CN102795949A - Smokeless cellulose - Google Patents
Smokeless cellulose Download PDFInfo
- Publication number
- CN102795949A CN102795949A CN201210334268XA CN201210334268A CN102795949A CN 102795949 A CN102795949 A CN 102795949A CN 201210334268X A CN201210334268X A CN 201210334268XA CN 201210334268 A CN201210334268 A CN 201210334268A CN 102795949 A CN102795949 A CN 102795949A
- Authority
- CN
- China
- Prior art keywords
- weight parts
- weight
- parts
- smokeless
- camphor
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000001913 cellulose Substances 0.000 title claims abstract description 24
- 229920002678 cellulose Polymers 0.000 title claims abstract description 24
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims abstract description 44
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims abstract description 40
- 239000000835 fiber Substances 0.000 claims abstract description 25
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 claims abstract description 22
- 241000723346 Cinnamomum camphora Species 0.000 claims abstract description 22
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims abstract description 22
- 229960000846 camphor Drugs 0.000 claims abstract description 22
- 229930008380 camphor Natural products 0.000 claims abstract description 22
- 229910017604 nitric acid Inorganic materials 0.000 claims abstract description 22
- 239000000203 mixture Substances 0.000 claims abstract description 20
- 229910000029 sodium carbonate Inorganic materials 0.000 claims abstract description 20
- 240000008042 Zea mays Species 0.000 claims abstract description 19
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 claims abstract description 19
- 235000002017 Zea mays subsp mays Nutrition 0.000 claims abstract description 19
- 235000005822 corn Nutrition 0.000 claims abstract description 19
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims abstract description 14
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000002699 waste material Substances 0.000 claims abstract description 12
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims abstract description 11
- 235000017491 Bambusa tulda Nutrition 0.000 claims abstract description 11
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims abstract description 11
- 239000011425 bamboo Substances 0.000 claims abstract description 11
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 9
- 230000000802 nitrating effect Effects 0.000 claims abstract description 9
- 235000014676 Phragmites communis Nutrition 0.000 claims abstract description 8
- 240000000111 Saccharum officinarum Species 0.000 claims abstract description 8
- 235000007201 Saccharum officinarum Nutrition 0.000 claims abstract description 8
- 239000002904 solvent Substances 0.000 claims abstract description 7
- 240000008790 Musa x paradisiaca Species 0.000 claims abstract 3
- 235000013311 vegetables Nutrition 0.000 claims description 34
- 239000003814 drug Substances 0.000 claims description 27
- NQPDZGIKBAWPEJ-UHFFFAOYSA-N pentanoic acid group Chemical group C(CCCC)(=O)O NQPDZGIKBAWPEJ-UHFFFAOYSA-N 0.000 claims description 20
- 235000017550 sodium carbonate Nutrition 0.000 claims description 19
- 241001330002 Bambuseae Species 0.000 claims description 10
- 239000002023 wood Substances 0.000 claims description 10
- 238000006396 nitration reaction Methods 0.000 claims description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 235000021015 bananas Nutrition 0.000 claims description 6
- 238000010298 pulverizing process Methods 0.000 claims description 5
- 240000006240 Linum usitatissimum Species 0.000 claims description 4
- 235000004431 Linum usitatissimum Nutrition 0.000 claims description 4
- 239000003595 mist Substances 0.000 claims description 4
- 239000003513 alkali Substances 0.000 claims description 3
- 241000196324 Embryophyta Species 0.000 abstract description 6
- 230000008901 benefit Effects 0.000 abstract description 4
- 230000007613 environmental effect Effects 0.000 abstract description 3
- 239000000779 smoke Substances 0.000 abstract description 2
- DMBHHRLKUKUOEG-UHFFFAOYSA-N diphenylamine Chemical compound C=1C=CC=CC=1NC1=CC=CC=C1 DMBHHRLKUKUOEG-UHFFFAOYSA-N 0.000 abstract 4
- 235000017060 Arachis glabrata Nutrition 0.000 abstract 1
- 244000105624 Arachis hypogaea Species 0.000 abstract 1
- 235000010777 Arachis hypogaea Nutrition 0.000 abstract 1
- 235000018262 Arachis monticola Nutrition 0.000 abstract 1
- 235000018290 Musa x paradisiaca Nutrition 0.000 abstract 1
- 244000082204 Phyllostachys viridis Species 0.000 abstract 1
- 125000003158 alcohol group Chemical group 0.000 abstract 1
- 239000000428 dust Substances 0.000 abstract 1
- 231100000956 nontoxicity Toxicity 0.000 abstract 1
- 239000002245 particle Substances 0.000 abstract 1
- 235000020232 peanut Nutrition 0.000 abstract 1
- 239000003381 stabilizer Substances 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 11
- 238000004519 manufacturing process Methods 0.000 description 10
- 238000012360 testing method Methods 0.000 description 10
- 238000001035 drying Methods 0.000 description 9
- 239000000843 powder Substances 0.000 description 9
- 150000001875 compounds Chemical class 0.000 description 8
- 230000008030 elimination Effects 0.000 description 6
- 238000003379 elimination reaction Methods 0.000 description 6
- 239000012535 impurity Substances 0.000 description 6
- 238000000034 method Methods 0.000 description 5
- 239000002994 raw material Substances 0.000 description 5
- 241000234295 Musa Species 0.000 description 4
- 229920002472 Starch Polymers 0.000 description 4
- 239000004519 grease Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 230000007935 neutral effect Effects 0.000 description 4
- 230000035945 sensitivity Effects 0.000 description 4
- 239000008107 starch Substances 0.000 description 4
- 235000019698 starch Nutrition 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 238000005406 washing Methods 0.000 description 4
- 239000002585 base Substances 0.000 description 3
- 235000019504 cigarettes Nutrition 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 239000008104 plant cellulose Substances 0.000 description 3
- 230000000007 visual effect Effects 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 230000003044 adaptive effect Effects 0.000 description 2
- 238000005422 blasting Methods 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000005034 decoration Methods 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000007654 immersion Methods 0.000 description 2
- 231100000252 nontoxic Toxicity 0.000 description 2
- 230000003000 nontoxic effect Effects 0.000 description 2
- 238000012216 screening Methods 0.000 description 2
- 238000002791 soaking Methods 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 230000009967 tasteless effect Effects 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- ZHLKXBJTJHRTTE-UHFFFAOYSA-N Chlorobenside Chemical compound C1=CC(Cl)=CC=C1CSC1=CC=C(Cl)C=C1 ZHLKXBJTJHRTTE-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 238000005474 detonation Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 235000011194 food seasoning agent Nutrition 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000008194 pharmaceutical composition Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 239000003380 propellant Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Medicines Containing Plant Substances (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
Description
Claims (5)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201210334268.XA CN102795949B (en) | 2012-09-12 | 2012-09-12 | Smokeless cellulose |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201210334268.XA CN102795949B (en) | 2012-09-12 | 2012-09-12 | Smokeless cellulose |
Publications (2)
Publication Number | Publication Date |
---|---|
CN102795949A true CN102795949A (en) | 2012-11-28 |
CN102795949B CN102795949B (en) | 2015-04-01 |
Family
ID=47195291
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201210334268.XA Expired - Fee Related CN102795949B (en) | 2012-09-12 | 2012-09-12 | Smokeless cellulose |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN102795949B (en) |
Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104003825A (en) * | 2014-05-30 | 2014-08-27 | 泸州北方化学工业有限公司 | Wood pulp nitrocellulose single-base propellant and preparation method thereof |
CN104817417A (en) * | 2015-04-13 | 2015-08-05 | 喻自达 | Bamboo charcoal fiber cotton |
CN108191588A (en) * | 2018-02-26 | 2018-06-22 | 湖南省浏阳金生花炮有限公司 | Bamboo cellulose propellant powder |
CN108559103A (en) * | 2018-02-08 | 2018-09-21 | 潘小秋 | A kind of nitro stalk element preparation method and product |
CN108774096A (en) * | 2018-08-30 | 2018-11-09 | 浏阳象形精品烟花出口制造有限公司 | A kind of micro- pyrotechnic composition of colloid and its preparation process of hardly possible solvent flashing |
CN109369926A (en) * | 2018-11-26 | 2019-02-22 | 潘小秋 | Smokeless lignocellulosic of nitro and preparation method thereof |
CN109764762A (en) * | 2019-03-07 | 2019-05-17 | 浏阳东顺花炮新材料技术开发有限公司 | The continuous process system and its production technology of novel firework biology powder |
CN111056884A (en) * | 2019-11-27 | 2020-04-24 | 江西吉润花炮新材料科技有限公司 | Safe smokeless and sulfur-free moisture-proof agent and preparation method thereof |
CN111533629A (en) * | 2020-05-27 | 2020-08-14 | 湖南坤普科技有限公司 | Firework and firecracker containing nitrocellulose and method for improving burning speed of firework and firecracker |
CN111848823A (en) * | 2020-08-18 | 2020-10-30 | 潘小秋 | Ester alcohol bamboo wood cellulose and preparation method thereof |
CN116497465A (en) * | 2023-05-17 | 2023-07-28 | 中应国强安全科技(北京)有限公司 | Amaranth plant fiber, preparation method thereof and firework |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2002026663A1 (en) * | 2000-09-26 | 2002-04-04 | Breed Automotive Technology, Inc. | Apparatus for igniting gas generating material |
CN101077846A (en) * | 2006-05-26 | 2007-11-28 | 比亚迪股份有限公司 | Safety belt pre-tightening instrument gas production medicine and preparation method thereof |
CN101275820A (en) * | 2008-05-06 | 2008-10-01 | 湖南省浏阳金生花炮有限公司 | Environment protection type micro-fume firecrackers |
CN101434506A (en) * | 2007-11-13 | 2009-05-20 | 比亚迪股份有限公司 | Safety belt pretensioner aerogenesis medicament and preparation method thereof |
CN101838332A (en) * | 2010-07-09 | 2010-09-22 | 北京理工大学 | Method for preparing nanometer nitro celluloses |
CN102584505A (en) * | 2012-01-16 | 2012-07-18 | 南京理工大学 | Modular smokeless firework ammunition capable of improving dampproof performance and preparation method for modular smokeless firework ammunition |
-
2012
- 2012-09-12 CN CN201210334268.XA patent/CN102795949B/en not_active Expired - Fee Related
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2002026663A1 (en) * | 2000-09-26 | 2002-04-04 | Breed Automotive Technology, Inc. | Apparatus for igniting gas generating material |
CN101077846A (en) * | 2006-05-26 | 2007-11-28 | 比亚迪股份有限公司 | Safety belt pre-tightening instrument gas production medicine and preparation method thereof |
CN101434506A (en) * | 2007-11-13 | 2009-05-20 | 比亚迪股份有限公司 | Safety belt pretensioner aerogenesis medicament and preparation method thereof |
CN101275820A (en) * | 2008-05-06 | 2008-10-01 | 湖南省浏阳金生花炮有限公司 | Environment protection type micro-fume firecrackers |
CN101838332A (en) * | 2010-07-09 | 2010-09-22 | 北京理工大学 | Method for preparing nanometer nitro celluloses |
CN102584505A (en) * | 2012-01-16 | 2012-07-18 | 南京理工大学 | Modular smokeless firework ammunition capable of improving dampproof performance and preparation method for modular smokeless firework ammunition |
Cited By (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104003825B (en) * | 2014-05-30 | 2016-08-24 | 泸州北方化学工业有限公司 | Wood pulp nitrocellulose single-base gun propellant and preparation method thereof |
CN104003825A (en) * | 2014-05-30 | 2014-08-27 | 泸州北方化学工业有限公司 | Wood pulp nitrocellulose single-base propellant and preparation method thereof |
CN104817417A (en) * | 2015-04-13 | 2015-08-05 | 喻自达 | Bamboo charcoal fiber cotton |
CN104817417B (en) * | 2015-04-13 | 2017-12-12 | 湖南浏花烟花有限公司 | A kind of method for preparing bamboo charcoal fiber cotton |
CN108559103B (en) * | 2018-02-08 | 2020-11-06 | 潘小秋 | Preparation method of nitro-straw extract and product |
CN108559103A (en) * | 2018-02-08 | 2018-09-21 | 潘小秋 | A kind of nitro stalk element preparation method and product |
CN108191588A (en) * | 2018-02-26 | 2018-06-22 | 湖南省浏阳金生花炮有限公司 | Bamboo cellulose propellant powder |
CN108774096A (en) * | 2018-08-30 | 2018-11-09 | 浏阳象形精品烟花出口制造有限公司 | A kind of micro- pyrotechnic composition of colloid and its preparation process of hardly possible solvent flashing |
CN109369926A (en) * | 2018-11-26 | 2019-02-22 | 潘小秋 | Smokeless lignocellulosic of nitro and preparation method thereof |
CN109369926B (en) * | 2018-11-26 | 2021-07-27 | 潘小秋 | Nitro smokeless lignocellulose and preparation method thereof |
CN109764762A (en) * | 2019-03-07 | 2019-05-17 | 浏阳东顺花炮新材料技术开发有限公司 | The continuous process system and its production technology of novel firework biology powder |
CN111056884A (en) * | 2019-11-27 | 2020-04-24 | 江西吉润花炮新材料科技有限公司 | Safe smokeless and sulfur-free moisture-proof agent and preparation method thereof |
CN111056884B (en) * | 2019-11-27 | 2023-04-25 | 江西吉润花炮新材料科技有限公司 | Safe, smokeless and sulfur-free dampproof agent and preparation method thereof |
CN111533629A (en) * | 2020-05-27 | 2020-08-14 | 湖南坤普科技有限公司 | Firework and firecracker containing nitrocellulose and method for improving burning speed of firework and firecracker |
CN111848823A (en) * | 2020-08-18 | 2020-10-30 | 潘小秋 | Ester alcohol bamboo wood cellulose and preparation method thereof |
CN116497465A (en) * | 2023-05-17 | 2023-07-28 | 中应国强安全科技(北京)有限公司 | Amaranth plant fiber, preparation method thereof and firework |
CN116497465B (en) * | 2023-05-17 | 2024-05-07 | 中应国强安全科技(北京)有限公司 | Amaranth plant fiber, preparation method thereof and firework |
Also Published As
Publication number | Publication date |
---|---|
CN102795949B (en) | 2015-04-01 |
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Legal Events
Date | Code | Title | Description |
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C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C53 | Correction of patent of invention or patent application | ||
CB02 | Change of applicant information |
Address after: 410300, Huai River Street office, Hunan, Liuyang Province, refers to the back road 50 Applicant after: Pan Xiaoqiu Address before: 410300, Hunan, Liuyang, refers to the back of the arch, No. 022, Beiqiao Applicant before: Pan Xiaoqiu |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right |
Effective date of registration: 20210918 Address after: 410300 No. 49, Shishuang Road, Jili street, Liuyang City, Changsha City, Hunan Province Patentee after: Hunan Xusheng New Material Technology Co.,Ltd. Address before: 410300 huaichuan sub district office, Liuyang City, Hunan Province, No. 50 zhibeichong Road Patentee before: Pan Xiaoqiu |
|
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20220831 Address after: Dasheng Village, Chengtanjiang Town, Liuyang City, Changsha City, Hunan Province 410300 Patentee after: Liuyang Huajin Fireworks Manufacturing Co.,Ltd. Address before: 410300 No. 49, Shishuang Road, Jili street, Liuyang City, Changsha City, Hunan Province Patentee before: Hunan Xusheng New Material Technology Co.,Ltd. |
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TR01 | Transfer of patent right | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150401 |
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CF01 | Termination of patent right due to non-payment of annual fee |