CN103191433A - Safe hollow capsules using plant starch as raw material and preparation process thereof - Google Patents
Safe hollow capsules using plant starch as raw material and preparation process thereof Download PDFInfo
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- CN103191433A CN103191433A CN2013101028476A CN201310102847A CN103191433A CN 103191433 A CN103191433 A CN 103191433A CN 2013101028476 A CN2013101028476 A CN 2013101028476A CN 201310102847 A CN201310102847 A CN 201310102847A CN 103191433 A CN103191433 A CN 103191433A
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Abstract
The invention discloses safe hollow capsules using plant starch as a raw material and a preparation process thereof. The hollow capsules comprise the following raw materials: 81-87 percent of purified water, 12.5-17.5 percent of plant starch, and 0.5-1 percent of carrageenan. The production cost of the hollow capsules prepared by adopting the preparation process is relatively low; because the plant starch is used as the main raw material, the hollow capsules are safe to human bodies and easy to absorb and decompose and completely meet the requirement of the pharmacopeia for quality; compared with the hollow capsules using a gelatin raw material, the hollow capsules have the advantage of wider crowd adaptability; and meanwhile, the hollow capsules are prevented from being crisp or soft due to the influence of humidity in the air to affect the use, so that the requirement for the production environment can be reduced.
Description
[technical field]
The present invention relates to a kind of Capsules and preparation technology thereof, be specifically related to a kind of plant amylum that utilizes and be safe Capsules and the preparation technology thereof of raw material.
[background technology]
The Capsules of China mainly is that raw material is made with the gelatin at present, and animal bone was boiled in the general employing of gelatin or leather-solid waste is made.The gelatine capsule general performance is good, but moisture is bigger to its influence, the easy deliquescing of capsule when air humidity is big, and when air was dry, capsule became fragile easily, thereby influences the use of product.Simultaneously gelatin is that the suitable crowd of raw material capsule is restricted, in the recent period since because to adopt gelatin be that the Capsules of primary raw material exists potential safety hazards such as serious chromium exceeds standard, be referred to as " toxic capsule ", and cause the extensive concern of society.
Prior art be the Capsules of primary raw material with the gelatin, its gelatin adopts the leather leftover pieces more, and leather needs to adopt tanning agent in the course of processing, therefore by its prepared Capsules, often crome metal exceeds standard.Accumulated in the tissue and chromium enters the chromium of human body, metabolism and the speed that is eliminated are very slow.After chromium entered blood, main iron ball albumen, albumin, r-globulin in blood plasma was combined, and Cr VI also can see through erythrocyte membrane, can have 50% Cr VI to enter cell in 15 minutes, was combined with hemoglobin after entering erythrocyte.The metabolite of chromium is mainly discharged from kidney, discharges through feces on a small quantity.Cr VI mainly is chronic murder by poisoning to the people, and it can pass through digestive tract, respiratory tract, skin and mucosa and invade human body, mainly accumulates in liver, kidney and the endocrine gland in vivo.Then easily accumulate in pulmonary by what respiratory tract entered.Cr VI has strong oxidation, so chronic poisoning often begins to develop into gradually incurable with local lesion.When respiratory tract is invaded human body, begin to encroach on upper respiratory tract, cause that rhinitis, pharyngitis and laryngitis, annual nearly 3,000 hundred million Capsules major part of bronchitis China adopt aforesaid way prepared, cause great medicinal potential safety hazard.
[summary of the invention]
For solving above deficiency, a kind of plant amylum that utilizes of the present invention is safe Capsules and the preparation technology thereof of raw material, Capsules by this technology preparation adopts plant amylum as primary raw material, its production cost is lower, do not contain simultaneously harmful heavy metal, be applicable to that each kind of groups is extensive, and be convenient to be absorbed by human body.
Technical problem to be solved by this invention is: the Capsules of prior art is owing to adopt gelatin to have the serious chromium problem that exceeds standard as the preparation technology of primary raw material, cause very big purpose for crowd's health, so need a kind of new safe Capsules to substitute existing technology.
Technical scheme provided by the present invention is: a kind of plant amylum that utilizes is safe Capsules and the preparation technology thereof of raw material, the various proportioning raw materials relations of its Capsules are as follows: pure water accounts for 81-87%, plant amylum 12.5-17.5%, carrageenan are 0.5%-1%.
Described Capsules can also contain surfactant, plasticizer and medicinal pigment, and its prescription is: pure water 80-86%, plant amylum are 12-17%, carrageenan is 0.5%-1%, surfactant is 0.03-0.05%, and plasticizer is 0.5%-0.7%, medicinal pigment 0.1-0.2%.
As preferably, described a kind of plant amylum that utilizes is safe Capsules and the preparation technology thereof of raw material, its plant amylum can be corn starch, sweet potato starch, Fructus Chaenomelis starch, Radix Puerariae starch, konjak starch, and surfactant is dodecyl sodium sulfate, and plasticizer is edible glycerol.
As preferably, described a kind of plant amylum that utilizes is safe Capsules and the preparation technology thereof of raw material, its preparation technology is as follows: be dissolved in plant amylum and carrageenan in the pure water respectively, further remove impurity by the doughnut membrane filtration, the starch fluid and the carrageenan solutions that merge gained, further stir, gelatinizing in the water-bath of 85-95 degree, add surfactant, plasticizer and medicinal pigment, dip in glue after further stirring, and then dried by the fire 1 hour under the 38-40 degree, further come unstuck, obtain described Capsules, further encapsulation is put in storage after the assay was approved.
Beneficial effect of the present invention is: adopt the made Capsules of preparation technology of the present invention, its production cost is lower, simultaneously because its adopt plant amylum as primary raw material to human body safety, be convenient to absorb decompose and reach the pharmacopeia prescription fully, it is more extensive that the Capsules of gelatin raw material adapts to colony relatively, be not subjected to simultaneously that humidity effect causes Capsules to become fragile or deliquescing in the air, influence is used, thereby production environment is required also can reduce.
Further understand feature of the present invention and technology contents for making, see embodiment for details, yet appended embodiment is only for reference and explanation usefulness, and the present invention is limited.
[specific embodiment]
Below in conjunction with specific embodiment the present invention is elaborated:
Embodiment 1, a kind of plant amylum that utilizes is safe Capsules and the preparation technology thereof of raw material, add 320 gram corn starchs in 1 liter of pure water, after the stirring and dissolving, adopt the doughnut membrane filtration to obtain corn starch liquid, carrageenan is added in 1 liter of pure water, above-mentioned solution is merged, and stir, gelatinizing in 90 degree water-baths adds dodecyl sodium sulfate 0.5 gram, 10 milliliters of edible glycerols, medicinal pigment 2 grams, dip in glue after stirring, and then dried by the fire 1 hour under the 38-40 degree, further come unstuck, obtain described Capsules, further encapsulation is put in storage after the assay was approved.
Embodiment 2, a kind of plant amylum that utilizes is safe Capsules and the preparation technology thereof of raw material, add 320 gram sweet potato starch in 1 liter of pure water, after the stirring and dissolving, adopt the doughnut membrane filtration to obtain sweet potato starch liquid, carrageenan is added in 1 liter of pure water, above-mentioned solution is merged, and stir, gelatinizing in 90 degree water-baths adds dodecyl sodium sulfate 0.5 gram, 10 milliliters of edible glycerols, medicinal pigment 2 grams, dip in glue after stirring, and then dried by the fire 1 hour under the 38-40 degree, further come unstuck, obtain described Capsules, further encapsulation is put in storage after the assay was approved.
Embodiment 3, a kind of plant amylum that utilizes is safe Capsules and the preparation technology thereof of raw material, add 320 gram Fructus Chaenomelis starch in 1 liter of pure water, after the stirring and dissolving, adopt the doughnut membrane filtration to obtain the Fructus Chaenomelis starch fluid, carrageenan is added in 1 liter of pure water, above-mentioned solution is merged, and stir, gelatinizing in 90 degree water-baths adds dodecyl sodium sulfate 0.5 gram, 10 milliliters of edible glycerols, medicinal pigment 2 grams, dip in glue after stirring, and then dried by the fire 1 hour under the 38-40 degree, further come unstuck, obtain described Capsules, further encapsulation is put in storage after the assay was approved.
Embodiment 4, a kind of plant amylum that utilizes is safe Capsules and the preparation technology thereof of raw material, add 320 gram Radix Puerariae starch in 1 liter of pure water, after the stirring and dissolving, adopt the doughnut membrane filtration to obtain Radix Puerariae starch liquid, carrageenan is added in 1 liter of pure water, above-mentioned solution is merged, and stir, gelatinizing in 90 degree water-baths adds dodecyl sodium sulfate 0.5 gram, 10 milliliters of edible glycerols, medicinal pigment 2 grams, dip in glue after stirring, and then dried by the fire 1 hour under the 38-40 degree, further come unstuck, obtain described Capsules, further encapsulation is put in storage after the assay was approved.
Embodiment 5, a kind of plant amylum that utilizes is safe Capsules and the preparation technology thereof of raw material, add 320 gram konjak starchs in 1 liter of pure water, after the stirring and dissolving, adopt the doughnut membrane filtration to obtain konjak starch liquid, carrageenan is added in 1 liter of pure water, above-mentioned solution is merged, and stir, gelatinizing in 90 degree water-baths adds dodecyl sodium sulfate 0.5 gram, 10 milliliters of edible glycerols, medicinal pigment 2 grams, dip in glue after stirring, and then dried by the fire 1 hour under the 38-40 degree, further come unstuck, obtain described Capsules, further encapsulation is put in storage after the assay was approved.
Embodiment 6, and a kind of plant amylum that utilizes is safe Capsules and the preparation technology thereof of raw material, add 320 gram corn starchs in 1 liter of pure water, after the stirring and dissolving, adopt the doughnut membrane filtration to obtain corn starch liquid, carrageenan is added in 1 liter of pure water, above-mentioned solution is merged, and stir, gelatinizing in 90 degree water-baths is dipped in glue after stirring, and then dried by the fire 1 hour under the 38-40 degree, further come unstuck, obtain described Capsules, further encapsulation is put in storage after the assay was approved.
Embodiment 7, and a kind of plant amylum that utilizes is safe Capsules and the preparation technology thereof of raw material, add 320 gram sweet potato starch in 1 liter of pure water, after the stirring and dissolving, adopt the doughnut membrane filtration to obtain sweet potato starch liquid, carrageenan is added in 1 liter of pure water, above-mentioned solution is merged, and stir, gelatinizing in 90 degree water-baths is dipped in glue after stirring, and then dried by the fire 1 hour under the 38-40 degree, further come unstuck, obtain described Capsules, further encapsulation is put in storage after the assay was approved.
Embodiment 8, and a kind of plant amylum that utilizes is safe Capsules and the preparation technology thereof of raw material, add 320 gram Fructus Chaenomelis starch in 1 liter of pure water, after the stirring and dissolving, adopt the doughnut membrane filtration to obtain the Fructus Chaenomelis starch fluid, carrageenan is added in 1 liter of pure water, above-mentioned solution is merged, and stir, gelatinizing in 90 degree water-baths is dipped in glue after stirring, and then dried by the fire 1 hour under the 38-40 degree, further come unstuck, obtain described Capsules, further encapsulation is put in storage after the assay was approved.
Embodiment 9, and a kind of plant amylum that utilizes is safe Capsules and the preparation technology thereof of raw material, add 320 gram konjak starchs in 1 liter of pure water, after the stirring and dissolving, adopt the doughnut membrane filtration to obtain konjak starch liquid, carrageenan is added in 1 liter of pure water, above-mentioned solution is merged, and stir, gelatinizing in 90 degree water-baths is dipped in glue after stirring, and then dried by the fire 1 hour under the 38-40 degree, further come unstuck, obtain described Capsules, further encapsulation is put in storage after the assay was approved.
Embodiment 10, and a kind of plant amylum that utilizes is safe Capsules and the preparation technology thereof of raw material, add 320 gram Radix Puerariae starch in 1 liter of pure water, after the stirring and dissolving, adopt the doughnut membrane filtration to obtain Radix Puerariae starch liquid, carrageenan is added in 1 liter of pure water, above-mentioned solution is merged, and stir, gelatinizing in 90 degree water-baths is dipped in glue after stirring, and then dried by the fire 1 hour under the 38-40 degree, further come unstuck, obtain described Capsules, further encapsulation is put in storage after the assay was approved.
Embodiment 11, a kind of plant amylum that utilizes is safe Capsules and the preparation technology thereof of raw material, add 350 gram corn starchs in 1 liter of pure water, after the stirring and dissolving, adopt the doughnut membrane filtration to obtain corn starch liquid, carrageenan is added in 1 liter of pure water, above-mentioned solution is merged, and stir, gelatinizing in 90 degree water-baths adds dodecyl sodium sulfate 0.5 gram, 10 milliliters of edible glycerols, medicinal pigment 2 grams, dip in glue after stirring, and then dried by the fire 1 hour under the 38-40 degree, further come unstuck, obtain described Capsules, further encapsulation is put in storage after the assay was approved.
Embodiment 12, a kind of plant amylum that utilizes is safe Capsules and the preparation technology thereof of raw material, add 400 gram corn starchs in 1 liter of pure water, after the stirring and dissolving, adopt the doughnut membrane filtration to obtain corn starch liquid, carrageenan is added in 1 liter of pure water, above-mentioned solution is merged, and stir, gelatinizing in 90 degree water-baths adds dodecyl sodium sulfate 0.5 gram, 10 milliliters of edible glycerols, medicinal pigment 2 grams, dip in glue after stirring, and then dried by the fire 1 hour under the 38-40 degree, further come unstuck, obtain described Capsules, further encapsulation is put in storage after the assay was approved.
Embodiment 13, and a kind of plant amylum that utilizes is safe Capsules and the preparation technology thereof of raw material, add 350 gram corn starchs in 1 liter of pure water, after the stirring and dissolving, adopt the doughnut membrane filtration to obtain corn starch liquid, carrageenan is added in 1 liter of pure water, above-mentioned solution is merged, and stir, gelatinizing in 90 degree water-baths is dipped in glue after stirring, and then dried by the fire 1 hour under the 38-40 degree, further come unstuck, obtain described Capsules, further encapsulation is put in storage after the assay was approved.
Embodiment 14, and a kind of plant amylum that utilizes is safe Capsules and the preparation technology thereof of raw material, add 400 gram corn starchs in 1 liter of pure water, after the stirring and dissolving, adopt the doughnut membrane filtration to obtain corn starch liquid, carrageenan is added in 1 liter of pure water, above-mentioned solution is merged, and stir, gelatinizing in 90 degree water-baths is dipped in glue after stirring, and then dried by the fire 1 hour under the 38-40 degree, further come unstuck, obtain described Capsules, further encapsulation is put in storage after the assay was approved.
Embodiment 15, and a kind of plant amylum that utilizes is safe Capsules and the preparation technology thereof of raw material, add 320 gram corn starchs in 1 liter of pure water, after the stirring and dissolving, adopt the doughnut membrane filtration to obtain corn starch liquid, carrageenan is added in 1 liter of pure water, above-mentioned solution is merged, and stir, gelatinizing in 95 degree water-baths is dipped in glue after stirring, and then dried by the fire 1 hour under the 38-40 degree, further come unstuck, obtain described Capsules, further encapsulation is put in storage after the assay was approved.
Embodiment 16, and a kind of plant amylum that utilizes is safe Capsules and the preparation technology thereof of raw material, add 350 gram corn starchs in 1 liter of pure water, after the stirring and dissolving, adopt the doughnut membrane filtration to obtain corn starch liquid, carrageenan is added in 1 liter of pure water, above-mentioned solution is merged, and stir, gelatinizing in 95 degree water-baths is dipped in glue after stirring, and then dried by the fire 1 hour under the 38-40 degree, further come unstuck, obtain described Capsules, further encapsulation is put in storage after the assay was approved.
Embodiment 17, and a kind of plant amylum that utilizes is safe Capsules and the preparation technology thereof of raw material, add 400 gram corn starchs in 1 liter of pure water, after the stirring and dissolving, adopt the doughnut membrane filtration to obtain corn starch liquid, carrageenan is added in 1 liter of pure water, above-mentioned solution is merged, and stir, gelatinizing in 95 degree water-baths is dipped in glue after stirring, and then dried by the fire 1 hour under the 38-40 degree, further come unstuck, obtain described Capsules, further encapsulation is put in storage after the assay was approved.
Adopt the made Capsules of preparation technology of the present invention, its production cost is lower, simultaneously because its adopt plant amylum as primary raw material to human body safety, be convenient to absorb decompose and reach the pharmacopeia prescription fully, it is more extensive that the Capsules of gelatin raw material adapts to colony relatively, be not subjected to simultaneously that humidity effect causes Capsules to become fragile or deliquescing in the air, influence is used, thereby production environment is required also can reduce.
Yet the preferable feasible embodiment of above-mentioned only the present invention, non-so limitation protection domain of the present invention is done various distortion or is applied mechanically all within this technical scheme protection domain according to above-described embodiment.
Claims (4)
1. one kind is utilized plant amylum for safe Capsules and the preparation technology thereof of raw material, it is characterized in that, the various proportioning raw materials relations of Capsules are as follows: pure water accounts for 81-87%, and plant amylum 12.5-17.5%, carrageenan are 0.5%-1%.
2. one kind is utilized plant amylum to be safe Capsules and the preparation technology thereof of raw material, it is characterized in that, described Capsules can also contain surfactant, plasticizer and medicinal pigment, its prescription is: pure water 80-86%, plant amylum is 12-17%, and carrageenan is 0.5%-1%, and surfactant is 0.03-0.05%, plasticizer is 0.5%-0.7%, medicinal pigment 0.1-0.2%.
3. a kind of plant amylum that utilizes according to claim 1 and 2 is safe Capsules and the preparation technology thereof of raw material, its plant amylum can be corn starch, sweet potato starch, Fructus Chaenomelis starch, Radix Puerariae starch, konjak starch, surfactant is dodecyl sodium sulfate, and plasticizer is edible glycerol.
4. a kind of plant amylum that utilizes according to claim 1 and 2 is safe Capsules and the preparation technology thereof of raw material, its preparation technology is as follows: be dissolved in plant amylum and carrageenan in the pure water respectively, further remove impurity by the doughnut membrane filtration, the starch fluid and the carrageenan solutions that merge gained, further stir, gelatinizing in the water-bath of 85-95 degree, add surfactant, plasticizer and medicinal pigment, dip in glue after further stirring, and then dried by the fire 1 hour under the 38-40 degree, further come unstuck, obtain described Capsules, further encapsulation is put in storage after the assay was approved.
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103830736A (en) * | 2014-03-05 | 2014-06-04 | 中国科学院青岛生物能源与过程研究所 | Production method of starch empty capsule |
CN103948561A (en) * | 2014-01-08 | 2014-07-30 | 天津科技大学 | High-calcium plant-derived hollow capsule and preparation method and application thereof |
CN104083768A (en) * | 2014-07-02 | 2014-10-08 | 湖南尔康制药股份有限公司 | Premix auxiliary and preparation method thereof |
EP2937082A1 (en) | 2014-04-21 | 2015-10-28 | Hunan Er-Kang Pharmaceutical Co., Ltd. | Film-forming composite used to make starch softgel capsules and the method to prepare it |
CN105456226A (en) * | 2015-12-16 | 2016-04-06 | 华南理工大学 | Hydroxypropyl methyl cellulose/hydroxypropyl starch plant empty capsule and preparation method |
CN108904464A (en) * | 2018-08-17 | 2018-11-30 | 苏州煜水生物科技有限公司 | A kind of starch empty pocket of pure plant and preparation method thereof |
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CN102342509A (en) * | 2011-09-15 | 2012-02-08 | 山东商业职业技术学院 | Konjak polysaccharide compound soft capsule shell and preparation method thereof |
CN102836142A (en) * | 2012-08-03 | 2012-12-26 | 青岛源海底海洋生物技术有限公司 | Hollow capsule and preparation method thereof |
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CN1623529A (en) * | 2004-12-09 | 2005-06-08 | 浙江工业大学 | Formula of making hollow capsule and its preparation method |
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Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103948561A (en) * | 2014-01-08 | 2014-07-30 | 天津科技大学 | High-calcium plant-derived hollow capsule and preparation method and application thereof |
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EP2937082A1 (en) | 2014-04-21 | 2015-10-28 | Hunan Er-Kang Pharmaceutical Co., Ltd. | Film-forming composite used to make starch softgel capsules and the method to prepare it |
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CN105456226A (en) * | 2015-12-16 | 2016-04-06 | 华南理工大学 | Hydroxypropyl methyl cellulose/hydroxypropyl starch plant empty capsule and preparation method |
CN105456226B (en) * | 2015-12-16 | 2018-11-02 | 华南理工大学 | Hydroxypropyl methyl cellulose/hydroxypropul starch plant hollow capsule and preparation method |
CN108904464A (en) * | 2018-08-17 | 2018-11-30 | 苏州煜水生物科技有限公司 | A kind of starch empty pocket of pure plant and preparation method thereof |
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Application publication date: 20130710 |