CN103015232A - Method for preparing color Setaria viridis - Google Patents
Method for preparing color Setaria viridis Download PDFInfo
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- CN103015232A CN103015232A CN2013100121181A CN201310012118A CN103015232A CN 103015232 A CN103015232 A CN 103015232A CN 2013100121181 A CN2013100121181 A CN 2013100121181A CN 201310012118 A CN201310012118 A CN 201310012118A CN 103015232 A CN103015232 A CN 103015232A
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Abstract
The invention discloses a method for preparing color Setaria viridis. The method comprises the following steps of: primarily soaking and drying greig, spilling and drying the greig, secondarily soaking and drying the greig, boiling silk, blackening, sand washing, dying plant dye, dying reactive dyes, dying acid dye and softening and treating. The color Setaria viridis prepared by using the method has both the wearability same as that of gambiered Guangdong silk and is in different colors, so that the defect that the gambiered Guangdong silk fabric is single in color is overcome; and the color Setaria viridis prepared by using the method is not only high in color fastness but also is bright in color, so that the gambiered Guangdong silk fabric has greater development prospect in application in clothes.
Description
Technical field
The present invention relates to the textile material technical field, relate in particular to a kind of method for preparing color Liang.
Background technology
Gambiered Guangdong silk claims again gambiered Guangdong gauze, be take Real Silk Habotai as end base after natural dye yam juice is contaminated Exposure to Sunlight again with mud in the weaving face fabric of the inferior light coffee color of front gloss black reverse side that forms of mineral instrumentality.Be used as the dye yam of dyestuff, its main component is to be easy to polyphenol and the tannin (tannin matter) that oxidative deformation produces freezing action, and itself can do Chinese herbal medicine.That gambiered Guangdong silk of dying with dye yam has is nice and cool, sweat proof, easily wash, sun-proof, the wearability such as antibiotic.But the color of gambiered Guangdong silk is more single, only has positive black and the coffee-like dichromatism of reverse side, this so that gambiered Guangdong silk in design and the application on clothes have great limitation.
Summary of the invention
The object of the invention is to for overcoming the defective of prior art, and a kind of method that the wearability that both has gambiered Guangdong silk has the color Liang of different colours for preparing is provided.
For achieving the above object, the present invention is by the following technical solutions: a kind of method for preparing color Liang may further comprise the steps:
(1) just soak the solarization greig: the mass ratio with dye yam fruit and water is that the first formulated dye yam liquid of 1:1-3 soaks greig 10-14h, then with its dehydration and be laid on and be exposed to the sun on the meadow to doing; The first dye yam liquid preferably uses the dye yam fruit formulated as 1:2 with the mass ratio of water, the preferred 12h of time that greig soaks;
(2) spill the solarization greig: the mass ratio with dye yam fruit and water is that the second formulated dye yam liquid of 3-4:200 evenly is spread across on the greig that step (1) is processed, and then is laid on the meadow and is exposed to the sun to doing; Repeat to spill and shine greig 5-7 time; The second dye yam liquid preferably uses dye yam fruit formulated as 3:200 with the mass ratio of water, repeats to spill preferred 6 times of the number of times that shines greig;
(3) the inferior solarization greig that soaks: the mass ratio with dye yam fruit and water is after the 3rd formulated dye yam liquid of 2-3:100 soaks greig 1-5 minute that processes through step (2), takes out and is exposed to the sun to doing; Repeat inferior soaking and shine greig 5-7 time; The 3rd dye yam liquid preferably uses dye yam fruit formulated as 2:100 with the mass ratio of water, repeats time to soak preferred 6 times of the number of times that shines greig;
(4) boil silk fabric: the greig that adds the 3rd dye yam liquid and process through step (3) in the saucepan, in 45-50 ℃, turn over and boil 4-5min, then dewater and dry; Described saucepan preferably copper pot;
(5) repeat inferior soaking and shine greig ten secondaries, then repeat to boil silk fabric once, and then repeat inferior soaking and shine greig once;
(6) excessively black: the river silt that will contain the high price iron ion is applied on a surface of second order of the greig that step (5) is processed, and before sunrise, greig is laid on 30min on the meadow, then the river silt on it is cleaned up and is refitted on the meadow and dry with the sunlight in the 3h after the sunrise, then with the 3rd dye yam liquid immersion 1h, again it is laid on 40min on the meadow of post sunset;
(7) sand washing: will place through the greig that step (6) is processed sand washing consistent lubricant content is that the water of 5-15g/L soaks 30-60min, be 5-20g/L to wherein add the sand washing powder making the content of sand washing powder in the solution then, sand washing 30-90min at room temperature is then with behind the weak acid neutralization solution greig being cleaned up and dewatering; Described weak acid preferable formic acid or acetic acid; The preferred 10g/L of the content of sand washing consistent lubricant, the preferred 15g/L of the content of sand washing powder, preferred 60min of sand washing time;
(8) dye on the vegetable colour: be added to the water with vegetable colour with through the greig that step (7) is processed, room temperature enters to dye to be warming up to behind the 10min 90 ℃ and be incubated 40min, and then washes with water clean; The mass ratio of greig and vegetable colour is 100:1.5-2.5, and bath raio is 1:18-22;
(9) dye on the REACTIVE DYES: put into water and be heated to 60 ℃ with REACTIVE DYES, levelling agent with through the greig that step (8) is processed, insulation 30min, the mass ratio of greig, REACTIVE DYES and levelling agent is 100:1.5-2.5:0.2, bath raio is 1:18-22; Then adding glauber salt in the solution, to make the content of glauber salt in the solution be 50-90g/L, and wherein glauber salt is divided into three parts, adds portion every 15min; Then adding sodium carbonate in the solution, to make the content of sodium carbonate in the solution be 18-22g/L, and water cleans greig behind the 45min; The mass ratio of greig, REACTIVE DYES and levelling agent is preferably 100:2:0.2, the preferred 70g/L of the content of glauber salt;
(10) dye on the ACID DYES: be added to the water with ACID DYES with through the greig that step (9) is processed, room temperature adds sodium sulphate after entering to dye 10min, in 45min temperature is risen to 90 ℃ and be incubated 40min by room temperature, and water cleans, then add color-fixing agent, and then wash with water clean and oven dry; The mass ratio of greig, ACID DYES, sodium sulphate and color-fixing agent is 100:1.5-2.5:2-5:1-2, and bath raio is 1:18-22; The mass ratio of greig, ACID DYES, sodium sulphate and color-fixing agent is preferably 100:2:3:2;
(11) the softening processing: be added to the water with softener with through the greig of step (10) processing, at 45-50 ℃ of lower the immersion 1-3 hour, then cleaning, drying; The content of softener is 5-20g/L in the water, and bath raio is 1:18-22; The preferred 15g/L of the content of softener.
The preferred natural-dehydration of dehydration described in the above-mentioned steps.
Compared with prior art, the invention has the beneficial effects as follows: the color Liang that uses the present invention's preparation had both had the wearability identical with gambiered Guangdong silk, can have various color again simultaneously, had remedied the single shortcoming of gambiered Guangdong silk fabric tone; The color Liang of the present invention's preparation not only COLOR FASTNESS is high but also bright in colour, makes the application of gambiered Guangdong silk fabric on clothes have larger development prospect.
The specific embodiment
In order to more fully understand technology contents of the present invention, below in conjunction with specific embodiment technical scheme of the present invention is further introduced and explanation.
Embodiment
The preparation method of a kind of color Liang may further comprise the steps:
(1) just soaks the solarization greig: be that the first formulated dye yam liquid of 1:2 (in other embodiments the mass ratio of dye yam fruit and water can in the scope of 1:1-3) soaks greig 12h with the mass ratio of dye yam fruit and water, soak time can be 10-14h in other embodiments, then with its natural-dehydration and be laid on and be exposed to the sun on the meadow to doing.
(2) spill the solarization greig: the mass ratio with dye yam fruit and water is that (the dye yam fruit can be in the scope of 3-4:200 with the mass ratio of water in other embodiments for the second formulated dye yam liquid of 3:200, do not affect effect of the present invention) evenly be spread across on the greig that step (1) is processed, then be laid on the meadow and be exposed to the sun to doing; Repeat to spill and shine greig 6 times, repeating in other embodiments to spill the number of times that shines greig can be for 5-7 time.
(3) the inferior solarization greig that soaks: the mass ratio with dye yam fruit and water is that (the dye yam fruit can be in the scope of 2-3:100 with the mass ratio of water in other embodiments for the 3rd formulated dye yam liquid of 2:100, do not affect effect of the present invention) soak greig 1-5 minute that processes through step (2) after, take out and be exposed to the sun to doing; Repeat inferior soaking and shine greig 6 times, repeating in other embodiments the inferior number of times that soaks the solarization greig can be for 5-7 time.
(4) boil silk fabric: the greig that adds the 3rd dye yam liquid and process through step (3) in the copper pot, turn in 45 ℃ and boil 4min, then natural-dehydration and drying; The intertwined point that can prevent greig by boiling silk fabric is stopped up.
(5) repeat inferior soaking and shine greig ten secondaries, then repeat to boil silk fabric once, and then repeat inferior soaking and shine greig once.
(6) excessively black: the river silt that will contain the high price iron ion is applied on a surface of second order of the greig that step (5) is processed, and before sunrise, greig is tiled in 30min on the meadow, then the river silt on it is cleaned up and is refitted on the meadow and dry with the sunlight in the 3h after the sunrise, then with the 3rd dye yam liquid immersion 1h, again it is laid on 40min on the meadow of post sunset.
(7) sand washing: will place through the greig that step (6) is processed sand washing consistent lubricant content is that the water of 10g/L soaks 50min, be 15g/L to wherein add the sand washing powder making the content of sand washing powder in the solution then, sand washing 60min at room temperature, then with behind formic acid or the acetic acid neutralization solution greig being cleaned up and natural-dehydration, can use in other embodiments other weak acid neutralization solution; The content of sand washing consistent lubricant can be 5-15g/L in other embodiments, and the content of sand washing powder can be 5-20g/L, and the sand washing time can be 30-90min.
(8) dye on the vegetable colour: be added to the water with vegetable colour with through the greig that step (7) is processed, room temperature enters to dye to be warming up to behind the 10min 90 ℃ and be incubated 40min, and then washes with water clean; The mass ratio of greig and vegetable colour is 100:2, and bath raio is 1:20; In other embodiments, the mass ratio of greig and vegetable colour can be 100:1.5-2.5, and vegetable colour is Flos Carthami dyestuff (in other embodiments, vegetable colour is visual to be dyed color on required and select, such as Radix Isatidis and bush etc.).
(9) dye on the REACTIVE DYES: put into water and be heated to 60 ℃ with REACTIVE DYES, levelling agent with through the greig that step (8) is processed, insulation 30min, the mass ratio of greig, REACTIVE DYES and levelling agent is 100:2:0.2, bath raio is 1:20; Then adding glauber salt in the solution, to make the content of glauber salt in the solution be 75g/L, and wherein glauber salt is divided into three parts, adds portion every 15min; Then adding sodium carbonate in the solution, to make the content of sodium carbonate in the solution be 20g/L, and water cleans greig behind the 45min; In other embodiments, the mass ratio of greig, REACTIVE DYES and levelling agent can be 100:1.5-2.5:0.2, and the content of glauber salt can be 50-90g/L; REACTIVE DYES is BF type REACTIVE DYES, and levelling agent is polyoxyethylene ether; Levelling agent is that silvalin, line or fabric are in dyeing course, for impelling even dyeing, the material that does not produce the faults such as vitta, color spot and add, dyestuff and levelling agent generate first certain " complex " in dye bath, in dyeing course, disengage dyestuff gradually and reach the effect of level dyeing, the material that belongs to this type of has some nonionic surface active agent, such as polyoxyethylene ether of fatty alcohol or alkyl phenol etc.
(10) dye on the ACID DYES: be added to the water with ACID DYES with through the greig that step (9) is processed, room temperature adds sodium sulphate after entering to dye 10min, in 45min temperature is risen to 90 ℃ and be incubated 40min by room temperature, and water cleans, then add color-fixing agent, and then wash with water clean and oven dry; The mass ratio of greig, azo dyes, sodium sulphate and color-fixing agent is 100:2:3:2, and bath raio is 1:20; The mass ratio of greig, ACID DYES, sodium sulphate and color-fixing agent can be 100:1.5-2.5:2-5:1-2 in other embodiments; ACID DYES is sulfonate sodium dyestuff (in other embodiments, also available anthraquinone dye or kiton colors are made ACID DYES, do not affect effect of the present invention), and color-fixing agent is the dicyandiamide formaldehyde resin.
(11) the softening processing: be added to the water with softener with through the greig of step (10) processing, at 45 ℃ of lower immersions 2 hours, then cleaning, dryings; The content of softener is 15g/L in the water, and bath raio is 1:20; The content of softener can be 5-20g/L in other embodiments; Softener is block polyether.
The above only further specifies technology contents of the present invention with embodiment, so that the reader is more readily understood, does not only limit to this but do not represent embodiments of the present invention, and any technology of doing according to the present invention is extended or recreation, all is subjected to protection of the present invention.
Claims (4)
1. method for preparing color Liang is characterized in that may further comprise the steps:
(1) just soak the solarization greig: the mass ratio with dye yam fruit and water is that the first formulated dye yam liquid of 1:1-3 soaks greig 10-14h, then with its dehydration and be laid on and be exposed to the sun on the meadow to doing;
(2) spill the solarization greig: the mass ratio with dye yam fruit and water is that the second formulated dye yam liquid of 3-4:200 evenly spills on the greig of processing through step (1), then is laid on the meadow and is exposed to the sun to doing; Repeat to spill and shine greig 5-7 time;
(3) the inferior solarization greig that soaks: the mass ratio with dye yam fruit and water is after the 3rd formulated dye yam liquid of 2-3:100 soaks greig 1-5 minute that processes through step (2), takes out and is exposed to the sun to doing; Repeat inferior soaking and shine greig 5-7 time;
(4) boil silk fabric: the greig that adds the 3rd dye yam liquid and process through step (3) in the saucepan, in 45-50 ℃, turn over and boil 4-5min, then dewater and dry;
(5) repeat inferior soaking and shine greig ten secondaries, then repeat to boil silk fabric once, and then repeat inferior soaking and shine greig once;
(6) excessively black: the river silt that will contain the high price iron ion is applied on a surface of second order of the greig that step (5) is processed, and before sunrise, greig is laid on 30min on the meadow, then the river silt on it is cleaned up and is refitted on the meadow and dry with the sunlight in the 3h after the sunrise, then with the 3rd dye yam liquid immersion 1h, again it is laid on 40min on the meadow of post sunset;
(7) sand washing: will place through the greig that step (6) is processed sand washing consistent lubricant content is that the water of 5-15g/L soaks 30-60min, be 5-20g/L to wherein add the sand washing powder making the content of sand washing powder in the solution then, sand washing 30-90min at room temperature is then with behind the weak acid neutralization solution greig being cleaned up and dewatering;
(8) dye on the vegetable colour: be added to the water with vegetable colour with through the greig that step (7) is processed, room temperature enters to dye to be warming up to behind the 10min 90 ℃ and be incubated 40min, and then washes with water clean; The mass ratio of greig and vegetable colour is 100:1.5-2.5, and bath raio is 1:18-22;
(9) dye on the REACTIVE DYES: put into water and be heated to 60 ℃ with REACTIVE DYES, levelling agent with through the greig that step (8) is processed, insulation 30min, the mass ratio of greig, REACTIVE DYES and levelling agent is 100:1.5-2.5:0.2, bath raio is 1:18-22; Then adding glauber salt in the solution, to make the content of glauber salt in the solution be 50-90g/L, and wherein glauber salt is divided into three parts, adds portion every 15min; Then adding sodium carbonate in the solution, to make the content of sodium carbonate in the solution be 18-22g/L, and water cleans greig behind the 45min;
(10) dye on the ACID DYES: be added to the water with ACID DYES with through the greig that step (9) is processed, room temperature adds sodium sulphate after entering to dye 10min, in 45min temperature is risen to 90 ℃ and be incubated 40min by room temperature, and water cleans, then add color-fixing agent, and then wash with water clean and oven dry; The mass ratio of greig, ACID DYES, sodium sulphate and color-fixing agent is 100:1.5-2.5:2-5:1-2, and bath raio is 1:18-22;
(11) the softening processing: be added to the water with softener with through the greig of step (10) processing, at 45-50 ℃ of lower the immersion 1-3 hour, then cleaning, drying; The content of softener is 5-20g/L in the water, and bath raio is 1:18-22.
2. described a kind of method for preparing color Liang according to claim 1 is characterized in that described dehydration is natural-dehydration.
3. described a kind of method for preparing color Liang according to claim 1 is characterized in that the saucepan in the described step (4) is the copper pot.
4. described a kind of method for preparing color Liang according to claim 1 is characterized in that the weak acid in the described step (7) is formic acid or acetic acid.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103950349A (en) * | 2014-05-08 | 2014-07-30 | 何炽斌 | Method to draw on gambiered Guangdong gauze |
| CN106149405A (en) * | 2015-04-17 | 2016-11-23 | 深圳市梁子时装实业有限公司 | Preparation method of a kind of color Liang and products thereof and application |
| CN108914559A (en) * | 2018-09-18 | 2018-11-30 | 昆明滇艺非物质文化遗产研发有限公司 | A kind of production method of refrigerant gambiered Guangdong gauze |
| CN110130123A (en) * | 2019-04-20 | 2019-08-16 | 深圳市易菲妮时装有限公司 | The preparation process of high-performance antimildew and antibacterial gelsemium cotton |
| CN112458757A (en) * | 2020-11-25 | 2021-03-09 | 浙江喜得宝丝绸科技有限公司 | Printing and dyeing method of gambiered canton |
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| CN102061631A (en) * | 2009-11-12 | 2011-05-18 | 上海甲秀工业设计有限公司 | Modern gambiered Canton gauze product processing and manufacturing method |
| CN102312374A (en) * | 2011-03-17 | 2012-01-11 | 苏州金科达纺织科技股份有限公司 | Dyeing method of interwoven fabric made of cuprammonium fibers and tencels |
| CN102733182A (en) * | 2012-07-11 | 2012-10-17 | 周晓刚 | Process for producing double-sided gambiered Guangdong silk |
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| CN101275365A (en) * | 2008-05-13 | 2008-10-01 | 杭州喜得宝集团有限公司 | Wash-free dyeing method for silk |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103950349A (en) * | 2014-05-08 | 2014-07-30 | 何炽斌 | Method to draw on gambiered Guangdong gauze |
| CN106149405A (en) * | 2015-04-17 | 2016-11-23 | 深圳市梁子时装实业有限公司 | Preparation method of a kind of color Liang and products thereof and application |
| CN108914559A (en) * | 2018-09-18 | 2018-11-30 | 昆明滇艺非物质文化遗产研发有限公司 | A kind of production method of refrigerant gambiered Guangdong gauze |
| CN110130123A (en) * | 2019-04-20 | 2019-08-16 | 深圳市易菲妮时装有限公司 | The preparation process of high-performance antimildew and antibacterial gelsemium cotton |
| CN112458757A (en) * | 2020-11-25 | 2021-03-09 | 浙江喜得宝丝绸科技有限公司 | Printing and dyeing method of gambiered canton |
| CN112458757B (en) * | 2020-11-25 | 2022-05-13 | 浙江喜得宝丝绸科技有限公司 | Printing and dyeing method of gambiered canton |
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