CN102935039A - Traditional Chinese medicine eucommia bark toothpaste and preparation method thereof - Google Patents
Traditional Chinese medicine eucommia bark toothpaste and preparation method thereof Download PDFInfo
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- CN102935039A CN102935039A CN2012102766196A CN201210276619A CN102935039A CN 102935039 A CN102935039 A CN 102935039A CN 2012102766196 A CN2012102766196 A CN 2012102766196A CN 201210276619 A CN201210276619 A CN 201210276619A CN 102935039 A CN102935039 A CN 102935039A
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Abstract
The invention relates to a traditional Chinese medicine eucommia bark toothpaste and a preparation method thereof, and belongs to the technical field of toothpastes. The traditional Chinese medicine eucommia bark toothpaste comprises the following raw materials, by weight, 30-50% of a friction agent, 15-30% of a wetting agent, 0.5-3% of a binder, 0.5-3% of a foaming agent, 0.1-0.5% of a sweetening agent, 0.1-0.3% of a preservative, 0.5-1.5% of a flavor, 0.1-2% of a eucommia bark extract, and the balance of deionized water. The traditional Chinese medicine eucommia bark toothpaste is prepared by sequentially adopting the following steps: (1) extracting a eucommia bark extract; (2) preparing a toothpaste; and (3) packaging. According to the present invention, ultrasonic waves are adopted to carry out assisted extraction on eucommia bark leaves so as to improve extraction rate of active ingredients in the eucommia bark leaves and save medicinal resources; and contents of the active ingredients in the eucommia bark leaves are increased, such that functions of bacterial inhibition, inflammation resistance, gingival bleeding reduction, oral ulcer repair and the like of the eucommia bark toothpaste are further enhanced.
Description
Technical field
The invention belongs to the toothpaste technical field, specifically belong to a kind of Chinese medicine Cortex Eucommiae toothpaste and preparation method thereof.
Background technology
Folium Eucommiae is the dried leaves of the Eucommiaceae plant Cortex Eucommiae, and its little suffering of distinguishing the flavor of is warm in nature.Modern study shows, functional component is a lot of in the Folium Eucommiae, and chlorogenic acid, aucubin, geniposide, Geniposidic acid, eucommoil and pinoresinol diglucoside etc. are arranged.These chemical compositions have the effects, particularly Chlorogenic Acid in Eucommia ulmoides Oliv. Leaves rich content such as anti-inflammation, hemostasis, blood pressure lowering, have good antibacterial and anti-inflammation functions.
At present, a lot of Chinese medicinal toothpastes are arranged on the market, these toothpaste all are by the Chinese herbal medicine functional component is added in the toothpaste matrix, and the dental care effect is each has something to recommend him, but have no the Cortex Eucommiae are applied to relevant report in the toothpaste.
Summary of the invention
The objective of the invention is for top described defective, provide a kind of tooth, gingiva are had anti-inflammation, alleviate gingival hemorrhage, repair the Chinese medicine Cortex Eucommiae toothpaste of oral ulcer.
Another object of the present invention provides a kind of preparation method of Chinese medicine Cortex Eucommiae toothpaste.
The objective of the invention is to be achieved by the following technical programs.
A kind of Chinese medicine Cortex Eucommiae toothpaste, it is characterized in that, raw material by following percentage by weight forms: abrasivus 30%-50%, wetting agent 15%-30%, binding agent 0.5%-3%, foaming agent 0.5%-3%, sweeting agent 0.1%-0.5%, antiseptic 0.1%-0.3%, essence 0.5%-1.5%, Folium Eucommiae extractum 0.1%-2%, and surplus is deionized water; And adopt successively following steps to make:
(1) with the Folium Eucommiae ultrasonic extraction, filter, filtrate is concentrated into relative density (d) for 1.2-1.3, gets Folium Eucommiae extractum, and is for subsequent use;
(2) paste manufacture process: at first under vacuum state, suck wetting agent in the vacuum Manufacturing medicine extract machine; After again Folium Eucommiae extractum, sweeting agent, antiseptic being stirred with deionized water dissolving, stir with wetting agent in the suction vacuum Manufacturing medicine extract machine; Again abrasivus, foaming agent and binding agent are added in the powder pot deionized water and stirring evenly after, suck and be stirred in the vacuum Manufacturing medicine extract machine evenly; Again essence is added in the vacuum Manufacturing medicine extract machine under vacuum state and stir, get mastic;
(3) carry out at last fill, sealing is packed and be get final product.
Described abrasivus is selected from one or both the combination in hydration Silicon stone, the calcium hydrogen phosphate.
Described wetting agent is selected from one or both the combination in glycerol, the sorbitol.
Described binding agent is selected from one or more the combination in sodium carboxymethyl cellulose, ripple chondrus ocellatus Holmes, the carrageenan.
Described foaming agent is selected sodium lauryl sulphate.
Described sweeting agent is selected from one or both the combination in saccharin sodium, the mannitol.
Described antiseptic is selected from one or both the combination in sodium benzoate, the ethyl hydroxybenzoate.
Described essence is selected menthol.
It is ultrasonic twice that microwave-assisted lixiviate described in the step (1) refers to, uses 50% ethanol ultrasonic extraction 15-45min at every turn, and ultrasonic power is 40-80kw, and temperature is 30 ℃.
The invention has the beneficial effects as follows: the present invention is by the Ultrasonic Wave-Assisted Extraction Folium Eucommiae, can improve the extraction ratio of effective ingredient in the Folium Eucommiae, save herb resource, simultaneously, the raising of active constituent content in the Folium Eucommiae, further strengthened Cortex Eucommiae toothpaste inhibiting bacteria and diminishing inflammation, alleviate gingival hemorrhage, repair the effects such as oral ulcer.
The specific embodiment
Below the invention will be further described by instantiation, it should be understood that these embodiment only are used for explanation the present invention, do not limit the scope of the invention.
Embodiment 1.
A kind of Chinese medicine Cortex Eucommiae toothpaste is comprised of the raw material of following percentage by weight:
Folium Eucommiae extractum 2%
Abrasivus: hydration Silicon stone 2%, calcium hydrogen phosphate 40%
Wetting agent: glycerol 5%, sorbitol 20%
Binding agent: sodium carboxymethyl cellulose 2%, ripple chondrus ocellatus Holmes 0.5%
Foaming agent: sodium lauryl sulphate 2.5%
Sweeting agent: mannitol 0.3%
Antiseptic: ethyl hydroxybenzoate 0.1%
Essence: menthol 1.5%
Deionized water: surplus.
Preparation method: (1) at first with the Folium Eucommiae raw material with 50% ethanol ultrasonic extraction twice, each 45min, ultrasonic power is 80kw, temperature is 30 ℃, collects filtrate, Recycled ethanol, be concentrated into relative density (d) and be 1.2-1.3, get Folium Eucommiae extractum, for subsequent use;
(2) paste manufacture process: at first under vacuum state, suck wetting agent in the vacuum Manufacturing medicine extract machine; After again Folium Eucommiae extractum, sweeting agent, antiseptic being stirred with deionized water dissolving, stir with wetting agent in the suction vacuum Manufacturing medicine extract machine; Again abrasivus, foaming agent and binding agent are added in the powder pot deionized water and stirring evenly after, suck and be stirred in the vacuum Manufacturing medicine extract machine evenly; Again essence is added in the vacuum Manufacturing medicine extract machine under vacuum state and stir, get mastic;
(3) carry out at last fill, sealing is packed and be get final product.
Embodiment 2.
A kind of Chinese medicine Cortex Eucommiae toothpaste is comprised of the raw material of following percentage by weight:
Folium Eucommiae extractum 0.5%
Abrasivus: hydration Silicon stone 5%, calcium hydrogen phosphate 40%
Wetting agent: glycerol 10%, sorbitol 15%
Binding agent: sodium carboxymethyl cellulose 1%, ripple chondrus ocellatus Holmes 1%
Foaming agent: sodium lauryl sulphate 1.5%
Sweeting agent: mannitol 0.5%
Antiseptic: ethyl hydroxybenzoate 0.3%
Essence: menthol 0.5%
Deionized water: surplus.
Preparation method: (1) at first with the Folium Eucommiae raw material with 50% ethanol with ultrasonic extraction twice, each 30min, ultrasonic power is 60kw, temperature is 30 ℃, collects filtrate, Recycled ethanol, be concentrated into relative density (d) and be 1.2-1.3, get Folium Eucommiae extractum, for subsequent use;
(2) paste manufacture process: at first under vacuum state, suck wetting agent in the vacuum Manufacturing medicine extract machine; After again Folium Eucommiae extractum, sweeting agent, antiseptic being stirred with deionized water dissolving, stir with wetting agent in the suction vacuum Manufacturing medicine extract machine; Again abrasivus, foaming agent and binding agent are added in the powder pot deionized water and stirring evenly after, suck and be stirred in the vacuum Manufacturing medicine extract machine evenly; Again essence is added in the vacuum Manufacturing medicine extract machine under vacuum state and stir, get mastic;
(3) carry out at last fill, sealing is packed and be get final product.
Embodiment 3.
A kind of Chinese medicine Cortex Eucommiae toothpaste is comprised of the raw material of following percentage by weight:
Folium Eucommiae extractum 0.1%
Abrasivus: hydration Silicon stone 5%, calcium hydrogen phosphate 45%
Wetting agent: glycerol 10%, sorbitol 15%
Binding agent: sodium carboxymethyl cellulose 2.5%, ripple chondrus ocellatus Holmes 0.5%
Foaming agent: sodium lauryl sulphate 3%
Sweeting agent: mannitol 0.5%
Antiseptic: ethyl hydroxybenzoate 0.2%
Essence: menthol 1%
Deionized water: surplus.
Preparation method: (1) at first extracts twice with 50% ethanol is super with sound wave with the Folium Eucommiae raw material, each 15min, and ultrasonic power is 40kw, temperature is 30 ℃, collects filtrate, Recycled ethanol, be concentrated into relative density (d) and be 1.2-1.3, get Folium Eucommiae extractum, for subsequent use;
(2) paste manufacture process: at first under vacuum state, suck wetting agent in the vacuum Manufacturing medicine extract machine; After again Folium Eucommiae extractum, sweeting agent, antiseptic being stirred with deionized water dissolving, stir with wetting agent in the suction vacuum Manufacturing medicine extract machine; Again abrasivus, foaming agent and binding agent are added in the powder pot deionized water and stirring evenly after, suck and be stirred in the vacuum Manufacturing medicine extract machine evenly; Again essence is added in the vacuum Manufacturing medicine extract machine under vacuum state and stir, get mastic;
(3) carry out at last fill, sealing is packed and be get final product.
Claims (10)
1. Chinese medicine Cortex Eucommiae toothpaste, it is characterized in that: the raw material by following percentage by weight forms: abrasivus 30%-50%, wetting agent 15%-30%, binding agent 0.5%-3%, foaming agent 0.5%-3%, sweeting agent 0.1%-0.5%, antiseptic 0.1%-0.3%, essence 0.5%-1.5%, Folium Eucommiae extractum 0.1%-2%, and surplus is deionized water; And adopt successively following steps to make:
(1) with the Folium Eucommiae Ultrasonic Wave-Assisted Extraction, filter, it is 1.2-1.3 that filtrate is concentrated into relative density d, gets Folium Eucommiae extractum, for subsequent use;
(2) paste manufacture process: at first under vacuum state, suck wetting agent in the vacuum Manufacturing medicine extract machine; After again Folium Eucommiae extractum, sweeting agent, antiseptic being stirred with deionized water dissolving, stir with wetting agent in the suction vacuum Manufacturing medicine extract machine; Again abrasivus, foaming agent and binding agent are added in the powder pot deionized water and stirring evenly after, suck and be stirred in the vacuum Manufacturing medicine extract machine evenly; Again essence is added in the vacuum Manufacturing medicine extract machine under vacuum state and stir, get mastic;
(3) carry out at last fill, sealing is packed and be get final product.
2. a kind of Chinese medicine Cortex Eucommiae toothpaste according to claim 1 is characterized in that: described abrasivus is selected from one or both the combination in hydration Silicon stone, the calcium hydrogen phosphate.
3. a kind of Chinese medicine Cortex Eucommiae toothpaste according to claim 1 is characterized in that: described wetting agent is selected from one or both the combination in glycerol, the sorbitol.
4. a kind of Chinese medicine Cortex Eucommiae toothpaste according to claim 1 is characterized in that: described binding agent is selected from one or more the combination in sodium carboxymethyl cellulose, ripple chondrus ocellatus Holmes, the carrageenan.
5. a kind of Chinese medicine Cortex Eucommiae toothpaste according to claim 1, it is characterized in that: described foaming agent is selected sodium lauryl sulphate.
6. a kind of Chinese medicine Cortex Eucommiae toothpaste according to claim 1 is characterized in that: described sweeting agent is selected from one or both the combination in saccharin sodium, the mannitol.
7. a kind of Chinese medicine Cortex Eucommiae toothpaste according to claim 1 is characterized in that: described antiseptic is selected from one or both the combination in sodium benzoate, the ethyl hydroxybenzoate.
8. a kind of Chinese medicine Cortex Eucommiae toothpaste according to claim 1, it is characterized in that: described essence is selected menthol.
9. the preparation method of a Chinese medicine Cortex Eucommiae toothpaste is characterized in that: adopt successively following steps to make:
(1) Folium Eucommiae is used the microwave-assisted lixiviate, filtered, it is 1.2-1.3 that filtrate is concentrated into relative density d, gets Folium Eucommiae extractum, for subsequent use;
(2) paste manufacture process: at first under vacuum state, suck wetting agent in the vacuum Manufacturing medicine extract machine; After again Folium Eucommiae extractum, sweeting agent, antiseptic being stirred with deionized water dissolving, stir with wetting agent in the suction vacuum Manufacturing medicine extract machine; Again abrasivus, foaming agent and binding agent are added in the powder pot deionized water and stirring evenly after, suck and be stirred in the vacuum Manufacturing medicine extract machine evenly; Again essence is added in the vacuum Manufacturing medicine extract machine under vacuum state and stir, get mastic;
(3) carry out at last fill, sealing is packed and be get final product.
10. the preparation method of a kind of Chinese medicine Cortex Eucommiae toothpaste according to claim 9, it is characterized in that: the microwave-assisted lixiviate described in the step (1) refers to ultrasonic twice, with 50% ethanol ultrasonic extraction 15-45min, ultrasonic power is 40-80kw at every turn, and temperature is 30 ℃.
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104997686A (en) * | 2015-07-23 | 2015-10-28 | 贵阳中医学院 | Anti-bacterial toothpaste and preparation method thereof |
| CN105012182A (en) * | 2015-07-23 | 2015-11-04 | 贵阳中医学院 | Anti-inflammatory toothpaste and preparation method thereof |
| CN105012183A (en) * | 2015-07-23 | 2015-11-04 | 贵阳中医学院 | Eucommia ulmoides toothpaste and preparation method thereof |
| CN105030592A (en) * | 2015-07-10 | 2015-11-11 | 贵州天健堂生物科技有限公司 | Qingyan Duzhong toothpaste and making method thereof |
| CN106236610A (en) * | 2016-08-17 | 2016-12-21 | 林少英 | A kind of toothpaste |
| CN107184492A (en) * | 2017-07-20 | 2017-09-22 | 重庆夫日用品有限责任公司 | Health-care toothpaste and preparation method thereof |
| CN107184421A (en) * | 2017-07-20 | 2017-09-22 | 重庆夫日用品有限责任公司 | A kind of efficient whitening mothproof toothpaste and preparation method thereof |
| CN109589287A (en) * | 2019-02-02 | 2019-04-09 | 江西普正制药有限公司 | A kind of callicarpa nudiflora toothpaste and preparation method thereof |
| CN109620774A (en) * | 2019-01-28 | 2019-04-16 | 荆楚理工学院 | A kind of herbal mixture care toothpaste and preparation method thereof |
| CN109700710A (en) * | 2017-10-26 | 2019-05-03 | 张家界茶坤缘生物科技开发有限公司 | Eucommia bark toothpaste and preparation method thereof |
| CN112716851A (en) * | 2021-01-15 | 2021-04-30 | 江苏福砳生物环保科技有限公司 | Halitosis-removing health toothpaste containing zeolite and preparation method thereof |
Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3655867A (en) * | 1970-05-01 | 1972-04-11 | Hoechst Ag | Dental preparations |
| US4931272A (en) * | 1987-02-24 | 1990-06-05 | Hoechst Aktiengesellschaft | Tooth pastes, cleaning agent for tooth pastes based on dicalcium phosphate-dihydrate, and process for making such cleaning agent |
| JPH0899850A (en) * | 1994-10-03 | 1996-04-16 | Lion Corp | Composition for oral cavity |
| CN1325676A (en) * | 2001-05-28 | 2001-12-12 | 中国科学院广州化学研究所 | Toothpaste |
| CN1660036A (en) * | 2004-12-22 | 2005-08-31 | 美晨集团股份有限公司 | Compound formula of toothpaste |
| JP2005289952A (en) * | 2004-03-31 | 2005-10-20 | Kobayashi Pharmaceut Co Ltd | Deodorizer comprising eucommia ulmoides |
| KR20060104095A (en) * | 2005-03-29 | 2006-10-09 | 재단법인서울대학교산학협력재단 | Toothpaste abrasive containing nano-sized carbonated apatite and toothpaste composition using the same |
| CN101129298A (en) * | 2007-09-17 | 2008-02-27 | 江西诚志日化有限公司 | Pure toothpaste |
| KR20100123423A (en) * | 2009-05-15 | 2010-11-24 | 황철수 | Composition of toothpaste for whitening and method of preparing thereof |
| US20110177012A1 (en) * | 2007-06-12 | 2011-07-21 | Rhodia Inc. | Mono-, di- and polyol alkoxylate phosphate esters in oral care formulations and methods for using same |
-
2012
- 2012-08-06 CN CN2012102766196A patent/CN102935039A/en active Pending
Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3655867A (en) * | 1970-05-01 | 1972-04-11 | Hoechst Ag | Dental preparations |
| US4931272A (en) * | 1987-02-24 | 1990-06-05 | Hoechst Aktiengesellschaft | Tooth pastes, cleaning agent for tooth pastes based on dicalcium phosphate-dihydrate, and process for making such cleaning agent |
| JPH0899850A (en) * | 1994-10-03 | 1996-04-16 | Lion Corp | Composition for oral cavity |
| CN1325676A (en) * | 2001-05-28 | 2001-12-12 | 中国科学院广州化学研究所 | Toothpaste |
| JP2005289952A (en) * | 2004-03-31 | 2005-10-20 | Kobayashi Pharmaceut Co Ltd | Deodorizer comprising eucommia ulmoides |
| CN1660036A (en) * | 2004-12-22 | 2005-08-31 | 美晨集团股份有限公司 | Compound formula of toothpaste |
| KR20060104095A (en) * | 2005-03-29 | 2006-10-09 | 재단법인서울대학교산학협력재단 | Toothpaste abrasive containing nano-sized carbonated apatite and toothpaste composition using the same |
| US20110177012A1 (en) * | 2007-06-12 | 2011-07-21 | Rhodia Inc. | Mono-, di- and polyol alkoxylate phosphate esters in oral care formulations and methods for using same |
| CN101129298A (en) * | 2007-09-17 | 2008-02-27 | 江西诚志日化有限公司 | Pure toothpaste |
| KR20100123423A (en) * | 2009-05-15 | 2010-11-24 | 황철수 | Composition of toothpaste for whitening and method of preparing thereof |
Non-Patent Citations (2)
| Title |
|---|
| 李艳红等: "6种云南天然药物对口腔优势菌的抗菌活性测定", 《华西口腔医学杂志》, vol. 28, no. 2, 30 April 2010 (2010-04-30) * |
| 程德军等: "均匀设计法优化杜仲叶中绿原酸的提取工艺", 《四川化工》, vol. 11, no. 2, 31 December 2008 (2008-12-31) * |
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105030592A (en) * | 2015-07-10 | 2015-11-11 | 贵州天健堂生物科技有限公司 | Qingyan Duzhong toothpaste and making method thereof |
| CN104997686A (en) * | 2015-07-23 | 2015-10-28 | 贵阳中医学院 | Anti-bacterial toothpaste and preparation method thereof |
| CN105012182A (en) * | 2015-07-23 | 2015-11-04 | 贵阳中医学院 | Anti-inflammatory toothpaste and preparation method thereof |
| CN105012183A (en) * | 2015-07-23 | 2015-11-04 | 贵阳中医学院 | Eucommia ulmoides toothpaste and preparation method thereof |
| CN105012183B (en) * | 2015-07-23 | 2017-12-01 | 贵阳中医学院 | A kind of eucommia bark toothpaste and preparation method thereof |
| CN106236610A (en) * | 2016-08-17 | 2016-12-21 | 林少英 | A kind of toothpaste |
| CN107184421A (en) * | 2017-07-20 | 2017-09-22 | 重庆夫日用品有限责任公司 | A kind of efficient whitening mothproof toothpaste and preparation method thereof |
| CN107184492A (en) * | 2017-07-20 | 2017-09-22 | 重庆夫日用品有限责任公司 | Health-care toothpaste and preparation method thereof |
| CN107184492B (en) * | 2017-07-20 | 2021-03-02 | 重庆一夫日用品有限责任公司 | Health-care toothpaste and preparation method thereof |
| CN109700710A (en) * | 2017-10-26 | 2019-05-03 | 张家界茶坤缘生物科技开发有限公司 | Eucommia bark toothpaste and preparation method thereof |
| CN109620774A (en) * | 2019-01-28 | 2019-04-16 | 荆楚理工学院 | A kind of herbal mixture care toothpaste and preparation method thereof |
| CN109589287A (en) * | 2019-02-02 | 2019-04-09 | 江西普正制药有限公司 | A kind of callicarpa nudiflora toothpaste and preparation method thereof |
| CN112716851A (en) * | 2021-01-15 | 2021-04-30 | 江苏福砳生物环保科技有限公司 | Halitosis-removing health toothpaste containing zeolite and preparation method thereof |
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Application publication date: 20130220 |