CN102764207A - Pu'er tea toothpaste and preparation method thereof - Google Patents
Pu'er tea toothpaste and preparation method thereof Download PDFInfo
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- CN102764207A CN102764207A CN2012101922996A CN201210192299A CN102764207A CN 102764207 A CN102764207 A CN 102764207A CN 2012101922996 A CN2012101922996 A CN 2012101922996A CN 201210192299 A CN201210192299 A CN 201210192299A CN 102764207 A CN102764207 A CN 102764207A
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- China
- Prior art keywords
- tea
- toothpaste
- sodium
- folium camelliae
- camelliae assamicae
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Landscapes
- Cosmetics (AREA)
Abstract
The present invention relates to a Pu'er tea toothpaste and a preparation method thereof. The Pu'er tea toothpaste is characterized by comprising a Pu'er tea extract, which is obtained by steps of low temperature pulverization, ultrasonic extraction, pressure filtration, separation and concentration. The Pu'er tea extract is combined with food-grade auxiliary materials comprising glycerin, sorbitol, PEG400, tetrasodium pyrophosphate, sodium dihydrogen phosphate, sodium phytate, sodium carboxymethyl cellulose, xanthan gum, sodium lauryl sulfate, calcium phosphate dihydrate, hydrated silica and essence to prepare the Pu'er tea toothpaste. The method fundamentally eliminates quality issues such as spoilage, degeneration, color changing, flavor changing and chemical safety of the tea toothpaste, and effectively prolongs a shelf period of the tea toothpaste. The tea toothpaste has multiple special efficacies, such as removing scale, decomposing residual smoke stains, tea stains and coffee stains in slits between the teeth, reducing plaque, preventing breeding of harmful bacteria, disinfecting, diminishing inflammation, stopping bleeding, eliminating odor, promoting the secretion of saliva, moisturizing mouth, recovering taste buds, improving taste sense, and enabling a user to taste better flavor of food, and is a natural healthful tea toothpaste.
Description
Technical field
The invention belongs to the articles for daily use and field of health care products, relate to Folium Camelliae sinensis toothpaste, particularly a kind of Folium camelliae assamicae toothpaste and preparation method thereof.
Background technology
Toothpaste is the indispensable cosmetics of everyday use of cleaning oral cavity tooth in people's daily life, generally is made up of abrasive, wetting agent, surfactant, sweeting agent, essence and flavoring agent and water.Along with expanding economy and growth in the living standard; People, also require to have auxiliary the reparation or prevention Buccodental disease, as help to remove the stain dirt except having the tooth protection that cleans one's teeth, removing the basic function of halitosis and stain dirt the requirement of toothpaste; Decompose cigarette stain, tobacco poisoning residual in the teeth space; Effects such as inhibition Buccodental noxious bacteria grows, the assisting sterilisation antiinflammatory, recovers taste bud, improves the sense of taste, and it is more flavoursome to eat.Under the promotion of powerful demand and chemical industry that emerges day by day and the industrial chemicals that becomes increasingly abundant; The toothpaste industrial development is rapid; Tooth paste product is more and more abundanter; Multiple efficacies type toothpaste arises at the historic moment, like anti-dentin hypersensitiveness toothpaste, go to steep whitening toothpaste, anti-caries toothpaste, odor type toothpaste, the auxiliary reparation or medicated toothpaste of prevention Buccodental disease or the like, for the consumer of different demands provides broad selection space.But; For there is healthy and safe hidden danger in the raw material of industry such as sodium fluoride, compound essence and the medicines etc. that reach the chemosynthesis that above-mentioned effect adds in toothpaste; This pays much attention to healthy and safe today people, undoubtedly toothpaste is produced used former, adjuvant and toothpaste efficiency is had higher requirement.
Folium Camelliae sinensis contains extremely abundant organic chemistry composition and inorganic mineral element as pure natural plants, just is used as the beverage of preventing and treating diseases, building body, life lengthening since ancient times, is described as the most healthy beverage.In recent years, people turn one's attention to Folium Camelliae sinensis one after another, expect that it can substitute industrial chemicals, medicine etc. and in toothpaste, bring into play effect.
CN 1686077A discloses a kind of toothpaste that contains Camellia nitidissima Chi; It has added the Camellia nitidissima Chi concentrated solution in lotion of toothpaste substrate commonly used; Utilize the composition of the aminoacid that is contained in the Camellia nitidissima Chi, tea polyphenol antibiotic, antiinflammatory, thereby had effects such as nutrition oral cavity, anti-inflammation.The toothpaste of this invention has utilized the effect of Camellia nitidissima Chi itself, but does not get rid of the potential safety hazard of other used industrial chemicals.
CN 100584309C discloses a kind of concave-convex bar mother chrysanthemum green tea toothpaste and production method; The main points of its technical scheme are: be made up of lip lipstick attapulgite clay, fresh tea leaf in its, new fresh honeysuckle, bright Herba Menthae, fresh Rhizoma Imperatae, sodium lauryl sulphate, potassium sorbate and deionized water; Make the concave-convex bar mother chrysanthemum green tea toothpaste finished product through technological processes such as steam beating, batching, stirring at low speed, pulverizing making beating, grinding, high-speed stirred, vacuum outgass; Have soft fine and smooth, clean even, refrigerant tasty and refreshing characteristics, can adsorb and remove the multiple foreign odor flavor in the oral cavity.The toothpaste of this invention does not possess the stain of removal dirt, decomposes cigarette stain residual in the teeth space, the effect of tobacco poisoning.
CN 102085166A discloses a kind of Folium Camelliae sinensis toothpaste, and it comprises combination thing by weight percentage: silica 1 5-25%, abrasive 0.1-0.5%, wetting agent 50-75%, binding agent 0.5-2%, foaming agent 1-3%, spice 0.5-3%, Folium Camelliae sinensis extract 0.1-0.5, surplus pure water.The toothpaste of this invention can be assisted the prevention oral disease, and there is the nursing health effect in the oral cavity.Shortcoming is not get rid of the potential safety hazard of other industrial chemicals, and does not possess and steep the effect of whitening.
CN 101543470A discloses a kind of algae tea nutrient toothpaste and preparation method thereof; Mainly form by small alga ball, green tea, calcium carbonate, Oleum Cocois, hydroxy methocel, edible essence, glucide, sodium lauryl sulphate, sodium benzoate and water; Its preparation method is: (1) green tea decocte with water gets green tea extract; (2) small alga ball, Oleum Cocois, hydroxy methocel are dissolved in the water, and heating is brewed into slurry; (3) calcium carbonate, green tea extract are dissolved in the water, stir into slurry; (4) step (2), (3) gained slurry are mixed, add other raw materials, stir, fine ground; (5) be packaged as finished product.This toothpaste has kept the effective ingredient of algae and green tea, can reduce the morbidity of dental caries and periodontal disease, the good effects that has the health care oral cavity and protect tooth.The toothpaste of this invention does not possess and steeps the effect of whitening.
CN 102106802A discloses a kind of tea salt toothpaste and preparation method thereof, and the percentage by weight of its raw material components is: tea salt 0.1-25%, tea polyphenols 0.01-1%, abrasive 20-50%, wetting agent 10-35%, surfactant 1-2%, thickening agent 0.5-1.5%, sweeting agent 0.01-1%, antiseptic 0.15-0.75%, essence 0.3-1.5%, water 20-40%; Tea salt be with tea and salt in proportion 1-10:20-1 mix, 900 ℃-1100 ℃ calcinings 22-26 hour, calcination process therebetween repeatedly eight times altogether; During the 9th calcining temperature is brought up to 1500-1600 ℃; Make salt fusing, will melt cooled salt block pulverizing, sieve tea salt.The tea salt toothpaste of this invention has caries prevention to tooth and periodontal tissue, and effects such as treatment gingivitis, periodontitis are to the human non-toxic side effect.Shortcoming is that process time is long, complicated condition, and is wayward.
The above-mentioned toothpaste of mentioning; Generally be utilize green tea etc. itself or bring into play the effect of anti-inflammation, prevention oral disease with the common effect of other plant composition; And do not see the report that Folium camelliae assamicae is used for its nursing health effect of toothpaste performance, and to trace it to its cause, key is that existing Folium camelliae assamicae extractive technique and 'Puer ' caffeine deep process technology level are low; Cause the extraction ratio of Folium camelliae assamicae low, and in toothpaste, be difficult for preserving.Folium camelliae assamicae contains abundant tea polyphenols, tea alkaloid, theasaponin, organic acid, vitamin and mineral; Have effects such as antioxidation, bactericidal antiphlogistic, promoting the production of body fluid to quench thirst, refreshment, refreshing and detoxicating; And Folium camelliae assamicae delicate fragrance is mellow, aftertaste is given birth to sweet; Liked by people from modern from ancient times; And the existence of foregoing problems makes this wide popular Folium Camelliae sinensis of Folium camelliae assamicae can't be applied to the articles for daily use that toothpaste follows people to live this every day, develop a kind ofly to have bactericidal antiphlogistic, refreshment, refreshing and detoxicating, whiten and very necessity of Folium camelliae assamicae toothpaste that numerous functions imitate such as steep.
Summary of the invention
The present invention is directed to above-mentioned prior art problem; A kind of Folium camelliae assamicae toothpaste is provided; Contain the Pu'er tea and the food stage adjuvant that extract according to method provided by the present invention in this toothpaste; Except that having the tooth protection that cleans one's teeth, removing the basic function of toothpaste such as halitosis and stain dirt, can also suppress that the Buccodental noxious bacteria grows, bactericidal antiphlogistic, particularly have and decompose cigarette stain residual in the teeth space, tobacco poisoning and recover taste bud, improve effects that other toothpaste does not possess such as the sense of taste.
For realizing above-mentioned purpose, the technical scheme that technical solution problem of the present invention is provided is following:
A kind of Folium camelliae assamicae toothpaste comprises Pu'er tea and food stage adjuvant.
Described Pu'er tea makes according to following method:
(1) gets puerh tea leaves, under cryogenic conditions, pulverize and grind to form tea powder and mince.
Said puerh tea leaves is preferably the ancient Camellia sinensis in Yunnan and shines QINGCHAYE.
Said low temperature is meant temperature≤25 ℃, preferably adopts cold water circulation, on the rocks or be that the cooling system of cold media is realized cryogenic conditions with liquid nitrogen, dry ice; Further preferably, said cold water circulating temperature scope is preferably 5-25 ℃, and said temperature range on the rocks is preferably 0-25 ℃, and said is that the cooling system temperature range of cold media is preferably-40-20 ℃ with liquid nitrogen, dry ice.Under cryogenic conditions, puerh tea leaves is pulverized grinding; Can broken Folium Camelliae sinensis cell and the biological activity effective ingredient in the Folium Camelliae sinensis is not destroyed; Can keep and discharge the bioactive ingredients in the puerh tea leaves to greatest extent again, keep the taste flavor of Folium camelliae assamicae simultaneously to greatest extent.
The size shape that said tea powder minces does not have special limitation; Preferred fineness is the 40-75 order, for example can be 40-60,41-55,45-56,47-62,50-70,54-73,58-65,59-75,40,42,44,46,51,53,57,64,66,68,69,71,74,75 orders; Further be preferably the 45-75 order; Most preferably be the 50-70 order.
In the tea powder that the pulverizing grinding obtains minces, contain a large amount of Plant fiber, not only can increase the denseness of lotion of toothpaste, can also improve the friction effect and the stability of toothpaste.
(2) under the room temperature tea powder of step (1) gained is minced and the water mix homogeneously, the ultrasound wave lixiviate, lixiviating solution.
Said room temperature is also referred to as general temperature or room temperature; It is the habitual saying of this area; Can be 10-30 ℃ of this wider temperature range in the present invention, for example can be 10 ℃, 13.5 ℃, 15 ℃, 16 ℃, 18 ℃, 20 ℃, 21 ℃, 22.6 ℃, 24 ℃, 27 ℃, 29.1 ℃, 30 ℃; Be preferably 15-25 ℃; Most preferably be 25 ℃.
Said lixiviate is meant transfers to the process in the suitable solvent with the DDGS in the medical material or in the plant; Be the technological means that those skilled in the art often use when extracting required effective ingredient, method commonly used has decocting method, percolation, steam distillation, circumfluence method, infusion process, supercritical extraction method and ultrasonic extraction etc.In the present invention, adopt the method for ultrasound wave lixiviate, " cavitation effect " and the mechanism of utilizing ultrasound wave in water, to produce; One side is fracturing cell walls effectively; Make the Folium camelliae assamicae effective ingredient be free state and dissolve in the water, can quicken the motion of hydrone on the other hand, make water contact fast with effective ingredient in the Folium camelliae assamicae; Fused each other, mixing, thus efficiently apace the effective ingredient of Folium camelliae assamicae is transferred in the lixiviating solution.
Said water is preferably distilled water, pure water or sterile deionized water.
Said tea powder mince with water preferably according to the mixed of parts by weight 1:100-200, for example can be 1:100,1:105,1:108,1:117,1:125,1:134,1:140,1:142,1:150,1:159,1:165,1:170,1:176,1:183,1:189:1:192,1:195,1:200; Be preferably 1:110-190; Further be preferably 1:120-180.
The time of said ultrasound wave lixiviate is preferably 10-40min, for example can be 10min, 11min, 12min, 15min, 17min, 20min, 25min, 26min, 28min, 30min, 33min, 34min, 35min, 39min, 40min; Further be preferably 15-30min; Most preferably be 20-25min.
The temperature of said ultrasound wave lixiviate is preferably 50-80 ℃, for example can be 50 ℃, 52 ℃, 55 ℃, 57 ℃, 60 ℃, 61 ℃, 64 ℃, 65 ℃, 68 ℃, 70 ℃, 73 ℃, 75 ℃, 76 ℃, 79 ℃, 80 ℃; Further be preferably 55-70 ℃; Most preferably be 60-70 ℃.
(3) lixiviating solution with step (2) gained is cooled to room temperature, and tea grounds is removed in filter pressing, stays extracting solution and centrifugal layering, shifts out centrifugal gained supernatant, and repeated centrifugation is operated to obtain spissated Pu'er tea.
Rapid temperature reduction way is preferably adopted in said cooling; Said rapid cooling is meant in the time of 30-60min and cools the temperature to room temperature, preferably in the time of 30-50min, cools the temperature to room temperature, most preferably in the time of 30-40min, cools the temperature to room temperature.Said rapid cooling can the cold wind through electric fan or air-conditioning be carried, cold water circulation or be that the cooling system of cold media is realized with liquid nitrogen, dry ice.
Said filter pressing is the common technology of this area, and those skilled in the art can select filter pressing equipment such as filter press, chamber-type press filter, belt filter press that tea grounds and extracting solution are separated through general knowledge and experience.
Said centrifugal rotation speed is preferably 4500-8000r/min, for example can be 4500r/min, 4600r/min, 4700r/min, 4850r/min, 5000r/min, 5200r/min, 5460r/min, 5700r/min, 6000r/min, 6100r/min, 6300r/min, 6500r/min, 6900r/min, 7000r/min, 7250r/min, 7500r/min, 7600r/min, 7740r/min, 7800r/min, 8000r/min; Further be preferably 5000-7500r/min, most preferably be 5000-7000r/min.
The said centrifugal time is preferably 5-25min, for example can be 5min, 6min, 7.5min, 9min, 12min, 14.5min, 16min, 18min, 20min; Further be preferably 10-20min; Most preferably be 10-15min.
Said repeated centrifugation is operated multiple number of times and is preferably 2-15 time, further is preferably 3-10 time, most preferably is 5-8 time.
Preferably, the moisture≤50wt% of the spissated Pu'er tea of gained for example can be 50wt%, 48wt%, 45wt%, 43wt%, 40wt%, 34wt%, 30wt%, 26wt%, 20wt%, 17wt%, 15wt%, 10wt%, 5wt%; Further be preferably≤45wt%; Most preferably be≤40wt%.Spissated Pu'er tea is fewer good for more with moisture, and so the extract concentrations of gained is high.The present invention adopts after the filter pressing repeatedly that centrifugation method obtains spissated Pu'er tea, has avoided a large amount of problems that reduce of volatile ingredient in the extract that method for concentration such as concentrating under reduced pressure bring, thereby has kept the active component in the Folium camelliae assamicae to greatest extent.
Preferably, Pu'er tea of the present invention makes according to the method for following optimization:
(1) get puerh tea leaves, under≤25 ℃ condition, pulverizing and grinding to form fineness is that 40-75 purpose tea powder minces;
(2) under 10-30 ℃ of temperature the tea powder of step (1) gained is minced even with water according to the mixed of parts by weight 1:100-200, ultrasound wave lixiviate 10-40min, extraction temperature 50-80 ℃, lixiviating solution;
(3) lixiviating solution with step (2) gained is cooled to 10-30 ℃ rapidly in 30-60min; Tea grounds is removed in filter pressing; The extracting solution that stays is centrifugal 5-25min under the condition of 4500-8000r/min at revolution; Shift out centrifugal gained supernatant, repeated centrifugation is operated 2-15 time, obtains the Pu'er tea of moisture≤50wt%.
Further preferably, Pu'er tea of the present invention makes according to the following method of further optimizing:
(1) gets puerh tea leaves, in cold water circulation, on the rocks or be to pulverize in the cooling system of cold media that to grind to form fineness be that 45-75 purpose tea powder minces with liquid nitrogen, dry ice;
(2) under 15-25 ℃ of temperature the tea powder of step (1) gained is minced even with water according to the mixed of parts by weight 1:110-190, ultrasound wave lixiviate 15-30min, extraction temperature 55-70 ℃, lixiviating solution;
(3) lixiviating solution with step (2) gained is cooled to 15-25 ℃ rapidly in 30-50min; Tea grounds is removed in filter pressing; The extracting solution that stays is centrifugal 10-20min under the condition of 5000-7500r/min at revolution; Shift out centrifugal gained supernatant, repeated centrifugation is operated 3-10 time, obtains the Pu'er tea of moisture≤45wt%.
More preferably, Pu'er tea of the present invention makes according to following optimized method:
(1) gets puerh tea leaves, in cold water circulation, on the rocks or be to pulverize in the cooling system of cold media that to grind to form fineness be that 50-70 purpose tea powder minces with liquid nitrogen, dry ice;
It is even according to the mixed of parts by weight 1:120-180 with distilled water under (2) 25 ℃ of temperature the tea powder of step (1) gained to be minced, ultrasound wave lixiviate 20-25min, extraction temperature 60-70 ℃, lixiviating solution;
(3) lixiviating solution with step (2) gained is cooled to 25 ℃ rapidly in 30-40min; Tea grounds is removed in filter pressing; The extracting solution that stays is centrifugal 10-15min under the condition of 5000-7000r/min at revolution; Shift out centrifugal gained supernatant, repeated centrifugation is operated 5-8 time, obtains the Pu'er tea of moisture≤40wt%.
Through measuring, contain main component tea polyphenols 45.6wt%, tea alkaloid 14.2wt%, organic acid 10.7wt%, tea polysaccharide 19.1wt% and vitamin C and tea fluorine trace in the Pu'er tea of the present invention (butt), surplus is a moisture.
The quality percentage composition of described Pu'er tea in Folium camelliae assamicae toothpaste of the present invention is preferably 0.5-10wt%, for example can be 0.5wt%, 1wt%, 1.6wt%, 2wt%, 2.4wt%, 3.5wt%, 4.2wt%, 4.7wt%, 5wt%, 6.2wt%, 7.8wt%, 8wt%, 9.1wt%, 10wt%; Further be preferably 1-5wt%.
The method of above-mentioned acquisition Pu'er tea provided by the invention; Pulverizing the whole process of grinding puerh tea leaves all carries out under cryogenic conditions; Can broken Folium Camelliae sinensis cell and do not destroy the biological activity effective ingredient in the Folium Camelliae sinensis; Therefore can keep and discharge the bioactive ingredients in the puerh tea leaves to greatest extent, keep the taste flavor of Folium camelliae assamicae simultaneously.Through the step of lixiviate and filter pressing, filtering compositions such as Folium Camelliae sinensis fiber, high molecular weight protein, saccharide and pectin, and biological activity effective ingredient such as tea polyphenols, tea alkaloid, organic acid, vitamin and mineral element are remained to greatest extent.These biological activity effective ingredient have numerous effects such as antioxidation, bactericidal antiphlogistic, promoting the production of body fluid to quench thirst, refreshment, refreshing and detoxicating.Folium camelliae assamicae delicate fragrance is mellow, aftertaste is living sweet, and its concentrated extract adds the natural effect that can play the raising sense of taste, improve mouthfeel in toothpaste.Again because antibacterial, detoxifcation, the antisepsis of Folium camelliae assamicae itself just do not need to add other chemical preservatives in its concentrated extract adding toothpaste again, perhaps also can with other food grade preservative synergism upgrading potentiation.In addition, also contain abundant natural fluorine in the Folium camelliae assamicae, its concentrated extract adds the effect that has significant enhancing tooth enamel and prevent to decay tooth in the toothpaste, effectively caries prevention.
Described food stage adjuvant comprises glycerol, sorbitol, PEG400, tetrasodium pyrophosphate, sodium dihydrogen phosphate, sodium phytate, sodium carboxymethyl cellulose, xanthan gum, sodium lauryl sulfate, calcium hydrogen phosphate two water things, hydration Silicon stone, essence etc.
Said glycerol is sweeting agent and wetting agent commonly used in the food processing industry, after absorption of human body, can not change blood glucose and insulin level, is used in the Folium camelliae assamicae toothpaste of the present invention and can produce any harm to human body, and can keep the good mouthfeel of toothpaste.Preferred biological elite glycerol, it also contains reducing sugar such as esters, glucose except that containing glycerin, belong to polyalcohols glycerol; Have preserve moisture, special efficacies such as humectation, antioxidation, short alcoholization.The quality percentage composition of said glycerol in Folium camelliae assamicae toothpaste of the present invention is preferably 3-15wt%, for example can be 3wt%, 4.5wt%, 5.2wt%, 6wt%, 6.5wt%, 7wt%, 7.6wt%, 8.4wt%, 9wt%, 9.7wt%, 10wt%, 11wt%, 12.3wt%, 14wt%, 15wt%; Further be preferably 5-10wt%.
Said sorbitol in industries such as food, daily use chemicals, medicine extensively as uses such as sweeting agent, wetting agent, excipient, antiseptic; Have effects such as low heat value, low sugar, anti-caries; Be used in the Folium camelliae assamicae toothpaste of the present invention and can not produce any harm to human body, decapacitation keeps the low-yield and anti-caries of toothpaste low sugar etc., and its hygroscopicity can prevent that toothpaste is dry and cracked; Its low sugariness is not utilized bacteria breed, and it does not contain aldehyde radical and is difficult for oxidized thereby has the effect that extends the shelf life.The quality percentage composition of said sorbitol in Folium camelliae assamicae toothpaste of the present invention is preferably 15-30wt%, for example can be 15wt%, 16.5wt%, 17.4wt%, 18wt%, 19.2wt%, 20wt%, 21wt%, 23.6wt%, 24wt%, 27.5wt%, 28wt%, 29wt%, 30wt%; Further be preferably 20-25wt%.
Said PEG400 (PEG400) has the extensive compatibility with all kinds of solvents; Be good solvent and solubilizing agent; Its quality percentage composition in Folium camelliae assamicae toothpaste of the present invention is preferably 1-10wt%, for example can be 1wt%, 2.5wt%, 3wt%, 4.2wt%, 5.7wt%, 6wt%, 7.5wt%, 8wt%, 9.3wt%, 10wt%; Further be preferably 2-5wt%.
Said tetrasodium pyrophosphate is claimed tetrasodium phosphate, anhydrous sodium pyrophosphate again, in Folium camelliae assamicae toothpaste of the present invention, can form colloid with another adjuvant calcium hydrogen phosphate two water things among the present invention and play Stabilization.The quality percentage composition of said tetrasodium pyrophosphate in Folium camelliae assamicae toothpaste of the present invention is preferably 0.1-0.5wt%, for example can be 0.1wt%, 0.15wt%, 0.17wt%, 0.21wt%, 0.25wt%, 0.26wt%, 0.32wt%, 0.35wt%, 0.4wt%, 0.43wt%, 0.45wt%, 0.49wt%, 0.5wt%; Further be preferably 0.2-0.3wt%.
Said sodium dihydrogen phosphate has in Folium camelliae assamicae toothpaste of the present invention increases effects such as dissolubility acid, that replenish phosphorus content and increase calcium; Its quality percentage composition in Folium camelliae assamicae toothpaste of the present invention is preferably 0.05-0.5wt%, for example can be 0.05wt%, 0.08wt%, 0.11wt%, 0.15wt%, 0.16wt%, 0.22wt%, 0.25wt%, 0.3wt%, 0.34wt%, 0.37wt%, 0.4wt%, 0.45wt%, 0.49wt%, 0.5wt%; Further be preferably 0.1-0.2wt%.
Said sodium phytate is claimed sodium phytate again; It is a kind of important fully natural green additive; With metal ion extremely strong sequestration effect is arranged; And have stronger non-oxidizability and color fixative property, be used in the Folium camelliae assamicae toothpaste of the present invention and can not produce any harm, even and effect with the blackout phenomenon that also can not occur after keeping toothpaste repeatedly to be exposed in the air turning to be yellow to human body.The quality percentage composition of said sodium phytate in Folium camelliae assamicae toothpaste of the present invention is preferably 0.2-2wt%, for example can be 0.2wt%, 0.25wt%, 0.3wt%, 0.4wt%, 0.55wt%, 0.69wt%, 0.73wt%, 0.8wt%, 0.91wt%, 1.05wt%, 1.2wt%, 1.34wt%, 1.5wt%, 1.68wt%, 1.7wt%, 1.8wt%, 1.9wt%, 2wt%; Further be preferably 0.5-1wt%.
Said sodium carboxymethyl cellulose is claimed sanlose, carboxymethyl cellulose, CMC again;, thickening bonding because of having, enhancing, emulsifying, water conservation, suspension etc. extensively effect become the maximum cellulose family of consumption in the world, are used in the Folium camelliae assamicae toothpaste of the present invention mainly as thickening agent.The quality percentage composition of said sodium carboxymethyl cellulose in Folium camelliae assamicae toothpaste of the present invention is preferably 0.5-1.5wt%, for example can be 0.5wt%, 0.65wt%, 0.7wt%, 0.82wt%, 0.9wt%, 1wt%, 1.1wt%, 1.25wt%, 1.3wt%, 1.44wt%, 1.5wt%; Further be preferably 0.6-0.8wt%.
Said xanthan gum is claimed HUANGJIAO, HANSHENGJIAO again; Yellow unit cell polysaccharide; It is the biogum that the best performance that integrates thickening, suspension, emulsifying, be stable at is got over; Be used in the Folium camelliae assamicae toothpaste of the present invention and play thickening, be easy to the lotion of toothpaste molding, improve toothpaste and attach the brush performance, increase sophistication, improve aesthetic quality, enhanced stability, the effect that extends the shelf life.The quality percentage composition of said xanthan gum in Folium camelliae assamicae toothpaste of the present invention is preferably 0.2-0.6wt%, for example can be 0.2wt%, 0.25wt%, 0.32wt%, 0.35wt%, 0.4wt%, 0.45wt%, 0.48wt%, 0.56wt%, 0.57wt%, 0.6wt%; Further be preferably 0.3-0.5wt%.
Said sodium lauryl sulfate has washing, emulsifying, moistening, help dye, effect such as diffusion, be used in the Folium camelliae assamicae toothpaste of the present invention mainly as foaming agent.The quality percentage composition of said sodium lauryl sulfate in Folium camelliae assamicae toothpaste of the present invention is preferably 1.5-2.5wt%, for example can be 1.5wt%, 1.6wt%, 1.78wt%, 1.8wt%, 1.95wt%, 2wt%, 2.05wt%, 2.1wt%, 2.14wt%, 2.2wt%, 2.25wt%, 2.27wt%, 2.33wt%, 2.39wt%, 2.4wt%, 2.45wt%, 2.5wt%; Further be preferably 2-2.3wt%.
Said calcium hydrogen phosphate two water things are claimed dicalcium phosphate, precipitated calcium phosphate, calcium hydrogen phosphate again, and are long as replenishing the calcium hardening agent, bulking agent, filler, stabilizing agent etc., are used in the Folium camelliae assamicae toothpaste of the present invention mainly as abrasivus.The quality percentage composition of said calcium hydrogen phosphate two water things in Folium camelliae assamicae toothpaste of the present invention is preferably 15-30wt%, for example can be 15wt%, 16wt%, 17.1wt%, 18.5wt%, 19wt%, 22wt%, 23.4wt%, 24wt%, 24.5wt%, 26wt%, 27wt%, 28wt%, 29.6wt%; Further be preferably 20-25wt%.
Said hydration Silicon stone is a hydrated SiO 2; A kind of for white carbon; Be used in the Folium camelliae assamicae toothpaste of the present invention as filler and abradant, can make that lotion of toothpaste is smooth, soft, abrasion is not well denuded toothpaste tube body again, keep the stability of other compositions such as Pu'er tea in the toothpaste; Also excellent compatibility is arranged, avoided calcium salt to make the drawback that abrasive material produces difficulty soluble salt simultaneously with fluoride.The quality percentage composition of said hydration Silicon stone in Folium camelliae assamicae toothpaste of the present invention is preferably 5-15wt%, for example can be 5wt%, 6.5wt%, 7.4wt%, 8.9wt%, 9wt%, 9.7wt%, 10.5wt%, 11wt%, 12.6wt%, 13wt%, 14.5wt%, 15wt%; Further be preferably 8-10wt%.
Said essence is by the imitation fruit of synthetic and the concentrated aromatic oil of natural perfume material abnormal smells from the patient; Used essence is edible essence among the present invention; Be used in the Folium camelliae assamicae toothpaste of the present invention and mainly play the effect that improves mouthfeel; Those skilled in the art can be under the prerequisite that does not break away from spirit of the present invention, and the hobby that reaches different crowd as required makes a choice to it easily.The quality percentage composition of said essence in Folium camelliae assamicae toothpaste of the present invention is preferably 0.5-2wt%, for example can be 0.5wt%, 0.6wt%, 0.71wt%, 0.83wt%, 0.9wt%, 1.05wt%, 1.1wt%, 1.26wt%, 1.38wt%, 1.4wt%, 1.5wt%, 1.67wt%, 1.75wt%, 1.8wt%, 1.9wt%, 2wt%.Further be preferably 1-1.2wt%.
Further, can also comprise xylitol, saccharin sodium, tranexamic acid, sodium benzoate etc. in the food stage adjuvant of the present invention.
Said xylitol is used for Folium camelliae assamicae toothpaste of the present invention, mainly as the sweeting agent existence of low heat value, low sugar, plays the effect that recovers taste bud, improves the sense of taste.Its quality percentage composition in Folium camelliae assamicae toothpaste of the present invention is preferably 1-8wt%, for example can be 1wt%, 1.5wt%, 2.4wt%, 3wt%, 3.6wt%, 4wt%, 4.5wt%, 5.2wt%, 6wt%, 6.5wt%, 7wt%, 7.3wt%, 7.5wt%, 8wt%; Further be preferably 2-5wt%.
Said saccharin sodium chemical name is a benzoic sulfimide sodium, and the sugariness of its glucide is 300-500 a times of sucrose, is used for Folium camelliae assamicae toothpaste of the present invention mainly as sweeting agent.The quality percentage composition of said saccharin sodium in Folium camelliae assamicae toothpaste of the present invention is preferably 0.1-0.5wt%, for example can be 0.1wt%, 0.15wt%, 0.22wt%, 0.25wt%, 0.28wt%, 0.31wt%, 0.35wt%, 0.39wt%, 0.4wt%, 0.44wt%, 0.45wt%, 0.47wt%, 0.5wt%; Further be preferably 0.2-0.3wt%.
Said tranexamic acid chemical name is to aminomethyl naphthenic acid, trans-4-aminomethyl-naphthenic acid, has significant anastalsis and white-skinned face function, is used for Folium camelliae assamicae toothpaste of the present invention and can effectively removes the stain dirt and prevent and treat gingiva bleeding gingival hemorrhage.The quality percentage composition of said tranexamic acid in Folium camelliae assamicae toothpaste of the present invention is preferably 0.02-0.2wt%, for example can be 0.02wt%, 0.03wt%, 0.04wt%, 0.07wt%, 0.08wt%, 0.12wt%, 0.13wt%, 0.15wt%, 0.16wt%, 0.19wt%, 0.2wt%; Further be preferably 0.05-0.1wt%.
Said sodium benzoate has stronger inhibitory action for yeast and antibacterial; In Folium camelliae assamicae toothpaste of the present invention mainly as antiseptic; Its quality percentage composition in Folium camelliae assamicae toothpaste of the present invention is preferably 0.05-0.3wt%, for example can be 0.05wt%, 0.08wt%, 0.11wt%, 0.15wt%, 0.17wt%, 0.18wt%, 0.22wt%, 0.25wt%, 0.26wt%, 0.29wt%, 0.3wt%; Further be preferably 0.1-0.2wt%.
In sum; The present invention provides a kind of Folium camelliae assamicae toothpaste, and it comprises following component according to the quality percentage composition: glycerol 3-15wt%, sorbitol 15-30wt%, PEG4001-10wt%, tetrasodium pyrophosphate 0.1-0.5wt%, sodium dihydrogen phosphate 0.05-0.5wt%, sodium phytate 0.2-2wt%, sodium carboxymethyl cellulose 0.5-1.5wt%, xanthan gum 0.2-0.6wt%, sodium lauryl sulfate 1.5-2.5wt%, calcium hydrogen phosphate two water thing 15-30wt%, hydration Silicon stone 5-15wt%, essence 0.5-2wt%, Pu'er tea 0.5-10wt% and balance of deionized water.
As an optional technical scheme; The present invention provides a kind of the have taste bud of recovery, the raising sense of taste; Make the user more sapid tooth protection effect type Folium camelliae assamicae toothpaste that cleans one's teeth of eating, it comprises following component according to the quality percentage composition: glycerol 3-15wt%, sorbitol 15-30wt%, PEG4001-10wt%, tetrasodium pyrophosphate 0.1-0.5wt%, sodium dihydrogen phosphate 0.05-0.5wt%, sodium phytate 0.2-2wt%, sodium carboxymethyl cellulose 0.5-1.5wt%, xanthan gum 0.2-0.6wt%, sodium lauryl sulfate 1.5-2.5wt%, calcium hydrogen phosphate two water thing 15-30wt%, hydration Silicon stone 5-15wt%, essence 0.5-2wt%, xylitol 1-8wt%, Pu'er tea 0.5-10wt% and balance of deionized water.
As an optional technical scheme; The present invention provides a kind of stain of removal dirt that has; Decompose cigarette stain, tobacco poisoning residual in the teeth space; The auxiliary tooth protection effect type that the cleans one's teeth Folium camelliae assamicae toothpaste that suppresses Buccodental noxious bacteria, reparation or prevention Buccodental disease problem, it comprises following component according to the quality percentage composition: glycerol 3-15wt%, sorbitol 15-30wt%, PEG4001-10wt%, tetrasodium pyrophosphate 0.1-0.5wt%, sodium dihydrogen phosphate 0.05-0.5wt%, sodium phytate 0.2-2wt%, sodium carboxymethyl cellulose 0.5-1.5wt%, xanthan gum 0.2-0.6wt%, sodium lauryl sulfate 1.5-2.5wt%, calcium hydrogen phosphate two water thing 15-30wt%, hydration Silicon stone 5-15wt%, essence 0.5-2wt%, saccharin sodium 0.1-0.5wt%, tranexamic acid 0.02-0.2wt%, sodium benzoate 0.05-0.3wt%, Pu'er tea 0.5-10wt% and balance of deionized water.
Technical scheme after the optimization of the present invention is:
A kind of Folium camelliae assamicae toothpaste, it comprises following component according to the quality percentage composition: glycerol 5-10wt%, sorbitol 20-25wt%, PEG4002-5wt%, tetrasodium pyrophosphate 0.2-0.3wt%, sodium dihydrogen phosphate 0.1-0.2wt%, sodium phytate 0.5-1wt%, sodium carboxymethyl cellulose 0.6-0.8wt%, xanthan gum 0.3-0.5wt%, sodium lauryl sulfate 2-2.3wt%, calcium hydrogen phosphate two water thing 20-25wt%, hydration Silicon stone 8-10wt%, essence 1-1.2wt%, Pu'er tea 1-5wt% and balance of deionized water.
As optimizing a back optional technical scheme: the present invention provides a kind of the have taste bud of recovery, the raising sense of taste; Make the user more sapid tooth protection effect type Folium camelliae assamicae toothpaste that cleans one's teeth of eating, it comprises following component according to the quality percentage composition: glycerol 5-10wt%, sorbitol 20-25wt%, PEG4002-5wt%, tetrasodium pyrophosphate 0.2-0.3wt%, sodium dihydrogen phosphate 0.1-0.2wt%, sodium phytate 0.5-1wt%, sodium carboxymethyl cellulose 0.6-0.8wt%, xanthan gum 0.3-0.5wt%, sodium lauryl sulfate 2-2.3wt%, calcium hydrogen phosphate two water thing 20-25wt%, hydration Silicon stone 8-10wt%, essence 1-1.2wt%, xylitol 2-5wt%, Pu'er tea 1-5wt% and balance of deionized water.
As optimizing a back optional technical scheme; The present invention provides a kind of stain of removal dirt that has; Decompose cigarette stain, tobacco poisoning residual in the teeth space; The auxiliary tooth protection effect type that the cleans one's teeth Folium camelliae assamicae toothpaste that suppresses Buccodental noxious bacteria, reparation or prevention Buccodental disease problem, it comprises following component according to the quality percentage composition: glycerol 5-10wt%, sorbitol 20-25wt%, PEG4002-5wt%, tetrasodium pyrophosphate 0.2-0.3wt%, sodium dihydrogen phosphate 0.1-0.2wt%, sodium phytate 0.5-1wt%, sodium carboxymethyl cellulose 0.6-0.8wt%, xanthan gum 0.3-0.5wt%, sodium lauryl sulfate 2-2.3wt%, calcium hydrogen phosphate two water thing 20-25wt%, hydration Silicon stone 8-10wt%, essence 1-1.2wt%, saccharin sodium 0.2-0.3wt%, tranexamic acid 0.05-0.1wt%, sodium benzoate 0.1-0.2wt%, Pu'er tea 1-5wt% and balance of deionized water.
Folium camelliae assamicae toothpaste of the present invention; Its preparation method there is not specific (special) requirements; After obtaining Pu'er tea; Those skilled in the art select this area means commonly used with Pu'er tea and other adjuvants and water fully stirs, behind the uniform mixing, through homogenizing, emulsifying, sterilization, the multiple tube vacuum filling, pack and get final product according to general knowledge and experience.
" comprising " of the present invention, mean it except that said component, can also contain other components, these other components are given said Folium camelliae assamicae toothpaste with different characteristic.In addition, " comprising " of the present invention, can also replace with enclosed " being " or " by ... process ".No matter which kind of composition Folium camelliae assamicae of the present invention comprises, the percentage by weight sum of said Folium camelliae assamicae toothpaste is 100%.
All be appreciated that the modification that adds term " about " in all cases at these used all expression technological parameters that in description and claims, use, constituent content, reaction condition etc.Therefore, only if point out on the contrary, the character that given numerical value can hope according to the present invention to obtain in following description and claims different and changing.At bottom line, and be not used in the scope that the application of equivalent principle is defined as claim, the value that each numerical value all should be accordinged to the significant digits of being reported at least makes an explanation through using common rounding method.And all scopes in this announcement all are appreciated that starting point and the end point values that comprises scope, comprise arbitrarily and all are included in wherein among a small circle.For example, certain scope " 1-10 " should be considered to comprise any of (being included) between minima 1 and the maximum 10 with all among a small circle; Promptly all are initial with the minima more than or equal to 1, and be less than or equal to that 10 maximum finishes all among a small circle, 5-10 for example, 3.3-6.7, or 1.5-8.8, these also only mention seldom several examples.All lists of references of in this file, being mentioned all are appreciated that all to include and are used for reference.
The present invention at first provides a kind of extraction process of effective component of Folium camelliae assamicae efficiently; Be through pulverize at low temperature, ultrasound wave lixiviate, filter pressing, separation, technology such as concentrate and obtain Pu'er tea; Be that raw material is processed Folium camelliae assamicae toothpaste with this Pu'er tea and health, safety, environmental protection, numerous food level adjuvant that human body is not had a potential safety hazard then; Eliminated fundamentally that tea toothpaste is putrid and deteriorated, variable color is spoiled and quality problems such as chemical industry safety, the quality guarantee period of having improved tea toothpaste effectively.The present invention prescription has demonstrated fully the characteristic of main ingredient collocation complementation, upgrading potentiation, nursing health, and it is limpid even that the Folium camelliae assamicae toothpaste that provides has color and luster, free from admixture; Fine and smooth nice and cool, the simple and elegant mellow characteristics of Folium camelliae assamicae fragrance of foam except that the basic function with toothpaste such as cleaning teeth, nursing oral cavities, also have the stain of removal dirt; Decompose cigarette stain residual in the teeth space, tea stain, coffee stain; Reduce bacterial plaque, prevent that noxious bacteria from growing, bactericidal antiphlogistic, flavor, the profit of the promoting the production of body fluid mouth of dispelling stops blooding; Recover taste bud, improve the sense of taste, make the user numerous special effects such as more flavoursome of eating; Be a kind of Folium Camelliae sinensis toothpaste of natural health,, have extremely wide application prospect in conjunction with China's resourceful advantage of Yunnan area Folium camelliae assamicae particularly.
Down in the face of further explain of the present invention.But following instance only is a simple and easy example of the present invention, does not represent or limits rights protection scope of the present invention, and interest field of the present invention is as the criterion with claims.
The specific embodiment
For the present invention is described better, be convenient to understand technical scheme of the present invention, typical case of the present invention but non-restrictive example is following:
Embodiment 1:
Prepare Pu'er tea according to following method:
(1) get puerh tea leaves 1kg, under the condition of cold water circulation (temperature range 5-25 ℃), pulverizing and grinding to form fineness is that 50-60 purpose tea powder minces;
Tea powder with step (1) gained under (2) 25 ℃ of temperature minces and 150kg distilled water mix homogeneously, ultrasound wave lixiviate 20min, 70 ℃ of extraction temperatures, lixiviating solution;
(3) lixiviating solution with step (2) gained is cooled to 25 ℃ rapidly in 30min; Tea grounds is removed in filter pressing; The extracting solution that stays is centrifugal 15min under the condition of 5000r/min at revolution; Shift out centrifugal gained supernatant, repeated centrifugation operation 5 times obtains the Pu'er tea that moisture is 30wt%.
Embodiment 2:
(1) get puerh tea leaves 1kg, under the condition of (temperature range 0-25 ℃) on the rocks, pulverizing and grinding to form fineness is that 55-70 purpose tea powder minces;
Tea powder with step (1) gained under (2) 20 ℃ of temperature minces and 120kg pure water mix homogeneously, ultrasound wave lixiviate 25min, 60 ℃ of extraction temperatures, lixiviating solution;
(3) lixiviating solution with step (2) gained is cooled to 20 ℃ rapidly in 40min; Tea grounds is removed in filter pressing; The extracting solution that stays is centrifugal 10min under the condition of 7000r/min at revolution; Shift out centrifugal gained supernatant, repeated centrifugation operation 8 times obtains the Pu'er tea that moisture is 35wt%.
Embodiment 3:
(1) get puerh tea leaves 1kg, in the cooling system that with the liquid nitrogen is cold media (temperature range-40-20 ℃) to pulverize and to grind to form fineness be that 45-65 purpose tea powder minces;
Tea powder with step (1) gained under (2) 15 ℃ of temperature minces and 180kg deionized water mix homogeneously, ultrasound wave lixiviate 15min, 55 ℃ of extraction temperatures, lixiviating solution;
(3) lixiviating solution with step (2) gained is cooled to 15 ℃ rapidly in 50min; Tea grounds is removed in filter pressing; The extracting solution that stays is centrifugal 20min under the condition of 7500r/min at revolution; Shift out centrifugal gained supernatant, repeated centrifugation operation 10 times obtains the Pu'er tea that moisture is 40wt%.
Embodiment 4:
Prepare Pu'er tea according to following method:
(1) get puerh tea leaves 1kg, in the cooling system that with dry ice is cold media (temperature range-40-20 ℃) to pulverize and to grind to form fineness be that 40-70 purpose tea powder minces;
Tea powder with step (1) gained under (2) 30 ℃ of temperature minces and 100kg distilled water mix homogeneously, ultrasound wave lixiviate 30min, 80 ℃ of extraction temperatures, lixiviating solution;
(3) lixiviating solution with step (2) gained is cooled to 30 ℃ rapidly in 60min; Tea grounds is removed in filter pressing; The extracting solution that stays is centrifugal 25min under the condition of 4500r/min at revolution; Shift out centrifugal gained supernatant, repeated centrifugation operation 3 times obtains the Pu'er tea that moisture is 45wt%.
Embodiment 5:
Prepare Pu'er tea according to following method:
(1) get puerh tea leaves 1kg, under the condition of cold water circulation (temperature range 5-25 ℃), pulverizing and grinding to form fineness is that 50-75 purpose tea powder minces;
Tea powder with step (1) gained under (2) 10 ℃ of temperature minces and 200kg pure water mix homogeneously, ultrasound wave lixiviate 40min, 50 ℃ of extraction temperatures, lixiviating solution;
(3) lixiviating solution with step (2) gained is cooled to 10 ℃ rapidly in 45min; Tea grounds is removed in filter pressing; The extracting solution that stays is centrifugal 5min under the condition of 8000r/min at revolution; Shift out centrifugal gained supernatant, repeated centrifugation operation 15 times obtains the Pu'er tea that moisture is 46wt%.
Embodiment 6:
A kind of have recover taste bud, improve the sense of taste, make the user more sapid tooth protection effect type Folium camelliae assamicae toothpaste that cleans one's teeth of eating, it comprises following component according to the quality percentage composition:
Pu'er tea 2wt% and the balance of deionized water of glycerol 6wt%, sorbitol 24wt%, PEG4003wt%, tetrasodium pyrophosphate 0.3wt%, sodium dihydrogen phosphate 0.2wt%, sodium phytate 0.9wt%, sodium carboxymethyl cellulose 0.7wt%, xanthan gum 0.5wt%, sodium lauryl sulfate 2.3wt%, calcium hydrogen phosphate two water thing 21wt%, hydration Silicon stone 8wt%, essence 1wt%, xylitol 2wt%, embodiment 1.
Embodiment 7
A kind of have recover taste bud, improve the sense of taste, make the user more sapid tooth protection effect type Folium camelliae assamicae toothpaste that cleans one's teeth of eating, it comprises following component according to the quality percentage composition:
Pu'er tea 4wt% and the balance of deionized water of glycerol 8wt%, sorbitol 20wt%, PEG4002wt%, tetrasodium pyrophosphate 0.2wt%, sodium dihydrogen phosphate 0.1wt%, sodium phytate 0.6wt%, sodium carboxymethyl cellulose 0.6wt%, xanthan gum 0.4wt%, sodium lauryl sulfate 2wt%, calcium hydrogen phosphate two water thing 20wt%, hydration Silicon stone 9wt%, essence 1.1wt%, xylitol 3wt%, embodiment 2.
Embodiment 8:
A kind of have recover taste bud, improve the sense of taste, make the user more sapid tooth protection effect type Folium camelliae assamicae toothpaste that cleans one's teeth of eating, it comprises following component according to the quality percentage composition:
Pu'er tea 1wt% and the balance of deionized water of glycerol 5wt%, sorbitol 20wt%, PEG4002wt%, tetrasodium pyrophosphate 0.25wt%, sodium dihydrogen phosphate 0.15wt%, sodium phytate 0.5wt%, sodium carboxymethyl cellulose 0.6wt%, xanthan gum 0.3wt%, sodium lauryl sulfate 2.1wt%, calcium hydrogen phosphate two water thing 20wt%, hydration Silicon stone 9wt%, essence 1.1wt%, xylitol 2wt%, embodiment 3.
Embodiment 9
A kind of have recover taste bud, improve the sense of taste, make the user more sapid tooth protection effect type Folium camelliae assamicae toothpaste that cleans one's teeth of eating, it comprises following component according to the quality percentage composition:
Pu'er tea 5wt% and the balance of deionized water of glycerol 10wt%, sorbitol 25wt%, PEG4005wt%, tetrasodium pyrophosphate 0.28wt%, sodium dihydrogen phosphate 0.16wt%, sodium phytate 1wt%, sodium carboxymethyl cellulose 0.8wt%, xanthan gum 0.5wt%, sodium lauryl sulfate 2.2wt%, calcium hydrogen phosphate two water thing 25wt%, hydration Silicon stone 8.5wt%, essence 1.2wt%, xylitol 5wt%, embodiment 4.
Embodiment 10
A kind of have recover taste bud, improve the sense of taste, make the user more sapid tooth protection effect type Folium camelliae assamicae toothpaste that cleans one's teeth of eating, it comprises following component according to the quality percentage composition:
Pu'er tea 0.5wt% and the balance of deionized water of glycerol 15wt%, sorbitol 30wt%, PEG4001wt%, tetrasodium pyrophosphate 0.1wt%, sodium dihydrogen phosphate 0.05wt%, sodium phytate 0.2wt%, sodium carboxymethyl cellulose 0.5wt%, xanthan gum 0.2wt%, sodium lauryl sulfate 1.5wt%, calcium hydrogen phosphate two water thing 15wt%, hydration Silicon stone 5wt%, essence 0.5wt%, xylitol 1wt%, embodiment 5.
Embodiment 11
A kind of have recover taste bud, improve the sense of taste, make the user more sapid tooth protection effect type Folium camelliae assamicae toothpaste that cleans one's teeth of eating, it comprises following component according to the quality percentage composition:
Pu'er tea 10wt% and the balance of deionized water of glycerol 3wt%, sorbitol 15wt%, PEG40010wt%, tetrasodium pyrophosphate 0.5wt%, sodium dihydrogen phosphate 0.5wt%, sodium phytate 2wt%, sodium carboxymethyl cellulose 1.5wt%, xanthan gum 0.6wt%, sodium lauryl sulfate 2.5wt%, calcium hydrogen phosphate two water thing 30wt%, hydration Silicon stone 15wt%, essence 2wt%, xylitol 8wt%, embodiment 1.
Embodiment 12
A kind of have remove the stain dirt, decompose cigarette stain, tobacco poisoning residual in the teeth space, the auxiliary tooth protection effect type that the cleans one's teeth Folium camelliae assamicae toothpaste that suppresses Buccodental noxious bacteria, reparation or prevention Buccodental disease problem, it comprises following component according to the quality percentage composition:
Pu'er tea 1wt% and the balance of deionized water of glycerol 5wt%, sorbitol 25wt%, PEG4005wt%, tetrasodium pyrophosphate 0.3wt%, sodium dihydrogen phosphate 0.2wt%, sodium phytate 0.5wt%, sodium carboxymethyl cellulose 0.6wt%, xanthan gum 0.5wt%, sodium lauryl sulfate 2wt%, calcium hydrogen phosphate two water thing 20wt%, hydration Silicon stone 8wt%, essence 1wt%, saccharin sodium 0.2wt%, tranexamic acid 0.1wt%, sodium benzoate 0.1wt%, embodiment 2.
Embodiment 13
A kind of have remove the stain dirt, decompose cigarette stain, tobacco poisoning residual in the teeth space, the auxiliary tooth protection effect type that the cleans one's teeth Folium camelliae assamicae toothpaste that suppresses Buccodental noxious bacteria, reparation or prevention Buccodental disease problem, it comprises following component according to the quality percentage composition:
Pu'er tea 5wt% and the balance of deionized water of glycerol 8wt%, sorbitol 20wt%, PEG4002wt%, tetrasodium pyrophosphate 0.2wt%, sodium dihydrogen phosphate 0.1wt%, sodium phytate 1wt%, sodium carboxymethyl cellulose 0.8wt%, xanthan gum 0.3wt%, sodium lauryl sulfate 2.3wt%, calcium hydrogen phosphate two water thing 25wt%, hydration Silicon stone 10wt%, essence 1.2wt%, saccharin sodium 0.3wt%, tranexamic acid 0.05wt%, sodium benzoate 0.2wt%, embodiment 3.
Embodiment 14
A kind of have remove the stain dirt, decompose cigarette stain, tobacco poisoning residual in the teeth space, the auxiliary tooth protection effect type that the cleans one's teeth Folium camelliae assamicae toothpaste that suppresses Buccodental noxious bacteria, reparation or prevention Buccodental disease problem, it comprises following component according to the quality percentage composition:
Pu'er tea 0.5wt% and the balance of deionized water of glycerol 15wt%, sorbitol 30wt%, PEG40010wt%, tetrasodium pyrophosphate 0.1wt%, sodium dihydrogen phosphate 0.5wt%, sodium phytate 0.2wt%, sodium carboxymethyl cellulose 0.5wt%, xanthan gum 0.2wt%, sodium lauryl sulfate 2.5wt%, calcium hydrogen phosphate two water thing 15wt%, hydration Silicon stone 5wt%, essence 2wt%, saccharin sodium 0.5wt%, tranexamic acid 0.2wt%, sodium benzoate 0.05wt%, embodiment 4.
Embodiment 15
A kind of have remove the stain dirt, decompose cigarette stain, tobacco poisoning residual in the teeth space, the auxiliary tooth protection effect type that the cleans one's teeth Folium camelliae assamicae toothpaste that suppresses Buccodental noxious bacteria, reparation or prevention Buccodental disease problem, it comprises following component according to the quality percentage composition:
Pu'er tea 10wt% and the balance of deionized water of glycerol 3wt%, sorbitol 15wt%, PEG4001wt%, tetrasodium pyrophosphate 0.5wt%, sodium dihydrogen phosphate 0.05wt%, sodium phytate 2wt%, sodium carboxymethyl cellulose 1.5wt%, xanthan gum 0.6wt%, sodium lauryl sulfate 2.5wt%, calcium hydrogen phosphate two water thing 30wt%, hydration Silicon stone 15wt%, essence 0.5wt%, saccharin sodium 0.1wt%, tranexamic acid 0.02wt%, sodium benzoate 0.3wt%, embodiment 5.
Should be noted that and understand, under the situation that does not break away from the desired the spirit and scope of the present invention of accompanying Claim, can make various modifications and improvement the present invention of above-mentioned detailed description.Therefore, the scope of the technical scheme of requirement protection does not receive the restriction of given any specific exemplary teachings.
Applicant's statement, the present invention explains detailed method of the present invention through the foregoing description, but the present invention is not limited to above-mentioned detailed method, does not mean that promptly the present invention must rely on above-mentioned detailed method and could implement.The person of ordinary skill in the field should understand, and to any improvement of the present invention, to the interpolation of the equivalence replacement of each raw material of product of the present invention and auxiliary element, the selection of concrete mode etc., all drops within protection scope of the present invention and the open scope.
Claims (10)
1. a Folium camelliae assamicae toothpaste is characterized in that, said toothpaste contains Pu'er tea.
2. Folium camelliae assamicae toothpaste according to claim 1 is characterized in that, described Pu'er tea makes according to following method:
(1) gets puerh tea leaves, under cryogenic conditions, pulverize and grind to form tea powder and mince;
(2) under the room temperature tea powder of step (1) gained is minced and the water mix homogeneously, the ultrasound wave lixiviate, lixiviating solution;
(3) lixiviating solution with step (2) gained is cooled to room temperature, and tea grounds is removed in filter pressing, stays extracting solution and centrifugal layering, shifts out centrifugal gained supernatant, and repeated centrifugation is operated to obtain spissated Pu'er tea.
3. Folium camelliae assamicae toothpaste according to claim 1 and 2 is characterized in that, the puerh tea leaves described in the said step (1) is preferably the ancient Camellia sinensis in Yunnan and shines QINGCHAYE;
Preferably, said low temperature is meant temperature≤25 ℃, preferably adopts cold water circulation, on the rocks or be that the cooling system of cold media is realized cryogenic conditions with liquid nitrogen, dry ice; Further preferably, said cold water circulating temperature scope is preferably 5-25 ℃, and said temperature range on the rocks is preferably 0-25 ℃, and said is that the cooling system temperature range of cold media is preferably-40-20 ℃ with liquid nitrogen, dry ice;
Preferably, the fineness that said tea powder minces is the 40-75 order, further is preferably the 45-75 order, most preferably is the 50-70 order.
4. according to the described Folium camelliae assamicae toothpaste of one of claim 1-3, it is characterized in that room temperature is 10-30 ℃ temperature range described in the said step (2), is preferably 15-25 ℃, most preferably be 25 ℃;
Preferably, said water is distilled water, pure water or sterile deionized water;
Preferably, said tea powder mince with water preferably according to the mixed of parts by weight 1:100-200, be preferably 1:110-190, further be preferably 1:120-180;
Preferably, the time of said ultrasound wave lixiviate is 10-40min, further is preferably 15-30min, most preferably is 20-25min;
Preferably, the temperature of said ultrasound wave lixiviate is 50-80 ℃, further is preferably 55-70 ℃, most preferably is 60-70 ℃.
5. according to the described Folium camelliae assamicae toothpaste of one of claim 1-4, it is characterized in that the rapid temperature reduction way of the preferred employing of cooling described in the said step (3); Said rapid cooling is meant in the time of 30-60min and cools the temperature to room temperature, preferably in the time of 30-50min, cools the temperature to room temperature, most preferably in the time of 30-40min, cools the temperature to room temperature;
Preferably, said centrifugal rotation speed is 4500-8000r/min, further is preferably 5000-7500r/min, most preferably is 5000-7000r/min;
Preferably, the said centrifugal time is 5-25min, further is preferably 10-20min, most preferably is 10-15min;
Preferably, it is 2-15 time that said repeated centrifugation is operated multiple number of times, further is preferably 3-10 time, most preferably is 5-8 time;
Preferably, the moisture≤50wt% of the Pu'er tea that obtains after concentrating further is preferably≤45wt%, most preferably is≤40wt%.
6. according to the described Folium camelliae assamicae toothpaste of one of claim 1-5, it is characterized in that described Pu'er tea makes according to following method:
(1) get puerh tea leaves, under≤25 ℃ condition, pulverizing and grinding to form fineness is that 40-75 purpose tea powder minces;
(2) under 10-30 ℃ of temperature the tea powder of step (1) gained is minced even with water according to the mixed of parts by weight 1:100-200, ultrasound wave lixiviate 10-40min, extraction temperature 50-80 ℃, lixiviating solution;
(3) lixiviating solution with step (2) gained is cooled to 10-30 ℃ rapidly in 30-60min; Tea grounds is removed in filter pressing; The extracting solution that stays is centrifugal 5-25min under the condition of 4500-8000r/min at revolution; Shift out centrifugal gained supernatant, repeated centrifugation is operated 2-15 time, obtains the Pu'er tea of moisture≤50wt%;
Preferably, described Pu'er tea makes according to following method:
(1) gets puerh tea leaves, in cold water circulation, on the rocks or be to pulverize in the cooling system of cold media that to grind to form fineness be that 45-75 purpose tea powder minces with liquid nitrogen, dry ice;
(2) under 15-25 ℃ of temperature the tea powder of step (1) gained is minced even with water according to the mixed of parts by weight 1:110-190, ultrasound wave lixiviate 15-30min, extraction temperature 55-70 ℃, lixiviating solution;
(3) lixiviating solution with step (2) gained is cooled to 15-25 ℃ rapidly in 30-50min; Tea grounds is removed in filter pressing; The extracting solution that stays is centrifugal 10-20min under the condition of 5000-7500r/min at revolution; Shift out centrifugal gained supernatant, repeated centrifugation is operated 3-10 time, obtains the Pu'er tea of moisture≤45wt%.
7. according to the described Folium camelliae assamicae toothpaste of one of claim 1-6, it is characterized in that described Pu'er tea makes according to following method:
(1) gets puerh tea leaves, in cold water circulation, on the rocks or be to pulverize in the cooling system of cold media that to grind to form fineness be that 50-70 purpose tea powder minces with liquid nitrogen, dry ice;
It is even according to the mixed of parts by weight 1:120-180 with distilled water under (2) 25 ℃ of temperature the tea powder of step (1) gained to be minced, ultrasound wave lixiviate 20-25min, extraction temperature 60-70 ℃, lixiviating solution;
(3) lixiviating solution with step (2) gained is cooled to 25 ℃ rapidly in 30-40min; Tea grounds is removed in filter pressing; The extracting solution that stays is centrifugal 10-15min under the condition of 5000-7000r/min at revolution; Shift out centrifugal gained supernatant, repeated centrifugation is operated 5-8 time, obtains the Pu'er tea of moisture≤40wt%.
8. according to the described Folium camelliae assamicae toothpaste of one of claim 1-7; It is characterized in that said Folium camelliae assamicae toothpaste comprises following component according to the quality percentage composition: glycerol 3-15wt%, sorbitol 15-30wt%, PEG4001-10wt%, tetrasodium pyrophosphate 0.1-0.5wt%, sodium dihydrogen phosphate 0.05-0.5wt%, sodium phytate 0.2-2wt%, sodium carboxymethyl cellulose 0.5-1.5wt%, xanthan gum 0.2-0.6wt%, sodium lauryl sulfate 1.5-2.5wt%, calcium hydrogen phosphate two water thing 15-30wt%, hydration Silicon stone 5-15wt%, essence 0.5-2wt%, Pu'er tea 0.5-10wt% and balance of deionized water;
Preferably, said Folium camelliae assamicae toothpaste comprises following component according to the quality percentage composition: glycerol 5-10wt%, sorbitol 20-25wt%, PEG4002-5wt%, tetrasodium pyrophosphate 0.2-0.3wt%, sodium dihydrogen phosphate 0.1-0.2wt%, sodium phytate 0.5-1wt%, sodium carboxymethyl cellulose 0.6-0.8wt%, xanthan gum 0.3-0.5wt%, sodium lauryl sulfate 2-2.3wt%, calcium hydrogen phosphate two water thing 20-25wt%, hydration Silicon stone 8-10wt%, essence 1-1.2wt%, Pu'er tea 1-5wt% and balance of deionized water.
9. according to the described Folium camelliae assamicae toothpaste of one of claim 1-8; It is characterized in that said Folium camelliae assamicae toothpaste comprises following component according to the quality percentage composition: glycerol 3-15wt%, sorbitol 15-30wt%, PEG4001-10wt%, tetrasodium pyrophosphate 0.1-0.5wt%, sodium dihydrogen phosphate 0.05-0.5wt%, sodium phytate 0.2-2wt%, sodium carboxymethyl cellulose 0.5-1.5wt%, xanthan gum 0.2-0.6wt%, sodium lauryl sulfate 1.5-2.5wt%, calcium hydrogen phosphate two water thing 15-30wt%, hydration Silicon stone 5-15wt%, essence 0.5-2wt%, xylitol 1-8wt%, Pu'er tea 0.5-10wt% and balance of deionized water;
Preferably, said Folium camelliae assamicae toothpaste comprises following component according to the quality percentage composition: glycerol 5-10wt%, sorbitol 20-25wt%, PEG4002-5wt%, tetrasodium pyrophosphate 0.2-0.3wt%, sodium dihydrogen phosphate 0.1-0.2wt%, sodium phytate 0.5-1wt%, sodium carboxymethyl cellulose 0.6-0.8wt%, xanthan gum 0.3-0.5wt%, sodium lauryl sulfate 2-2.3wt%, calcium hydrogen phosphate two water thing 20-25wt%, hydration Silicon stone 8-10wt%, essence 1-1.2wt%, xylitol 2-5wt%, Pu'er tea 1-5wt% and balance of deionized water.
10. according to the described Folium camelliae assamicae toothpaste of one of claim 1-9; It is characterized in that said Folium camelliae assamicae toothpaste comprises following component according to the quality percentage composition: glycerol 3-15wt%, sorbitol 15-30wt%, PEG4001-10wt%, tetrasodium pyrophosphate 0.1-0.5wt%, sodium dihydrogen phosphate 0.05-0.5wt%, sodium phytate 0.2-2wt%, sodium carboxymethyl cellulose 0.5-1.5wt%, xanthan gum 0.2-0.6wt%, sodium lauryl sulfate 1.5-2.5wt%, calcium hydrogen phosphate two water thing 15-30wt%, hydration Silicon stone 5-15wt%, essence 0.5-2wt%, saccharin sodium 0.1-0.5wt%, tranexamic acid 0.02-0.2wt%, sodium benzoate 0.05-0.3wt%, Pu'er tea 0.5-10wt% and balance of deionized water;
Preferably, said Folium camelliae assamicae toothpaste comprises following component according to the quality percentage composition: glycerol 5-10wt%, sorbitol 20-25wt%, PEG4002-5wt%, tetrasodium pyrophosphate 0.2-0.3wt%, sodium dihydrogen phosphate 0.1-0.2wt%, sodium phytate 0.5-1wt%, sodium carboxymethyl cellulose 0.6-0.8wt%, xanthan gum 0.3-0.5wt%, sodium lauryl sulfate 2-2.3wt%, calcium hydrogen phosphate two water thing 20-25wt%, hydration Silicon stone 8-10wt%, essence 1-1.2wt%, saccharin sodium 0.2-0.3wt%, tranexamic acid 0.05-0.1wt%, sodium benzoate 0.1-0.2wt%, Pu'er tea 1-5wt% and balance of deionized water.
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| CN103239369A (en) * | 2013-04-24 | 2013-08-14 | 朱天南 | Functional biological toothpaste |
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| CN103239369B (en) * | 2013-04-24 | 2015-05-13 | 朱天南 | Functional biological toothpaste |
| CN103536496A (en) * | 2013-10-30 | 2014-01-29 | 昆明理工大学 | Toothpaste and preparation method thereof |
| CN103536496B (en) * | 2013-10-30 | 2015-05-20 | 昆明理工大学 | Toothpaste and preparation method thereof |
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| CN106420441A (en) * | 2016-08-29 | 2017-02-22 | 陈思 | Method for preparing toothpaste |
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| CN107041859A (en) * | 2017-03-01 | 2017-08-15 | 广东金山百草健康产业有限公司 | A kind of formula of beautiful millettia root toothpaste |
| CN106626941A (en) * | 2017-03-22 | 2017-05-10 | 王培彪 | Compound tea mud and interior decoration artwork made of compound tea mud |
| CN108969413A (en) * | 2017-06-05 | 2018-12-11 | 狮王株式会社 | Composition for oral cavity |
| CN108653045A (en) * | 2018-06-08 | 2018-10-16 | 广东南方洁灵科技实业有限公司 | A kind of toothpaste and its manufacturing method improving the black yellow problem of tooth |
| EP3771343A1 (en) | 2019-07-31 | 2021-02-03 | Laboratoires Arkopharma | Method and device for obtaining an aqueous liquid plant maceration |
| FR3099341A1 (en) * | 2019-07-31 | 2021-02-05 | Laboratoires Arkopharma | Process and device for obtaining a liquid aqueous vegetable macerate |
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| CN114681382A (en) * | 2022-05-07 | 2022-07-01 | 云南花王生物科技有限公司 | Flower toothpaste and preparation method thereof |
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