CN102660171A - High-gloss abrasion-resisting ultraviolet (UV) gold-stamping gloss oil for the field of cigarette packet printing and preparation method thereof - Google Patents
High-gloss abrasion-resisting ultraviolet (UV) gold-stamping gloss oil for the field of cigarette packet printing and preparation method thereof Download PDFInfo
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Abstract
The invention provides high-gloss abrasion-resisting ultraviolet (UV) gold-stamping gloss oil for the field of cigarette packet printing and a preparation method thereof. The high-gloss abrasion-resisting UV gold-stamping gloss oil is gold-stamping gloss oil with the viscosity of 130-150 cps/25 DEG C and is prepared by mixing and stirring, by mass, 20-25 parts of CN9006 N six-functionality polyurethane acrylate, 25-30 parts of CN117 modified epoxy acrylate, 15-15.6 parts of SR399NS dipentaerythritol quinary/senary acrylic ester, 15-18 parts of SR238NS 1,6- hexylene glycol diacrylate, 5-8 parts of photoinitiator, 5-10 parts of photosensitivity sensitizer and1-3 parts of auxiliaries. The high-gloss abrasion-resisting UV gold-stamping gloss oil adopts monomers and resin with small acid value and corrosivity, has the advantages of being high in glossiness, good in adhesive force, friction-resisting, quick in drying speed and the like and has good gold-stamping effect when used for the cigarette packet printing.
Description
Technical field
The invention belongs to print field, specifically is a kind of gold stamping oil of high light wearable UV that is used for the tobacco bale print field and preparation method thereof.
Background technology
At present, the gilding technology application of printing on the cigarette-brand accounts for more than 85%, the gold stamping back of product clear patterns, attractive in appearance, color glow, wear-resisting weather-proof.Therefore, in the tobacco bale typography, in order to increase the crocking resistance of printing ink, the protection printed matter improves printed matter brightness, need on printing packaging, use the gold stamping gloss oil of high light wearable UV, makes packing more vividly brilliant.And directly gold stamping on UV gloss oil surface, its technology itself than higher, but when gloss oil is coated with, note controlling the size of oil mass to the requirement of UV gloss oil, guarantee the relatively stable of entire block gloss oil coating, and oil reservoir will approach peace as far as possible.The recoat bronzing effect of the gold stamping gloss oil of present existing ultraviolet light polymerization is relatively poor, some in addition also can corrode hectograph, had a strong impact on the gold stamping mass effect of gloss oil.
Summary of the invention
The present invention proposes the gold stamping gloss oil of a kind of high light wearable UV through the component design to printing ink, can be gold stamping to satisfy the print product postorder, and the requirement that bronzing effect is good.
A kind of gold stamping gloss oil of high light wearable UV that is used for the tobacco bale print field is characterized in that being made up of the component of following mass fraction:
Wherein: described UV-cured resin is that the six functionality urethane acrylates (the chemical ltd of Sartomer (Guangzhou)) of CN9006N and modified epoxy acrylic ester (the chemical ltd of Sartomer (Guangzhou)) that model is CN117 are formed by model; In its total umber 50～53, comprise 20～25 parts of CN9006N and 25～30 parts of CN117;
Said monomer reactivity thinner is to be that Dipentaerythritol five/six propenoate (the chemical ltd of Sartomer (Guangzhou)) and the model of SR399NS is 1 of SR238NS by model; 6-hexanediyl ester (the chemical ltd of Sartomer (Guangzhou)) is formed, and comprises 15～15.6 parts of SR399NS and 15～18 parts of SR238NS in its total umber 30～33.6;
Described light trigger is selected ITX (Tianjin Jiuri Chemical Co., Ltd.'s production model is the 2-isopropyl thioxanthone of JRCure ITX) and one or both combinations of DETX (Tianjin Jiuri Chemical Co., Ltd. produces 2 of JRCure DETX, 4-diethyl thioxanthone) for use;
Said photosensitive sensitizing agent is selected EHA (the different monooctyl ester of p-(dimethylamino)-benzoic acid that Insight High Technology Co., Ltd. (Jiangsu) produces) for use;
Said auxiliary agent is by flow agent RF339 (Guangzhou Yu Chang chemical science and technology), skimmer DF258 (Guangzhou Yu Chang chemical science and technology), dispersion agent 497 (Guangzhou Yu Chang chemical science and technology), 2; 5-two uncles base Resorcinol (Shanghai nation becomes chemical industry ltd) is formed; All can on market, buy; In 1～3 part of wherein total umber, comprise 497,0.05～0.1 part 2 of 0.3～0.5 part of flow agent RF339,0.3～0.6 part of skimmer DF258,0.35～0.6 part of dispersion agent, 5-two uncles base Resorcinol.
Described light trigger comprises 3～5 mass parts JRCure ITX, 2～3 mass parts JRCure DETX during by two kinds of combinations of JRCure ITX and JRCure DETX.
The mass fraction of each material is by 497,0.1 part 2 of 0.3 part of flow agent RF339,0.5 part of skimmer DF258,0.5 part of dispersion agent in the said auxiliary agent, 5-two uncles base Resorcinol.
A kind of method for preparing the gold stamping gloss oil of high light wearable UV comprises the stainless steel stirred vessel, it is characterized in that may further comprise the steps:
(1) taking by weighing the six functionality urethane acrylates that 20～25 mass parts models are CN9006N, the modified epoxy acrylic ester that 25～30 mass parts models are CN117, Dipentaerythritol five/six propenoate, 15～18 mass parts models that 15～15.6 mass parts models are SR399NS is 1 of SR238NS; 497,0.05～0.1 part 2 of 6-hexanediyl ester, 5～8 mass parts light triggers, the photosensitive sensitizing agent of 5～10 mass parts, 0.3～0.5 part of flow agent RF339,0.3～0.6 part of skimmer DF258,0.35～0.6 part of dispersion agent, 5-two uncles base Resorcinol;
(2) be that Dipentaerythritol five/six propenoate, 15～18 mass parts models of SR399NS are 1 of SR238NS with 15～15.6 mass parts models successively; 6-hexanediyl ester, 20～25 mass parts, six functionality polyurethane acrylate resins and 25～30 mass parts models were that the modified epoxy acrylic ester of CN117 adds the stainless steel stirred vessel respectively, with the rotating speed dispersed with stirring of 1000rpm 10～20 minutes;
(3) add whole light triggers, photosensitive sensitizing agent EHA, auxiliary agent successively after stirring, with the rotating speed dispersed with stirring of 2000rpm one hour, to viscosity be 130～150cps/25 ℃, filter and get final product.
The present invention select for use acid number little with little monomer and the resin of corrodibility, and optimize the component design of printing ink, have the glossiness height, sticking power is good, advantage such as rub resistance, rate of drying are fast, it is good to be used for the typographic bronzing effect of tobacco bale; Wherein the effect of flow agent mainly is a flowability of improving printing ink, improves the surface finish that printing ink is filmed; The effect of skimmer is to reduce printing ink in use because of a large amount of bubbles appears in flow circuit, prevent the bubble that produces and have influence on print product surface seal unreal, ignore appears; The effect of dispersion agent is the dispersing uniformity that improves above component.
Embodiment
Through specific embodiment the present invention is further described below, but the present invention is not limited in these embodiment.
Embodiment 1: a kind of gold stamping gloss oil of high light wearable UV that is used for the tobacco bale print field is characterized in that being made up of the component of following parts by weight:
A kind of method for preparing the gold stamping gloss oil of above-mentioned high light wearable UV comprises the stainless steel stirred vessel, it is characterized in that may further comprise the steps:
(1) taking by weighing the six functionality urethane acrylates that 20～25 mass parts models are CN9006N, the modified epoxy acrylic ester that 25 mass parts models are CN117, Dipentaerythritol five/six propenoate, the 18 mass parts models that 15.6 mass parts models are SR399NS is 1 of SR238NS; 6-hexanediyl ester, 5 mass parts light triggers (JRCure ITX), the photosensitive sensitizing agent EHA of 10 mass parts, 0.3 mass parts flow agent RF339,0.5 mass parts skimmer DF258,0.5 mass parts dispersion agent 497 and 0.1 mass parts 2,5-two uncles base Resorcinol;
(2) be that Dipentaerythritol five/six propenoate, the 18 mass parts models of SR399NS are 1 of SR238NS with 15.6 mass parts models successively; 6-hexanediyl ester, 25 mass parts, six functionality polyurethane acrylate resins and 25 mass parts models were that the modified epoxy acrylic ester of CN117 adds the stainless steel stirred vessel respectively, with the rotating speed dispersed with stirring of 1000rpm 10～20 minutes;
(3) adding whole light triggers, photosensitive sensitizing agent EHA, auxiliary agent successively after stirring, with the rotating speed dispersed with stirring of 2000rpm one hour, is that 130～150cps/25 ℃ of filtration gets final product to viscosity.
Embodiment 2:
A kind of gold stamping gloss oil of high light wearable UV that is used for the tobacco bale print field is characterized in that being made up of the component of parts by weight:
A kind of method for preparing the gold stamping gloss oil of above-mentioned high light wearable UV comprises the stainless steel stirred vessel, it is characterized in that may further comprise the steps:
(1) taking by weighing the six functionality urethane acrylates that 20 mass parts models are CN9006N, the modified epoxy acrylic ester that 30 mass parts models are CN117, Dipentaerythritol five/six propenoate, the 18 mass parts models that 15.6 mass parts models are SR399NS is 1 of SR238NS; 6-hexanediyl ester, 5 mass parts light triggers (JRCure DETX), the photosensitive sensitizing agent EHA of 10 mass parts, 0.3 mass parts flow agent RF339,0.5 mass parts skimmer DF258,0.5 mass parts dispersion agent 497 and 0.1 mass parts 2,5-two uncles base Resorcinol;
(2) be that Dipentaerythritol five/six propenoate, the 18 mass parts models of SR399NS are 1 of SR238NS with 15.6 mass parts models successively; 6-hexanediyl ester, 20 mass parts, six functionality polyurethane acrylate resins and 30 mass parts models were that the modified epoxy acrylic ester of CN117 adds the stainless steel stirred vessel respectively, with the rotating speed dispersed with stirring of 1000rpm 10～20 minutes;
(3) adding whole light triggers, photosensitive sensitizing agent EHA, auxiliary agent successively after stirring, with the rotating speed dispersed with stirring of 2000rpm one hour, is that 130～150cps/25 ℃ of filtration gets final product to viscosity.
Embodiment 3:
A kind of gold stamping gloss oil of high light wearable UV that is used for the tobacco bale print field is characterized in that being made up of following components in weight percentage content:
A kind of method for preparing the gold stamping gloss oil of above-mentioned high light wearable UV comprises the stainless steel stirred vessel, it is characterized in that may further comprise the steps:
(1) taking by weighing the six functionality urethane acrylates that 23 mass parts models are CN9006N, the modified epoxy acrylic ester that 28 mass parts models are CN117, Dipentaerythritol five/six propenoate, the 17 mass parts models that 15.6 mass parts models are SR399NS is 1 of SR238NS; 6-hexanediyl ester, 2 mass parts light triggers (JRCure DETX), 3 mass parts light triggers (JRCureITX), the photosensitive sensitizing agent EHA of 10 mass parts, 0.3 mass parts flow agent RF339,0.5 mass parts skimmer DF258,0.5 mass parts dispersion agent 497 and 0.1 mass parts 2,5-two uncles base Resorcinol;
(2) be that Dipentaerythritol five/six propenoate, the 17 mass parts models of SR399NS are 1 of SR238NS with 15.6 mass parts models successively; 6-hexanediyl ester, 23 mass parts, six functionality polyurethane acrylate resins and 28 mass parts models were that the modified epoxy acrylic ester of CN117 adds the stainless steel stirred vessel respectively, with the rotating speed dispersed with stirring of 1000rpm 10～20 minutes;
(3) adding whole light triggers, photosensitive sensitizing agent EHA, auxiliary agent successively after stirring, with the rotating speed dispersed with stirring of 2000rpm one hour, is that 130～150cps/25 ℃ of filtration gets final product to viscosity.
According to the gold stamping gloss oil of UV that above embodiment produces, its test data is following:
Claims (4)
1. gold stamping gloss oil of high light wearable UV that is used for the tobacco bale print field is characterized in that being made up of the component of following mass fraction:
Wherein: described UV-cured resin is that the six functionality urethane acrylates of CN9006N and modified epoxy acrylic ester that model is CN117 are formed by model, in its total umber 50～53, comprises 20～25 parts of CN9006N and 25～30 parts of CN117;
Said monomer reactivity thinner is to be that Dipentaerythritol five/six propenoate and the model of SR399NS is 1 of SR238NS by model; The 6-hexanediyl ester is formed, and comprises 15～15.6 parts of SR399NS and 15～18 parts of SR238NS in its total umber 30～33.6;
It is that 2-isopropyl thioxanthone and the model of JRCure ITX is 2 of JRCure DETX that said light trigger is selected model for use, one or both combinations of 4-diethyl thioxanthone;
Said photosensitive sensitizing agent is selected the different monooctyl ester of p-(dimethylamino)-benzoic acid for use;
Said auxiliary agent is by flow agent RF339, skimmer DF258, dispersion agent 497,2; Four kinds of materials of 5-two uncles base Resorcinol are formed; In 1～3 part of wherein total umber; Comprise 497,0.05～0.1 part 2 of 0.3～0.5 part of flow agent RF339,0.3～0.6 part of skimmer DF258,0.35～0.6 part of dispersion agent, 5-two uncles base Resorcinol.
2. a kind of gold stamping gloss oil of high light wearable UV that is used for the tobacco bale print field according to claim 1; It is characterized in that: described light trigger comprises 3～5 mass parts JRCure ITX, 2～3 mass parts JRCure DETX during by two kinds of combinations of JRCure ITX and JRCure DETX.
3. a kind of gold stamping gloss oil of high light wearable UV that is used for the tobacco bale print field according to claim 1; It is characterized in that: the mass fraction of each material is for by 497,0.1 part 2 of 0.3 part of flow agent RF339,0.5 part of skimmer DF258,0.5 part of dispersion agent, 5-two uncles base Resorcinol in the said auxiliary agent.
4. a method for preparing the gold stamping gloss oil of claims 1 described high light wearable UV comprises the stainless steel stirred vessel, it is characterized in that may further comprise the steps:
(1) taking by weighing the six functionality urethane acrylates that 20～25 mass parts models are CN9006N, the modified epoxy acrylic ester that 25～30 mass parts models are CN117, Dipentaerythritol five/six propenoate, 15～18 mass parts models that 15～15.6 mass parts models are SR399NS is 1 of SR238NS; 497,0.05～0.1 part 2 of 6-hexanediyl ester, 5～8 mass parts light triggers, the photosensitive sensitizing agent of 5～10 mass parts, 0.3～0.5 part of flow agent RF339,0.3～0.6 part of skimmer DF258,0.35～0.6 part of dispersion agent, 5-two uncles base Resorcinol;
(2) be that Dipentaerythritol five/six propenoate, 15～18 mass parts models of SR399NS are 1 of SR238NS with 15～15.6 mass parts models successively; 6-hexanediyl ester, 20～25 mass parts, six functionality polyurethane acrylate resins and 25～30 mass parts models were that the modified epoxy acrylic ester of CN117 adds the stainless steel stirred vessel respectively, with the rotating speed dispersed with stirring of 1000rpm 10～20 minutes;
(3) add whole light triggers, photosensitive sensitizing agent EHA, auxiliary agent successively after stirring, with the rotating speed dispersed with stirring of 2000rpm one hour, to viscosity be 130～150cps/25 ℃, filter and get final product.
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| CN2012101296263A CN102660171B (en) | 2012-04-28 | 2012-04-28 | High-gloss abrasion-resisting ultraviolet (UV) gold-stamping gloss oil for the field of cigarette packet printing and preparation method thereof |
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| CN2012101296263A CN102660171B (en) | 2012-04-28 | 2012-04-28 | High-gloss abrasion-resisting ultraviolet (UV) gold-stamping gloss oil for the field of cigarette packet printing and preparation method thereof |
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| CN102925027A (en) * | 2012-11-15 | 2013-02-13 | 深圳市深赛尔股份有限公司 | UV (ultraviolet) duct gloss oil |
| CN103819963A (en) * | 2014-02-28 | 2014-05-28 | 惠州市立美特环保油墨有限公司 | UV benzene-free gloss oil and preparing method thereof |
| CN104999820A (en) * | 2015-07-10 | 2015-10-28 | 祥和彩瓷制造(上海)有限公司 | Preparation method for low-temperature embossed gold stamping patterned paper and low-temperature embossed gold stamping patterned paper |
| CN107400457A (en) * | 2017-08-31 | 2017-11-28 | 安徽骏飞标识设计制作有限公司 | One kind beats bottom UV gloss oil and preparation method thereof for metal surface |
| CN107629543A (en) * | 2017-10-19 | 2018-01-26 | 区汉女 | A kind of UV cured printing inks and preparation method thereof |
| CN108467611A (en) * | 2018-03-21 | 2018-08-31 | 湖北中烟工业有限责任公司 | A kind of water-mist-proof gloss oil |
| CN108485371A (en) * | 2018-04-17 | 2018-09-04 | 广州市恒远彩印有限公司 | The paper wrapper printing faces UV oil and preparation method thereof |
| CN108705872A (en) * | 2018-05-29 | 2018-10-26 | 徐冬雪 | A kind of cold wave hot transfer foil and its process for making with metallic pigments layer |
| CN110317483A (en) * | 2018-03-28 | 2019-10-11 | 常州格林感光新材料有限公司 | Photocurable composition for metal surface and the composition comprising it |
| CN110525076A (en) * | 2019-09-20 | 2019-12-03 | 湖北中烟工业有限责任公司 | A kind of not frangible dedicated 3D raster print product and preparation method thereof |
| CN110746861A (en) * | 2019-10-17 | 2020-02-04 | 广州宁为科技有限公司 | Anti-scalding oil, preparation method thereof and ink-jet gold stamping system applying anti-scalding oil |
| CN112552758A (en) * | 2020-12-11 | 2021-03-26 | 广东昊辉新材料有限公司 | UV-cured high-surface-tension gloss oil, and preparation method and application thereof |
| CN114773906A (en) * | 2022-04-19 | 2022-07-22 | 广州亦盛环保科技有限公司 | Ink composition and preparation method and application thereof |
| CN116445033A (en) * | 2023-04-06 | 2023-07-18 | 绍兴翔宇绿色包装有限公司 | Printing ink for gold stamping transfer and preparation method thereof |
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| CN1896156A (en) * | 2006-06-23 | 2007-01-17 | 中国乐凯胶片集团公司 | Ultraviolet light-curing sand vein ink |
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| CN1896156A (en) * | 2006-06-23 | 2007-01-17 | 中国乐凯胶片集团公司 | Ultraviolet light-curing sand vein ink |
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| CN102925027A (en) * | 2012-11-15 | 2013-02-13 | 深圳市深赛尔股份有限公司 | UV (ultraviolet) duct gloss oil |
| CN103819963A (en) * | 2014-02-28 | 2014-05-28 | 惠州市立美特环保油墨有限公司 | UV benzene-free gloss oil and preparing method thereof |
| CN103819963B (en) * | 2014-02-28 | 2016-02-10 | 惠州市立美特环保油墨有限公司 | A kind of UV is without benzene gloss oil and preparation method thereof |
| CN104999820A (en) * | 2015-07-10 | 2015-10-28 | 祥和彩瓷制造(上海)有限公司 | Preparation method for low-temperature embossed gold stamping patterned paper and low-temperature embossed gold stamping patterned paper |
| CN107400457A (en) * | 2017-08-31 | 2017-11-28 | 安徽骏飞标识设计制作有限公司 | One kind beats bottom UV gloss oil and preparation method thereof for metal surface |
| CN107629543A (en) * | 2017-10-19 | 2018-01-26 | 区汉女 | A kind of UV cured printing inks and preparation method thereof |
| CN108467611A (en) * | 2018-03-21 | 2018-08-31 | 湖北中烟工业有限责任公司 | A kind of water-mist-proof gloss oil |
| CN110317483A (en) * | 2018-03-28 | 2019-10-11 | 常州格林感光新材料有限公司 | Photocurable composition for metal surface and the composition comprising it |
| CN108485371A (en) * | 2018-04-17 | 2018-09-04 | 广州市恒远彩印有限公司 | The paper wrapper printing faces UV oil and preparation method thereof |
| CN108705872A (en) * | 2018-05-29 | 2018-10-26 | 徐冬雪 | A kind of cold wave hot transfer foil and its process for making with metallic pigments layer |
| CN110525076A (en) * | 2019-09-20 | 2019-12-03 | 湖北中烟工业有限责任公司 | A kind of not frangible dedicated 3D raster print product and preparation method thereof |
| CN110746861A (en) * | 2019-10-17 | 2020-02-04 | 广州宁为科技有限公司 | Anti-scalding oil, preparation method thereof and ink-jet gold stamping system applying anti-scalding oil |
| CN112552758A (en) * | 2020-12-11 | 2021-03-26 | 广东昊辉新材料有限公司 | UV-cured high-surface-tension gloss oil, and preparation method and application thereof |
| CN114773906A (en) * | 2022-04-19 | 2022-07-22 | 广州亦盛环保科技有限公司 | Ink composition and preparation method and application thereof |
| CN114773906B (en) * | 2022-04-19 | 2023-08-29 | 广州亦盛环保科技有限公司 | Ink composition and preparation method and application thereof |
| CN116445033A (en) * | 2023-04-06 | 2023-07-18 | 绍兴翔宇绿色包装有限公司 | Printing ink for gold stamping transfer and preparation method thereof |
| CN116445033B (en) * | 2023-04-06 | 2024-02-09 | 绍兴翔宇绿色包装有限公司 | Printing ink for gold stamping transfer and preparation method thereof |
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