CN102730719A - 一种连续提纯工业氨装置及工艺 - Google Patents
一种连续提纯工业氨装置及工艺 Download PDFInfo
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- CN102730719A CN102730719A CN2012102232837A CN201210223283A CN102730719A CN 102730719 A CN102730719 A CN 102730719A CN 2012102232837 A CN2012102232837 A CN 2012102232837A CN 201210223283 A CN201210223283 A CN 201210223283A CN 102730719 A CN102730719 A CN 102730719A
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- Prior art keywords
- tower
- distillation
- strainer
- hot water
- ammonia
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- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 title claims abstract description 88
- 229910021529 ammonia Inorganic materials 0.000 title claims abstract description 34
- 238000005516 engineering process Methods 0.000 title claims abstract description 16
- 238000000746 purification Methods 0.000 title abstract description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 33
- 238000004821 distillation Methods 0.000 claims abstract description 31
- 238000010438 heat treatment Methods 0.000 claims abstract description 19
- 239000012535 impurity Substances 0.000 claims abstract description 9
- 239000002994 raw material Substances 0.000 claims abstract description 8
- 238000001816 cooling Methods 0.000 claims abstract description 5
- 239000012530 fluid Substances 0.000 claims abstract description 4
- 238000003860 storage Methods 0.000 claims abstract description 4
- 229910000069 nitrogen hydride Inorganic materials 0.000 claims description 9
- 241000282326 Felis catus Species 0.000 claims description 6
- 238000009833 condensation Methods 0.000 claims description 6
- 230000005494 condensation Effects 0.000 claims description 6
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 3
- 229910000831 Steel Inorganic materials 0.000 claims description 3
- 235000011089 carbon dioxide Nutrition 0.000 claims description 3
- 239000000470 constituent Substances 0.000 claims description 3
- 235000019628 coolness Nutrition 0.000 claims description 3
- JEGUKCSWCFPDGT-UHFFFAOYSA-N h2o hydrate Chemical compound O.O JEGUKCSWCFPDGT-UHFFFAOYSA-N 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 3
- 238000012856 packing Methods 0.000 claims description 3
- 239000010959 steel Substances 0.000 claims description 3
- 238000009834 vaporization Methods 0.000 claims description 3
- 230000008016 vaporization Effects 0.000 claims description 3
- 238000010521 absorption reaction Methods 0.000 abstract description 4
- 238000003889 chemical engineering Methods 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 239000004065 semiconductor Substances 0.000 description 3
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000004377 microelectronic Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
Description
Claims (2)
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CN201210223283.7A CN102730719B (zh) | 2012-07-02 | 2012-07-02 | 一种连续提纯工业氨装置及工艺 |
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CN201210223283.7A CN102730719B (zh) | 2012-07-02 | 2012-07-02 | 一种连续提纯工业氨装置及工艺 |
Publications (2)
Publication Number | Publication Date |
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CN102730719A true CN102730719A (zh) | 2012-10-17 |
CN102730719B CN102730719B (zh) | 2014-02-26 |
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CN201210223283.7A Active CN102730719B (zh) | 2012-07-02 | 2012-07-02 | 一种连续提纯工业氨装置及工艺 |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103073026A (zh) * | 2013-02-07 | 2013-05-01 | 周礼誉 | 一种氨气回收*** |
CN106495183A (zh) * | 2016-11-07 | 2017-03-15 | 广东华特气体股份有限公司 | 一种氨气的纯化方法 |
WO2018090460A1 (zh) * | 2016-11-17 | 2018-05-24 | 天津大学 | 炼油废水生产中不合格液氨的再精制工艺及*** |
CN112299445A (zh) * | 2020-11-20 | 2021-02-02 | 苏州金宏气体股份有限公司 | 一种填料精馏制备超纯氨的方法 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN202030539U (zh) * | 2011-03-15 | 2011-11-09 | 苏州金宏气体股份有限公司 | 精馏分离生产7n电子级超纯氨的装置 |
CN102249259A (zh) * | 2010-05-19 | 2011-11-23 | 上海普锐克索特种气体有限公司 | 一种高纯氨的纯化工艺 |
CN102464341A (zh) * | 2010-11-02 | 2012-05-23 | 住友精化株式会社 | 氨精制*** |
CN202705056U (zh) * | 2012-07-02 | 2013-01-30 | 大连保税区科利德化工科技开发有限公司 | 一种连续提纯工业氨装置 |
-
2012
- 2012-07-02 CN CN201210223283.7A patent/CN102730719B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102249259A (zh) * | 2010-05-19 | 2011-11-23 | 上海普锐克索特种气体有限公司 | 一种高纯氨的纯化工艺 |
CN102464341A (zh) * | 2010-11-02 | 2012-05-23 | 住友精化株式会社 | 氨精制*** |
CN202030539U (zh) * | 2011-03-15 | 2011-11-09 | 苏州金宏气体股份有限公司 | 精馏分离生产7n电子级超纯氨的装置 |
CN202705056U (zh) * | 2012-07-02 | 2013-01-30 | 大连保税区科利德化工科技开发有限公司 | 一种连续提纯工业氨装置 |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103073026A (zh) * | 2013-02-07 | 2013-05-01 | 周礼誉 | 一种氨气回收*** |
CN103073026B (zh) * | 2013-02-07 | 2015-07-01 | 上海兄弟微电子技术有限公司 | 一种氨气回收*** |
CN106495183A (zh) * | 2016-11-07 | 2017-03-15 | 广东华特气体股份有限公司 | 一种氨气的纯化方法 |
CN106495183B (zh) * | 2016-11-07 | 2018-12-18 | 广东华特气体股份有限公司 | 一种氨气的纯化方法 |
WO2018090460A1 (zh) * | 2016-11-17 | 2018-05-24 | 天津大学 | 炼油废水生产中不合格液氨的再精制工艺及*** |
CN112299445A (zh) * | 2020-11-20 | 2021-02-02 | 苏州金宏气体股份有限公司 | 一种填料精馏制备超纯氨的方法 |
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Publication number | Publication date |
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CN102730719B (zh) | 2014-02-26 |
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Effective date of registration: 20180607 Address after: No. 8, Huayuan street, Shangcheng, Ganjingzi District, Dalian, Liaoning 2-4-1 Co-patentee after: Zhao Chao Patentee after: Zhao Yi Co-patentee after: Ji Yanqiu Co-patentee after: Wang Tianyuan Address before: 116600 Liaoning Dalian bonded area storage processing area IE-33 Patentee before: DALIAN FREE TRADE ZONE CREDIT CHEMICAL SCIENCE AND TECHNOLOGY DEVELOPMENT CO.,LTD. |
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Application publication date: 20121017 Assignee: Quanjiao kelide Electronic Materials Co.,Ltd. Assignor: Zhao Yi|Zhao Chao|Ji Yanqiu|Wang Tianyuan Contract record no.: X2020340000006 Denomination of invention: A device and process for continuous purification of industrial ammonia Granted publication date: 20140226 License type: Exclusive License Record date: 20200806 |
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Effective date of registration: 20210317 Address after: 116600 Liaoning Dalian bonded area storage processing area IE-33 Patentee after: DALIAN FREE TRADE ZONE CREDIT CHEMICAL SCIENCE AND TECHNOLOGY DEVELOPMENT Co.,Ltd. Address before: No. 8, Huayuan street, Shangcheng, Ganjingzi District, Dalian, Liaoning 2-4-1 Patentee before: Zhao Yi Patentee before: Zhao Chao Patentee before: Ji Yanqiu Patentee before: Wang Tianyuan |
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Denomination of invention: A device and process for continuous purification of industrial ammonia Effective date of registration: 20220927 Granted publication date: 20140226 Pledgee: China Minsheng Bank Co.,Ltd. Dalian Branch Pledgor: DALIAN FREE TRADE ZONE CREDIT CHEMICAL SCIENCE AND TECHNOLOGY DEVELOPMENT CO.,LTD. Registration number: Y2022980016620 |
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Address after: No. 1-1, Haike Road, Dalian Free Trade Zone, Liaoning 116600 Patentee after: Dalian Kelide Semiconductor Materials Co.,Ltd. Address before: 116600 Liaoning Dalian bonded area storage processing area IE-33 Patentee before: DALIAN FREE TRADE ZONE CREDIT CHEMICAL SCIENCE AND TECHNOLOGY DEVELOPMENT CO.,LTD. |
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Assignee: Quanjiao kelide Electronic Materials Co.,Ltd. Assignor: Zhao Yi|Zhao Chao|Ji Yanqiu|Wang Tianyuan Contract record no.: X2020340000006 Date of cancellation: 20230419 |
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Date of cancellation: 20230529 Granted publication date: 20140226 Pledgee: China Minsheng Bank Co.,Ltd. Dalian Branch Pledgor: DALIAN FREE TRADE ZONE CREDIT CHEMICAL SCIENCE AND TECHNOLOGY DEVELOPMENT CO.,LTD. Registration number: Y2022980016620 |