CN102796618B - Method for extracting essential oil from orange peel - Google Patents
Method for extracting essential oil from orange peel Download PDFInfo
- Publication number
- CN102796618B CN102796618B CN 201210310127 CN201210310127A CN102796618B CN 102796618 B CN102796618 B CN 102796618B CN 201210310127 CN201210310127 CN 201210310127 CN 201210310127 A CN201210310127 A CN 201210310127A CN 102796618 B CN102796618 B CN 102796618B
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- CN
- China
- Prior art keywords
- orange peel
- volatile oil
- essential oil
- ethanol
- filtrate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000000341 volatile oil Substances 0.000 title claims abstract description 35
- 238000000034 method Methods 0.000 title claims description 21
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 32
- 238000004519 manufacturing process Methods 0.000 claims abstract description 11
- 239000000284 extract Substances 0.000 claims description 11
- WBZKQQHYRPRKNJ-UHFFFAOYSA-L disulfite Chemical compound [O-]S(=O)S([O-])(=O)=O WBZKQQHYRPRKNJ-UHFFFAOYSA-L 0.000 claims description 10
- 239000000243 solution Substances 0.000 claims description 10
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 8
- 239000003795 chemical substances by application Substances 0.000 claims description 8
- 239000000706 filtrate Substances 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 6
- 235000010987 pectin Nutrition 0.000 claims description 5
- 229920001277 pectin Polymers 0.000 claims description 5
- 239000001814 pectin Substances 0.000 claims description 5
- 239000000047 product Substances 0.000 claims description 5
- 239000007864 aqueous solution Substances 0.000 claims description 4
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 4
- 230000003750 conditioning effect Effects 0.000 claims description 4
- 230000006837 decompression Effects 0.000 claims description 4
- 238000001035 drying Methods 0.000 claims description 4
- 238000001914 filtration Methods 0.000 claims description 4
- 239000012634 fragment Substances 0.000 claims description 4
- 238000002390 rotary evaporation Methods 0.000 claims description 4
- 229920006395 saturated elastomer Polymers 0.000 claims description 4
- 238000000926 separation method Methods 0.000 claims description 4
- 238000009423 ventilation Methods 0.000 claims description 4
- 239000011780 sodium chloride Substances 0.000 claims description 3
- 238000005516 engineering process Methods 0.000 abstract description 8
- 238000000605 extraction Methods 0.000 abstract description 7
- 230000032683 aging Effects 0.000 abstract description 4
- 238000002360 preparation method Methods 0.000 abstract 1
- 239000003921 oil Substances 0.000 description 5
- 235000019198 oils Nutrition 0.000 description 5
- 230000008569 process Effects 0.000 description 5
- 241001672694 Citrus reticulata Species 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000003205 fragrance Substances 0.000 description 3
- 238000003801 milling Methods 0.000 description 3
- XMGQYMWWDOXHJM-JTQLQIEISA-N (+)-α-limonene Chemical compound CC(=C)[C@@H]1CCC(C)=CC1 XMGQYMWWDOXHJM-JTQLQIEISA-N 0.000 description 2
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 2
- MOYAFQVGZZPNRA-UHFFFAOYSA-N Terpinolene Chemical compound CC(C)=C1CCC(C)=CC1 MOYAFQVGZZPNRA-UHFFFAOYSA-N 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- UAHWPYUMFXYFJY-UHFFFAOYSA-N beta-myrcene Chemical compound CC(C)=CCCC(=C)C=C UAHWPYUMFXYFJY-UHFFFAOYSA-N 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- -1 salt ion Chemical class 0.000 description 2
- 238000001256 steam distillation Methods 0.000 description 2
- GJYKUZUTZNTBEC-IVZWLZJFSA-N (1R,4S,5R)-4-methyl-1-propan-2-ylbicyclo[3.1.0]hex-2-ene Chemical compound CC(C)[C@@]12C[C@@H]1[C@@H](C)C=C2 GJYKUZUTZNTBEC-IVZWLZJFSA-N 0.000 description 1
- 241000207199 Citrus Species 0.000 description 1
- 239000004278 EU approved seasoning Substances 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 244000061176 Nicotiana tabacum Species 0.000 description 1
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- VYBREYKSZAROCT-UHFFFAOYSA-N alpha-myrcene Natural products CC(=C)CCCC(=C)C=C VYBREYKSZAROCT-UHFFFAOYSA-N 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 230000000259 anti-tumor effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 230000000711 cancerogenic effect Effects 0.000 description 1
- 231100000315 carcinogenic Toxicity 0.000 description 1
- 210000002421 cell wall Anatomy 0.000 description 1
- 229930002875 chlorophyll Natural products 0.000 description 1
- 235000019804 chlorophyll Nutrition 0.000 description 1
- ATNHDLDRLWWWCB-AENOIHSZSA-M chlorophyll a Chemical compound C1([C@@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC(C(CC)=C3C)=[N+]4C3=CC3=C(C=C)C(C)=C5N3[Mg-2]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 ATNHDLDRLWWWCB-AENOIHSZSA-M 0.000 description 1
- 235000020971 citrus fruits Nutrition 0.000 description 1
- 239000001071 citrus reticulata blanco var. mandarin Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000011194 food seasoning agent Nutrition 0.000 description 1
- 125000000524 functional group Chemical group 0.000 description 1
- 238000002290 gas chromatography-mass spectrometry Methods 0.000 description 1
- 235000020710 ginseng extract Nutrition 0.000 description 1
- 210000004907 gland Anatomy 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000003317 industrial substance Substances 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 210000003097 mucus Anatomy 0.000 description 1
- 238000011017 operating method Methods 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 239000000825 pharmaceutical preparation Substances 0.000 description 1
- 229940127557 pharmaceutical product Drugs 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 238000005185 salting out Methods 0.000 description 1
- 239000008159 sesame oil Substances 0.000 description 1
- 235000011803 sesame oil Nutrition 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 235000017557 sodium bicarbonate Nutrition 0.000 description 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229930006978 terpinene Natural products 0.000 description 1
- 150000003507 terpinene derivatives Chemical class 0.000 description 1
- 238000007669 thermal treatment Methods 0.000 description 1
- 238000001149 thermolysis Methods 0.000 description 1
- 210000004881 tumor cell Anatomy 0.000 description 1
Landscapes
- Fats And Perfumes (AREA)
- Edible Oils And Fats (AREA)
Abstract
Description
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 201210310127 CN102796618B (en) | 2012-08-23 | 2012-08-23 | Method for extracting essential oil from orange peel |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 201210310127 CN102796618B (en) | 2012-08-23 | 2012-08-23 | Method for extracting essential oil from orange peel |
Publications (2)
Publication Number | Publication Date |
---|---|
CN102796618A CN102796618A (en) | 2012-11-28 |
CN102796618B true CN102796618B (en) | 2013-08-28 |
Family
ID=47195928
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN 201210310127 Active CN102796618B (en) | 2012-08-23 | 2012-08-23 | Method for extracting essential oil from orange peel |
Country Status (1)
Country | Link |
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CN (1) | CN102796618B (en) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103989781B (en) * | 2014-06-17 | 2016-03-16 | 陈智辉 | The Pericarpium Citri Reticulatae concocting method that a kind of speed is fragrant |
CN104130864B (en) * | 2014-07-16 | 2016-09-07 | 湖北中烟工业有限责任公司 | A kind of preparation method of cigarette sweet orange spices |
CN106539053A (en) * | 2016-11-08 | 2017-03-29 | 上海应用技术大学 | A kind of preparation method of gold bergamot quintessence oil |
CN111304000A (en) * | 2020-03-02 | 2020-06-19 | 南京喜之郎食品有限公司 | Preparation method for extracting mandarin orange essence from mandarin orange peel and product thereof |
CN111205928B (en) * | 2020-03-03 | 2020-10-27 | 珠海积家世纪日化有限公司 | Cosmetic plant essential oil filtering and extracting system and filtering and extracting process |
CN115894155A (en) * | 2022-10-25 | 2023-04-04 | 青岛日晟源作物营养有限公司 | Extraction method of D-limonene |
CN116286192A (en) * | 2023-03-28 | 2023-06-23 | 广西冰客食品有限公司 | Process for producing Wo orange peel oil |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101643686A (en) * | 2008-08-04 | 2010-02-10 | 北京科技桥科贸有限公司 | Orange peel essential oil |
CN101768516A (en) * | 2010-02-09 | 2010-07-07 | 浙江工业大学 | Tangerine oil and preparation method and application thereof |
CN102229680A (en) * | 2011-06-06 | 2011-11-02 | 浙江师范大学 | Method for combined production of essential oil, pigment, pectin and flavone from orange peel |
CN102268327A (en) * | 2010-06-01 | 2011-12-07 | 浙江省柑桔研究所 | Method for orange peel essential oil and pectin combined production |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ZA83854B (en) * | 1982-02-17 | 1983-11-30 | Tropicana Prod Inc | Process for production of useful products from citrus fruit peel |
-
2012
- 2012-08-23 CN CN 201210310127 patent/CN102796618B/en active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101643686A (en) * | 2008-08-04 | 2010-02-10 | 北京科技桥科贸有限公司 | Orange peel essential oil |
CN101768516A (en) * | 2010-02-09 | 2010-07-07 | 浙江工业大学 | Tangerine oil and preparation method and application thereof |
CN102268327A (en) * | 2010-06-01 | 2011-12-07 | 浙江省柑桔研究所 | Method for orange peel essential oil and pectin combined production |
CN102229680A (en) * | 2011-06-06 | 2011-11-02 | 浙江师范大学 | Method for combined production of essential oil, pigment, pectin and flavone from orange peel |
Non-Patent Citations (1)
Title |
---|
李于善,等.柑橘香精油的提取及提高其香气品质的研究.《食品与发酵工业》.2004,第30卷(第11期),对比文件2的第52页第2.3节、53页第4节. * |
Also Published As
Publication number | Publication date |
---|---|
CN102796618A (en) | 2012-11-28 |
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Effective date of registration: 20170926 Address after: 402460, Rongchang County, Panlong County, Panlong County, Chongqing province 2 clubs Patentee after: Chongqing Yong Qing Huaqing agricultural science and Technology Development Co., Ltd. Address before: 273306 Shandong city of Linyi Province town Pingyi County Linyi Qiwei Canned Food Co. Ltd. Patentee before: Gao Wei |
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TR01 | Transfer of patent right |
Effective date of registration: 20190925 Address after: Room 501, Office Building of Market Supervision Bureau of Langchuan Avenue, Jianping Town, Langxi County, Xuancheng City, Anhui Province Patentee after: Xuancheng Geith Intellectual Property Operations Co., Ltd. Address before: 402460 Changzhou Village 2 Society, Panlong Town, Rongchang County, Chongqing Patentee before: Chongqing Yong Qing Huaqing agricultural science and Technology Development Co., Ltd. |
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Effective date of registration: 20191025 Address after: 1007-1, floor 10, building 6, No. 170, Beiyuan Road, Chaoyang District, Beijing 100020 Patentee after: Beijing biyou Yayun Technology Co. Ltd. Address before: Room 501, Office Building of Market Supervision Bureau of Langchuan Avenue, Jianping Town, Langxi County, Xuancheng City, Anhui Province Patentee before: Xuancheng Geith Intellectual Property Operations Co., Ltd. |
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TR01 | Transfer of patent right |