CN103127389B - Compound liver protection jewel orchid submicron powder and preparation method thereof - Google Patents
Compound liver protection jewel orchid submicron powder and preparation method thereof Download PDFInfo
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- CN103127389B CN103127389B CN201210577066.8A CN201210577066A CN103127389B CN 103127389 B CN103127389 B CN 103127389B CN 201210577066 A CN201210577066 A CN 201210577066A CN 103127389 B CN103127389 B CN 103127389B
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- 210000004185 liver Anatomy 0.000 title claims abstract description 41
- 239000000843 powder Substances 0.000 title claims abstract description 32
- 150000001875 compounds Chemical class 0.000 title claims abstract description 29
- 238000002360 preparation method Methods 0.000 title claims abstract description 8
- 240000000001 Ludisia discolor Species 0.000 title abstract 7
- 239000002994 raw material Substances 0.000 claims description 38
- 238000010298 pulverizing process Methods 0.000 claims description 22
- 239000002245 particle Substances 0.000 claims description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 238000001291 vacuum drying Methods 0.000 claims description 8
- 238000004806 packaging method and process Methods 0.000 claims description 7
- 239000003390 Chinese drug Substances 0.000 claims description 6
- 241000628997 Flos Species 0.000 claims description 4
- 239000008280 blood Substances 0.000 claims description 4
- 210000004369 blood Anatomy 0.000 claims description 4
- 210000003734 kidney Anatomy 0.000 claims description 4
- 241000222336 Ganoderma Species 0.000 claims description 2
- 238000010926 purge Methods 0.000 claims description 2
- 230000004304 visual acuity Effects 0.000 claims description 2
- 239000003814 drug Substances 0.000 abstract description 5
- 238000000034 method Methods 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 230000008569 process Effects 0.000 abstract description 3
- 230000007547 defect Effects 0.000 abstract description 2
- 238000004090 dissolution Methods 0.000 abstract description 2
- 239000000463 material Substances 0.000 abstract 2
- 235000017784 Mespilus germanica Nutrition 0.000 abstract 1
- 244000182216 Mimusops elengi Species 0.000 abstract 1
- 235000000560 Mimusops elengi Nutrition 0.000 abstract 1
- 240000006079 Schisandra chinensis Species 0.000 abstract 1
- 235000008422 Schisandra chinensis Nutrition 0.000 abstract 1
- 235000007837 Vangueria infausta Nutrition 0.000 abstract 1
- 238000009835 boiling Methods 0.000 abstract 1
- 235000008216 herbs Nutrition 0.000 abstract 1
- 230000000361 pesticidal effect Effects 0.000 abstract 1
- 230000000704 physical effect Effects 0.000 abstract 1
- 238000003672 processing method Methods 0.000 description 5
- 210000000170 cell membrane Anatomy 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 235000013305 food Nutrition 0.000 description 4
- 230000006978 adaptation Effects 0.000 description 3
- 230000003203 everyday effect Effects 0.000 description 3
- 230000002443 hepatoprotective effect Effects 0.000 description 3
- 235000012054 meals Nutrition 0.000 description 3
- 210000004027 cell Anatomy 0.000 description 2
- 210000003494 hepatocyte Anatomy 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 239000012567 medical material Substances 0.000 description 2
- 230000001954 sterilising effect Effects 0.000 description 2
- 241000934230 Anoectochilus roxburghii Species 0.000 description 1
- 206010008909 Chronic Hepatitis Diseases 0.000 description 1
- 101100256850 Drosophila melanogaster EndoA gene Proteins 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 208000004930 Fatty Liver Diseases 0.000 description 1
- 206010019708 Hepatic steatosis Diseases 0.000 description 1
- 206010067125 Liver injury Diseases 0.000 description 1
- 206010067482 No adverse event Diseases 0.000 description 1
- 208000031971 Yin Deficiency Diseases 0.000 description 1
- 230000001154 acute effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000001413 cellular effect Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000001989 choleretic effect Effects 0.000 description 1
- 230000000857 drug effect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 208000010706 fatty liver disease Diseases 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 230000002440 hepatic effect Effects 0.000 description 1
- 208000006454 hepatitis Diseases 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000003908 liver function Effects 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000001473 noxious effect Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 231100000915 pathological change Toxicity 0.000 description 1
- 230000036285 pathological change Effects 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 231100000240 steatosis hepatitis Toxicity 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
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- Medicines Containing Plant Substances (AREA)
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Abstract
The invention discloses compound liver protection jewel orchid submicron powder and a preparation method of the compound liver protection jewel orchid submicron powder. Medicinal materials such as jewel orchid, medlar and schisandra chinensis are matched and processed to submicron powder. The submicron powder is good in taste and convenient to carry due to the facts that the submicron powder can be directly taken after being brewed without boiling and has no dregs. By means of the preparation method of the compound liver protection jewel orchid submicron powder, the inherent pesticide effect basis and the physical property of the jewel orchid are contained, and a cell breakage degree can reach more than 95%, so that the dissolution rate of effective components is greatly improved, consumption of the medicine materials is reduced, and medicinal herbs resource are saved. The preparation method of the compound liver protection jewel orchid submicron powder is simple in technical process, low in equipment requirement, capable of overcoming the defect of environment pollution due to the fact that a large amount of menstruum and energy consumed in prior art is saved, capable of saving energy and the medicinal herb resource, economical, environment-friendly and suitable for industrialized production.
Description
Technical field
The invention belongs to Chinese medicine manufacture field, be specifically related to a kind of compound recipe and protect the liver Herba Anoectochili roxburghii superfine powder and processing method thereof.
Background technology
Herba Anoectochili roxburghii is among the peoplely used for the treatment of acute, chronic hepatitis at Fujian platform, hepatocarcinoma has the centuries to the applicating history of more than one thousand years, except applying with other Chinese medicine formulas, current Fujian You Duojia hospital is made compound Jin Anoectochilus roxburghii oral liquid hospital preparation and is applied to clinical, evident in efficacy, and has no adverse reaction.
According to a large amount of Herba Anoectochili roxburghii pharmacological experiment study bibliographical information, Herba Anoectochili roxburghii energy direct effect what liver plasma membrane, protects the complete of liver plasma membrane, prevents noxious agents damage liver plasma membrane, and prevents the pathological changes of hepatocyte from becoming downright bad.Can liver plasma membrane be permeated simultaneously, promote the metabolism of liver, injured cell is brought back to life, so regeneration, and the function of hepatocyte endo enzyme can be recovered again, promote cellular oxidation, make the every test value of liver function recover normal.In addition powerful choleretic effect is still had.
Herba Anoectochili roxburghii take tradition to decoct or the mode that brews, these instructions of taking are time-consuming, take and carry inconvenience, and decoct or in medicinal residues after brewing still containing part effective ingredient, it is poor that food mouthfeel chewed by medicinal residues, generally discards, cause waste.
Summary of the invention
The object of the invention is to overcome prior art defect, provide a kind of compound recipe to protect the liver Herba Anoectochili roxburghii superfine powder and processing method thereof.
Technical scheme of the present invention is as follows:
A kind of compound recipe protects the liver Herba Anoectochili roxburghii superfine powder, comprises the component of following weight portion:
Herba Anoectochili roxburghii 30 ~ 50 weight portion;
Fructus Lycii 15 ~ 25 weight portion;
Fructus Schisandrae Chinensis 15 ~ 25 weight portion.
Another technical scheme of the present invention is as follows:
Compound recipe protects the liver a processing method for Herba Anoectochili roxburghii superfine powder, it is characterized in that: comprise the steps:
(1) take each raw material components by such as following weight parts, comprising:
Herba Anoectochili roxburghii 30 ~ 50 weight portion
Fructus Lycii 15 ~ 25 weight portion
Fructus Schisandrae Chinensis 15 ~ 25 weight portion;
(2) each raw material components of step (1) is carried out low-temperature vacuum drying;
(3) dried each raw material components is carried out coarse pulverization;
(4) each raw material components after coarse pulverization is carried out micronizing, and fully mix, obtain described compound recipe and protect the liver Herba Anoectochili roxburghii superfine powder;
In a preferred embodiment of the invention, described step (2) is: by each raw material components of step (1) 40 ~ 60 DEG C, carry out low-temperature vacuum drying 4 ~ 6 hours under the condition of 2.6 ~ 2.8kPa, the water content to each raw material components is less than 6%.
In a preferred embodiment of the invention, described step (3) is: by dried each raw material components coarse pulverization to particle diameter 2 ~ 4mm.
In a preferred embodiment of the invention, described step (4) is: each raw material components after coarse pulverization is carried out at 25 ~ 45 DEG C micronizing to fineness 1000 order ~ 2500 order, particle diameter is less than 10 μm, and fully mixes, and obtains described compound recipe and protects the liver Herba Anoectochili roxburghii superfine powder.
In a preferred embodiment of the invention, also comprise step (5): step (4) gained compound recipe is protected the liver Herba Anoectochili roxburghii superfine powder and carries out sterilizing, carry out packaging and get product.
In a preferred embodiment of the invention, the sterilizing of described step (5) is the microwave sterilizating of 3 ~ 5 minutes.
The invention has the beneficial effects as follows:
1, the present invention is by Herba Anoectochili roxburghii and the medical material such as Fructus Lycii, Fructus Schisandrae Chinensis compatibility, is processed into superfine powder, directly can brew and take, need not decoct, and without slag, makes to take mouthfeel good, carry convenient;
2, micronizing processing method of the present invention, not only maintain intrinsic drug effect basis and the physical characteristic of Herba Anoectochili roxburghii, and cell breakage reaches more than 95%, the dissolution rate of effective ingredient improves greatly, reduces medical material consumption, saves medicine source;
3 method technical processs of the present invention are simple, and equipment requirements is low, save tradition and extract a large amount of solvent of consumption and the energy, cause the drawback of environmental pollution, save the energy and medicine source, economic environmental protection, be applicable to suitability for industrialized production.
Detailed description of the invention
Below by way of detailed description of the invention, technical scheme of the present invention is further detailed and is described.
Embodiment 1
(1) take each raw material components by such as following weight parts, comprising: Herba Anoectochili roxburghii 30g, Fructus Lycii, Fructus Schisandrae Chinensis, Folium Nelumbinis, Fructus Crataegi, Ganoderma, each 15 ~ 25g of Herba Silybi mariani;
(2) by each raw material components of step (1) 60 DEG C, carry out low-temperature vacuum drying 4 hours under the condition of 2.8kPa, the water content to each raw material components is 4%;
(3) by dried each raw material components coarse pulverization to particle diameter 2mm;
(4) each raw material components after coarse pulverization is dropped into Study on Supermicro-pulverization of Traditional Chinese Drugs machine, at 30 ± 5 DEG C, carry out micronizing to fineness 2000 order, particle diameter is less than 10 μm, and fully mixes, and obtains described compound recipe and protects the liver Herba Anoectochili roxburghii superfine powder.
(5) step (4) gained compound recipe is protected the liver Herba Anoectochili roxburghii superfine powder and carry out microwave sterilizating 3 minutes, carry out packaging and get product.
[effect] flat invigorating the liver and kidney, blood fat reducingization is turbid.
[adaptation population] is for preventing the nourishing the liver hepatoprotective of fatty liver and subhealth state personage.
[usage and dosage] is bfore meals, every day three times, and each 5g, is about 500ml by warm water and brews.
[attention] avoids pungent greasy food.
Embodiment 2
(1) take each raw material components by such as following weight parts, comprising:: Herba Anoectochili roxburghii 40g, Fructus Lycii, Fructus Schisandrae Chinensis, Flos puerariae lobatae, Flos Chrysanthemi, Rhizoma Alismatis, each 15 ~ 25g of Radix Glycyrrhizae;
(2) by each raw material components of step (1) 40 DEG C, carry out low-temperature vacuum drying 6 hours under the condition of 2.6kPa, the water content to each raw material components is 5%;
(3) by dried each raw material components coarse pulverization to particle diameter 3mm;
(4) each raw material components after coarse pulverization is dropped into Study on Supermicro-pulverization of Traditional Chinese Drugs machine, at 35 ± 5 DEG C, carry out micronizing to fineness 1500 order, particle diameter is less than 10 μm, and fully mixes, and obtains described compound recipe and protects the liver Herba Anoectochili roxburghii superfine powder.
(5) step (4) gained compound recipe is protected the liver Herba Anoectochili roxburghii superfine powder and carry out microwave sterilizating 4 minutes, carry out packaging and get product.
[effect] nourishing yin and purging fire, nourishing the liver to improve visual acuity.
[adaptation population] is for the nourishing the liver of the personage that smokes, drinks, hepatoprotective.
[usage and dosage] is bfore meals, every day three times, and each 5g, is about 500ml by warm water and brews.
[attention] avoids pungent greasy food.
Embodiment 3
(1) take each raw material components by such as following weight parts, comprising:: Herba Anoectochili roxburghii 50g, Fructus Lycii, Fructus Schisandrae Chinensis, Fructus Ligustri Lucidi, Fructus Jujubae, each 15 ~ 25g of Fructus Corni
(2) by each raw material components of step (1) 60 DEG C, carry out low-temperature vacuum drying 5 hours under the condition of 2.67kPa, the water content to each raw material components is less than 6%;
(3) by dried each raw material components coarse pulverization to particle diameter 4mm;
(4) each raw material components after coarse pulverization is dropped into Study on Supermicro-pulverization of Traditional Chinese Drugs machine, at 40 ± 5 DEG C, carry out micronizing to fineness 1000 order, particle diameter is less than 10 μm, and fully mixes, and obtains described compound recipe and protects the liver Herba Anoectochili roxburghii superfine powder.
(5) step (4) gained compound recipe is protected the liver Herba Anoectochili roxburghii superfine powder and carry out microwave sterilizating 5 minutes, carry out packaging and get product.
[effect] nourishing the liver and kidney, QI invigorating and blood producing.
[adaptation population] is for the nourishing the liver hepatoprotective of the hepatic and renal YIN deficiency and Mrs blood-deficiency type.
[usage and dosage] is bfore meals, every day three times, and each 5g, is about 500ml by warm water and brews.
[attention] avoids pungent greasy food.
The above, be only preferred embodiment of the present invention, therefore can not limit scope of the invention process according to this, the equivalence change namely done according to the scope of the claims of the present invention and description with modify, all should still belong in scope that the present invention contains.
Claims (3)
1. a flat invigorating the liver and kidney, the turbid compound recipe of blood fat reducingization protects the liver Herba Anoectochili roxburghii superfine powder, it is characterized in that: be made up of the component of following weight:
Herba Anoectochili roxburghii 30g;
Fructus Lycii 15 ~ 25g;
Fructus Schisandrae Chinensis 15 ~ 25 g;
Folium Nelumbinis 15-25g;
Fructus Crataegi 15-25g;
Ganoderma 15-25g;
Herba Silybi mariani 15-25g;
Its preparation method is, (1) takes each raw material components by as above weight;
(2) by each raw material components of step (1) 60 DEG C, carry out low-temperature vacuum drying 4 hours, to the water content 4% of each raw material components under the condition of 2.8kPa;
(3) dried each raw material components is carried out coarse pulverization to particle diameter 2mm;
(4) each raw material components after coarse pulverization is dropped into Study on Supermicro-pulverization of Traditional Chinese Drugs machine, at 30 ± 5 DEG C, carry out micronizing to fineness 2000 order, particle diameter is less than 10 μm, and fully mixes, and obtains described compound recipe and protects the liver Herba Anoectochili roxburghii superfine powder;
(5) step (4) gained compound recipe is protected the liver Herba Anoectochili roxburghii superfine powder and carry out microwave sterilizating 3 minutes, carry out packaging and get product.
2. the compound recipe of nourishing yin and purging fire, nourishing the liver to improve visual acuity protects the liver a Herba Anoectochili roxburghii superfine powder, it is characterized in that: be made up of the component of following weight:
Herba Anoectochili roxburghii 40g;
Fructus Lycii 15 ~ 25g;
Fructus Schisandrae Chinensis 15 ~ 25 g;
Flos puerariae lobatae 15-25g;
Flos Chrysanthemi 15-25g;
Rhizoma Alismatis 15-25g;
Radix Glycyrrhizae 15-25g;
Its preparation method is, (1) takes each raw material components by as above weight;
(2) by each raw material components of step (1) 40 DEG C, carry out low-temperature vacuum drying 6 hours, to the water content 5% of each raw material components under the condition of 2.6kPa;
(3) dried each raw material components is carried out coarse pulverization to particle diameter 3mm;
(4) each raw material components after coarse pulverization is dropped into Study on Supermicro-pulverization of Traditional Chinese Drugs machine, at 35 ± 5 DEG C, carry out micronizing to fineness 1500 order, particle diameter is less than 10 μm, and fully mixes, and obtains described compound recipe and protects the liver Herba Anoectochili roxburghii superfine powder;
(5) step (4) gained compound recipe is protected the liver Herba Anoectochili roxburghii superfine powder and carry out microwave sterilizating 4 minutes, carry out packaging and get product.
3. the compound recipe of nourishing the liver and kidney, QI invigorating and blood producing protects the liver a Herba Anoectochili roxburghii superfine powder, it is characterized in that: be made up of the component of following weight:
Herba Anoectochili roxburghii 50g;
Fructus Lycii 15 ~ 25g;
Fructus Schisandrae Chinensis 15 ~ 25 g;
Fructus Ligustri Lucidi 15-25g;
Fructus Jujubae 15-25g;
Fructus Corni 15-25g;
Its preparation method is, (1) takes each raw material components by as above weight;
(2) by each raw material components of step (1) 60 DEG C, carry out low-temperature vacuum drying 5 hours under the condition of 2.67kPa, the water content to each raw material components is less than 6%;
(3) dried each raw material components is carried out coarse pulverization to particle diameter 4mm;
(4) each raw material components after coarse pulverization is dropped into Study on Supermicro-pulverization of Traditional Chinese Drugs machine, at 40 ± 5 DEG C, carry out micronizing to fineness 1000 order, particle diameter is less than 10 μm, and fully mixes, and obtains described compound recipe and protects the liver Herba Anoectochili roxburghii superfine powder;
(5) step (4) gained compound recipe is protected the liver Herba Anoectochili roxburghii superfine powder and carry out microwave sterilizating 5 minutes, carry out packaging and get product.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210577066.8A CN103127389B (en) | 2012-12-26 | 2012-12-26 | Compound liver protection jewel orchid submicron powder and preparation method thereof |
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| CN201210577066.8A CN103127389B (en) | 2012-12-26 | 2012-12-26 | Compound liver protection jewel orchid submicron powder and preparation method thereof |
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| CN103127389A CN103127389A (en) | 2013-06-05 |
| CN103127389B true CN103127389B (en) | 2014-12-17 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106177474A (en) * | 2016-09-06 | 2016-12-07 | 福建虎伯寮药业有限责任公司 | A kind of roxburgh anoectochilus terminal bud buccal tablet with treatment chronic hepatitis effect |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105641440A (en) * | 2016-01-25 | 2016-06-08 | 湖北妙莲天香生物科技有限公司 | Food therapy stewing product with hypertension, hyperlipidemia and hyperglycemia reducing function |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101327288A (en) * | 2008-07-25 | 2008-12-24 | 四川大千药业有限公司 | Method for preparing Liaoyuanqili super fine powder |
| CN102258740A (en) * | 2011-07-15 | 2011-11-30 | 陈春山 | Medicinal composition with effects of improving immunity of organisms and liver functions |
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2012
- 2012-12-26 CN CN201210577066.8A patent/CN103127389B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101327288A (en) * | 2008-07-25 | 2008-12-24 | 四川大千药业有限公司 | Method for preparing Liaoyuanqili super fine powder |
| CN102258740A (en) * | 2011-07-15 | 2011-11-30 | 陈春山 | Medicinal composition with effects of improving immunity of organisms and liver functions |
Non-Patent Citations (3)
| Title |
|---|
| "枸杞多糖与五味子对四氯化碳所致小鸭急性肝损伤的影响";纪丽莎等;《中兽医学杂志》;20091231(第3期);无 * |
| "金线莲的药理活性研究进展";唐健等;《海峡药学》;20081231(第12期);第77-79页 * |
| 金线莲化学成分及药理活性研究进展;张红艳等;《海峡药学》;20090115(第01期);第82-84页 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106177474A (en) * | 2016-09-06 | 2016-12-07 | 福建虎伯寮药业有限责任公司 | A kind of roxburgh anoectochilus terminal bud buccal tablet with treatment chronic hepatitis effect |
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Effective date of registration: 20180209 Address after: 361000 Fujian Province, Xiamen city Xiangan District Haixiang Boulevard Hai Ming Road No. 506-508 Patentee after: Minwang Pharmaceutical Co. Ltd. (Xiamen) Address before: 361000 Fujian Province, Xiamen city Xiangan District Haixiang Boulevard Hai Ming Road No. 506-508 Patentee before: FUJIAN JINCAO BIOLOGICAL GROUP CO., LTD. |
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