CN103111087B - Extraction device of plant active ingredient - Google Patents
Extraction device of plant active ingredient Download PDFInfo
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- CN103111087B CN103111087B CN201310080571.6A CN201310080571A CN103111087B CN 103111087 B CN103111087 B CN 103111087B CN 201310080571 A CN201310080571 A CN 201310080571A CN 103111087 B CN103111087 B CN 103111087B
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Abstract
The invention discloses an extraction device of a plant active ingredient. The device comprises a homogenate equipment tank body (1) and an end cover arranged at the upper end, wherein the end cover (13) and the homogenate equipment tank body (1) are sealed through a C-shaped clamp and a gasket; a feed funnel (12), an anchor agitator (6), a high-speed shearing agitator (9) and an ultrasonic generator (8) are mounted on the end cover (13); an agitating paddle of the anchor agitator (6), the high-speed shearing agitator (9) and a probe (10) of the ultrasonic generator all extend into a working cavity of the homogenate equipment tank body (1) from the end cover (13); the anchor agitator (6) comprises a motor (7) providing power, a rotation shaft and an agitating paddle; the high-speed shearing agitator (9) and the probe (10) of the ultrasonic generator are located between the agitating paddle and the rotation shaft; and a detachable blade (11) is mounted on the rotation shaft. The device disclosed by the invention has a simple structure and is easy to clean; and the working efficiency is high, and the operation range is wide.
Description
Technical field
The present invention relates to a kind of chemical extraction device, be specifically related to a kind of extraction element of effective ingredients in plant.
Background technology
The extract of effective ingredients in plant has larger economic worth, such as orange peel essential oil, and micro-algae oil, Rosa Damascana, and the effective effective component in rare Chinese herbal medicine, they are widely used in the industries such as medicine, cosmetics, food.Saturated and the unrighted acid (also referred to as thick grease) of effective ingredients in plant mainly C14-18, the extraction for effective ingredients in plant has been come by extraction element, and the quality of the performance of extraction element is vital factor in producing.
But the operating efficiency of the extraction element of prior art is all lower, produces length consuming time, adds production cost.Meanwhile, the extraction element of prior art usually can only be used for certain specific raw material and extract specific extract, in process of production, usually will adopt different extraction elements according to raw material with for the difference of the active ingredient extracted.
Summary of the invention
In order to solve above-mentioned Problems existing, the object of the present invention is to provide a kind of extraction element of effective ingredients in plant, this device adopts the tactic pattern of fixing end cap, is beneficial to the replacing of parts, cleaning and raw-material interpolation; At end cap welding liquid make-up charging aperture, be convenient to add solvent in leaching process; By ultrasonic extraction combine with technique in extraction element, be conducive to the simplification of separating step; Adopt circulation, to accelerate leaching process, raise the efficiency, rare Chinese herbal medicine is fallen and better keeps its property of medicine.This device is by jet strengthened for high speed shear and ultrasonic cavitation strengthening coupling simultaneously, apply in the extraction of plant active principle, adopt stirring at low speed and low velocity shear effect, structure refinement is delivered in useful effect region, utilize ultrasonic technology and high speed shear, rapid destruction eucaryotic cell structure, makes active ingredient discharge.
The present invention is achieved by the following technical solutions:
The extraction element of effective ingredients in plant provided by the invention, comprises the end cap 13 of homogenate equipment tank body 1 and the setting of its upper end, and described end cap 13, is characterized in that by C-type clamp and gasket seal with homogenate equipment tank body 1:
Described loading hopper 12, anchor agitator 6, high shear agitation device 9 and supersonic generator 8 are installed on end cap 13; The probe 10 of the paddle of described anchor agitator 6, high shear agitation device 9 and supersonic generator all stretches into from described end cap 13 in the working chamber of homogenate equipment tank body 1; Described anchor agitator 6 comprises for it provides the motor 7 of power, turning cylinder and paddle, and the paddle of described anchor agitator 6 is fixedly connected with motor 7 by turning cylinder; Described paddle is " U " shape paddle, and described high shear agitation device 9 and supersonic generator pop one's head in 10 between described paddle and power transmission shaft; Described turning cylinder is provided with dismountable blade 11.
According to the extraction element of effective ingredients in plant provided by the invention, preferably, described loading hopper 12 is welded on end cap 13; Its lower end diameter is 10-25mm, middle connection globe valve; Described loading hopper 12 material is stainless steel.
According to the extraction element of effective ingredients in plant provided by the invention, preferably, the lower end of described motor 7 is welded on end cap 13 center.
According to the extraction element of effective ingredients in plant provided by the invention, preferably, described high shear agitation device 9 and supersonic generator 8 are connected on end cap 13 by end face seal.
According to the extraction element of effective ingredients in plant provided by the invention, preferably, the diameter of described high shear agitation device 9 outer shaft stator is 20mm, and there are 6 rectangular teeths end, and long is 3.4mm, wide 2.0mm, high 7.1mm; Interior axle rotor is 3 teeth, the long 2.51mm of upper section of tooth, the long 6.1mm of lower section, width 2.5mm, height 8.2mm, and the gap of rotor is 0.4mm; The material of described fast shearing stirrer 9 is selected from stainless steel.
According to the extraction element of effective ingredients in plant provided by the invention, preferably, described supersonic generator 10 diameters of popping one's head in are 18-24mm, and material is selected from stainless steel.
According to the extraction element of effective ingredients in plant provided by the invention, preferably, the length of described blade 11 is 1/3 of homogenate equipment tank body radius, and the width of blade is 1-2.5cm; Described blade is positioned at 1/2-2/3 tank body total height at the bottom of distance homogenate equipment tank body 1 tank; Described blade material is selected from stainless steel.
According to the extraction element of effective ingredients in plant provided by the invention, preferably, described high shear agitation device 9 and ultrasonic disperser 10 symmetries of popping one's head in are fixedly installed in apart from end cap 13 center 1/7-6/7 end cap radius; Described high shear agitation 9 and ultrasonic disperser are popped one's head in 10 oblique installations, are 5-15 degree with the counterclockwise angle of tank body center line; Described high shear agitation 9 bottom is 1/8 distance of the total height of tank body at the bottom of tank, and described ultrasonic disperser 10 bottoms of popping one's head in are 3/8 distance of the total height of tank body apart from pot bottoms.
According to the extraction element of effective ingredients in plant provided by the invention, preferably, the tank skin of described homogenate equipment tank body 1 is provided with insulation jacket 3; Described insulation jacket 3 is provided with water inlet 4 and discharge outlet 5; The lower end of described homogenate equipment tank body 1 is provided with the discharging opening 2 that be communicated with inner with it, and described discharging opening 2 is provided with discharge valve.
According to the extraction element of effective ingredients in plant provided by the invention, preferably, described homogenate equipment tank body 1 is dismountable tank body, and it is connected with lowering or hoisting gear; Described tank diameter and aspect ratio are 0.6:1-0.8:1.
The invention provides a kind of using method of extraction element of effective ingredients in plant, step is as follows:
1) will the plant of extracting be needed to clean up, after pretreatment size (concrete much scopes), be 1:3 ~ 1:10 with deionized water mixing match mass ratio, open extraction element C-type clamp, starting lowering or hoisting gear pours in tank body by mixture, and rising tank body also seals;
2) start anchor agitator, rotating speed is 50-250r/min, starts circulator bath simultaneously, and the temperature controlling mixed material in agitator tank is open rotating blade after 0-60 ° of C, 1-5min, and arranging rotating speed is 50-500r/min, stirs 2-8min;
3) open high shear agitation device, open supersonic generator simultaneously, ultrasonic power is set;
4), after high shear agitation device stirs 15-30min, stop high shear agitation device and rotating blade, open charging aperture, add the benzinum of 1/8 ~ 2/8 of tank body cumulative volume, then close charging aperture;
5), after continuing to stir 10-20min, stop stirring and ultrasonic generator, extract upper strata benzinum, lower floor's mixture is discharged by discharging opening;
6) can obtain required active ingredient by concentrated for extract decompression distillation, described active ingredient is the saturated of C14-18 and unrighted acid.
According to the using method of extraction element that the invention provides a kind of effective ingredients in plant, preferably, in step (1), mixture addition will exceed the height of rotating blade.
According to the using method of extraction element that the invention provides a kind of effective ingredients in plant, preferably, after step (5) continues to stir 10-20min, stop stirring and ultrasonic generator, extract upper strata benzinum, by lower floor's mixture by starting lowering or hoisting gear, take off tank body, pour out mixture.
According to the using method of extraction element that the invention provides a kind of effective ingredients in plant, preferably, active ingredient is water-soluble substances, and extraction step is described step (1) (2) (3) (5) (6).
According to the using method of extraction element that the invention provides a kind of effective ingredients in plant, preferably, high shear agitation device rotating speed is 10000-28000r/min.
According to the using method of extraction element that the invention provides a kind of effective ingredients in plant, further preferably, high shear agitation device rotating speed is 10000-20000r/min.
According to the using method of extraction element that the invention provides a kind of effective ingredients in plant, preferably, supersonic generator power is 50-500w, and frequency is 50-25khz,
According to the using method of extraction element that the invention provides a kind of effective ingredients in plant, preferably, supersonic generator power is 100-150W.
According to the using method of extraction element that the invention provides a kind of effective ingredients in plant, preferably, anchor agitator rotating speed is 80-150r/min.
According to the using method of extraction element that the invention provides a kind of effective ingredients in plant, preferably, rotating blade rotating speed is 200-350r/min.
According to the extraction element of effective ingredients in plant provided by the invention, mainly comprise one for destroying the homogenate equipment of plant cell, a circulation be connected with homogenate equipment, a position lowering or hoisting gear that can adjust tank body.
According to homogenate equipment tank body of the present invention, diameter and aspect ratio are 0.6-0.8, and a lowering or hoisting gear is connected with tank body, tank body can disassemble, and is convenient to its cleaning, and the interpolation of material, tank body material is fiberglass, is beneficial to and observes its internal-response state, and the interpolation of material.Tank body lower part offers a discharging opening, is beneficial to the discharge of its inner material
According to chuck layer of the present invention, its material is fiberglass, wherein walks circulation, is convenient to the temperature environment arranged in tank body according to reaction needed, is beneficial to the efficiency of extraction.And extract is fresh-keeping, its external circulation.
According to anchor agitator of the present invention, be two paddle, the width of blade is 5-15mm, and preferred 10mm, is fixed on upper cover center, 3-7mm at the bottom of the distance tank of bottom, and agitator radius is slightly less than tank body radius, design benefit: 1) prevent from occurring dead angle in whipping process; 2) prevent extract to be bonded on tank wall, during work, agitator speed is 50-100r/min, to be delivered to by material in the mixing destructive power zone of action, the material of whole agitator is 304 stainless steels.Miniature motor of the present invention, for parts anchor agitator and blade provide power source.
According to high shear agitation device of the present invention, the diameter of outer shaft stator is 20mm, there are 6 rectangular teeths end, size: long is 3.4mm wide 2.0mm height 7.1mm, and interior axle rotor is 3 teeth, the long 2.51mm of upper section of tooth, the long 6.1mm of lower section, width 2.5mm, height 8.2mm, the gap of rotor is 0.4mm, material 304 stainless steel.
Popping one's head according to supersonic generator of the present invention, is the preferred 20mm of 18-24mm, material 304 stainless steel.
Be 4 on chip according to blade of the present invention, the length of blade is the width of 1/3. blade of tank body radius is 1-2.5cm, and material is 304 stainless steels, is loaded in and is about about 2/3 of tank body total height at the bottom of tank, blade adopts Quick-disassembling device to install, and is convenient to it and changes and safeguard.
According to liquid make-up charging aperture of the present invention, as required extract is diluted in leaching process, and the supplementary charging aperture of Extraction solvent, these parts are welded on end cap, lower end diameter is 10-25mm, and the middle globe valve that connects carrys out gauge tap, and upper end is connected to a funnel, be convenient to charging, material is 304 stainless steels.
According to end cap of the present invention, material is 304 stainless steels, high shear agitation device adopts end face seal technology to be connected with supersonic generator probe with end cap, charging aperture is welded on end cap, end cap and motor bottom cabinet are welded into an entirety, make whole mechanical damage functional component place close structure.
According to the present invention, anchor agitator is fixed on upper cover center, 3-7mm high shear agitation device at the bottom of the distance tank of bottom and ultrasonic disperser probe symmetry are fixedly installed in apart from upper cover vertical center line 1/7-6/7d place, d is the internal diameter of tank body, high shear agitation and ultrasonic disperser are popped one's head in oblique installation, setting angle is identical, be 5-15 degree with the counterclockwise angle of tank body center line, high shear agitation device bottom is 1/8h at the bottom of tank, supersonic generator probe bottom distance pot bottom is 3/8h, h is the total height of tank body, blade is installed on apart from pot bottom 1/2h place, wherein upper cover and tank body are by C-type clamp and gasket seal, symmetrical 6 C-type clamp of periphery.
According to the present invention, high shear agitation device is adjustable rotating speed is at 10000-28000r/min, preferred rotating speed is 10000r/min, and grade-adjustable has A-G7 grade, and ultrasonic disperser power is 50-500w, frequency is 50-25khz, preferred power is 150W, the rotating speed of anchor agitator 6 at 50-250r/min, preferred 80r/min, the rotating speed of blade 11 at 50-500r/min, preferred rotating speed 200r/min.
The using method of the extraction element of effective ingredients in plant provided by the invention, step is as follows:
1) will the plant of extracting be needed to clean up, particle diameter≤6mm after pretreatment, desired concn is allowed to carry out mixing match 1:3 ~ 1:10(mass ratio with deionized water), open C-type clamp, starting lowering or hoisting gear imports in tank body by mixture, cumulative volume at least will exceed the height of parts 11, rising tank body sealed shell of tank.
2) starting anchor agitator rotating speed is 50-100r/min, and start after circulator bath controls temperature 0-60 ° of C, 3min of mixed material in agitator tank simultaneously and open blade 11, rotating speed is 100-250r/min, stirs 3-15min.
3) open high shear agitation device, rotating speed is set to 10000-28000r/min, opens supersonic generator simultaneously, and ultrasonic power is 50-500W.
4), after stirring 15-30min, stop high shear agitation device 9 and rotating blade 11 to open the ball valve of 12, add the benzinum (V is the cumulative volume of tank body) of 1/8 ~ 2/8V from charging aperture, then close ball valve.
5) after stirring 10-20min, stop, extracting upper strata benzinum, lower floor's mixture is discharged by 2, or directly starts lowering or hoisting gear, tank body is taken off, pours out mixture.
6) if required active ingredient is water-soluble substances, then without the need to using step 4.
7) extract decompression distillation can be obtained required concentrated active ingredient, described active ingredient is the saturated of C14-18 and unrighted acid.
According to device provided by the invention in mechanism process, after anchor agitator mixes entirety, avoid the blind spot occurred in stirring, and each several part mixture is delivered in effect effective coverage, rotating blade adds the disturbance of strong center stirring region on the one hand, on the other hand Large stone material that is floating or that be suspended in top is cut, accelerate the frequency that it is sent to active region.Anchor agitator and blade help out.In the high speed shear zone of action, fluid rotating speed is high, the mutual friction of iuntercellular phase, or directly impinges upon on stator and rotor end face, causes, cyto-architectural destruction by larger extruding and collision.The violent variation of bubble in another aspect ultrasonic cavitation process, producing additive effect has turbulence effect, perturbation effect, interfacial effect, the comprehensive effects such as Mohaupt effect, makes cell be subject to serious damage so that destroy.The synergy that both are formed and Main Function, thus the chemical composition in cell is released, directly dissolve, shorten extraction time widely, improve extraction efficiency.The booster action of anchor agitator and blade, the effect of the chief destructive cell of high shear agitation device and ultrasonic disperser probe, form this device energy rapid damage eucaryotic cell structure, chemical composition is made to be released dissolving, the latter extracts under ultrasound environments, utilize ultrasonic extraction technology also to substantially increase, extraction efficiency, shorten the time.
Present invention incorporates existing ultrasonic technology and high speed shear technology, puddler and supersonic generator is utilized to destroy cell membrane rapidly, active ingredient in release cells, the low speed rotation of recycling stirring at low speed oar, cell in container is obtained fully, effective break process, adopt the method for mechanical damage from cell, to obtain active ingredient efficiently, rapidly; Insulation jacket can ensure the temperature of the extract in fiberglass retort, and operator can regulate the temperature of recirculated water according to the difference of extract, this makes operation strategies of the present invention comparatively wide, and the grease and protein extraction, orange peel extraction of essential oil, the rose ethereal oil that may be used for micro-algae extract, the extraction of active ingredient in the extraction of natural plant pigment and some Chinese herbal medicine.In sum, the present invention has the advantage that operating efficiency is high, operation strategies is wide.
Beneficial effect of the present invention:
The extraction element of effective ingredients in plant provided by the invention, this device adopts the tactic pattern of fixing end cap, is beneficial to the replacing of parts, cleaning and raw-material interpolation; At end cap welding liquid make-up charging aperture, be convenient to add solvent in leaching process; By ultrasonic extraction combine with technique in extraction element, be conducive to the simplification of separating step; Adopt circulation, during raised temperature, can leaching process be accelerated, raise the efficiency, temperature is reduced for rare Chinese herbal medicine, its property of medicine can be kept more fully.This device is by jet strengthened for high speed shear and ultrasonic cavitation strengthening coupling simultaneously, apply in the extraction of plant active principle, adopt stirring at low speed and low velocity shear effect, structure refinement is delivered in useful effect region, utilizes ultrasonic technology and high speed shear, destroy eucaryotic cell structure rapidly, active ingredient is discharged, dissolve, controlled in whole process by circulation, in tank body, temperature ensures the activity of extract.
Accompanying drawing explanation
Fig. 1 is the structural representation of the extraction element of effective ingredients in plant provided by the invention.
In the drawings: 1-homogenate equipment tank body, 2-discharging opening, 3-insulation jacket, 4-water inlet, 5-discharge outlet, 6-anchor agitator, 7-motor, 8-supersonic generator, 9-high shear agitation device, 10-supersonic generator is popped one's head in, 11-blade, 12-charging aperture, 13-end cap, 14-lowering or hoisting gear.
Detailed description of the invention
Below in conjunction with accompanying drawing, the present invention is described in detail.
As shown in Figure 1, a kind of extraction element of effective ingredients in plant, comprise the end cap 13 of homogenate equipment tank body 1 and the setting of its upper end, described end cap 13 by C-type clamp and gasket seal, end cap 13 is provided with loading hopper 12, anchor agitator 6, high shear agitation device 9 and supersonic generator 8 with homogenate equipment tank body 1; The probe 10 of the paddle of described anchor agitator 6, high shear agitation device 9 and supersonic generator all stretches into from described end cap 13 in the working chamber of homogenate equipment tank body 1; Described anchor agitator 6 comprises for it provides the motor 7 of power, turning cylinder and paddle, and the paddle of described anchor agitator 6 is fixedly connected with motor 7 by turning cylinder; Described paddle is " U " shape paddle, and described high shear agitation device 9 and supersonic generator pop one's head in 10 between described paddle and power transmission shaft; Described turning cylinder is provided with dismountable blade 11.
Embodiment 1: the extraction of grease in chlorella
1) by chlorella (by being adjusted to corresponding proportioning needed for reality) the 1:10(quality after concentrated than algae: water) open C-type clamp, start lowering or hoisting gear, poured into by mixture in tank body, cumulative volume is the 2/3V of tank body, then rise tank body sealed shell of tank.
2) starting anchor agitator rotating speed is 80r/min, starts circulator bath simultaneously, and the temperature controlling mixed material in agitator tank is 60 ° of about C, and open rotating blade 11 after 3 minutes, rotating speed is 150r/min, stirs 5 minutes.
3) open high shear agitation device, rotating speed is set to 15000r/min, opens supersonic generator simultaneously, and ultrasonic power is 150W, and frequency is 20KHZ.
4) after work 25min, stop high shear agitation device 9 and rotating blade 11, circulation temperature is arranged on room temperature range 25 ° of about C, opens the ball valve of 12, add the benzinum (V is the cumulative volume of tank body) of 3/16V from charging aperture, then close ball valve.
5) after stirring 15min, stop, extracting upper strata benzinum, lower floor's mixture is discharged by 2, then by benzinum mixed phase, decompression distillation can obtain required algae oil, then lower floor's mixture washing can be obtained water soluble protein composition.
Destroy the contrast effect of chlorella structure apparatus of the present invention and other method, wherein be extracted the aliphatic acid that thick grease is C14-18, after first carrying out esterification, pass through chromatography again, detect the content of its fatty acid methyl ester, calculate the total content of grease again, and compare with total content in plant, calculate extraction efficiency.
Comparing result:
Embodiment 2: the extraction of orange peel essential oil
1) by the orange skin 1:15(quality after concentrated than orange peel: deionized water) open C-type clamp, start lowering or hoisting gear, poured into by mixture in tank body, cumulative volume is the 3/4V of tank body, then rise tank body sealed shell of tank.
2) starting anchor agitator rotating speed is 100r/min, and start circulator bath simultaneously and control, in agitator tank, the temperature of mixed material is 60 ° of about C, opens blade 11 after 3 minutes, and rotating speed is 200r/min, stirs 5 minutes.
3) open high shear agitation device, rotating speed is set to 15000r/min, opens supersonic generator simultaneously, and ultrasonic power is 200W, and frequency is 20KHZ.
4) after work 30min, stop all parts, first stop high shear agitation device 9 and rotating blade 11, then stop high speed shear and ultrasonication, open C-type clamp, start lowering or hoisting gear, mixture is poured out, or directly gets rid of from bottom, finally go back rotary device, mixture is all carried out isolated by filtration, and then by liquid phase decompression distillation thick Panongchus citri.
The present invention may be used for the grease of micro-algae and protein extraction, orange peel extraction of essential oil, rose ethereal oil extract, the extraction of active ingredient in the extraction of natural plant pigment and some Chinese herbal medicine.
The extraction element of effective ingredients in plant provided by the invention, this device adopts the tactic pattern of fixing end cap, is beneficial to the replacing of parts, cleaning and raw-material interpolation; At end cap welding liquid make-up charging aperture, be convenient to add solvent in leaching process; By ultrasonic extraction combine with technique in extraction element, be conducive to the simplification of separating step; Adopt circulation, during raised temperature, can leaching process be accelerated, raise the efficiency, temperature is reduced for rare Chinese herbal medicine, its property of medicine can be kept more fully.This device is by jet strengthened for high speed shear and ultrasonic cavitation strengthening coupling simultaneously, apply in the extraction of plant active principle, adopt stirring at low speed and low velocity shear effect, structure refinement is delivered in useful effect region, utilizes ultrasonic technology and high speed shear, destroy eucaryotic cell structure rapidly, active ingredient is discharged, dissolve, controlled in whole process by circulation, in tank body, temperature ensures the activity of extract.
Claims (8)
1. an extraction element for effective ingredients in plant, comprise the end cap (13) of homogenate equipment tank body (1) and the setting of its upper end, described end cap (13) and homogenate equipment tank body (1), by C-type clamp and gasket seal, is characterized in that:
Described end cap (13) is provided with loading hopper (12), anchor agitator (6), high shear agitation device (9) and supersonic generator (8); The probe (10) of the paddle of described anchor agitator (6), high shear agitation device (9) and supersonic generator all stretches into from described end cap (13) in the working chamber of homogenate equipment tank body (1); Described anchor agitator (6) comprises for it provides the motor (7) of power, turning cylinder and paddle, and the paddle of described anchor agitator (6) is fixedly connected with motor (7) by turning cylinder; Described paddle is " U " shape paddle, and described high shear agitation device (9) and supersonic generator pop one's head in (10) between described paddle and power transmission shaft; Described turning cylinder is provided with dismountable blade (11);
The length of described blade (11) is 1/3 of homogenate equipment tank body radius, and the width of blade is 1-2.5cm; Described blade is positioned at 1/2-2/3 tank body total height at the bottom of distance homogenate equipment tank body (1) tank; Described blade material is selected from stainless steel;
Described high shear agitation device (9) and ultrasonic disperser probe (10) symmetry are fixedly installed in apart from end cap (13) center 1/7-6/7 end cap radius; Described high shear agitation (9) and (10) the oblique installation of ultrasonic disperser probe are 5-15 degree with the counterclockwise angle of tank body center line; Described high shear agitation (9) bottom is 1/8 distance of the total height of tank body at the bottom of tank, and described ultrasonic disperser probe (10) bottom is 3/8 distance of the total height of tank body apart from pot bottom.
2. the extraction element of effective ingredients in plant according to claim 1, is characterized in that, described loading hopper (12) is welded on end cap (13); Its lower end diameter is 10-25mm, middle connection globe valve; Described loading hopper (12) material is stainless steel.
3. the extraction element of effective ingredients in plant according to claim 1, is characterized in that, welding end cap (13) center, lower end of described motor (7).
4. the extraction element of effective ingredients in plant according to claim 1, is characterized in that, described high shear agitation device (9) and supersonic generator (8) are connected on end cap (13) by end face seal.
5. the extraction element of effective ingredients in plant according to claim 4, is characterized in that, the diameter of described high shear agitation device (9) outer shaft stator is 20mm, and there are 6 rectangular teeths end, and long is 3.4mm, wide 2.0mm, high 7.1mm; Interior axle rotor is 3 teeth, the long 2.51mm of upper section of tooth, the long 6.1mm of lower section, width 2.5mm, height 8.2mm, and the gap of rotor is 0.4mm; The material of described high shear agitation device (9) is selected from stainless steel.
6. the extraction element of effective ingredients in plant according to claim 1, is characterized in that, described supersonic generator probe (10) diameter is 18-24mm, and material is selected from stainless steel.
7. the extraction element of effective ingredients in plant according to claim 1, is characterized in that, the tank skin of described homogenate equipment tank body (1) is provided with insulation jacket (3); Described insulation jacket (3) is provided with water inlet (4) and discharge outlet (5); The lower end of described homogenate equipment tank body (1) is provided with the discharging opening (2) that be communicated with inner with it, and described discharging opening (2) is provided with discharge valve.
8. the extraction element of effective ingredients in plant according to claim 1, is characterized in that, described homogenate equipment tank body (1) is dismountable tank body, and it is connected with lowering or hoisting gear; Described tank diameter and aspect ratio are 0.6:1-0.8:1.
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| CN201310080571.6A CN103111087B (en) | 2013-03-13 | 2013-03-13 | Extraction device of plant active ingredient |
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| CN201310080571.6A CN103111087B (en) | 2013-03-13 | 2013-03-13 | Extraction device of plant active ingredient |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103265645B (en) * | 2013-06-03 | 2016-01-20 | 浙江宇翔生物科技有限公司 | A kind of device and method of ultrasonic-assisted extraction Sargassum polysaccharides |
| CN108421271A (en) * | 2018-03-22 | 2018-08-21 | 安徽睿知信信息科技有限公司 | A kind of pharmacy extraction inspissator |
| TWI671107B (en) * | 2018-12-20 | 2019-09-11 | 黃長義 | Oscillating device of extraction system |
| CN110605085A (en) * | 2019-09-11 | 2019-12-24 | 陕西羊老大服饰股份有限公司 | Purification equipment for wool and soybean protein fibers |
| CN110559685A (en) * | 2019-09-29 | 2019-12-13 | 贾小军 | High-efficient separation and purification equipment of plant active ingredient |
| TWI783508B (en) * | 2021-06-07 | 2022-11-11 | 國立嘉義大學 | Ultrasonic extraction system and its equipment |
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| CN2463040Y (en) * | 2000-12-28 | 2001-12-05 | 上海理日科技发展有限公司 | Special anchor-shape stirrer |
| CN200995136Y (en) * | 2006-08-30 | 2007-12-26 | 上海迪赛诺医药发展有限公司 | High-shearing micro-powder reactor |
| CN202044951U (en) * | 2011-03-22 | 2011-11-23 | 湖北中烟工业有限责任公司 | Efficient extracting device for extracting active ingredients of plants |
| CN202638039U (en) * | 2012-06-16 | 2013-01-02 | 中国热带农业科学院热带作物品种资源研究所 | Traditional Chinese medicine extracting device |
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