CN102816027A - Preparation method of composite coated fertilizer containing amino acid chelating solution specially used for soybean basal fertilizer - Google Patents

Preparation method of composite coated fertilizer containing amino acid chelating solution specially used for soybean basal fertilizer Download PDF

Info

Publication number
CN102816027A
CN102816027A CN201210267337XA CN201210267337A CN102816027A CN 102816027 A CN102816027 A CN 102816027A CN 201210267337X A CN201210267337X A CN 201210267337XA CN 201210267337 A CN201210267337 A CN 201210267337A CN 102816027 A CN102816027 A CN 102816027A
Authority
CN
China
Prior art keywords
weight part
fertilizer
parts
preparation
weight
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201210267337XA
Other languages
Chinese (zh)
Other versions
CN102816027B (en
Inventor
杨柳
唐旺全
杨红兵
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nantong Huinong Bio-organic Fertilizer Co.,Ltd.
Original Assignee
Maanshan Kebang Eco Fertilizer Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Maanshan Kebang Eco Fertilizer Co Ltd filed Critical Maanshan Kebang Eco Fertilizer Co Ltd
Priority to CN201210267337.XA priority Critical patent/CN102816027B/en
Publication of CN102816027A publication Critical patent/CN102816027A/en
Application granted granted Critical
Publication of CN102816027B publication Critical patent/CN102816027B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Fertilizers (AREA)

Abstract

The invention discloses a preparation method of a composite coated fertilizer containing amino acid chelating solution specially used for a soybean basal fertilizer. The preparation method comprises the steps of mixing the following materials by weight: 10-12 parts of urea, 22-25 parts of diammonium phosphate, 18-22 parts of potassium chloride, 2-5 parts of zinc sulfate, 1-2 parts of borax, 1-3 parts of radix sophorae flavescentis powder, 1-2 parts of gelatin powder, and 3-5 parts of compound powder; spraying 4-6 parts of amino acid chelating solution and 4-5 parts of a binding solution; granulating to obtain compound fertilizer granules; and spraying 7-10 parts of molten paraffin wax to surface of 100 parts of the fertilizer granules and then coating. The preparation method reasonably formulates various nutrition elements required by soybean growth to obtain the composite fertilizer with light weight, and excellent water-retaining, fertilizer-retaining and sustained-release properties.

Description

The special use of a kind of soybean base fertilizer contains the preparation method of the composite coated fertilizer of chelating amino acids liquid
Technical field
The present invention relates to fertilizer field, exactly is the preparation method that the special use of a kind of soybean base fertilizer contains the composite coated fertilizer of chelating amino acids liquid.
Background technology
Coated fertilizer is claimed coated fertilizer, film fertilizer again.Wrap up the fertilizer that the quick-acting chemical fertilizer granule forms with semipermeability or opacity film substrate.Filmogen has plastics, resin, paraffin, Vilaterm and elementary sulfur etc.The purpose of coating is that coated fertilizer is discharged at the available nutrient of the inside, back that is manured into soil lentamente, to prolong fertilizer efficiency.Rate of release is decided by coating kind, thickness, particle diameter, fertilizer solvability, the soil moisture, soil moisture content and soil microbial activities etc.Be applicable to that economic worth is high, breeding time is long, fertilizer requirement is big but the crop of inconvenient split application, and nutrient is easy to that the temperature of leaching loss is high, area of heavy rainfull or irrigate the area, especially on the light sand loam soil of quality.Existing coated fertilizer lacks specific aim more.
Summary of the invention
The object of the present invention is to provide a kind of with strong points, effective soybean base fertilizer special use to contain the preparation method of the composite coated fertilizer of chelating amino acids liquid.
Above-mentioned purpose realizes through following scheme:
The special use of a kind of soybean base fertilizer contains the preparation method of the composite coated fertilizer of chelating amino acids liquid, it is characterized in that: may further comprise the steps:
(1) mixing raw material 1-3 weight part lime carbonate, 1-2 weight part iron sand, 1-2 weight part rhombspar, 1-2 weight part potassium felspar sand, 1-2 weight part slag; The back is after 400-500 ℃ of scaling loss 6-8 hour; The Semen Maydis oil grind into powder that adds above-mentioned raw materials gross weight 1-2%; After 2-4 weight part xanthohumic acid mixed by weight, it was subsequent use promptly to get composite powder;
(2) earlier animal feather being added concentration is sulfuric acid 100-110 ℃ of following hydrolysis 1-2 hour of 25-35%; Generate amino acid, add lime then and be neutralized to Ph value 6.0-6.8, get hydrolyzed solution; Per 15 weight part hydrolysis liquid add 3-4 weight part CMC 99.5; Add 1-2 parts by weight of ferrous sulfate, the dissolving of 3-4 weight part ammonium molybdate again, 90-105 ℃ of reaction 5-6 hour, it was subsequent use promptly to get chelating amino acids liquid;
(3) 10-12 weight part urea, 22-25 weight part diammonium phosphate, 18-22 weight part Repone K, 2-5 weight part zinc sulfate, 1-2 weight part borax, 1-3 weight part kuh-seng powder, 1-2 weight part gelatin powder, the composite powder of 3-5 weight part are mixed by weight; Spray into 4-6 weight part chelating amino acids liquid and 4-5 weight part binding liquid again; Granulation promptly gets compound fertilizer granule;
(4) at 100 weight part compound fertilizer granule surface sprinkling 7-10 weight part melt paraffin coatings, promptly get product.
The special use of described a kind of soybean base fertilizer contains the preparation method of the composite coated fertilizer of chelating amino acids liquid, it is characterized in that: described binding liquid refers to a kind of in water glass, benzene emulsion, acrylate and vinyl acetate emulsion, resol, polyvinyl acetate emulsion and the rosin.
The special use of described a kind of soybean base fertilizer contains the preparation method of the composite coated fertilizer of chelating amino acids liquid, it is characterized in that: described hydrolyzed solution proportion is 1.1-1.3g/ml.
The special use of described a kind of soybean base fertilizer contains the preparation method of the composite coated fertilizer of chelating amino acids liquid, it is characterized in that: it is the sulphuric acid hydrolysis of 25-35% that every 80-150g animal feather adopts the concentration of 200-300ml.
The special use of described a kind of soybean base fertilizer contains the preparation method of the composite coated fertilizer of chelating amino acids liquid, it is characterized in that: step (4) operating procedure is: in rotary drum dressing machine, put into compound fertilizer granule by weight, 60-70 ℃ of following preheating 12-15min; The rotating speed of dressing machine is at 40-50r/min; Spray the paraffin of heating and melting in the rotary drum bag, sprayed paraffin by weight after, cool the temperature to 20-30 ℃; Dressing machine rotating speed is 35-45r/min; After 12-15 minute, discharging promptly gets product behind the normal temperature cooling drying.
Beneficial effect of the present invention is:
The present invention makes compound manure through each required nutritive element of reasonable re-compounded soybean growth, and light weight, water holding, the guarantor is fertile, sustained release performance is outstanding.Kuh-seng has the sterilization and disinsection effect, wears into pulvis, sneaks in the compound manure, helps prevention and elimination of disease and pests.Chelating amino acids liquid mixes little, moderate-element wherein, when having increased the nutrition of fertilizer, can let little, moderate-element discharge more slowly.
Paraffin can be regulated the slow release effect of coated fertilizer as outer coating agent.Through composite powder the favourable absorption effect of chemical fertilizer nutrient, the retardation that soil pore water is permeated are delayed the release to chemical fertilizer nutrient, obtained good result, also enriched the nutritive element of fertilizer simultaneously with chelating amino acids liquid.
Embodiment
The special use of a kind of soybean base fertilizer contains the preparation method of the composite coated fertilizer of chelating amino acids liquid, may further comprise the steps:
(1) mixing raw material 3kg lime carbonate, 1kg iron sand, 1kg rhombspar, 1kg potassium felspar sand, 1kg slag; The back is in 500 ℃ of scaling loss after 6 hours; Add the Semen Maydis oil grind into powder of above-mentioned raw materials gross weight 1%, after the 4kg xanthohumic acid mixed by weight, it was subsequent use promptly to get composite powder;
(2) earlier animal feather being added concentration is 30% sulfuric acid 100-110 ℃ of following hydrolysis 1-2 hour; Generate amino acid, add lime then and be neutralized to Ph value 6.0-6.8, get hydrolyzed solution; Every 15kg hydrolyzed solution adds the 3kg CMC 99.5; Add 1kg ferrous sulfate, the dissolving of 3kg ammonium molybdate again, 90-105 ℃ of reaction 5-6 hour, it was subsequent use promptly to get chelating amino acids liquid;
(3) 10kg urea, 25kg diammonium phosphate, 20kg Repone K, 3kg zinc sulfate, 1kg borax, 1.5kg kuh-seng powder, 1.5kg gelatin powder, the composite powder of 3kg are mixed by weight; Spray into 5kg chelating amino acids liquid and 4kg acrylate and vinyl acetate emulsion again; Granulation promptly gets compound fertilizer granule;
(4) in rotary drum dressing machine, put into the 100kg compound fertilizer granule, 70 ℃ of following preheating 15min, the rotating speed of dressing machine is at 50r/min; Spray the paraffin of 10kg heating and melting in the rotary drum bag, sprayed paraffin after, cool the temperature to 25 ℃; Dressing machine rotating speed is 40r/min; After 15 minutes, discharging promptly gets product behind the normal temperature cooling drying.
The concentration of every 150g animal feather employing 300ml is 25% sulphuric acid hydrolysis.
Compare with using the common nitrogenous fertilizer of equivalent, use gained fertilizer of the present invention soybean yields and on average improved 20-30%.
According to " slow release fertilizer " national standard (GB/T 23348-2009), slow release fertilizer will soak 24 hour initial stage nutrient release rate and accumulate the nutrient release rate less than 80% less than 15%, 28 day in 25 ℃ of hydrostatic.
The contrast of table 1 product index
Project The GB/T23348-2009 index Product of the present invention
Nutrient release rate in 24 hours <15% 11.31%
28 days accumulation nutrient release rates <80% 59.39%
Visible by table 1, present embodiment makes the product National standard.

Claims (5)

1. soybean base fertilizer special use contains the preparation method of the composite coated fertilizer of chelating amino acids liquid, it is characterized in that: may further comprise the steps:
(1) mixing raw material 1-3 weight part lime carbonate, 1-2 weight part iron sand, 1-2 weight part rhombspar, 1-2 weight part potassium felspar sand, 1-2 weight part slag; The back is after 400-500 ℃ of scaling loss 6-8 hour; The Semen Maydis oil grind into powder that adds above-mentioned raw materials gross weight 1-2%; After 2-4 weight part xanthohumic acid mixed by weight, it was subsequent use promptly to get composite powder;
(2) earlier animal feather being added concentration is sulfuric acid 100-110 ℃ of following hydrolysis 1-2 hour of 25-35%; Generate amino acid, add lime then and be neutralized to Ph value 6.0-6.8, get hydrolyzed solution; Per 15 weight part hydrolysis liquid add 3-4 weight part CMC 99.5; Add 1-2 parts by weight of ferrous sulfate, the dissolving of 3-4 weight part ammonium molybdate again, 90-105 ℃ of reaction 5-6 hour, it was subsequent use promptly to get chelating amino acids liquid;
(3) 10-12 weight part urea, 22-25 weight part diammonium phosphate, 18-22 weight part Repone K, 2-5 weight part zinc sulfate, 1-2 weight part borax, 1-3 weight part kuh-seng powder, 1-2 weight part gelatin powder, the composite powder of 3-5 weight part are mixed by weight; Spray into 4-6 weight part chelating amino acids liquid and 4-5 weight part binding liquid again; Granulation promptly gets compound fertilizer granule;
(4) at 100 weight part compound fertilizer granule surface sprinkling 7-10 weight part melt paraffin coatings, promptly get product.
2. a kind of soybean base fertilizer according to claim 1 special use contains the preparation method of the composite coated fertilizer of chelating amino acids liquid, it is characterized in that: described binding liquid refers to a kind of in water glass, benzene emulsion, acrylate and vinyl acetate emulsion, resol, polyvinyl acetate emulsion and the rosin.
3. a kind of soybean base fertilizer according to claim 1 special use contains the preparation method of the composite coated fertilizer of chelating amino acids liquid, it is characterized in that: described hydrolyzed solution proportion is 1.1-1.3g/ml.
4. a kind of soybean base fertilizer according to claim 1 special use contains the preparation method of the composite coated fertilizer of chelating amino acids liquid, it is characterized in that: it is the sulphuric acid hydrolysis of 25-35% that every 80-150g animal feather adopts the concentration of 200-300ml.
5. a kind of soybean base fertilizer according to claim 1 special use contains the preparation method of the composite coated fertilizer of chelating amino acids liquid, it is characterized in that: step (4) operating procedure is: in rotary drum dressing machine, put into compound fertilizer granule by weight, 60-70 ℃ of following preheating 12-15min; The rotating speed of dressing machine is at 40-50r/min; Spray the paraffin of heating and melting in the rotary drum bag, sprayed paraffin by weight after, cool the temperature to 20-30 ℃; Dressing machine rotating speed is 35-45r/min; After 12-15 minute, discharging promptly gets product behind the normal temperature cooling drying.
CN201210267337.XA 2012-07-31 2012-07-31 Preparation method of composite coated fertilizer containing amino acid chelating solution specially used for soybean basal fertilizer Active CN102816027B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201210267337.XA CN102816027B (en) 2012-07-31 2012-07-31 Preparation method of composite coated fertilizer containing amino acid chelating solution specially used for soybean basal fertilizer

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201210267337.XA CN102816027B (en) 2012-07-31 2012-07-31 Preparation method of composite coated fertilizer containing amino acid chelating solution specially used for soybean basal fertilizer

Publications (2)

Publication Number Publication Date
CN102816027A true CN102816027A (en) 2012-12-12
CN102816027B CN102816027B (en) 2014-07-09

Family

ID=47300531

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201210267337.XA Active CN102816027B (en) 2012-07-31 2012-07-31 Preparation method of composite coated fertilizer containing amino acid chelating solution specially used for soybean basal fertilizer

Country Status (1)

Country Link
CN (1) CN102816027B (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104030789A (en) * 2014-05-13 2014-09-10 马鞍山市心洲葡萄专业合作社 Modified-acrylic-acid coated synergic sustained-release composite fertilizer
CN104803767A (en) * 2015-04-16 2015-07-29 凤阳嘉禾农业科技有限公司 Special efficient amino acid chelate fertilizer for soybeans and preparation method of fertilizer

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1137030A (en) * 1996-04-26 1996-12-04 北京市海玉生化高新技术研究所 Effective amino-acid compound fertilizer and producing process thereof
CN1785924A (en) * 2005-11-04 2006-06-14 袁登辉 Amino acid organic fertilizer, its preparation method and use
CN102219610A (en) * 2011-05-19 2011-10-19 湖南省中科农业有限公司 Amino acid compound leaf fertilizer and preparation method thereof
US20120090366A1 (en) * 2010-04-16 2012-04-19 Taylor Pursell Controlled release fertilizer with biopolymer coating and process for making same

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1137030A (en) * 1996-04-26 1996-12-04 北京市海玉生化高新技术研究所 Effective amino-acid compound fertilizer and producing process thereof
CN1785924A (en) * 2005-11-04 2006-06-14 袁登辉 Amino acid organic fertilizer, its preparation method and use
US20120090366A1 (en) * 2010-04-16 2012-04-19 Taylor Pursell Controlled release fertilizer with biopolymer coating and process for making same
CN102219610A (en) * 2011-05-19 2011-10-19 湖南省中科农业有限公司 Amino acid compound leaf fertilizer and preparation method thereof

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
MARK C.GARDENER,等: "The effects of soil fertilizer on amino acids in the floral nectar of corncockle,Agrostemma githago(Caryophyllaceae)", 《OIKOS》, vol. 92, no. 1, 15 April 2003 (2003-04-15) *
周仕涛: "我国植物源农药的研究及前景", 《西南农业学报》, vol. 17, no. 4, 31 December 2004 (2004-12-31) *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104030789A (en) * 2014-05-13 2014-09-10 马鞍山市心洲葡萄专业合作社 Modified-acrylic-acid coated synergic sustained-release composite fertilizer
CN104030789B (en) * 2014-05-13 2016-03-02 马鞍山市心洲葡萄专业合作社 A kind of modified acroleic acid coating Synergistic slow release compound manure
CN104803767A (en) * 2015-04-16 2015-07-29 凤阳嘉禾农业科技有限公司 Special efficient amino acid chelate fertilizer for soybeans and preparation method of fertilizer

Also Published As

Publication number Publication date
CN102816027B (en) 2014-07-09

Similar Documents

Publication Publication Date Title
CN102826901B (en) Preparation method for special amino acid chelating liquid-containing composite coated base fertilizer for rape
CN102815991B (en) Fertilizer special for peanuts
CN104058891B (en) A kind of micro-composite coated fertilizer of crops and preparation method thereof that is rich in
CN103351211A (en) Machine-applied controlled-release fertilizer special for winter wheat and preparation method thereof
CN105399544A (en) Slow release composite fertilizer and preparation method thereof
WO2017206743A1 (en) Method for rapid manufacturing of novel micronutrient-containing urea
CN102531758A (en) Organic-inorganic sustained-release compound fertilizer applied at one time, and production method thereof
CN102815995B (en) Preparation method of composite envelope fertilizer containing amino acid chelate liquid special for peanut base fertilizer
CN103880554A (en) Controlled-release fertilizer taking isobutylidene diurea as coating material and preparation method thereof
CN102816019B (en) Fertilizer special for canola
CN102826936B (en) Preparation method of special base fertilizer for spring corn
CN102826882A (en) Carbamide chelated controlled release fertilizer and its preparation method
CN107986874A (en) A kind of method of watery fusion technique productions high tower fertilizer
CN103193553A (en) Production technology of water-soluble water retention drop irrigation slow release fertilizer
CN102815994A (en) Special fertilizer for paddy rice
CN104163670A (en) Method for producing tobacco special fertilizer
CN103739406A (en) Humic acid chelated boron, magnesium, zinc and iron fertilizer and preparation method thereof
CN103724117B (en) Special slow-release organic fertilizer for potato and a preparation method thereof
CN104892323A (en) Humic acid water-soluble compound fertilizer and method for manufacturing same
CN110698305A (en) Fulvic acid compound fertilizer suitable for corn planting in northeast region and preparation method thereof
CN102816027B (en) Preparation method of composite coated fertilizer containing amino acid chelating solution specially used for soybean basal fertilizer
CN110218116A (en) A kind of granular compound fertilizer adhesive for granulating and preparation method thereof
CN102826897B (en) Preparation method of special fertilizer for rice base fertilizer
CN107935664A (en) A kind of water-soluble fertilizer and preparation method thereof
CN104109598A (en) Banana peel-containing composite coated fertilizer and preparation method thereof

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CB03 Change of inventor or designer information
CB03 Change of inventor or designer information

Inventor after: Zhou Yujie

Inventor after: Wang Yongmei

Inventor before: Yang Liu

Inventor before: Tang Wangquan

Inventor before: Yang Hongbing

TR01 Transfer of patent right
TR01 Transfer of patent right

Effective date of registration: 20170901

Address after: 300202 20-505-507, Xincheng District, Tianjin, Hexi District

Co-patentee after: Wang Yongmei

Patentee after: Zhou Yujie

Address before: 243100 Anhui city of Ma'anshan province Dangtu County Economic Development Zone

Patentee before: Maanshan Kebang Eco-Fertilizer Co.,Ltd.

TR01 Transfer of patent right
TR01 Transfer of patent right

Effective date of registration: 20181026

Address after: 221600 Jiangsu, Xuzhou, Peixian, Han Xiang Road East, Yu Jia dress North

Patentee after: Jiangsu Guilin animal husbandry Group Co., Ltd.

Address before: 300202 Tianjin Hexi District new town 20-505-507

Co-patentee before: Wang Yongmei

Patentee before: Zhou Yujie

TR01 Transfer of patent right
TR01 Transfer of patent right

Effective date of registration: 20210323

Address after: 226600 industrial concentration area, Libu Town, Hai'an City, Nantong City, Jiangsu Province

Patentee after: Nantong Huinong Bio-organic Fertilizer Co.,Ltd.

Address before: 221600 Jiangsu, Xuzhou, Peixian, Han Xiang Road East, Yu Jia dress North

Patentee before: JIANGSU GUILIU ANIMAL HUSBANDRY GROUP Co.,Ltd.