CN102512353A - Dictyophora indusiata water extract and preparation method and application thereof - Google Patents
Dictyophora indusiata water extract and preparation method and application thereof Download PDFInfo
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- CN102512353A CN102512353A CN2011104439724A CN201110443972A CN102512353A CN 102512353 A CN102512353 A CN 102512353A CN 2011104439724 A CN2011104439724 A CN 2011104439724A CN 201110443972 A CN201110443972 A CN 201110443972A CN 102512353 A CN102512353 A CN 102512353A
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Abstract
The invention discloses a Dictyophora indusiata water extract and a preparation method and application thereof. The preparation method comprises the following steps of: (1) mixing Dictyophora indusiata powder and deionized water, and performing ultrasonic extraction to obtain an extracting solution; (2) standing and precipitating the extracting solution, and filtering to obtain a recovered solution; (3) concentrating the recovered solution to obtain a concentrated solution; and (4) adding dextrin into the concentrated solution, stirring uniformly, and freeze-drying to obtain a product. The preparation method is easy to operate and is low in production cost; the obtained Dictyophora indusiata water extract is high in purity and high in yield; the Dictyophora indusiata water extract can be powdered easily, and is light yellow or yellow; and a cosmetic product prepared by using the Dictyophora indusiata water extract has a remarkable anti-aging effect and a more remarkable moisturizing effect.
Description
Technical field
The present invention relates to a kind of Caulis Bambusae In Taeniam water extract and preparation method thereof and application, be specifically related to preserve moisture in a kind of Caulis Bambusae In Taeniam and defying age effective ingredient and preparation method thereof and application.
Background technology
Caulis Bambusae In Taeniam (Dictyophora indusiata) is that pen terrible section (Phallaceae) Caulis Bambusae In Taeniam belongs to (Dictyophora) fungus; Have another name called bamboo fungus, bamboo ginseng, grenadine bacterium etc.; Be having concurrently of a kind of preciousness dual-purpose fungus edible and medical value, mainly be distributed in areas such as Yunnan, Sichuan, Hunan, Fujian and three provinces in the northeast of China in China.
Caulis Bambusae In Taeniam is a kind of famous and precious edible fungi; Be rich in multiple quality plant nutrient protein; Protein content is high and contain a complete set of aminoacid of constitutive protein matter, and wherein essential amino acids content accounts for more than 1/3 of total amino acids, surpasses corn and some meat; Glutamic is the abundantest, accounts for more than 17.0% of total amino acid content.The sporophore palatable crisp of Caulis Bambusae In Taeniam, aromatic flavor, delicious flavour, other tool local flavor have " queen in the bacterium ", " king's of delicacy from mountain " laudatory title.Caulis Bambusae In Taeniam belongs to physiological alkalinity food, can regulate the content of hematic acid and fatty acid in the human body, and the hypotensive activity effect is obvious, and Caulis Bambusae In Taeniam can also reduce the body inner cholesterol, reduce stomach wall fat stores up.The highly active macromolecular substances polysaccharide component that is contained in the Caulis Bambusae In Taeniam has curative effects such as the tumor of inhibition, anticoagulation, anti-inflammatory, immune stimulatory and blood sugar lowering, and AIDS is also had inhibitory action.The effective ingredient that contains in the Caulis Bambusae In Taeniam is also better to the beautifying whitening effect.
Research to Caulis Bambusae In Taeniam at present focuses mostly at the extraction and the aspects such as zymocyte and sporophore nutritional labeling of liquid culture condition, polysaccharide; In recent years along with the Caulis Bambusae In Taeniam extract antidotal efficacy study of preserving moisture; Caulis Bambusae In Taeniam becomes the source material of fashion cosmetics effective ingredient gradually; But do not find to produce the effective means of Caulis Bambusae In Taeniam extract at present as yet, adopt the preparation method of conventional medicine and cosmetics effective ingredient to be difficult to obtain fine, as to meet cosmetics specification requirement standard Caulis Bambusae In Taeniam material.
Summary of the invention
The purpose of this invention is to provide a kind of Caulis Bambusae In Taeniam water extract and preparation method thereof and application.
The method for preparing of a kind of Caulis Bambusae In Taeniam water extract provided by the invention comprises the steps:
(1) the Caulis Bambusae In Taeniam powder is mixed with deionized water after supersound extraction gets extracting solution;
(2) said extracting solution through staticly settling after filter and obtain reclaiming liquid;
(3) concentrate said recovery liquid and get concentrated solution;
(4) in said concentrated solution, add dextrin, and stir after lyophilization promptly gets product.
In the above-mentioned method for preparing, in the step (1), the granularity of said Caulis Bambusae In Taeniam powder can be 40 orders～80 orders, like 40 orders or 80 orders; The ratio of quality and the number of copies of said Caulis Bambusae In Taeniam powder and deionized water can be 1: (30～60), and as 1: 30 or 1: 60.
In the above-mentioned method for preparing, in the step (1), the temperature of said supersound extraction can be 50 ℃～100 ℃, specifically can be 50 ℃ or 100 ℃, and frequency can be 20～150KHZ, specifically can be 20KHZ or 150KHZ, and the time can be 0.5h～5h, specifically can be 0.5h or 5h; Said supersound extraction specifically can be carried out in tank body formula supersound extraction equipment or duct type cylindrical shell supersound extraction equipment.
In the above-mentioned method for preparing, in the step (2), the said time that staticly settles can be 0.5h～1h, specifically can be 0.5h or 1h; In the step (3), said spissated temperature can be 70 ℃～80 ℃, specifically can be 70 ℃ or 80 ℃, and the ratio of quality and the number of copies of said concentrated solution and said recovery liquid can be 1: (4～6) specifically can be 1: 4 or 1: 6.
In the above-mentioned method for preparing, in the step (4), the ratio of quality and the number of copies of soluble solid can be 1 in said dextrin and the said concentrated solution: (2～3) specifically can be 1: 2 or 1: 3; Specifically can adopt digital refractometer to measure the content of soluble solid in the said concentrated solution.
In the above-mentioned method for preparing, in the step (4), said lyophilization step can be carried out in vacuum freeze drier; Said cryodesiccated temperature can be-70 ℃, and the time can be 8h～24h, specifically can be 8h or 24h.
The present invention also provides the Caulis Bambusae In Taeniam water extract of method for preparing.
The present invention also further provides the application of above-mentioned Caulis Bambusae In Taeniam water extract in the preparation cosmetics, and these cosmetics have defying age and the effect of preserving moisture.
Method for preparing provided by the invention is simple to operate, and production cost is low, and the Caulis Bambusae In Taeniam water extract that obtains has higher purity, and productive rate is high; Caulis Bambusae In Taeniam water extract provided by the invention becomes powder easily, and it is faint yellow or yellow that color is; The cosmetic product of Caulis Bambusae In Taeniam water extract preparation provided by the invention has tangible defying age effect, and moistening effect is more remarkable.
Description of drawings
Fig. 1 is the process chart of the embodiment of the invention 1 preparation Caulis Bambusae In Taeniam water extract.
Fig. 2 is the Caulis Bambusae In Taeniam water extract photo of the embodiment of the invention 1 preparation.
Fig. 3 is the change curve of experimental group and blank control group hydration rate in the embodiment of the invention 1.
Fig. 4 is the change curve of experimental group and blank control group percentage of water loss in the embodiment of the invention 1.
Fig. 5 is the clearance rate curve of the ultra-oxygen anion free radical of variable concentrations Caulis Bambusae In Taeniam water extract aqueous solution in the embodiment of the invention 2.
The specific embodiment
Employed experimental technique is conventional method like no specified otherwise among the following embodiment.
Used material, reagent etc. like no specified otherwise, all can obtain from commercial sources among the following embodiment.
The preparation of embodiment 1, Caulis Bambusae In Taeniam water extract and moisture-keeping efficacy test
1, preparation Caulis Bambusae In Taeniam water extract
Present embodiment prepares Caulis Bambusae In Taeniam water, and to get the process chart of thing as shown in Figure 1.
1) preparation sample: 80 mesh sieves are also crossed in Caulis Bambusae In Taeniam pulverizing (disintegrating apparatus: multifunctional crusher GX-04, Gao Xiang, Shanghai food machinery factory) obtained powder, place aeration-drying place to preserve, subsequent use, take by weighing Caulis Bambusae In Taeniam powder 100g;
2) supersound extraction: is that 1: 30 mixed stirs with Caulis Bambusae In Taeniam powder and the deionized water of preparation with ratio of quality and the number of copies; (firing equipment: electric heater 98-1-B type adjusts the temperature electronically to place 50 ℃ of conditions; Tianjin Tai Site Instr Ltd.) supersound extraction (ultrasonic device adopts tank body formula supersound extraction equipment) 5h gets extracting solution down, and supersonic frequency is 20KHZ;
4) deposition sucking filtration: extracting solution is staticly settled 0.5h, carry out sucking filtration (pumping and filtering device: SHZ-III type circulation ability of swimming use vacuum pump, Shanghai know reliable test Instr Ltd.) with filter plate more and obtain reclaiming liquid;
5) concentrate: 400g is reclaimed liquid place concentrated (concentrator: rotary evaporator RE2000 type under 80 ℃ of conditions; Shanghai Yarong Biochemical Instrument Plant) to the 100g concentrated solution; Wherein concentrated solution is 1: 4 with the ratio of quality and the number of copies that reclaims liquid, and employing contains admittedly, and soluble solid content is 8% in appearance (the digital refractometer PR-101 of ATAGO α) the mensuration concentrated solution;
6) add dextrin: in concentrated solution, add 2 times of dextrin 16g and get mixed liquor to the soluble solid quality; Mixed liquor is stirred, fully after the dissolving, place-70 ℃ of vacuum freezing 8h of vacuum freeze drier (U.S. VIRTIS company); Obtain Caulis Bambusae In Taeniam powdery water extract, as shown in Figure 2.
2, the moisture-keeping efficacy of the Caulis Bambusae In Taeniam water extract of above-mentioned preparation test
Human test's mode is all adopted in following various moisture-keeping efficacy test, measures the moisture and the aqueous dispersion vector (being the TEWL value) of skin with moisture tester; Choose 30 volunteers, the men and women half and half.
(1) moisture of Caulis Bambusae In Taeniam water extract and hydration rate change
Experimental group is the aqueous solution of the Caulis Bambusae In Taeniam water extract of embodiment 1 preparation, and the quality percentage composition is 8%;
Blank control group is a deionized water;
Moisture content change was reflected in test period, Experimental Area moisture change with time.Its value is big more, and moisture is big more, otherwise moisture is more little.
Moisture difference (Δ T)=each time point moisture (Th) of use back-initial moisture (T0).
The moisture difference of table 1 Caulis Bambusae In Taeniam water extract
Use and compare with blank control group after 1 hour, the moisture of experimental group obviously increases; In 4 hours test periods, the moisture of experimental group is higher than blank control group always.
Hydration rate=(using each time point moisture of back-initial moisture)/initial moisture; Then the hydration rate change curve of experimental group and blank control group is as shown in Figure 3; Can be known that by this figure the hydration rate of blank control group changes relatively stable, experimental group is after sample uses 1 hour; Its hydration rate is apparently higher than blank control group, and the hydration rate of experimental group is higher than blank control group always in 4 hours.
(2) the moisture loss situation of Caulis Bambusae In Taeniam water extract
Experimental group is the aqueous solution of the Caulis Bambusae In Taeniam water extract of embodiment 1 preparation, and the quality percentage composition is 8%;
Blank control group is a deionized water;
The moisture loss variation is reflected in test period Experimental Area moisture loss change with time.Its value is more little, and moisture loss is few more, and the lock outlet capacity is strong more; Otherwise, the lock outlet capacity more a little less than.
Fluid loss difference (Δ T)=each time point aqueous dispersion vector (Th) of use back-initial aqueous dispersion vector (T0).
The fluid loss difference of table 2 Caulis Bambusae In Taeniam water extract
Use and compare with blank control group after 1 hour, the aqueous dispersion vector of experimental group obviously reduces; In 4 hours test periods, the fluid loss of experimental group is lower than blank control group always.
Percentage of water loss=(using each time point aqueous dispersion vector of back-initial aqueous dispersion vector)/initial aqueous dispersion vector, this value is more little, explains that moisture loss is few more, and test specimen lock water effect is obvious more; The percentage of water loss change curve of experimental group and blank control group is as shown in Figure 4, can be known by this figure, is tried the position and smears sample after 1 hour, and the percentage of water loss of experimental group is starkly lower than blank control group; In 4 hours test periods, the percentage of water loss of experimental group is lower than blank control group always, and is negative value always; Experimental group is compared with blank control group, and instant lock water effect is arranged, and it is good to continue the lock outlet capacity.
The preparation of embodiment 2, Caulis Bambusae In Taeniam water extract and senile-resistant efficacy test
1, preparation Caulis Bambusae In Taeniam water extract
1) preparation sample: 40 mesh sieves are also crossed in Caulis Bambusae In Taeniam pulverizing (disintegrating apparatus: multifunctional crusher GX-04, Gao Xiang, Shanghai food machinery factory) obtained powder, place aeration-drying place to preserve, subsequent use, take by weighing Caulis Bambusae In Taeniam powder 100g;
2) supersound extraction: is that 1: 60 mixed stirs with Caulis Bambusae In Taeniam powder and the deionized water of preparation with ratio of quality and the number of copies; (firing equipment: electric heater 98-1-B type adjusts the temperature electronically to place 100 ℃ of conditions; Tianjin Tai Site Instr Ltd.) supersound extraction (ultrasonic device adopts duct type cylindrical shell supersound extraction equipment) 0.5h gets extracting solution down, and supersonic frequency is 150KHZ;
4) deposition sucking filtration: extracting solution is staticly settled 1.0h, carry out sucking filtration (pumping and filtering device: SHZ-III type circulation ability of swimming use vacuum pump, Shanghai know reliable test Instr Ltd.) with filter plate more and obtain reclaiming liquid;
5) concentrate: 600g is reclaimed liquid place concentrated (concentrator: rotary evaporator RE2000 type under 70 ℃ of conditions; Shanghai Yarong Biochemical Instrument Plant) to the 100g concentrated solution; Wherein concentrated solution is 1: 6 with the ratio of quality and the number of copies that reclaims liquid, and employing contains admittedly, and soluble solid content is 12% in appearance (the digital refractometer PR-101 of ATAGO α) the mensuration concentrated solution;
6) add dextrin: in concentrated solution, add 3 times of dextrin 36g and get mixed liquor to the soluble solid quality; Mixed liquor is stirred; Fully after the dissolving, place-70 ℃ of vacuum freezing 24h of vacuum freeze drier (U.S. VIRTIS company), obtain Caulis Bambusae In Taeniam powdery water extract.
2, the senile-resistant efficacy test-removing ultra-oxygen anion free radical of the Caulis Bambusae In Taeniam water extract of above-mentioned preparation experiment
Get the Tris-HCl buffer 4.5ml of 0.05mol/L pH 8.2; Place 25 ℃ of water-bath preheating 20min, add Caulis Bambusae In Taeniam water extract lyophilized powder aqueous solution and the pyrogallol solution of 0.4ml 25mmol/L of the above-mentioned preparation of 1ml variable concentrations respectively, in 25 ℃ of water-baths, react 5min behind the mixing; The HCl cessation reaction that adds 1.0ml 8mol/L; Make reference with the Tris-HCl buffer, measure absorbance at the 299nm place, calculate clearance rate.
The blank group replaces sample with the 1ml deionized water, and each is handled and all does three repetitions.
The computing formula of clearance rate: ultra-oxygen anion free radical clearance rate (%)=100 (A1-A2)/A1, wherein A1 is the mean light absorbency of blank, A2 is the mean light absorbency of lyophilized powder aqueous solution.
The Caulis Bambusae In Taeniam water extraction lyophilized powder of above-mentioned preparation is as shown in Figure 5 to the scavenging action result of ultra-oxygen anion free radical; The result shows that Caulis Bambusae In Taeniam water extraction lyophilized powder concentration is at 40% o'clock, and the clearance rate of ultra-oxygen anion free radical is 49.2%, explains that Caulis Bambusae In Taeniam water extraction lyophilized powder has the effect of slow down aging.
Claims (9)
1. the method for preparing of a Caulis Bambusae In Taeniam water extract comprises the steps:
(1) the Caulis Bambusae In Taeniam powder is mixed with deionized water after supersound extraction gets extracting solution;
(2) said extracting solution through staticly settling after filter and obtain reclaiming liquid;
(3) concentrate said recovery liquid and get concentrated solution;
(4) in said concentrated solution, add dextrin, and stir after lyophilization promptly gets product.
2. method according to claim 1 is characterized in that: in the step (1), the granularity of said Caulis Bambusae In Taeniam powder is 40 orders～80 orders; The ratio of quality and the number of copies of said Caulis Bambusae In Taeniam powder and deionized water is 1: (30～60).
3. method according to claim 1 and 2 is characterized in that: in the step (1), the temperature of said supersound extraction is 50 ℃～100 ℃, and frequency is 20～150KHZ, and the time is 0.5h～5h; Said supersound extraction is carried out in tank body formula supersound extraction equipment or duct type cylindrical shell supersound extraction equipment.
4. according to arbitrary described method among the claim 1-3, it is characterized in that: in the step (2), the said time that staticly settles is 0.5h～1h; In the step (3), said spissated temperature is 70 ℃～80 ℃, and the ratio of quality and the number of copies of said concentrated solution and said recovery liquid is 1: (4～6).
5. according to arbitrary described method among the claim 1-4, it is characterized in that: in the step (4), the ratio of quality and the number of copies of soluble solid is 1 in said dextrin and the said concentrated solution: (2～3); Measure the content of soluble solid in the said concentrated solution with digital refractometer.
6. according to arbitrary described method among the claim 1-5, it is characterized in that: in the step (4), said lyophilization step is carried out in vacuum freeze drier; Said cryodesiccated temperature is-70 ℃, and the time is 8h～24h.
7. the Caulis Bambusae In Taeniam water extract that arbitrary said method prepares among the claim 1-6.
8. the application of the said Caulis Bambusae In Taeniam water extract of claim 7 in the preparation cosmetics.
9. cosmetics comprise the described Caulis Bambusae In Taeniam water extract of claim 7.
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103720634A (en) * | 2012-10-16 | 2014-04-16 | 李丹榕 | Facial cleanser |
| KR20140081984A (en) * | 2012-12-21 | 2014-07-02 | 주식회사 뉴메디온 | A skin-care agent containig Dictyophora indusiata fruit body extract or Dictyophora indusiata mycelium extract |
| JP2015020997A (en) * | 2013-07-23 | 2015-02-02 | 日本メナード化粧品株式会社 | Stem cell-derived growth factor production promoter |
| CN105250209A (en) * | 2014-07-18 | 2016-01-20 | 上海家化联合股份有限公司 | Deep fermentation dictyophora indusiata mycelium preparation and applications of deep fermentation dictyophora indusiata mycelium in cosmetics |
| CN105534801A (en) * | 2016-01-07 | 2016-05-04 | 福建农林大学 | Moistening lipstick containing bamboo fungus extract and preparing method of moistening lipstick |
| CN111357976A (en) * | 2019-10-06 | 2020-07-03 | 杏辉天力（杭州）药业有限公司 | Dictyophora indusiata extract and industrial preparation method and application thereof |
| CN112137919A (en) * | 2020-08-06 | 2020-12-29 | 西安交通大学 | Beauty external product or edible product based on bamboo fungus egg extract and application |
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| CN1165148A (en) * | 1996-05-10 | 1997-11-19 | 中国科学院大连化学物理研究所 | Method for preparing dictyophora fungus polysaccharide |
| CN102258448A (en) * | 2010-05-28 | 2011-11-30 | 贾简华 | Skincare cream, its preparation and healthcare treatment |
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2011
- 2011-12-27 CN CN 201110443972 patent/CN102512353B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1165148A (en) * | 1996-05-10 | 1997-11-19 | 中国科学院大连化学物理研究所 | Method for preparing dictyophora fungus polysaccharide |
| CN102258448A (en) * | 2010-05-28 | 2011-11-30 | 贾简华 | Skincare cream, its preparation and healthcare treatment |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103720634A (en) * | 2012-10-16 | 2014-04-16 | 李丹榕 | Facial cleanser |
| KR20140081984A (en) * | 2012-12-21 | 2014-07-02 | 주식회사 뉴메디온 | A skin-care agent containig Dictyophora indusiata fruit body extract or Dictyophora indusiata mycelium extract |
| KR102101950B1 (en) * | 2012-12-21 | 2020-04-28 | 주식회사 코씨드바이오팜 | A skin-care agent or cosmetics containig Dictyophora indusiata fruit body extract or Dictyophora indusiata mycelium extract |
| JP2015020997A (en) * | 2013-07-23 | 2015-02-02 | 日本メナード化粧品株式会社 | Stem cell-derived growth factor production promoter |
| CN105250209A (en) * | 2014-07-18 | 2016-01-20 | 上海家化联合股份有限公司 | Deep fermentation dictyophora indusiata mycelium preparation and applications of deep fermentation dictyophora indusiata mycelium in cosmetics |
| CN105534801A (en) * | 2016-01-07 | 2016-05-04 | 福建农林大学 | Moistening lipstick containing bamboo fungus extract and preparing method of moistening lipstick |
| CN105534801B (en) * | 2016-01-07 | 2018-06-15 | 福建农林大学 | A kind of moist lipstick containing Caulis Bambusae In Taeniam extract and preparation method thereof |
| CN111357976A (en) * | 2019-10-06 | 2020-07-03 | 杏辉天力（杭州）药业有限公司 | Dictyophora indusiata extract and industrial preparation method and application thereof |
| CN112137919A (en) * | 2020-08-06 | 2020-12-29 | 西安交通大学 | Beauty external product or edible product based on bamboo fungus egg extract and application |
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| CN102512353B (en) | 2013-07-10 |
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