CN102531038B - 一种浅色棒状zao导电粉体的制备方法 - Google Patents
一种浅色棒状zao导电粉体的制备方法 Download PDFInfo
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- CN102531038B CN102531038B CN 201210042647 CN201210042647A CN102531038B CN 102531038 B CN102531038 B CN 102531038B CN 201210042647 CN201210042647 CN 201210042647 CN 201210042647 A CN201210042647 A CN 201210042647A CN 102531038 B CN102531038 B CN 102531038B
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- zao
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- zinc
- calcining
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- 239000000843 powder Substances 0.000 title claims abstract description 22
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 title abstract description 7
- 229910000611 Zinc aluminium Inorganic materials 0.000 title abstract description 3
- 238000001354 calcination Methods 0.000 claims abstract description 22
- 238000001027 hydrothermal synthesis Methods 0.000 claims abstract description 17
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims abstract description 15
- 229910052725 zinc Inorganic materials 0.000 claims abstract description 15
- 239000002243 precursor Substances 0.000 claims abstract description 13
- 239000011701 zinc Substances 0.000 claims abstract description 12
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229910052782 aluminium Inorganic materials 0.000 claims abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 238000006243 chemical reaction Methods 0.000 claims abstract description 7
- 238000003756 stirring Methods 0.000 claims abstract description 7
- 238000001035 drying Methods 0.000 claims abstract description 5
- 239000004411 aluminium Substances 0.000 claims abstract description 4
- NSOXQYCFHDMMGV-UHFFFAOYSA-N Tetrakis(2-hydroxypropyl)ethylenediamine Chemical compound CC(O)CN(CC(C)O)CCN(CC(C)O)CC(C)O NSOXQYCFHDMMGV-UHFFFAOYSA-N 0.000 claims description 6
- 238000005119 centrifugation Methods 0.000 claims description 6
- 238000001556 precipitation Methods 0.000 claims description 6
- LZZYPRNAOMGNLH-UHFFFAOYSA-M Cetrimonium bromide Chemical compound [Br-].CCCCCCCCCCCCCCCC[N+](C)(C)C LZZYPRNAOMGNLH-UHFFFAOYSA-M 0.000 claims description 5
- 239000007858 starting material Substances 0.000 claims description 3
- 230000035484 reaction time Effects 0.000 claims description 2
- ONDPHDOFVYQSGI-UHFFFAOYSA-N zinc nitrate Chemical group [Zn+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ONDPHDOFVYQSGI-UHFFFAOYSA-N 0.000 claims 2
- BNGXYYYYKUGPPF-UHFFFAOYSA-M (3-methylphenyl)methyl-triphenylphosphanium;chloride Chemical group [Cl-].CC1=CC=CC(C[P+](C=2C=CC=CC=2)(C=2C=CC=CC=2)C=2C=CC=CC=2)=C1 BNGXYYYYKUGPPF-UHFFFAOYSA-M 0.000 claims 1
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 claims 1
- 239000000463 material Substances 0.000 abstract description 14
- 239000011858 nanopowder Substances 0.000 abstract description 7
- 238000000034 method Methods 0.000 abstract description 3
- PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 230000007547 defect Effects 0.000 abstract 1
- 238000004377 microelectronic Methods 0.000 abstract 1
- 230000003647 oxidation Effects 0.000 abstract 1
- 238000007254 oxidation reaction Methods 0.000 abstract 1
- 230000001105 regulatory effect Effects 0.000 abstract 1
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 8
- 230000005540 biological transmission Effects 0.000 description 4
- 239000011787 zinc oxide Substances 0.000 description 4
- 238000005054 agglomeration Methods 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 239000002105 nanoparticle Substances 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 238000000975 co-precipitation Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000009841 combustion method Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 230000001143 conditioned effect Effects 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 230000002596 correlated effect Effects 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 239000012767 functional filler Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 235000015110 jellies Nutrition 0.000 description 1
- 239000008274 jelly Substances 0.000 description 1
- 239000005344 low-emissivity glass Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000002086 nanomaterial Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 239000006104 solid solution Substances 0.000 description 1
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- Inorganic Compounds Of Heavy Metals (AREA)
Abstract
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CN 201210042647 CN102531038B (zh) | 2012-02-23 | 2012-02-23 | 一种浅色棒状zao导电粉体的制备方法 |
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CN 201210042647 CN102531038B (zh) | 2012-02-23 | 2012-02-23 | 一种浅色棒状zao导电粉体的制备方法 |
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CN102531038A CN102531038A (zh) | 2012-07-04 |
CN102531038B true CN102531038B (zh) | 2013-12-25 |
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CN106702534A (zh) * | 2016-11-18 | 2017-05-24 | 江南大学 | 一种掺铝氧化锌(azo)中空纳米纤维的制备方法 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101665237A (zh) * | 2009-09-30 | 2010-03-10 | 西北稀有金属材料研究院 | 球形铝掺杂氧化锌纳米粉体的制备方法 |
CN101857428A (zh) * | 2010-05-21 | 2010-10-13 | 华东理工大学 | 一种导电氧化锌粉体的制备方法 |
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- 2012-02-23 CN CN 201210042647 patent/CN102531038B/zh not_active Expired - Fee Related
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN101665237A (zh) * | 2009-09-30 | 2010-03-10 | 西北稀有金属材料研究院 | 球形铝掺杂氧化锌纳米粉体的制备方法 |
CN101857428A (zh) * | 2010-05-21 | 2010-10-13 | 华东理工大学 | 一种导电氧化锌粉体的制备方法 |
Non-Patent Citations (4)
Title |
---|
Shoucang Shen et al..Simple hydrothermal synthesis of nanostructured and nanorod Zn–Al complex oxides as novel nanocatalysts.《Advanced Materials》.2004,第16卷(第6期),第541-545页. |
Simple hydrothermal synthesis of nanostructured and nanorod Zn–Al complex oxides as novel nanocatalysts;Shoucang Shen et al.;《Advanced Materials》;20040318;第16卷(第6期);第541-545页 * |
导电ZAO纳米晶的超声-模板法合成、表征及应用;罗重霄等;《物理化学学报》;20080630;第24卷(第6期);第1007-1011页 * |
罗重霄等.导电ZAO纳米晶的超声-模板法合成、表征及应用.《物理化学学报》.2008,第24卷(第6期),第1007-1011页. |
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Inventor after: Liu Jinku Inventor after: Wang Shihui Inventor after: Wang Jing Inventor after: Luo Zhongxiao Inventor after: Zhang Naiqian Inventor after: Wang Rong Inventor after: Tong Qin Inventor after: Liu Chang Inventor before: Liu Jinku Inventor before: Wang Shihui Inventor before: Wang Jing Inventor before: Luo Zhongxiao Inventor before: Zhang Naiqian Inventor before: Wang Rong |
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Application publication date: 20120704 Assignee: Shanghai tongue Science and Technology Ltd. Assignor: East China University of Science and Technology Contract record no.: 2014310000120 Denomination of invention: Preparation method of light color rodlike ZAO (Zinc Aluminium Oxide) conductive powder Granted publication date: 20131225 License type: Exclusive License Record date: 20140703 |
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