CN102599321A - Manufacturing method for crystallized fruit - Google Patents
Manufacturing method for crystallized fruit Download PDFInfo
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- CN102599321A CN102599321A CN2012100719612A CN201210071961A CN102599321A CN 102599321 A CN102599321 A CN 102599321A CN 2012100719612 A CN2012100719612 A CN 2012100719612A CN 201210071961 A CN201210071961 A CN 201210071961A CN 102599321 A CN102599321 A CN 102599321A
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Abstract
The invention relates to a manufacturing method for crystallized fruit, which comprises the following steps: (1) preparing the following raw materials by weight percent: 20-67.7% of fruit embryos, 32.05-53.0% of sugar crops, 0.1-5% of filling materials, 0-5% of medicinal and food homologous traditional Chinese medicines, 0.05-10% of seasoning spices, 0.1-2.0% of preservatives and 0-5% of pigments; (2) pre-treating the raw materials by preparing liquid sugar, filling material liquid, traditional Chinese medicine extracts and preservative solution; (3) soaking: adding the liquid sugar material, the seasoning spices, the pigments, the liquid sugar, the filling material liquid and the traditional Chinese medicine extracts into a soaking cylinder and mixing uniformly to form the mixed material liquid, adding the fruit embryos into the soaking cylinder, increasing the temperature of the mixed material liquid to 50-60 DEG C and keeping the temperature for 10-15 hours; (4) leaching and drying; and (5) drying to obtain the crystallized fruit. The manufacturing method for crystallized fruit is easily performed, the full utilization of fruit resource is realized, and the manufactured crystallized fruit is full of nutrition and tastes fresh and cool.
Description
Technical field
The present invention relates to the preparation method of preserved fruit, specifically, relate to a kind of preparation method of candied fruits.
Background technology
Present some fruit, the olive that abounds with like the area, Guangdong, green plum, oranges and tangerines, red bayberry etc. have very high value, but as yet not by extensive cognition, industrialization level are lower.These fruit are mainly to be eaten raw, and part is processed as products such as preserved fruit, curing food, can, and generally speaking, product processing technique falls behind, and most products still are in traditional state basically after processing, of low grade, and product increment level is not enough.
In traditional candied fruits preparation method, need repeat repeatedly the process of " reinforced dipping-drying " to fruit, its purpose partly is exactly to remove the bitter taste that wherein tannin, volatile oil and part flavonoids function factor bring, and makes the fruit embryo.Make the process of fruit embryo and need last more than 20 day usually, processing technology complicacy and process-cycle are long; The discharging of maceration extract in the process not only can cause comparatively serious pollution to environment, and causes the very big waste (some functional components with higher-value are dissolved in the maceration extract in the fruit) of resource, and the comprehensive utilization degree of resource is lower.
In recent years; Along with the research to function factor in the food resource deepens continuously; The effect of function factor constantly is proved; And market improving constantly and the continuous growth of demand for the functional food cognition degree; How further to make good use of functional component in the fruit resource, improve the characteristic fruit resource availability, improve fruit resource deep processing level and added value of product, with further raising farmers' income, improve people's livelihood scientific and technological level, improve local economy the capability of sustainable development, reduce the pollution level of food industry for environment, become one of pendulum most important problem in face of ours.
Summary of the invention
Technical problem to be solved by this invention provides a kind of preparation method of candied fruits, and this preparation method is simple, and can realize making full use of of fruit resource.The technical scheme that adopts is following:
A kind of preparation method of candied fruits is characterized in that comprising the steps: successively
(1) is equipped with raw material by following weight proportion: fruit embryo 20-67.7%, sugar material 32.05-53.0%, casting resin 0.1-5%; Integration of drinking and medicinal herbs class Chinese medicine 0-5%, seasoning and adjusting incense material 0.05-10%, anticorrisive agent 0.1-2.0%; Pigment 0-5%, wherein the weight proportion of sugar material is by dry;
(2) preliminary treatment of raw material comprises:
(a) the solid-state sugar material in the sugar material (like sucrose, glucose, sorbierite, xylitol, hydroxyl isomaltulose, mannitol, xylo-oligosaccharide, FOS, oligomeric maltose alcohol) water dissolve fully (usually with solid-state sugar material with after water mixes; Be heated to 95-100 ℃; Be beneficial to the dissolving more fast of sugar material); Water consumption is 5-10 a times of solid-state sugar material weight, obtains liquid glucose;
(b) use temperature to steep 2-5 hour as 20-25 ℃ water logging casting resin, water consumption is 15-25 a times of casting resin weight; Be heated to 80-85 ℃ then, casting resin is dissolved fully, obtain the filling feed liquid;
(c) active ingredient in the extraction integration of drinking and medicinal herbs class Chinese medicine obtains Chinese medical extract;
The method for distilling of integration of drinking and medicinal herbs class Chinese medicine can adopt conventional method (like decocting method, infusion process, percolation, circumfluence method etc., its extract is a herb liquid); Also can adopt the commercially available ready-made Chinese medical extract of respective amount to substitute;
(d) water dissolving anticorrisive agent, water consumption is 10-20 a times of anticorrisive agent weight, obtains antiseptic solution;
Liquid sugar material (like glucose syrup, HFCS), seasoning and adjusting incense material in the sugar material, pigment then directly are used for subsequent step;
(3) soak: liquid sugar material, seasoning and adjusting incense material and pigment in the sugar material that step (1) is equipped with, and step (2) liquid glucose, filling feed liquid, Chinese medical extract and the antiseptic solution that obtain join and soak in the cylinder and mix, and forms mixed liquor; The fruit embryo that then step (1) is equipped with joins to soak in the cylinder and (need stir slightly usually after adding the fruit embryo, be beneficial to the fruit embryo and in mixed liquor, evenly distribute), and the fruit embryo is fully immersed in the mixed liquor; Temperature with mixed liquor is raised to 50-60 ℃ then, and is incubated 10-15 hour;
The preferred fruit that soaks whenever stirred the material that soaks in the cylinder at a distance from 4-5 hour between embryonic stage;
In this step (3), contain at the seasoning and adjusting incense material under the situation of essence, essence also can be postponed adding, when the preparation mixed liquor, does not add earlier essence that is:; The fruit embryo is fully immersed in the mixed liquor, the temperature of mixed liquor is being raised to 50-60 ℃, and after insulation 10-15 hour, again essence is being added in the mixed liquor, soaking again 2-3 hour;
(4) drain: the fruit embryo that immersion is finished takes out and drains;
Drain when handling, can the material that soak in the cylinder be poured in the shaker screen that has filter screen, drain mixed liquor, the fruit embryo is then stayed in the shaker screen; Above-mentioned filter screen can adopt 20 purpose filter screens;
(5) drying: remove the moisture in the fruit embryo, making the water content of fruit embryo is 10-15%, obtains candied fruits.
In the preferred steps (5), adopt dehumidifier method or natural suning method that the fruit embryo is carried out dried.Also can adopt oven drying method (bake out temperature is 45-65 ℃) to carry out dried.
The fruit embryo of preferred above-mentioned steps (1) is through Subcritical Water Extraction technology; With the volatile oil, flavone compound and the triterpene compound that have the specific function composition in the fruit (like olive, green plum, oranges and tangerines, red bayberry) extract and separate the back remaining solid residue, like olive embryo, green plum embryo, oranges and tangerines embryo, red bayberry embryo.
In the concrete scheme, the fruit embryo of above-mentioned steps (1) obtains through following step:
(1 ') pretreatment of raw material: with fresh fruit (like the fresh fruit of olive, green plum, oranges and tangerines, red bayberry) is raw material, fruit is carried out pin hole processing back water clean up (red bayberry can carry out pin hole handles, and directly water cleans up and gets final product); Then fruit being put into temperature is that 95-100 ℃, mass percent concentration are the aqueous citric acid solution of 0.1-0.2%, soaks 2-5 minute; Then fruit is taken out from aqueous citric acid solution and be cooled to 30-45 ℃;
(2 ') Subcritical Water Extraction: will place extraction kettle through the pretreated fruit of step (1 '), and in extraction kettle, add deionized water then, the addition of deionized water is 20-30 a times of fruit weight, and fruit is fully immersed in the deionized water; The extracting pressure of controlling extraction kettle then is that 5-10Mpa, extraction temperature are that 200-270 ℃, extraction time are 20-60 minute, and fruit is extracted; Extraction finishes the back and opens the relief valve on the extraction kettle; Make the extraction kettle pressure release; And the material in the extraction kettle (this material is the mixture of extract and fruit solid residue) is cooled to 20-25 ℃, and isolate extract then, promptly obtain fruit embryo (being the fruit solid residue).
In the above-mentioned steps (1 '), it is to utilize pin a plurality of apertures in acupuncture on the fruit that fruit is carried out the pin hole processing, and aperture should penetrate the pulp layer from fruit surface usually, is beneficial to the middle deionized water of step (2 ') and is penetrated into fruit internal, and fruit is fully extracted.
The extract that extracts and separate through Subcritical Water Extraction technology contains tannin, volatile oil, flavone compound and the triterpene compound with specific function composition, is the functional new product with high added value, is used in addition after the collection.The isolated extract of above-mentioned steps (2 ') can be handled as follows: extract is rotated evaporation and concentration; Concentrate is gone up the macroreticular resin chromatographic column again and is adsorbed; The alcoholic solution of water, concentration 70-90% is as eluant, eluent successively; With the aldehydes matter separation and concentration, and, freeze drying concentrated through vacuum, extract product obtained.
Because fruit embryo of the present invention is that fruit Subcritical Water Extraction premenstruum (premenstrua) technology removes the solid residue that obtains behind the materials such as tannin, volatile oil, flavone compound, therefore there is not bitter taste, can directly be used for soaking.Therefore, the present invention need not the repeatedly process of " reinforced dipping-drying " of fruit in traditional candied fruits manufacture craft when producing the fruit embryo, simplified processing technology greatly, has shortened the process-cycle, and has reduced the discharging of maceration extract, and reduction is to the pollution of environment.
Above-mentioned sugared material can be a kind of or wherein multiple combination in sucrose, glucose, sorbierite, xylitol, hydroxyl isomaltulose, mannitol, xylo-oligosaccharide, FOS, oligomeric maltose alcohol, glucose syrup and the HFCS.Wherein sucrose, glucose, sorbierite, xylitol, hydroxyl isomaltulose, mannitol, xylo-oligosaccharide, FOS and oligomeric maltose alcohol are solid-state sugar material, and glucose syrup and HFCS are liquid sugar material.
Above-mentioned casting resin can be a kind of or wherein multiple combination in carragheen, xanthans, gum arabic, pectin, guar gum, locust bean gum, tragacanth, tamarind gum, alginic acid, sodium alginate, chitin, carboxymethyl cellulose, sodium carboxymethyl starch, HPMC, microcrystalline cellulose, converted starch, dextrin, cyclodextrin and the pregelatinized starch.The main effect of casting resin is the fruit embryo that fibre structure receives partial destruction to be filled full, replys its original full outward appearance and mouthfeel, and casting resin simultaneously contains nutriments such as dietary fiber, makes candied fruits also possess the function of ease constipation, defaecation and fat-reducing.
Above-mentioned integration of drinking and medicinal herbs class Chinese medicine can be cloves; Chinese anise; Sword bean; Fennel seeds; Field thistle; Chinese yam; Hawthorn; Purslane; Zaocys dhumnade; Dark plum; Pawpaw; Fructus cannabis; Bitter orange flower; Radix polygonati officinalis; Radix Glycyrrhizae; The root of Dahurain angelica; Gingko; Semen Lablab Album; Flos Semen Lablab Album; Arillus longan; Cassia seed; Lily; Nutmeg; Chinese cassia tree; Emblic; Buddha's hand; Almond (comprises dessert almond; Semen armeniacae amarae); Sea-buckthorn; Oyster; Gorgon fruit; Chinese prickly ash; Rde bean; Donkey-hide gelatin; The membrane of a chicken's gizzard; Fructus Hordei Germinatus; Kelp; Jujube (comprises date; Wild jujube; Dateplum persimmon); Momordica grosvenori; Brush-cherry seed; Honeysuckle; Chinese olive; Cordate houttuynia; Ginger (comprises ginger; Rhizoma zingiberis); Hoveniae semoveniae semen; The fruit of Chinese wolfberry; Cape jasmine; Fructus amomi; The sterculia seed; Poria cocos; Citron; Elscholtiza; Peach kernel; Mulberry leaf; Mulberry fruit; Orange; Balloonflower root; Fructus alpiniae oxyphyllae; Lotus leaf; Radish seed; Lotus seeds; Galangal; Lophatherum gracile; Fermented Soybean; Chrysanthemum; Witloof; SEMEN SINAPIS ALBAE; Sealwort; Purple perilla; The purple perilla seed; The root of kudzu vine; Semen sesami nigrum; Black pepper; The sophora bud; Sophora flower; Dandelion; Honey; Chinese torreyanut; Spina date seed; Fresh Rhizoma Imperatae; Fresh Rhizoma Phragmitis; Pallas pit viper; Orange peel; Peppermint; Coix seed; Longstamen Onion Bulb; A kind of or wherein multiple combination in raspberry and the wrinkled giant hyssop.Wherein honey need not to extract in advance, can directly be used for step (3) and join to soak in the cylinder and prepare mixed liquor, perhaps obtains honey solution behind the water dissolving honey, again honey solution is used for step (3) and joins to soak in the cylinder and prepare mixed liquor.
Above-mentioned seasoning and adjusting incense material can be a kind of or wherein multiple combination in citric acid, malic acid, tartaric acid, essence, salt, asccharin, saccharin sodium, honey element, acesulfame potassium, Sucralose, Aspartame, vegetable juice (like Celery Juice, spinach juice) and the fruit syrup (like sweet orange juice, pineapple juice).The seasoning and adjusting incense material can give candied fruits various local flavor.
Foregoing preservatives can be potassium sorbate, benzoic acid or Sodium Benzoate.Anticorrisive agent mainly plays the effect that prolongs the candied fruits shelf-life.
Above-mentioned pigment can be natural colouring matter or synthetic dyestuff, like curcumin, light blue pigment, amaranth pigment, carmine pigment, sodium copper chlorophyllin, lemon yellow pigment, sunset yellow, sunset haematochrome etc.Pigment mainly plays toning, can be according to the odor type of product or custom toning sanctified by usage.
The present invention utilizes fruit remaining fruit embryo after the abstraction function sexual element, in immersion process, adds other nutriment and processes candied fruits, realizes making full use of of fruit resource; The candied fruits of processing has not only kept the original outward appearance of fruit, color and luster and local flavor, and has new functional component after adding other nutriment, comprehensive nutrition, clean taste; And preparation method is simple, and equipment investment is few, and production cost is lower.The present invention optimizes traditional handicraft significantly, can produce multiple different flavor candied fruits product, for comprehensive utilization of resources new technical support, have very strong promotional value.The candied fruits that the present invention makes is old man, pregnant woman, puerpera's a ultimate food, also is children's diatery supplement food, also is fit to very much the mental worker, often to add night shift person edible.
The specific embodiment
Embodiment 1
In the present embodiment, the preparation method of candied fruits comprises the steps: successively
(1) by 100 parts of raw material gross weight; Be equipped with following raw material: 47.5 parts of green plum embryos, 46 parts in sugar material (wherein 20 parts of sucrose, weight percent concentration are 65% glucose syrup 40 parts (glucose syrup is by 26 parts of dries)), 1 part of casting resin (being carboxymethyl cellulose); 3 parts in integration of drinking and medicinal herbs class Chinese medicine (being Momordica grosvenori); 2.1 parts in seasoning and adjusting incense material (wherein 0.1 part of Sucralose, 2 parts of citric acids), 0.3 part of anticorrisive agent (being Sodium Benzoate), 0.1 part of pigment (being sodium copper chlorophyllin);
(2) preliminary treatment of raw material comprises:
(a) solid-state sugar material (the being sucrose) water in the sugar material dissolves (sucrose with after water mixes, is heated to 98 ℃, is beneficial to sucrose and dissolves more fast) fully, and water consumption is 10 times of sucrose weight, obtains liquid glucose;
(b) temperature being used in casting resin is 22 ℃ water logging bubble 4 hours, and water consumption is 20 times of casting resin weight; Be heated to 82 ℃ then, casting resin is dissolved fully, obtain the filling feed liquid;
(c) active ingredient in the extraction Momordica grosvenori obtains Fructus Monordicae extract;
The method for distilling of Momordica grosvenori can adopt conventional decocting method, and its extract is a herb liquid;
(d) water dissolving anticorrisive agent, water consumption is 10 times of anticorrisive agent weight, obtains antiseptic solution;
(3) soak: liquid sugar material (being glucose syrup), seasoning and adjusting incense material and the pigment in the sugar material of step (1) outfit; And step (2) liquid glucose, filling feed liquid, Fructus Monordicae extract and the antiseptic solution that obtain join and soak in the cylinder and mix, and forms mixed liquor; The green plum embryo that then step (1) is equipped with joins to soak in the cylinder and (stirs slightly after adding the green plum embryo, be beneficial to the fruit embryo and in mixed liquor, evenly distribute), and the green plum embryo is fully immersed in the mixed liquor; Temperature with mixed liquor is raised to 55 ℃ then, and is incubated 15 hours;
Soak green plum and whenever stirred the material that soaks in the cylinder between embryonic stage at a distance from 5 hours;
(4) drain: the green plum embryo that immersion is finished takes out and drains;
Drain when handling, the material that soaks in the cylinder is poured in the shaker screen that has filter screen, drain mixed liquor, the green plum embryo is then stayed in the shaker screen; Above-mentioned filter screen adopts 20 purpose filter screens;
(5) drying: adopt natural suning method that the green plum embryo is carried out dried, remove the moisture in the green plum embryo, making the water content of green plum embryo is 12%, obtains candied fruits.
In the present embodiment, the green plum embryo of above-mentioned steps (1) obtains through following step:
(1 ') pretreatment of raw material: with fresh green plum is raw material, green plum is carried out pin hole processing back water clean up; Then green plum being put into temperature is that 95 ℃, mass percent concentration are 0.15% aqueous citric acid solution, soaks 5 minutes; Then green plum is taken out from aqueous citric acid solution and be cooled to 30 ℃;
(2 ') Subcritical Water Extraction: will place extraction kettle through the pretreated green plum of step (1 '), and in extraction kettle, add deionized water then, the addition of deionized water is 30 times of green plum weight, and green plum is fully immersed in the deionized water; The extracting pressure of controlling extraction kettle then is that 5Mpa, extraction temperature are that 270 ℃, extraction time are 40 minutes, and green plum is extracted; Extraction finishes the back and opens the relief valve on the extraction kettle, makes the extraction kettle pressure release, and the material in the extraction kettle (this material is the mixture of extract and green plum solid residue) is cooled to 25 ℃, isolates extract then, promptly obtains green plum embryo (being the green plum solid residue).
In the above-mentioned steps (1 '), it is to utilize pin a plurality of apertures in acupuncture on the green plum that green plum is carried out the pin hole processing, and aperture penetrates the pulp layer from fruit surface, is beneficial to the middle deionized water of step (2 ') and is penetrated into fruit internal, and fruit is fully extracted.
Green plum extract through Subcritical Water Extraction technology is extracted and separated is used after the collection in addition.
Embodiment 2
In the present embodiment, the preparation method of candied fruits comprises the steps: successively
(1) by 100 parts of raw material gross weight; Be equipped with following raw material: 58.55 parts of red bayberry embryos; 32.9 parts in sugar material (weight percent concentration is 47 parts of 70% HFCSs, by 32.9 parts of dries), 1 part of casting resin (wherein 0.5 part of xanthans, 0.5 part of pectin); 5 parts in integration of drinking and medicinal herbs class Chinese medicine (being honey); 2.35 parts in seasoning and adjusting incense material (wherein 0.3 part of acesulfame potassium, 0.05 part of saccharin sodium, 1 part of citric acid, 1 part of malic acid), 0.1 part of anticorrisive agent (being potassium sorbate), 0.1 part of pigment (being the sunset haematochrome);
(2) preliminary treatment of raw material comprises:
(a) temperature being used in casting resin is 25 ℃ water logging bubble 2 hours, and water consumption is 25 times of casting resin weight; Be heated to 80 ℃ then, casting resin is dissolved fully, obtain the filling feed liquid;
(b) water honey dissolving obtains honey solution;
(c) water dissolving anticorrisive agent, water consumption is 15 times of anticorrisive agent weight, obtains antiseptic solution;
(3) soak: liquid sugar material (being HFCS), seasoning and adjusting incense material and pigment in the sugar material that step (1) is equipped with, and step (2) the filling feed liquid, honey solution and the antiseptic solution that obtain join and soak in the cylinder and mix, and forms mixed liquor; The red bayberry embryo that then step (1) is equipped with joins to soak in the cylinder and (stirs slightly after adding the red bayberry embryo, be beneficial to the red bayberry embryo and in mixed liquor, evenly distribute), and the red bayberry embryo is fully immersed in the mixed liquor; Temperature with mixed liquor is raised to 60 ℃ then, and is incubated 12 hours;
Soak red bayberry and whenever stirred the material that soaks in the cylinder between embryonic stage at a distance from 4 hours;
(4) drain: the red bayberry embryo that immersion is finished takes out and drains;
Drain when handling, the material that soaks in the cylinder is poured in the shaker screen that has filter screen, drain mixed liquor, the red bayberry embryo is then stayed in the shaker screen; Above-mentioned filter screen adopts 20 purpose filter screens;
(5) drying: adopt the dehumidifier method that the red bayberry embryo is carried out dried, remove the moisture in the red bayberry embryo, making the water content of red bayberry embryo is 15%, obtains candied fruits.
In the present embodiment, the red bayberry embryo of above-mentioned steps (1) obtains through following step:
(1 ') pretreatment of raw material: with fresh red bayberry is raw material, and water cleans up red bayberry; Then red bayberry being put into temperature is that 98 ℃, mass percent concentration are 0.1% aqueous citric acid solution, soaks 4 minutes; Then red bayberry is taken out from aqueous citric acid solution and be cooled to 35 ℃;
(2 ') Subcritical Water Extraction: will place extraction kettle through the pretreated red bayberry of step (1 '), and in extraction kettle, add deionized water then, the addition of deionized water is 20 times of fruit weight, and red bayberry is fully immersed in the deionized water; The extracting pressure of controlling extraction kettle then is that 7Mpa, extraction temperature are that 250 ℃, extraction time are 20 minutes, and red bayberry is extracted; Extraction finishes the back and opens the relief valve on the extraction kettle, makes the extraction kettle pressure release, and the material in the extraction kettle (this material is the mixture of extract and red bayberry solid residue) is cooled to 20 ℃, isolates extract then, promptly obtains red bayberry embryo (being the red bayberry solid residue).
Red bayberry extract through Subcritical Water Extraction technology is extracted and separated is used after the collection in addition.
Embodiment 3
In the present embodiment, the preparation method of candied fruits comprises the steps: successively
(1) by 100 parts of raw material gross weight; Be equipped with following raw material: 51.3 parts of olive embryos, 47.4 parts in sugar material (wherein 30 parts of sucrose, weight percent concentration are 65% glucose syrup 26.77 parts (glucose syrup is by 17.4 parts of dries)), 0.5 part of casting resin (being gum arabic); 0.5 part in integration of drinking and medicinal herbs class Chinese medicine (being Radix Glycyrrhizae); 0.1 part in seasoning and adjusting incense material (being Sucralose), 0.1 part of anticorrisive agent (being potassium sorbate), 0.1 part of pigment (being sodium copper chlorophyllin);
(2) preliminary treatment of raw material comprises:
(a) solid-state sugar material (the being sucrose) water in the sugar material dissolves (sucrose with after water mixes, is heated to 100 ℃, is beneficial to sucrose and dissolves more fast) fully, and water consumption is 8 times of sucrose weight, obtains liquid glucose;
(b) temperature being used in casting resin is 20 ℃ water logging bubble 5 hours, and water consumption is 15 times of casting resin weight; Be heated to 85 ℃ then, casting resin is dissolved fully, obtain the filling feed liquid;
(c) active ingredient in the extraction Radix Glycyrrhizae obtains licorice;
The method for distilling of Radix Glycyrrhizae can adopt conventional decocting method, and its extract is a herb liquid;
(d) water dissolving anticorrisive agent, water consumption is 20 times of anticorrisive agent weight, obtains antiseptic solution;
(3) soak: liquid sugar material (being glucose syrup), seasoning and adjusting incense material and the pigment in the sugar material of step (1) outfit; And step (2) liquid glucose, filling feed liquid, licorice and the antiseptic solution that obtain join and soak in the cylinder and mix, and forms mixed liquor; The olive embryo that then step (1) is equipped with joins to soak in the cylinder and (stirs slightly after adding the olive embryo, be beneficial to the olive embryo and in mixed liquor, evenly distribute), and the olive embryo is fully immersed in the mixed liquor; Temperature with mixed liquor is raised to 50 ℃ then, and is incubated 15 hours;
Soak olive and whenever stirred the material that soaks in the cylinder between embryonic stage at a distance from 5 hours;
(4) drain: the olive embryo that immersion is finished takes out and drains;
Drain when handling, the material that soaks in the cylinder is poured in the shaker screen that has filter screen, drain mixed liquor, the olive embryo is then stayed in the shaker screen; Above-mentioned filter screen adopts 20 purpose filter screens;
(5) drying: adopt natural suning method that the olive embryo is carried out dried, remove the moisture in the olive embryo, making the water content of olive embryo is 10%, obtains candied fruits.
In the present embodiment, the olive embryo of above-mentioned steps (1) obtains through following step:
(1 ') pretreatment of raw material: with fresh olive is raw material, olive is carried out pin hole processing back water clean up; Then olive being put into temperature is that 100 ℃, mass percent concentration are 0.1% aqueous citric acid solution, soaks 5 minutes; Then olive is taken out from aqueous citric acid solution and be cooled to 45 ℃;
(2 ') Subcritical Water Extraction: will place extraction kettle through the pretreated olive of step (1 '), and in extraction kettle, add deionized water then, the addition of deionized water is 25 times of olive weight, and olive is fully immersed in the deionized water; The extracting pressure of controlling extraction kettle then is that 10Mpa, extraction temperature are that 200 ℃, extraction time are 60 minutes, and olive is extracted; Extraction finishes the back and opens the relief valve on the extraction kettle, makes the extraction kettle pressure release, and the material in the extraction kettle (this material is the mixture of extract and olive solid residue) is cooled to 22 ℃, isolates extract then, promptly obtains olive embryo (being the olive solid residue).
In the above-mentioned steps (1 '), it is to utilize pin a plurality of apertures in acupuncture on the olive that olive is carried out the pin hole processing, and aperture penetrates the pulp layer from the olive surface, is beneficial to the middle deionized water of step (2 ') and is penetrated into olive inside, and olive is fully extracted.
Olive extract through Subcritical Water Extraction technology is extracted and separated is used after the collection in addition.
Embodiment 4
In the present embodiment, the preparation method of candied fruits comprises the steps: successively
(1) by 100 parts of raw material gross weight; Be equipped with following raw material: 41.2 parts of oranges and tangerines embryos, 53 parts (wherein 30 parts of sucrose, 23 parts of FOSs) of sugar material, 3 parts of casting resins (being sodium alginate); 2 parts in integration of drinking and medicinal herbs class Chinese medicine (being peppermint); 0.6 part in seasoning and adjusting incense material (being honey element), 0.1 part of anticorrisive agent (being potassium sorbate), 0.1 part of pigment (being lemon yellow pigment);
(2) preliminary treatment of raw material comprises:
(a) solid-state sugar material (being sucrose, the FOS) water in the sugar material dissolves (solid-state sugar material with after water mixes, is heated to 95 ℃, is beneficial to the dissolving more fast of sugar material) fully, and water consumption is solid-state sugared 5 times of expecting weight, obtains liquid glucose;
(b) temperature being used in casting resin is 20 ℃ water logging bubble 5 hours, and water consumption is 25 times of casting resin weight; Be heated to 84 ℃ then, casting resin is dissolved fully, obtain the filling feed liquid;
(c) active ingredient in the extraction peppermint obtains mint extract;
The method for distilling of peppermint can adopt conventional infusion process, and its extract is a herb liquid;
(d) water dissolving anticorrisive agent, water consumption is 18 times of anticorrisive agent weight, obtains antiseptic solution;
(3) soak: seasoning and adjusting incense material, pigment in the sugar material that step (1) is equipped with, and step (2) liquid glucose, filling feed liquid, mint extract and the antiseptic solution that obtain join and soak in the cylinder and mix, and forms mixed liquor; The oranges and tangerines embryo that then step (1) is equipped with joins to soak in the cylinder and (stirs slightly after adding the oranges and tangerines embryo, be beneficial to the oranges and tangerines embryo and in mixed liquor, evenly distribute), and the oranges and tangerines embryo is fully immersed in the mixed liquor; Temperature with mixed liquor is raised to 60 ℃ then, and is incubated 10 hours;
Soak oranges and tangerines and whenever stirred the material that soaks in the cylinder between embryonic stage at a distance from 4 hours;
(4) drain: the oranges and tangerines embryo that immersion is finished takes out and drains;
Drain when handling, the material that soaks in the cylinder is poured in the shaker screen that has filter screen, drain mixed liquor, the oranges and tangerines embryo is then stayed in the shaker screen; Above-mentioned filter screen adopts 20 purpose filter screens;
(5) drying: adopt natural suning method that the oranges and tangerines embryo is carried out dried, remove the moisture in the oranges and tangerines embryo, making the water content of oranges and tangerines embryo is 14%, obtains candied fruits.
In the present embodiment, the oranges and tangerines embryo of above-mentioned steps (1) obtains through following step:
(1 ') pretreatment of raw material: with fresh oranges and tangerines is raw material, oranges and tangerines is carried out pin hole processing back water clean up; Then oranges and tangerines being put into temperature is that 99 ℃, mass percent concentration are 0.2% aqueous citric acid solution, soaks 2 minutes; Then oranges and tangerines are taken out from aqueous citric acid solution and be cooled to 40 ℃;
(2 ') Subcritical Water Extraction: will place extraction kettle through the pretreated oranges and tangerines of step (1 '), and in extraction kettle, add deionized water then, the addition of deionized water is 22 times of oranges and tangerines weight, and oranges and tangerines are fully immersed in the deionized water; The extracting pressure of controlling extraction kettle then is that 8Mpa, extraction temperature are that 220 ℃, extraction time are 50 minutes, and oranges and tangerines are extracted; Extraction finishes the back and opens the relief valve on the extraction kettle, makes the extraction kettle pressure release, and the material in the extraction kettle (this material is the mixture of extract and citrus solids residue) is cooled to 21 ℃, isolates extract then, promptly obtains oranges and tangerines embryo (being the citrus solids residue).
In the above-mentioned steps (1 '), it is to utilize pin a plurality of apertures in acupuncture on the oranges and tangerines that oranges and tangerines are carried out the pin hole processing, and aperture penetrates the pulp layer from the oranges and tangerines surface, is beneficial to the middle deionized water of step (2 ') and is penetrated into oranges and tangerines inside, and oranges and tangerines are fully extracted.
Oranges and tangerines extract through Subcritical Water Extraction technology is extracted and separated is used after the collection in addition.
Embodiment 5
In the present embodiment, the preparation method of candied fruits comprises the steps: successively
(1) by 100 parts of raw material gross weight; Be equipped with following raw material: 20 parts of green plum embryos, 53.0 parts in sugar material (wherein 33 parts of sorbierites, 20 parts of oligomeric maltose alcohol), 5 parts of casting resins (wherein 2 parts of HPMCs, 3 parts in dextrin); 5 parts in integration of drinking and medicinal herbs class Chinese medicine (wherein 2 parts of chrysanthemums, 2 parts of Momordica grosvenoris, 1 part of emblic); 10 parts in seasoning and adjusting incense material (wherein 2 parts of salt, 5 parts of malic acid, 3 parts of Aspartames), 2.0 parts of anticorrisive agents (being benzoic acid), 5 parts of pigments (being sodium copper chlorophyllin);
(2) preliminary treatment of raw material comprises:
(a) solid-state sugar material (comprising sorbierite and the oligomeric maltose alcohol) water in the sugar material dissolves (solid-state sugar material with after water mixes, is heated to 96 ℃, is beneficial to the sugar material and dissolves more fast) fully, and water consumption is solid-state sugared 10 times of expecting weight, obtains liquid glucose;
(b) temperature being used in casting resin is 24 ℃ water logging bubble 3 hours, and water consumption is 22 times of casting resin weight; Be heated to 81 ℃ then, casting resin is dissolved fully, obtain the filling feed liquid;
(c) active ingredient in the extraction integration of drinking and medicinal herbs class Chinese medicine (comprising chrysanthemum, Momordica grosvenori, emblic) obtains Chinese medical extract;
The method for distilling of integration of drinking and medicinal herbs class Chinese medicine adopts conventional decocting method, and its extract is a herb liquid;
(d) water dissolving anticorrisive agent, water consumption is 16 times of anticorrisive agent weight, obtains antiseptic solution;
(3) soak: seasoning and adjusting incense material and pigment in the sugar material that step (1) is equipped with, and step (2) liquid glucose, filling feed liquid, Chinese medical extract and the antiseptic solution that obtain join and soak in the cylinder and mix, and forms mixed liquor; The green plum embryo that then step (1) is equipped with joins to soak in the cylinder and (stirs slightly after adding the green plum embryo, be beneficial to the green plum embryo and in mixed liquor, evenly distribute), and the green plum embryo is fully immersed in the mixed liquor; Temperature with mixed liquor is raised to 54 ℃ then, and is incubated 14 hours;
Soak green plum and whenever stirred the material that soaks in the cylinder between embryonic stage at a distance from 4 hours;
(4) drain: the fruit embryo that immersion is finished takes out and drains;
Drain when handling, the material that soaks in the cylinder is poured in the shaker screen that has filter screen, drain mixed liquor, the green plum embryo is then stayed in the shaker screen; Above-mentioned filter screen adopts 20 purpose filter screens;
(5) drying: adopt oven drying method that the green plum embryo is carried out dried (bake out temperature is 50 ℃), remove the moisture in the green plum embryo, making the water content of green plum embryo is 11%, obtains candied fruits.
The acquisition methods reference implementation example 1 of the green plum embryo of above-mentioned steps (1).
Embodiment 6
In the present embodiment, the preparation method of candied fruits comprises the steps: successively
(1) by 100 parts of raw material gross weight; Be equipped with following raw material: 67.7 parts of olive embryos; 32.05 parts (wherein 20 parts of xylitols, 12.05 parts of mannitols) of sugar material; 0.1 part of casting resin (being chitin), 0.05 part in seasoning and adjusting incense material (wherein 0.03 part of honey element, 0.02 part in essence), 0.1 part of anticorrisive agent (being Sodium Benzoate);
(2) preliminary treatment of raw material comprises:
(a) solid-state sugar material (comprising xylitol and the mannitol) water in the sugar material dissolves (solid-state sugar material with after water mixes, is heated to 100 ℃, is beneficial to the dissolving more fast of sugar material) fully, and water consumption is solid-state sugared 6 times of expecting weight, obtains liquid glucose;
(b) temperature being used in casting resin is 25 ℃ water logging bubble 3 hours, and water consumption is 22 times of casting resin weight; Be heated to 85 ℃ then, casting resin is dissolved fully, obtain the filling feed liquid;
(c) water dissolving anticorrisive agent, water consumption is 19 times of anticorrisive agent weight, obtains antiseptic solution;
(3) soak: seasoning and adjusting incense material and pigment in the sugar material that step (1) is equipped with, and step (2) liquid glucose, filling feed liquid and the antiseptic solution that obtain join and soak in the cylinder and mix, and forms mixed liquor; The olive embryo that then step (1) is equipped with joins to soak in the cylinder and (stirs slightly after adding the olive embryo, be beneficial to the olive embryo and in mixed liquor, evenly distribute), and the olive embryo is fully immersed in the mixed liquor; Temperature with mixed liquor is raised to 50 ℃ then, and is incubated 15 hours;
Soak olive and whenever stirred the material that soaks in the cylinder between embryonic stage at a distance from 5 hours;
(4) drain: the fruit embryo that immersion is finished takes out and drains;
Drain when handling, the material that soaks in the cylinder is poured in the shaker screen that has filter screen, drain mixed liquor, the olive embryo is then stayed in the shaker screen; Above-mentioned filter screen adopts 20 purpose filter screens;
(5) drying: adopt oven drying method (bake out temperature is 65 ℃) that the olive embryo is carried out dried, remove the moisture in the olive embryo, making the water content of olive embryo is 12%, obtains candied fruits.
The acquisition methods reference implementation example 3 of the olive embryo of above-mentioned steps (1).
In the step of present embodiment 6 (3), also can adopt following method to soak: the honey element that step (1) is equipped with, and step (2) liquid glucose, filling feed liquid and the antiseptic solution that obtain join and soak in the cylinder and mix, and forms mixed liquor; The olive embryo that then step (1) is equipped with joins to soak in the cylinder and (stirs slightly after adding the olive embryo, be beneficial to the olive embryo and in mixed liquor, evenly distribute), and the olive embryo is fully immersed in the mixed liquor; Temperature with mixed liquor is raised to 50 ℃ then, and is incubated 15 hours; Insulation adds essence in the mixed liquor after finishing again, soaks 2-3 hour again; Soak olive and whenever stirred the material that soaks in the cylinder between embryonic stage at a distance from 5 hours.
Though in the foregoing description; Integration of drinking and medicinal herbs class Chinese medicine only provides the example of Momordica grosvenori, honey, Radix Glycyrrhizae, peppermint; But because the function and the effect of various integration of drinking and medicinal herbs class Chinese medicines be well known to those skilled in the art, so those skilled in the art are according to the prompting of the foregoing description, in conjunction with the additional function that need realize of the candied fruits that will make; Can choose integration of drinking and medicinal herbs class Chinese medicine or its combination of corresponding kind fully, produce corresponding candied fruits.
Claims (9)
1. the preparation method of a candied fruits is characterized in that comprising the steps: successively
(1) is equipped with raw material by following weight proportion: fruit embryo 20-67.7%; Sugar material 32.05-53.0%, casting resin 0.1-5%, integration of drinking and medicinal herbs class Chinese medicine 0-5%; Seasoning and adjusting incense material 0.05-10%; Anticorrisive agent 0.1-2.0%, pigment 0-5%, wherein the weight proportion of sugar material is by dry;
(2) preliminary treatment of raw material comprises:
(a) the solid-state sugar material water during sugar is expected dissolves fully, and water consumption is 5-10 a times of solid-state sugar material weight, obtains liquid glucose;
(b) use temperature to steep 2-5 hour as 20-25 ℃ water logging casting resin, water consumption is 15-25 a times of casting resin weight; Be heated to 80-85 ℃ then, casting resin is dissolved fully, obtain the filling feed liquid;
(c) active ingredient in the extraction integration of drinking and medicinal herbs class Chinese medicine obtains Chinese medical extract;
(d) water dissolving anticorrisive agent, water consumption is 10-20 a times of anticorrisive agent weight, obtains antiseptic solution;
(3) soak: liquid sugar material, seasoning and adjusting incense material and pigment in the sugar material that step (1) is equipped with, and step (2) liquid glucose, filling feed liquid, Chinese medical extract and the antiseptic solution that obtain join and soak in the cylinder and mix, and forms mixed liquor; The fruit embryo that then step (1) is equipped with joins and soaks in the cylinder, and the fruit embryo is fully immersed in the mixed liquor; Temperature with mixed liquor is raised to 50-60 ℃ then, and is incubated 10-15 hour;
(4) drain: the fruit embryo that immersion is finished takes out and drains;
(5) drying: remove the moisture in the fruit embryo, making the water content of fruit embryo is 10-15%, obtains candied fruits.
2. the preparation method of candied fruits according to claim 1, it is characterized in that: the fruit embryo of step (1) obtains through following step:
(1 ') pretreatment of raw material: with fresh fruit is raw material, fruit is carried out pin hole processing back water clean up; Then fruit being put into temperature is that 95-100 ℃, mass percent concentration are the aqueous citric acid solution of 0.1-0.2%, soaks 2-5 minute; Then fruit is taken out from aqueous citric acid solution and be cooled to 30-45 ℃;
(2 ') Subcritical Water Extraction: will place extraction kettle through the pretreated fruit of step (1 '), and in extraction kettle, add deionized water then, the addition of deionized water is 20-30 a times of fruit weight, and fruit is fully immersed in the deionized water; The extracting pressure of controlling extraction kettle then is that 5-10Mpa, extraction temperature are that 200-270 ℃, extraction time are 20-60 minute, and fruit is extracted; Extraction finishes the back and opens the relief valve on the extraction kettle, makes the extraction kettle pressure release, and the material in the extraction kettle is cooled to 20-25 ℃, isolates extract then, promptly obtains the fruit embryo.
3. the preparation method of candied fruits according to claim 1 and 2 is characterized in that: in the step (3), soak the material that fruit stirred in the immersion cylinder between embryonic stage in every separated 4-5 hour.
4. the preparation method of candied fruits according to claim 1 and 2 is characterized in that: in the step (4), drain when handling, the material that soaks in the cylinder is poured in the shaker screen that has filter screen, drain mixed liquor, the fruit embryo is stayed in the shaker screen.
5. the preparation method of candied fruits according to claim 1 and 2 is characterized in that: said sugar material is a kind of or wherein multiple combination in sucrose, glucose, sorbierite, xylitol, hydroxyl isomaltulose, mannitol, xylo-oligosaccharide, FOS, oligomeric maltose alcohol, glucose syrup and the HFCS.
6. the preparation method of candied fruits according to claim 1 and 2, it is characterized in that: said casting resin is a kind of or wherein multiple combination in carragheen, xanthans, gum arabic, pectin, guar gum, locust bean gum, tragacanth, tamarind gum, alginic acid, sodium alginate, chitin, carboxymethyl cellulose, sodium carboxymethyl starch, HPMC, microcrystalline cellulose, converted starch, dextrin, cyclodextrin and the pregelatinized starch.
7. the preparation method of candied fruits according to claim 1 and 2 is characterized in that: said integration of drinking and medicinal herbs class Chinese medicine is a kind of or wherein multiple combination in cloves, Chinese anise, sword bean, fennel seeds, field thistle, Chinese yam, hawthorn, purslane, zaocys dhumnade, dark plum, pawpaw, fructus cannabis, bitter orange flower, radix polygonati officinalis, Radix Glycyrrhizae, the root of Dahurain angelica, gingko, Semen Lablab Album, Flos Semen Lablab Album, arillus longan, cassia seed, lily, nutmeg, Chinese cassia tree, emblic, Buddha's hand, almond, sea-buckthorn, oyster, Gorgon fruit, Chinese prickly ash, rde bean, donkey-hide gelatin, the membrane of a chicken's gizzard, Fructus Hordei Germinatus, kelp, jujube, Momordica grosvenori, brush-cherry seed, honeysuckle, Chinese olive, cordate houttuynia, ginger, hoveniae semoveniae semen, the fruit of Chinese wolfberry, cape jasmine, fructus amomi, the sterculia seed, Poria cocos, citron, elscholtiza, peach kernel, mulberry leaf, mulberry fruit, orange, balloonflower root, fructus alpiniae oxyphyllae, lotus leaf, radish seed, lotus seeds, galangal, lophatherum gracile, Fermented Soybean, chrysanthemum, witloof, SEMEN SINAPIS ALBAE, sealwort, purple perilla, purple perilla seed, the root of kudzu vine, Semen sesami nigrum, black pepper, the sophora bud, sophora flower, dandelion, honey, Chinese torreyanut, spina date seed, fresh Rhizoma Imperatae, fresh Rhizoma Phragmitis, pallas pit viper, orange peel, peppermint, coix seed, Longstamen Onion Bulb, raspberry and the wrinkled giant hyssop.
8. the preparation method of candied fruits according to claim 1 and 2, it is characterized in that: said seasoning and adjusting incense material is a kind of or wherein multiple combination in citric acid, malic acid, tartaric acid, essence, salt, asccharin, saccharin sodium, honey element, acesulfame potassium, Sucralose, Aspartame, vegetable juice and the fruit syrup.
9. the preparation method of candied fruits according to claim 1 and 2, it is characterized in that: said anticorrisive agent is potassium sorbate, benzoic acid or Sodium Benzoate.
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Address after: Room 602, Management Committee Building of Jinping Science and Technology Park, University Road, Shantou City, Guangdong Province Co-patentee after: Jiangnan University Patentee after: Shantou City Tianyue Light Industry Technology Co., Ltd. Co-patentee after: Guangdong Fuwei Health Technology Co., Ltd. Co-patentee after: Shantou Maohuat Foodstuffs Co., Ltd. Address before: Room 602, Management Committee Building of Jinping Science and Technology Park, University Road, Shantou City, Guangdong Province Co-patentee before: Jiangnan University Patentee before: Shantou City Tianyue Light Industry Technology Co., Ltd. Co-patentee before: Fuwei Food Stuff Factory Co., Ltd., Guangdong Prov. Co-patentee before: Shantou Maohuat Foodstuffs Co., Ltd. |