebum secretion, blocks pore, causes cutin slightly thick.Computer radiate, makes skin dim, tarnish.Wind, the loss of moisture of skin.
Chinese invention patent application (application number: 200910010837.3 applyings date: 2009-03-24) disclose a kind of skincare humectant.It consists of according to the following number of weight ratio following component: skin protection base material: natural dimethylamino proline acid: glycerol: Mel: shea butter: vitamin E=80-120: 5-12: 1-3: 10-20: 1-3: 2-4.This invention is nourished moisturizing composition containing shea butter, glycerol, Mel isoreactivity, can help rapidly to moisten dry skin, makes skin exquisiteness soft and smooth.
Chinese invention patent application (application number: 200710150410.4 applyings date: 2007-11-26) disclose a kind of cosmetic humectant that contains xylitol, it is comprised of the raw material of following portions by weight: 2-10 part wetting agent, 0.1-2 part oils and fats, emulsifying agent 5-15 part, 60～80 parts, water.The cosmetic humectant of this invention can more deeply be diffused into skin depths, is combined with deep water, keeps the moist of skin.
Summary of the invention
In order to reduce the loss of moisture, an object of the present invention is to provide a kind of astringent compositions that comprises skin conditioning agent and water-soluble silicon wax, said composition can keep the skin wet to skin, soft skin, make skin be full of elasticity, and improve skin quality, skin is taken on an entirely new look.Another one object of the present invention is to provide a kind of preparation method of above-mentioned astringent compositions.
In order to realize above-mentioned first object, the present invention has adopted following technical scheme:
An astringent compositions that comprises skin conditioning agent and water-soluble silicon wax, described compositions comprises following component by mass percentage:
(a) 0.01% to 30% wetting agent;
(b) 0.01% to 10% water-soluble silicon wax;
(c) 0.01% to 8% hydrophilic surfactant active;
(d) 0.01% to 5% high molecular weight water soluble polymer, described high molecular weight water soluble polymer provides 500 to 100000mPas viscosity for described astringent;
(e) 0.01% to 20% skin conditioning agent; With
(f) 10% to 90% deionized water.
As preferably, described compositions comprises following component by mass percentage:
(a) 1% to 20% wetting agent;
(b) 0.01% to 10% water-soluble silicon wax;
(c) 0.01% to 8% hydrophilic surfactant active;
(d) 0.01% to 5% high molecular weight water soluble polymer, described high molecular weight water soluble polymer provides 500 to 100000mPas viscosity for described astringent;
(e) 0.01% to 20% skin conditioning agent; With
(f) 10% to 90% deionized water.
As preferred again, described compositions comprises following component by mass percentage:
(a) 2% to 20% wetting agent;
(b) 0.01% to 10% water-soluble silicon wax;
(c) 0.01% to 8% hydrophilic surfactant active;
(d) 0.01% to 5% high molecular weight water soluble polymer, described high molecular weight water soluble polymer provides 500 to 100000mPas viscosity for described astringent;
(e) 0.01% to 20% skin conditioning agent; With
(f) 10% to 90% deionized water.
As preferably, above-mentioned wetting agent is selected from propylene glycol, sorbitol, butanediol, 1, one or more of 2-hexanediol, caprylyl glycol, dipropylene glycol, glycerol, diglycerol, pentanediol, Polyethylene Glycol, what be preferred for this compositions is glycerol, 1,2-hexanediol/caprylyl glycol.
As preferably, above-mentioned hydrophilic surfactant active is polyacrylamide polymers preferably, especially the polyacrylamide polymers of nonionic, more preferably with the non-ionic polymers of CTFA called after polyacrylamide/C13-14 isoparaffin/laureth-7.
As preferably, above-mentioned thickening agent is selected from the synthetic high molecular polymer of carboxylic acid polyalcohol, cross-linked polyacrylate polymer, cellulose ethers, natural high molecular polymer, the synthetic high molecular polymer of cellulose ethers preferably, more preferably presses the material of CTFA called after hydroxyethyl-cellulose.
As preferably, above-mentioned skin conditioning agent is selected from one or more in hydrolyzed pearl, hyaluronate sodium, chamomile extract, allantoin, hydrolyzed pearl, hyaluronate sodium, cocoa/Sargassum composite extract and Radix Ginseng extract.
As preferably, above-mentioned composition has also comprised one or more in food coloring, antiseptic, essence and solubilizing agent.
The present composition also can comprise various other compositions.The function of the concrete composition of compositions of the present invention and effect will be described in more detail below.
Wetting agent
Approximately 0.01% to 20% wetting agent by weight in the present invention is polyhydric alcohol, compositions described herein preferably comprises by weight of the composition approximately 1% to 20%, the wetting agent of 2%-20% more preferably, example comprises propylene glycol, sorbitol, butanediol, 1,2-hexanediol, caprylyl glycol, dipropylene glycol, glycerol, diglycerol, pentanediol, Polyethylene Glycol, and their mixture, what be preferred for this compositions is glycerol, 1,2-hexanediol/caprylyl glycol.
Water-soluble silicon wax
Water-soluble silicon wax in the present invention is a kind of water miscible organosilicon ethylene glycol copolymer wax, and fusing point is lower.Its advantage has been to remove the viscosity of general cosmetic composition, and has improved the texture of other compositions, and 20 experts are contained and containing the cosmetic composition of this water-soluble silicon wax, do not carried out sensory evaluation following table and as shown in Fig. 1～Fig. 7 multiple.
Intermiscibility test result
This sensory evaluation scheme is followed the method that the E18.03.01 of ASTM committee advises aspect sensory evaluation.In this scheme, 20 were subject to the personnel of professional training by the description of several organoleptic parameters quantitative analyses being evaluated to the skinfeel characteristic of raw material and formulation product.
Hydrophilic surfactant active
Hydrophilic surfactant active in this invention compositions is polyacrylamide polymers preferably, especially the polyacrylamide polymers of nonionic, these polymer more preferably, with the non-ionic polymers of CTFA called after polyacrylamide/C13-14 isoparaffin/laureth-7, derive from France match Bicc Public Ltd. Co with commodity SEPIGEL305 by name.Hydrophilic surfactant plays dispersion, solubilising and osmosis, also has certain thickening capabilities.
Thickening agent
In some embodiments, compositions of the present invention can also comprise one or more thickening agents, and if present, described compositions comprises by weight of the composition approximately 0.01% to 5%, preferably be about 0.01% to 4%, more preferably from about 0.01% to 3% thickening agent.
The non-limiting kind of thickening agent comprises and is selected from following material: carboxylic acid polyalcohol (as Carbopol980), cross-linked polyacrylate polymer, synthetic high molecular polymer (as cellulose ethers), natural high molecular polymer (as natural gum), cellulose ethers preferably, more preferably press the material of CTFA called after hydroxyethyl-cellulose, this material is sold with trade name Natrosol250HHR by Aqualon Corporation.
Skin conditioning agent
The various skin conditioner that the present composition adds is chamomile extract, allantoin, hydrolyzed pearl, hyaluronate sodium, cocoa/Sargassum composite extract and Radix Ginseng extract.
The content of the Flos Chrysanthemi extract that the present composition adds is preferably approximately 0.01% to 20% by weight of the composition, more preferably from about 0.01% to 10%, the active quantities of the Flos Chrysanthemi extract of the present composition by weight of the composition preferably approximately 0.001% to 10%, more preferably from about 0.001% to 5%.
The chamomile extract that the present composition adds, contains flavone compound, aminoacid, macroelement and trace element, also contains micro-ellagic acid, adenine, choline, echinacoside, vitamin E etc., separately has chlorogenic acid, quinovic acid-4-coffee ester etc.This Flos Matricariae chamomillae extract has antiinflammatory, sterilization, antioxidation.Chrysan Yellow ketone compounds has the ability of removing free radical and superoxide anion, can obviously suppress the lipid peroxidation that D2 galactose causes, reduce MDA content, MAO vigor in blood, improve SOD, GSH-PX vigor in blood, the scavenging action of enhancing body to free radical, alleviate superoxide anion to biomembranous damage, delaying senility course.
The Flos Chrysanthemi extract of the present composition can be followed the example of by hot water extraction method, alcohol extraction, ultrasonic extraction and microwave extraction method make.
The allantoin of the present composition is a kind of amphoteric compound, can form double salt in conjunction with many kinds of substance.The content of the allantoin that the present composition adds is preferably approximately 0.01% to 20% by weight of the composition, and more preferably from about 0.01% to 10%.
Above-mentioned allantoin has shading, sterilization and anticorrosion, pain relieving, antioxidation, can make skin keep moisture content, moist and soft, is the additive of the cosmetics such as cosmetology.The cosmetics that add allantoin have protective tissue, hydrophilic, absorb water and the effect such as prevent that moisture from distributing; Make skin softness and high resilience, and have beautiful gloss.Allantoin can also promote tissue growth, cell metabolism, soften cuticle albumen.Because traditional handicraft extracts from natural animal-plant that the content of natural allantoin is very low, complex process, cost be too high, cannot use on a large scale, therefore the existing main chemical synthesis that adopts is extracted synthetic allantoin, as carbamide glyoxalic acid direct condensing method, acetic acid acid calcium salt acid-soluble method, carbamide dichloroacetic acid heating, oxalic acid electrolysis oxidation of glyoxal, Chloral synthetic method etc.
The hydrolyzed pearl of the present composition, its content is pressed the weighing scale approximately 0.01% to 20% of the present composition, preferably be about 0.01% to 15%, be more preferably 0.01% to 10%, its active matter content is pressed the weighing scale approximately 0.001% to 10% of the present composition, preferably approximately 0.001% to 8%, more preferably from about 0.001% to 5%.
The hydrolyzed pearl of the present composition, is that the enzymolysis process by Margarita powder obtains, and contains a large amount of calcium ions and pearl protein, has elimination oxygen-derived free radicals, anti-aging effects, and light speckle, makes the beautiful gloss of skin.
The hyaluronate sodium of the present composition, is the glutinous sugar of a kind of bionical thing, and molecular weight is greater than 1,000,000, and the hyaluronic acid sodium content of the present composition is by invention composition weight meter approximately 0.01% to 10%, preferably approximately 0.01% to 5%, be more preferably 0.01% to 3%.
In normal human skin horny layer, contain 10% to 20% moisture, it prevents skin aging, prevents that the various stimulations of external environment from having significant role skin care.With advancing age or the variation of environment, moisture can drop to below 10%, and skin can be dried, and produces wrinkle.The hyaluronate sodium of the present composition can be alleviated this problem, and its theoretical water retention value reaches 1000ml/g, is the key component of water conservation in human body skin, and not only moistening effect is good, and without greasy feeling and stop up pore etc. shortcoming.Can also eliminate oxygen-derived free radicals, repair the skin of damage after shining.
Cocoa/Sargassum composite extract in the present composition, it is a mixed extract, its content is pressed the weighing scale approximately 0.01% to 20% of the present composition, preferably be about 0.01% to 15%, be more preferably 0.01% to 10%, its active matter content is pressed the weighing scale approximately 0.001% to 10% of the present composition, and preferably approximately 0.001% to 8%, more preferably from about 0.001% to 5%.
Cocoa/Sargassum composite extract of the present composition, is natural plants source, and cocoa extract contains caffeine, theobromine isoreactivity composition, has antioxidation, antibacterial action, and activating cell, makes fragile muscle and skin white light pool.Sargassum extract contains special polysaccharide, protein, lipid, pigment and lower-molecular substance; also, containing taurine, methionine, cystine and derivant thereof etc., can make skin give gloss, can safeguard that epithelial cell grows up healthy and sound; reduce pigmentation, also have antibacterial action.
Radix Ginseng extract in the present composition, its content is pressed the weighing scale approximately 0.01% to 20% of the present composition, preferably be about 0.01% to 15%, be more preferably 0.01% to 10%, its active matter content is pressed the weighing scale approximately 0.001% to 10% of the present composition, preferably approximately 0.001% to 8%, more preferably from about 0.001% to 5%.
The Radix Ginseng extract of the present composition, for natural plants source, contains Saponin, protein, aminoacid, saccharide, vitamins, organic acid and various trace elements etc.Contained Radix Ginseng Saponin in Radix Ginseng extract, can significantly improve the content of hydroxyproline in skin, makes skin delicacy smooth, prevents wrinkle.The contained protein synthesis factor in Radix Ginseng extract, can increase skin elasticity.Contained aminoacid, can improve blood circulation and metabolism, and skin obtains required nutrition and moistens delicate.
As preferred again, described compositions consists of following component by mass percentage:
It is not 0 that above-mentioned hydrolyzed pearl, chamomile extract, cocoa/Sargassum composite extract and Radix Ginseng extract at least have a kind of.
In order to realize second above-mentioned object, the present invention has adopted following technical scheme:
A preparation method of preparing the above-mentioned astringent compositions that comprises skin conditioning agent and water-soluble silicon wax, the method comprises the following steps:
1) water, allantoin, glycerol, hydroxyethyl-cellulose, hyaluronate sodium mix, and are heated to 75～85 ℃, dissolve completely;
2) while being cooled to 50 ℃, add water-soluble silicon wax, chamomile extract, allantoin, hydrolyzed pearl, hyaluronate sodium, cocoa/Sargassum composite extract, Radix Ginseng extract, pigment, antiseptic, essence, 1,2-hexanediol/caprylyl glycol and solubilizing agent, stir;
3) add polyacrylamide/C13-14 isoparaffin/laureth-7 after stirring, rapid stirring 5 minutes, filters discharging;
4) storage → inspection of semifinished product → fill → product inspection → warehouse-in.
The present invention is owing to having adopted above-mentioned technical scheme, and product, after use, can keep the skin wet to skin, and soft skin makes skin be full of elasticity, and improves skin quality, and skin is taken on an entirely new look.
Accompanying drawing explanation
Fig. 1 is that sticky property evaluation map-water-soluble silicon wax and test substances ratio are 1: 3.
Fig. 2 is that wax sense evaluation map-water-soluble silicon wax and test substances ratio are 1: 3.
Fig. 3 is that emulsion viscosity evaluation map-water-soluble silicon wax and test substances ratio are 1: 3.
Fig. 4 is that spreadability evaluation map-water-soluble silicon wax and test substances ratio are 1: 3.
Fig. 5 is that smoothness evaluation map-water-soluble silicon wax and test substances ratio are 1: 3.
Fig. 6 is that greasy evaluation Tu – water-soluble silicon wax and test substances ratio are 1: 3.
Fig. 7 is water-soluble silicon wax sensory evaluation figure.
The specific embodiment
Preparation process of the present invention is the state of comparison homogeneous that each composition is mixed to, and step is:
1. water, allantoin, glycerol, hydroxyethyl-cellulose, hyaluronate sodium mix, and are heated to 80 ℃ of left and right, dissolve completely.
2. while being cooled to 50 ℃, add water-soluble silicon wax, chamomile extract, allantoin, hydrolyzed pearl, hyaluronate sodium,
Cocoa/Sargassum composite extract, Radix Ginseng extract, pigment, antiseptic, essence, 1,2-hexanediol/caprylyl glycol and solubilizing agent, stir.
3. after stirring, add polyacrylamide/C13-14 isoparaffin/laureth-7, rapid stirring 5 minutes, filters discharging.
4. storage → the inspection of semifinished product → fill → product inspection → warehouse-in.
Specific embodiment:
* 1. carbomers, derive from Lubrizol
* 2. couples-PEG-18 methyl ether dimethylsilane, derives from Dowcorning
Mutually 1 put into container and mix, be heated to 80 ℃, stirring and dissolving is complete; Be cooled to 50 ℃, add phase 2, stir; Add again phase 3, rapid stirring 5 minutes, mix homogeneously, discharging.
Method of testing:
In order to test moisturizing cosmetic result of the present invention, carried out investigation experiment on probation:
1, respondent: each department ordinary consumer 30 people, 20 parts of the trial state feedback forms of finally regaining.
2, control time: on October 20th, 1 2007 on August 20th, 2007.
3, use product: No. 1 product is the product of preparing according to formula of the present invention; No. 2 products are rival factory similar products.
4, method of testing: after tester face is clean, respectively No. 1 product and No. 2 products are coated on two cheek in left and right, observe and experience result of use.
5, test form is as follows:
The use of No. 1 product of table 1 (60 days) feedback conclusive table
No. 2 products of table 2 are used (60 days) feedback conclusive table
No. 1 product of table 3 and No. 2 products improve the contrast statistical table of the colour of skin
The statistical table of table 4 tester recommended products model
| Proposed model | No. 1 | No. 2 |
| Recommendation number | 18 | 2 |
| Percentage ratio | 90% | 10% |
6, feedback conclusion:
Tester all represents, is all better than No. 2 product in the moisture-retaining capacity of No. 1 product and sticky sense, and moisturizing is lasting, and there is no special sticky sense; Aspect horny layer softening, both evaluations are identical; In test process, although No. 1 product is absorbing and compacting in effect, slightly inferior, most consumers thinks that No. 1 product moisture-retaining capacity is stronger, and is improving aspect the colour of skin especially outstandingly, all No. 1 product is expressed one's approval; And there is not people to have allergic phenomena in the questionnaire reclaiming.
As shown in Table 5, No. 1 product of people's recommendation of 90%, only has No. 2 products of people's recommendation of 10%.
Claims (1)
1.
oneplant the preparation method containing the astringent compositions of plant extract and hydrolyzed pearl, it is characterized in that the method consists of following step:
1) mutually 1 put into container and mix, be heated to 80 ℃, stirring and dissolving is complete; Described phase 1 is by weight percentage by glycerol 8%, allantoin 2%, and hydroxyethyl-cellulose 0.6%, hyaluronate sodium 0.5% and deionized water surplus form, and above-mentioned deionized water surplus is water for other weight of this astringent compositions except other materials;
2) be cooled to 50 ℃, add phase 2, stir; Described phase 2 is by weight percentage by two-PEG-18 methyl ether dimethylsilane 5%, chamomile extract 10%, hydrolyzed pearl 2%, 1,2-hexanediol/caprylyl glycol 0.5%, cocoa/Sargassum composite extract 1%, Radix Ginseng extract 2%, essence 0.25%, antiseptic 0.4%, solubilizing agent 0.25% and pigment form in right amount;
3) add again phase 3, rapid stirring 5 minutes, mix homogeneously, discharging; Described phase 3 is 0.8% formation by polyacrylamide/C13-14 isoparaffin/laureth-7 by weight percentage.
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| CN106389263A (en) * | 2015-07-27 | 2017-02-15 | 杭州韩旭化妆品有限公司 | Composition with effects of moisturizing, repairing and free radical removing, preparation method and applications thereof |
| CN107875114A (en) * | 2017-12-27 | 2018-04-06 | 广西还珠海洋生物科技有限公司 | Humidity-preserving type surfactant |
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| JP3513873B2 (en) * | 1999-01-26 | 2004-03-31 | 株式会社コーセー | External preparation for skin |
| JP2001039848A (en) * | 1999-07-27 | 2001-02-13 | Kao Corp | Skin lotion |
| JP2003095915A (en) * | 2001-09-25 | 2003-04-03 | Shiseido Co Ltd | Skin care composition |
| KR20110087420A (en) * | 2010-01-26 | 2011-08-03 | 한림대학교 산학협력단 | Composition for preventing or improving diabetes induced complication containing anthemis tinctoria extract |
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| CN101664371A (en) * | 2009-09-29 | 2010-03-10 | 广东名臣有限公司 | Acne treatment cosmetic composition |
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Effective date of registration: 20230113 Address after: 313200 No. 99, Pearl Street, Moganshan high tech Industrial Development Zone, Deqing County, Huzhou City, Zhejiang Province Patentee after: OSMUN BIOLOGICAL Co.,Ltd. Address before: No. 518, Zhongxin North Road, Wukang Town, Deqing County, Huzhou City, Zhejiang Province, 313200 Patentee before: Shen Zhirong |