CN102925250B - 一种含磷硼酸酯水基润滑剂 - Google Patents
一种含磷硼酸酯水基润滑剂 Download PDFInfo
- Publication number
- CN102925250B CN102925250B CN201210399531.3A CN201210399531A CN102925250B CN 102925250 B CN102925250 B CN 102925250B CN 201210399531 A CN201210399531 A CN 201210399531A CN 102925250 B CN102925250 B CN 102925250B
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- Prior art keywords
- boric acid
- temperature
- raw material
- reaction
- reaction kettle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 29
- 239000004327 boric acid Substances 0.000 title claims abstract description 25
- 239000000314 lubricant Substances 0.000 title claims abstract description 23
- -1 boric acid ester Chemical class 0.000 title claims abstract description 13
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 title abstract description 5
- 229910052698 phosphorus Inorganic materials 0.000 title abstract description 5
- 239000011574 phosphorus Substances 0.000 title abstract description 5
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 33
- 238000003756 stirring Methods 0.000 claims abstract description 28
- 238000006243 chemical reaction Methods 0.000 claims abstract description 27
- 239000002994 raw material Substances 0.000 claims abstract description 23
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims abstract description 11
- 238000007599 discharging Methods 0.000 claims abstract description 7
- 238000002360 preparation method Methods 0.000 claims abstract description 3
- GNTDGMZSJNCJKK-UHFFFAOYSA-N divanadium pentaoxide Chemical compound O=[V](=O)O[V](=O)=O GNTDGMZSJNCJKK-UHFFFAOYSA-N 0.000 claims description 18
- 230000035484 reaction time Effects 0.000 claims description 6
- 229910052751 metal Inorganic materials 0.000 abstract description 5
- 239000002184 metal Substances 0.000 abstract description 5
- 239000000463 material Substances 0.000 abstract description 3
- 238000009835 boiling Methods 0.000 abstract description 2
- 230000009965 odorless effect Effects 0.000 abstract description 2
- DLYUQMMRRRQYAE-UHFFFAOYSA-N tetraphosphorus decaoxide Chemical compound O1P(O2)(=O)OP3(=O)OP1(=O)OP2(=O)O3 DLYUQMMRRRQYAE-UHFFFAOYSA-N 0.000 abstract 4
- 238000001816 cooling Methods 0.000 abstract 2
- 150000002739 metals Chemical class 0.000 abstract 1
- 230000009972 noncorrosive effect Effects 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 230000007613 environmental effect Effects 0.000 description 4
- 239000002480 mineral oil Substances 0.000 description 3
- 235000010446 mineral oil Nutrition 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- 239000004094 surface-active agent Substances 0.000 description 3
- 238000003786 synthesis reaction Methods 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000032050 esterification Effects 0.000 description 2
- 238000005886 esterification reaction Methods 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 229910000398 iron phosphate Inorganic materials 0.000 description 2
- WBJZTOZJJYAKHQ-UHFFFAOYSA-K iron(3+) phosphate Chemical group [Fe+3].[O-]P([O-])([O-])=O WBJZTOZJJYAKHQ-UHFFFAOYSA-K 0.000 description 2
- 230000001050 lubricating effect Effects 0.000 description 2
- 238000005461 lubrication Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- BTBUEUYNUDRHOZ-UHFFFAOYSA-N Borate Chemical compound [O-]B([O-])[O-] BTBUEUYNUDRHOZ-UHFFFAOYSA-N 0.000 description 1
- 239000005069 Extreme pressure additive Substances 0.000 description 1
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical group OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 1
- 241000282849 Ruminantia Species 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 229910052810 boron oxide Inorganic materials 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000000536 complexating effect Effects 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- JKWMSGQKBLHBQQ-UHFFFAOYSA-N diboron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 description 1
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 150000001457 metallic cations Chemical group 0.000 description 1
- 238000005555 metalworking Methods 0.000 description 1
- 230000009456 molecular mechanism Effects 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
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- Lubricants (AREA)
Abstract
Description
Claims (1)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210399531.3A CN102925250B (zh) | 2012-10-19 | 2012-10-19 | 一种含磷硼酸酯水基润滑剂 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210399531.3A CN102925250B (zh) | 2012-10-19 | 2012-10-19 | 一种含磷硼酸酯水基润滑剂 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102925250A CN102925250A (zh) | 2013-02-13 |
| CN102925250B true CN102925250B (zh) | 2014-04-02 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210399531.3A Active CN102925250B (zh) | 2012-10-19 | 2012-10-19 | 一种含磷硼酸酯水基润滑剂 |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102925250B (zh) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114892174A (zh) * | 2022-05-20 | 2022-08-12 | 镇江纳润特高新科技发展有限公司 | 一种具有除锈功能的黑色金属抛光液及其制备方法 |
| CN114717561A (zh) * | 2022-05-20 | 2022-07-08 | 镇江纳润特高新科技发展有限公司 | 一种含磷硼酸酯的黑色金属抛光液及其制备方法 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6352962B1 (en) * | 2000-04-03 | 2002-03-05 | Idemitsu Kosan Co., Ltd. | Lubricant additive comprising reaction product of phosphate or phosphite and boronated dispersant |
| CN101063060A (zh) * | 2006-04-29 | 2007-10-31 | 北京天宝同辉材料防护技术有限公司 | 油溶性复配高效防锈添加剂及其制备方法 |
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2012
- 2012-10-19 CN CN201210399531.3A patent/CN102925250B/zh active Active
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| Publication number | Publication date |
|---|---|
| CN102925250A (zh) | 2013-02-13 |
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| C06 | Publication | ||
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| C53 | Correction of patent for invention or patent application | ||
| CB02 | Change of applicant information |
Address after: District 214000 of Jiangsu province Wuxi Xian Lu Mei Cunxi 129-1 (530 business center) Applicant after: Song Xiaolin Applicant after: Yang Jinbing Address before: Mei Binhu Cunxi Xian Lu 214000 Jiangsu city of Wuxi province 129-1 (530 business center) Applicant before: Song Xiaolin Applicant before: Yang Jinbing |
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| ASS | Succession or assignment of patent right |
Free format text: FORMER OWNER: YANG JINBING Effective date: 20131119 |
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| C41 | Transfer of patent application or patent right or utility model | ||
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Inventor after: Song Xiaolin Inventor before: Song Xiaolin Inventor before: Yang Jinbing |
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| COR | Change of bibliographic data |
Free format text: CORRECT: INVENTOR; FROM: SONG XIAOLIN YANG JINBING TO: SONG XIAOLIN |
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Effective date of registration: 20131119 Address after: District 214000 of Jiangsu province Wuxi Xian Lu Mei Cunxi 129-1 (530 business center) Applicant after: Song Xiaolin Address before: District 214000 of Jiangsu province Wuxi Xian Lu Mei Cunxi 129-1 (530 business center) Applicant before: Song Xiaolin Applicant before: Yang Jinbing |
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| C14 | Grant of patent or utility model | ||
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Owner name: WUXI NANOLUBTECH SCIENCE + TECHNOLOGY CO., LTD. Free format text: FORMER OWNER: SONG XIAOLIN Effective date: 20150727 Owner name: SONG XIAOLIN Effective date: 20150727 |
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Effective date of registration: 20150727 Address after: 214000, No. 210, Xinzhou Road, Mei Cun town, Wuxi national hi tech Industrial Development Zone, Wuxi, Jiangsu Patentee after: NANOLUBTECH (WUXI) SCI&TECH CO., LTD. Patentee after: Song Xiaolin Address before: District 214000 of Jiangsu province Wuxi Xian Lu Mei Cunxi 129-1 (530 business center) Patentee before: Song Xiaolin |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Phosphorus-containing boric acid ester water-based lubricant Effective date of registration: 20160919 Granted publication date: 20140402 Pledgee: Agricultural Bank of China Limited by Share Ltd Wuxi science and Technology Branch Pledgor: Wuxi Technology Co., Ltd.|Song Xiaolin Registration number: 2016990000793 |
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| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20181219 Granted publication date: 20140402 Pledgee: Agricultural Bank of China Limited by Share Ltd Wuxi science and Technology Branch Pledgor: NANOLUBTECH (WUXI) SCI&TECH CO., LTD.|Song Xiaolin Registration number: 2016990000793 |