CN102980826A - Quartz crystal microbalance detection cell - Google Patents

Quartz crystal microbalance detection cell Download PDF

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Publication number
CN102980826A
CN102980826A CN2011102585942A CN201110258594A CN102980826A CN 102980826 A CN102980826 A CN 102980826A CN 2011102585942 A CN2011102585942 A CN 2011102585942A CN 201110258594 A CN201110258594 A CN 201110258594A CN 102980826 A CN102980826 A CN 102980826A
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CN
China
Prior art keywords
quartz crystal
flange
housing
detection cell
inwall
Prior art date
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Pending
Application number
CN2011102585942A
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Chinese (zh)
Inventor
崔学晨
张利群
封雷
崔实
孙宪光
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崔学晨
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Priority to CN2011102585942A priority Critical patent/CN102980826A/en
Publication of CN102980826A publication Critical patent/CN102980826A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a quartz crystal microbalance detection cell and belongs to the field of scientific detection instruments. The quartz crystal microbalance detection cell is used for detection of a liquid-phase sample. The quartz crystal microbalance detection cell is composed of a flange-shaped housing and quartz crystal plates in the flange-shaped housing. A flange-shaped housing inner-wall part close to a flange end is provided with a raised step. The quartz crystal plates are put on the raised step. Diameters of the quartz crystal plates gaplessly match with an inner diameter of the flange-shaped housing. The flange-shaped housing is made of an elastic material. Two electrode contacts of each one of the quartz crystal plates are in the same level. The quartz crystal microbalance detection cell can effectively avoid installation stress influences on the quartz crystal plates in an oscillation direction, has a simple structure and can be dismounted, assembled or replaced flexibly.

Description

A kind of detection cell of quartz crystal microbalance
Technical field
The present invention relates to a kind of detection cell of quartz crystal microbalance, the detection cell of quartz crystal slice namely is housed, be used for the liquid phase sample and detect.
Background technology
QCM (Quartz Crystal Microbalance) (QCM) is a kind of novel sensor measuring technique.The principle that it utilizes the frequency change of quartz vibrator to be directly proportional with the mass change of plane of crystal, but the mass change of detecting electrode surface n g level and solution viscosity, density, the isoparametric variation of modified membrane viscoelasticity, have highly sensitive, the characteristics such as can measure in real time, can be used as the means that on-line tracing monitoring microprocess changes, in the exploratory development of microprocess and the mechanism of action is carried out in the aspects such as modern chemistry, material science, biology and medical science, present good development prospect.
For QCM (Quartz Crystal Microbalance) (QCM) detecting instrument of liquid phase detected object, its core component is the detection cell that quartz crystal slice is housed.Because the characteristic that has of quartz crystal slice, so that its mounting design in detection cell has higher requirement, that is: in the situation of strict sealing and insulation, avoid the additional installation stress of its orientation of oscillation as far as possible.Prior art adopts O type O-ring seal or usually in measures such as quartz crystal slice outer rim heap glue, can solve sealing and Insulation Problems, but can not well solve additional installation stress problem, although perhaps consider simultaneously installation stress problem, its design exists complex structure, the flexible drawback of dismounting or replacing.For example Chinese patent application number is 200910065451.2 " a kind of quartz crystal sensor detecting tank ", on April 14th, 2004 disclosed " CN1489825 chip quartz oscillator and liquid-phase sensor " and " CN2328998 electrochemical insite quartz crystal micro balance detection pool " that on June 5th, 1999, bulletin was authorized.
Summary of the invention
The present invention is directed to above-mentioned the deficiencies in the prior art, a kind of detection cell of quartz crystal microbalance is provided, be intended to avoid quartz crystal slice to be installed in the installation stress of suffered orientation of oscillation in the detection cell, and flexibly dismounting or replacing.
For solving the problems of the technologies described above, the present invention takes following technical scheme, a kind of detection cell of quartz crystal microbalance, consisted of by the in-built quartz crystal slice of flange-like housing, near flange flange end place raised step is set in the flange-like inner walls, quartz crystal slice places this step place, the quartz crystal slice diameter cooperates with flange-like housing internal diameter zero stand-off, be in tightening state to reach sealing effectiveness, the flange-like housing adopts resilient material, quartz crystal slice adopts two electrode contacts to be positioned at the quartz crystal slice of one side, and two electrode contacts are towards the flange flange end, and flange flange is convenient to be connected flexibly with contact conductor mechanism as buckle.
For quartz crystal slice is cooperated with fit sealing with flange-like inner walls zero stand-off, can take the different structure form, one, with the heating of flange-like housing, cooling gets final product after installing before installing; Its two, first quartz crystal slice is placed in step place in the flange-like housing, again with a rigid pipe cuff at flange-like housing outer wall, the outer wall interference fit of the inwall of described rigidity pipe collar and flange-like housing; Its three, make it and the flange-like inner walls forms resilient tight fit at quartz crystal slice outer rim suit O RunddichtringO.
The beneficial effect of detection cell of quartz crystal microbalance provided by the invention is, can effectively avoid quartz crystal slice to be installed in the installation stress of suffered orientation of oscillation in the detection cell and simple in structure, flexibly dismounting or replacing.
Description of drawings
Fig. 1 is the outside drawing of flange-like housing of the present invention;
Fig. 2 is the cut-open view of flange-like housing of the present invention;
Fig. 3 is embodiments of the invention 1 with pack into the cut-open view of flange-like housing of quartz crystal slice;
Fig. 4 is pack into the cut-open views of quartz crystal slice and overcoat rigidity pipe collar of embodiments of the invention 2;
Fig. 5 is the cut-open view that embodiments of the invention 3 are installed in O RunddichtringO mode.
Among the figure, 1-flange-like housing, 2-inwall step, 3-quartz crystal slice, 4-rigidity pipe collar, 5-O RunddichtringO.
Embodiment
The invention will be further described below in conjunction with accompanying drawing.
As shown in drawings, a kind of detection cell of quartz crystal microbalance, consisted of by flange-like housing 1 in-built quartz crystal slice 3, the inwall step 2 of projection is set near flange flange end place at flange-like housing 1 inwall, quartz crystal slice 3 places this step place, quartz crystal slice 3 diameters cooperate with flange-like housing 1 internal diameter zero stand-off, be in tightening state and reach sealing effectiveness, flange-like housing 1 adopts resilient material, quartz crystal slice 3 adopts two electrode contacts to be positioned at the special-purpose quartz crystal slice of one side, two electrode contacts are towards the flange flange end, and flange flange is convenient to be connected flexibly with contact conductor mechanism as buckle.For quartz crystal slice 3 is cooperated with fit sealing with flange-like housing 1 inwall zero stand-off, can take different structure type.
Embodiment 1, such as Fig. 2, shown in Figure 3, makes flange-like housing 1 with elastic-plastic material, 1 heating of flange-like housing slightly softened and made it expand, and quartz crystal slice 3 is placed in flange-like housing 1 inwall step 2 places again, and cooling gets final product.
Embodiment 2, such as Fig. 2, shown in Figure 4, first quartz crystal slice 3 are placed in flange-like housing 1 inwall step 2 places, again a rigidity pipe collar 4 are enclosed within flange-like housing 1 outer wall, the outer wall interference fit of the inwall of described rigidity pipe collar 4 and flange-like housing 1.
Embodiment 3, such as Fig. 2, shown in Figure 5, at quartz crystal slice 3 outer rims suit O RunddichtringO 5, then are placed in flange-like housing 1 inwall step 2 places, make it to form resilient tight fit with flange-like housing 1 inwall.

Claims (4)

1. detection cell of quartz crystal microbalance, mainly consisted of by flange-like housing and quartz crystal slice, it is characterized in that, the inwall step (2) of projection is set at described flange-like housing (1) inwall, quartz crystal slice (3) places this step place, quartz crystal slice (3) diameter cooperates with flange-like housing (1) internal diameter zero stand-off, and flange-like housing (1) adopts resilient material, and quartz crystal slice (3) adopts two electrode contacts to be positioned at the quartz crystal slice of one side.
2. detection cell of quartz crystal microbalance according to claim 1 is characterized in that, with flange-like housing (1) thermoplastic, again quartz crystal slice (3) is placed in flange-like housing (1) inwall step (2) and locates.
3. detection cell of quartz crystal microbalance according to claim 1, it is characterized in that, quartz crystal slice (3) is placed in flange-like housing (1) inwall step (2) to be located, again a rigidity pipe collar (4) is enclosed within flange-like housing (1) outer wall, the outer wall interference fit of the inwall of described rigidity pipe collar (4) and flange-like housing (1).
4. detection cell of quartz crystal microbalance according to claim 1, it is characterized in that, at quartz crystal slice (3) outer rim suit O RunddichtringO (5), then be placed in flange-like housing (1) inwall step (2) and locate, make it to form resilient tight fit with flange-like housing (1) inwall.
CN2011102585942A 2011-09-03 2011-09-03 Quartz crystal microbalance detection cell Pending CN102980826A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2011102585942A CN102980826A (en) 2011-09-03 2011-09-03 Quartz crystal microbalance detection cell

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Application Number Priority Date Filing Date Title
CN2011102585942A CN102980826A (en) 2011-09-03 2011-09-03 Quartz crystal microbalance detection cell

Publications (1)

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CN102980826A true CN102980826A (en) 2013-03-20

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2018146348A1 (en) * 2017-02-13 2018-08-16 Advanced Wave Sensors, S.L. Measuring cell

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2328998Y (en) * 1998-02-23 1999-07-14 中国科学院长春应用化学研究所 Electrochemical insite quartz crystal micro balance detection pool
CN1325026A (en) * 2001-07-10 2001-12-05 重庆大学 Piezoelectric biological chip miniflow detector
CN101241125A (en) * 2008-03-10 2008-08-13 施晓燕 Piezoelectric sensor for liquid phase measuring and encapsulation method
EP1794574A4 (en) * 2004-09-15 2009-09-23 Agency Science Tech & Res Surface plasmon resonance and quartz crystal microbalance sensor
CN101957297A (en) * 2009-07-16 2011-01-26 河南科瑞科技有限公司 Quartz crystal sensor detecting tank
CN102135525A (en) * 2010-12-31 2011-07-27 重庆工商大学 Mechanics analysis device and mechanics analysis method for piezomodulated and sensed single cell
CN202256088U (en) * 2011-09-03 2012-05-30 崔学晨 Detection cell of quartz crystal microbalance

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2328998Y (en) * 1998-02-23 1999-07-14 中国科学院长春应用化学研究所 Electrochemical insite quartz crystal micro balance detection pool
CN1325026A (en) * 2001-07-10 2001-12-05 重庆大学 Piezoelectric biological chip miniflow detector
EP1794574A4 (en) * 2004-09-15 2009-09-23 Agency Science Tech & Res Surface plasmon resonance and quartz crystal microbalance sensor
CN101241125A (en) * 2008-03-10 2008-08-13 施晓燕 Piezoelectric sensor for liquid phase measuring and encapsulation method
CN101957297A (en) * 2009-07-16 2011-01-26 河南科瑞科技有限公司 Quartz crystal sensor detecting tank
CN102135525A (en) * 2010-12-31 2011-07-27 重庆工商大学 Mechanics analysis device and mechanics analysis method for piezomodulated and sensed single cell
CN202256088U (en) * 2011-09-03 2012-05-30 崔学晨 Detection cell of quartz crystal microbalance

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2018146348A1 (en) * 2017-02-13 2018-08-16 Advanced Wave Sensors, S.L. Measuring cell

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SE01 Entry into force of request for substantive examination
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Application publication date: 20130320

Assignee: Henan Kerui Science and Technology Co., Ltd.

Assignor: Cui Xuechen

Contract record no.: 2012410000017

Denomination of invention: Quartz crystal microbalance detection cell

License type: Exclusive License

Record date: 20120313

LICC Enforcement, change and cancellation of record of contracts on the licence for exploitation of a patent or utility model
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Application publication date: 20130320