CN102391905A - Formula and production process of engine oil - Google Patents
Formula and production process of engine oil Download PDFInfo
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- CN102391905A CN102391905A CN2011102921661A CN201110292166A CN102391905A CN 102391905 A CN102391905 A CN 102391905A CN 2011102921661 A CN2011102921661 A CN 2011102921661A CN 201110292166 A CN201110292166 A CN 201110292166A CN 102391905 A CN102391905 A CN 102391905A
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Abstract
The invention relates to a formula and a production process of engine oil. The engine oil comprises base oil and additives, wherein the base oil comprises mineral base oil and synthetic base oil; the additives comprise complexing agent OLOA59766, anti-wear and anti-oxidation agent DAN8000, viscosity increaser V112, viscosity increaser V261, pour point reducer P156 and anti-foaming agent T901; and the base oil and the additives are mixed in a certain ratio. The engine oil is a product with ultra-long oil change period and low oil consumption, has good abrasion performance and high bearing capacity, has repair function on the abraded surface, has no pollution to the environment, improves energy conservation and prolongs the service life.
Description
Technical field
The present invention relates to a kind of prescription and production technique thereof of engine oil.
Background technology
China is third place in the world big lubricating oil country of consumption, nearly 4,000,000 tons of year consumption, and present the trend that rises year by year.On Chinese lubricating oil market; Through contention for many years, competition situation forms day by day, and China high-end automobile oil market is most of to be occupied by external famous brand name; Domestic enterprise mainly captures middle-grade oil product market, during most of places and private enterprise rely on, low-grade oil product market is able to existence.Practical situation from internal lube oil manufacturing enterprise; Though we have had the lubricating oil enterprise with international most advanced level; Like the Great Wall lubricant corporation under the China Petrochemical Industry; But the small-scale enterprise that also has some deprofessionalizations to produce in the internal lube oil enterprise, they can't accomplish the production of high-end lube product for oneself, so its product focuses mostly in low and middle-grade scopes.From the lubricating oil consumption, 2002 be 3,750,000 tons, 2003 3900000 tons, broke through 4,000,000 tons in 2004, wherein China's automobile is high-end has accounted for more than 20% of the lubricating oil market share with oil.The high-end consumption 78% with oil of automobile comes from foreign brand name; Like shell, Mobil etc.; And the profit of automobile oil 80% is from high-end market; And at 3～5 years from now on, automobile is high-end will to reach 5% with the annual rate of growth of oil, and therefore high-end lubricating oil market will become the focus of following lubricating oil industry competition.With respect to crude oil and other processed oils; Lubricating oil is one of open market early of Chinese foreign; In recent years, under the effect of market economy, market is progressively to the standardization development; Formed the present three minutes market structures all over the world: the one, Sinopec and lubricating oil enterprise of CNPC occupy the market share in Chinese lubricating oil market recent 60% with its resource, technology and brand advantage; The 2nd, be the transnational lubricating oil enterprise of representative with shell, Exxon Mobil, occupy domestic high-end lubricating oil market with the absolute predominance of its brand, and kept nearly 80% the market share; The 3rd, be the local private lubricating oil enterprise of representative with unification, Rec, on market, formed the competitive capacity that can't neglect with operating mechanism flexibly with the brand awareness of waking up suddenly.
The growth of world economy will continue to improve the lubricating oil consumption; Increase the most fast and will appear at developing country; Through analysis expert; China, India and Brazil will be the zones of high growth, and increasing rapidly of motor vehicle, ship and manufacturing concern will make these national increases that keeps the lubricating oil consumptions.In the more developed country of lubricating oil consumption, demand for lubricating oil will not have tangible growth, and aspect main performance enhancing at lubricating oil, drain period prolongation, produce business opportunity.In the face of great demand, internal lube oil enterprise has hated to and has rested on middle and low-end market, in the middle and low-end market share stable with the resources advantage maintenance; They begin to put forth effort to build brand; And the communication of reinforcement and OEM, obtain moment of cooperation, thereby break through high-end market.
The lube product of low and middle-end is not high because of scientific and technological content, and production technique and fill a prescription outmodedly brings market competition fierce unusually; Consequently enterprise profit is low, and enterprise wants to run business big and strong, and promotes enterprise profit; Must strengthen the scientific and technological content of product; Improve production technique, adopt brand-new lubricant formula, thus release a series of adaptations now the lube product of automobile and industrial system current situation be the important development strategy of enterprise.The motive force of development of following lubricating oil is mainly from two aspects: the one, reduce the oiling system cost, and prolong the oil draining period through equipment manufacturing or equipment user; The 2nd, through the operation of equipment long lifetime process cost is significantly reduced.These problems; Can progressively replace MO through the ucon oil of some property, adopt new additive, modes such as lubricating oil blending technology with high content of technology to solve; Therefore the lubricating oil processing technology directly high in technological content, that the product suitability is wide from external introducing; Adjustment production technique and lubricant formula improve the lube product performance, improve the quality of products and class is the most convenient feasible way.
Constantly the raising up of oil price make many relevant industries particularly the development of energy industry received influence in various degree; Raised by oil price influences, and base oil supply before this is critical, and is the collection of the oil product excise again; In this a series of market change warp is released with policy; Domestic lubricating oil processing producer is just standing various tests, yet resources regulation is strengthened day by day when the excise is levied, and adds the raising that lubricated foxy old hand tax items will promote China market lubricating oil usage level; Make it rapidly from the applied technical application type that turns to of resource; Thereby promote the optimization utilization of petroleum resources, and along with the enforcement of mandatory Abgasgesetz and the introduction of new work engine, the upgrading of engine oil specification is being accelerated also.There is a series of problem in existing engine oil, and, oil consumption too much like charcoal is big, wearing and tearing are bigger etc.
One Chinese patent application number: 200810241687.2; A kind of lubricating oil is disclosed; Contain base oil, purification agent and dispersion agent, contain or do not contain auxiliary addition agent,, can not prevent the wearing and tearing of mover though this lubricating oil can reduce the growing amount of greasy filth in the mover use; Stability, oxidation stability can be also general.
Summary of the invention
Technical problem to be solved by this invention is to overcome existing above-mentioned deficiency in the prior art; And a kind of prescription and production technique thereof of engine oil are provided; This engine oil oil film is ultra steady, for mover provides more comprehensively protection, prolongs the work-ing life of mover.
The present invention solves the problems of the technologies described above the technical scheme that is adopted: a kind of prescription of engine oil is characterized in that: its raw material comprises base oil and additive, and described base oil comprises mineral base oil and synthetic base oil; Described additive comprises recombiner OLOA59766, wear-resistant oxidation inhibitor DAN8000, tackifier V112, tackifier V261, pour point depressant P156 and kilfoam T901; The mass percent of each component is in the raw material: recombiner OLOA59766 is 9%～11%; Wear-resistant oxidation inhibitor DAN8000 is 2.5%～3.4%; Tackifier V112 is 2%～4%, and tackifier V261 is 7%～9%, and pour point depressant P156 is 0.2%～0.7%; Kilfoam T901 is 0.0005%～0.003%, and all the other compositions are base oil.
In the raw material of the present invention each component mass percent be: recombiner OLOA59766 is 10%, and wear-resistant oxidation inhibitor DAN8000 is 3%, and tackifier V112 is 3%; Tackifier V261 is 8%; Pour point depressant P156 is 0.5%, and kilfoam T901 is 0.001%, and all the other compositions are base oil.
The staple of recombiner OLOA59766 according to the invention is calcium, molybdenum, boron, nitrogen, zinc, act as splendid oilness and anti-extreme pressure, reduces frictional coefficient and wearing and tearing greatly, reaches splendid energy-saving effect; The DAN8000 staple of wear-resistant oxidation inhibitor is a di-tert-butylphenol, vinylformic acid formicester and alcohol, and it is obvious to act as the extreme-pressure anti-wear effect, prolongs the oil oxidation time; The staple of tackifier V112 is a poly-methyl acrylate, act as the increase oil viscosity, improves the oil product viscosity temperature characteristic; The staple of tackifier V261 is an ethylene-propylene copolymer, act as the increase oil viscosity, improves the oil product viscosity temperature characteristic; The staple of pour point depressant P156 is an alkylnaphthalene, act as the growing direction that changes wax crystallization, destroys the crystalline structure, and it is small to make it composition, does not influence the crystallization of oil product mobile; The staple of kilfoam T901 is a dimethyl silicone oil, act as the destruction foam, shortens the time that foam exists.
The invention allows for a kind of production technique of engine oil, its production stage is:
1) under normal temperature, normal pressure, earlier base oil is filtered, can filter out various suspended substances, impurity, fiber in refining and the transportation;
2) base oil after will filtering through feedstock pump is squeezed into and is in harmonious proportion in the still, carries out pulse and is in harmonious proportion, and is warmed to 60 ℃ gradually simultaneously;
3) additive is added the mediation still, mixed base oil carries out pulse and is in harmonious proportion, and carries out static mixing, stirs synchronously then 1 hour;
4) after mediation is stirred and accomplished, take out processed oil, the analysis of testing, qualified back can.
Base oil of the present invention is main with III class mineral base oil, through the oil product after the hydrotreatment repeatedly, in color, smell, anti-, the antioxygen property of stability; Each item technical indicators such as pour point more are superior to I, II class; Synthetic base oil ester class is auxilliary with gathering a-alkene, the fabulous oil product high and low temperature that improves, and viscosity index is high; Oxidation stability is good, and it is strong that additive and mover are produced the greasy filth dissolving power when the high temperature.
The present invention compared with prior art has following positive effect: the present invention is a kind of superpower drain period and low oil consumption product, and prescription adopts low-carbon (LC) DAN8000; Have good polishing machine, high bearing capacity has repairing effect to wear surface; Environmentally safe; Improve energy-conservation and prolongs life, can satisfy the lubricating requirement of the mover of working under the various severe condition, mover is played unique " wear-resistant, reparation, fuel-economizing, environmental protection " four large effects; More can keep the cylinder body cleaning, continue the protection mover, prolong engine life.
Embodiment
Below in conjunction with embodiment the present invention is done further detailed description, following examples are to explanation of the present invention and the present invention is not limited to following examples.
Embodiment 1:
The raw material of present embodiment comprises base oil and additive, and described base oil comprises mineral base oil and synthetic base oil; Described additive comprises recombiner OLOA59766, wear-resistant oxidation inhibitor DAN8000, tackifier V112, tackifier V261, pour point depressant P156 and kilfoam T901; In the raw material each component mass percent be: recombiner OLOA59766 is 10%, and wear-resistant oxidation inhibitor DAN8000 is 3%, and tackifier V112 is 3%, and tackifier V261 is 8%, and pour point depressant P156 is 0.5%, and kilfoam T901 is 0.001%, and all the other compositions are base oil.
In the present embodiment, the staple of recombiner OLOA59766 is calcium, molybdenum, boron, nitrogen, zinc, act as splendid oilness and anti-extreme pressure, reduces frictional coefficient and wearing and tearing greatly, reaches splendid energy-saving effect.
The DAN8000 staple of wear-resistant oxidation inhibitor is a di-tert-butylphenol, vinylformic acid formicester and alcohol, and it is obvious to act as the extreme-pressure anti-wear effect, prolongs the oil oxidation time.
The staple of tackifier V112 is a poly-methyl acrylate, act as the increase oil viscosity, improves the oil product viscosity temperature characteristic; The staple of tackifier V261 is an ethylene-propylene copolymer, act as the increase oil viscosity, improves the oil product viscosity temperature characteristic.
The staple of pour point depressant P156 is an alkylnaphthalene, act as the growing direction that changes wax crystallization, destroys the crystalline structure, and it is small to make it composition, does not influence the crystallization of oil product mobile.
The staple of kilfoam T901 is a dimethyl silicone oil, act as the destruction foam, shortens the time that foam exists.
In the present embodiment, the step of the production technique of engine oil is:
1) under normal temperature, normal pressure, earlier base oil is filtered;
2) base oil after will filtering through feedstock pump is squeezed into and is in harmonious proportion in the still, carries out pulse and is in harmonious proportion, and is warmed to 60 ℃ gradually simultaneously;
3) additive is added the mediation still, mixed base oil carries out pulse and is in harmonious proportion, and carries out static mixing, stirs synchronously then 1 hour;
4) after mediation is stirred and accomplished, take out processed oil, the analysis of testing, qualified back can.
In the present embodiment, mainly need two kinds of starting material in the harmonic process of lubricating oil: base oil and additive, base oil and additive become processed oil through being in harmonious proportion, and its production process does not produce the three wastes, and resource utilization is almost 100%.During blending, by feedstock pump base oil is squeezed in the blending kettle earlier, the metering of base oil can be measured through a under meter or a jar mode that detects; Again additive is heated to 60 ℃ and pour additive tank into by formula rate; By additive pump it is squeezed in the blending kettle; If little additive can directly add the charging opening of blending kettle, after heating pulse stirs, oil product is delivered in the product tank by pump.During can, oil product is sent into the packing that the finished product filling machine carries out all size by discharge pump.
In the present embodiment, adopt pulse mediation mode in the mediation still, realize through the pulse pneumatic blending system.The pulse pneumatic blending system is operated with pressurized air; It is a kind of from bottom to top, top-down motion; The air pocket that its powerful motivation produces can be scraped and sweep at the whole jar of end, makes the whole jar of end not have the dead angle, thereby improves the disposable qualification rate of product.Air pocket all is heated the oil product picking-up to the bottom at every turn and delivers to the top liquid level; Heat-up time has been shortened in motion repeatedly; And the degree of oxidation of oil product reduces greatly; Because pressurized air acts on air pocket and produces and to make the violent vertical convection campaign up and down of pasta, cause additive fully to dissolve making its function in the parts that use give full play to, it is mass-producing blending plant 21 century the best blending equipment.Pulse mediation mode is energy-efficient, cost is low; Maintenance free; Adopt intelligent control; Disposed the industriallization control computer system at intelligent coloured image center, all kinds of mediation parameters, mediation pattern can be set through system, can the several full-automatic control equipments that are in harmonious proportion simultaneously to tens mediation stills of remote control.
In the present embodiment, static mixing is a kind of auspicious stream and eddy current of under velocity pressure, forming after the actuating fluid intense impact, the shearing force that tool is extremely strong, and utilize blending that excess power is set and accomplish, special energy-saving effect is arranged.Oil product, additive are with bubble dispersion, polymerization during pulse pneumatic blending work; And static mixer is to replenish to improve the best facility of pneumatic blending shear effect; Especially the shearing action to high-molecular weight polymer OCP glue is irreplaceable; Through the oil product after the static mixer technology, viscosity temperature characteristic is protected, and mechanical shearing stability and thermal shear stability are better.
Embodiment 2:
The present invention can adjust the mass percent between each composition according to actual needs, referring to table 1.
All the other compositions are base oil.
The production technique of present embodiment is identical with embodiment 1.
Though the present invention with embodiment openly as above; But it is not in order to limit protection scope of the present invention; Any technician who is familiar with this technology, change and the retouching in not breaking away from design of the present invention and scope, done all should belong to protection scope of the present invention.
Claims (4)
1. the prescription of an engine oil, it is characterized in that: its raw material comprises base oil and additive, described base oil comprises mineral base oil and synthetic base oil; Described additive comprises recombiner OLOA59766, wear-resistant oxidation inhibitor DAN8000, tackifier V112, tackifier V261, pour point depressant P156 and kilfoam T901; The mass percent of each component is in the raw material: recombiner OLOA59766 is 9%～11%; Wear-resistant oxidation inhibitor DAN8000 is 2.5%～3.4%; Tackifier V112 is 2%～4%, and tackifier V261 is 7%～9%, and pour point depressant P156 is 0.2%～0.7%; Kilfoam T901 is 0.0005%～0.003%, and all the other compositions are base oil.
2. the prescription of engine oil according to claim 1; It is characterized in that: in the described raw material each component mass percent be: recombiner OLOA59766 is 10%, and wear-resistant oxidation inhibitor DAN8000 is 3%, and tackifier V112 is 3%; Tackifier V261 is 8%; Pour point depressant P156 is 0.5%, and kilfoam T901 is 0.001%, and all the other compositions are base oil.
3. the prescription of engine oil according to claim 1 and 2; It is characterized in that: the staple of said recombiner OLOA59766 is calcium, molybdenum, boron, nitrogen, zinc, and the DAN8000 staple of wear-resistant oxidation inhibitor is a di-tert-butylphenol, vinylformic acid formicester and alcohol; The staple of tackifier V112 is a poly-methyl acrylate; The staple of tackifier V261 is an ethylene-propylene copolymer, and the staple of pour point depressant P156 is an alkylnaphthalene, and the staple of kilfoam T901 is a dimethyl silicone oil.
4. the production technique of the described engine oil of claim 1, its production stage is:
1) under normal temperature, normal pressure, earlier base oil is filtered;
2) base oil after will filtering through feedstock pump is squeezed into and is in harmonious proportion in the still, carries out pulse and is in harmonious proportion, and is warmed to 60 ℃ gradually simultaneously;
3) additive is added the mediation still, mixed base oil carries out pulse and is in harmonious proportion, and carries out static mixing, stirs synchronously then 1 hour;
4) after mediation is stirred and accomplished, take out processed oil, the analysis of testing, qualified back can.
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| CN201110292166.1A CN102391905B (en) | 2011-09-30 | 2011-09-30 | Formula and production process of engine oil |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102719304A (en) * | 2012-06-21 | 2012-10-10 | 浙江丹弗王力润滑油有限公司 | Low-carbon lubricating oil for diesel locomotive and production method thereof |
| CN103266001A (en) * | 2013-05-22 | 2013-08-28 | 江苏紫石化工科技有限公司 | Engine oil |
| CN104031723A (en) * | 2014-05-15 | 2014-09-10 | 山东力牌石油化学有限公司 | Engineering machinery dedicated lubricating oil formula and production process thereof |
| CN104109573A (en) * | 2014-07-01 | 2014-10-22 | 山东力牌石油化学有限公司 | Formula and production process for special lubricating oil for turbosupercharged engine |
| CN104109572A (en) * | 2014-07-01 | 2014-10-22 | 山东力牌石油化学有限公司 | Formula and production technology of special lubricating oil for high-pressure common rail diesel engine |
| CN104119992A (en) * | 2014-07-01 | 2014-10-29 | 山东力牌石油化学有限公司 | Formula as well as production technology of special lubricating oil for dual-fuel engine |
| CN104893793A (en) * | 2015-05-14 | 2015-09-09 | 浙江工贸职业技术学院 | Production process of engine oil |
| CN104974830A (en) * | 2015-06-24 | 2015-10-14 | 李云军 | Preparation method for concentrated type anti-rust oil |
| CN105001951A (en) * | 2015-06-24 | 2015-10-28 | 李云军 | Manufacturing method for anti-rust oil used for processing of precision components |
| CN105018196A (en) * | 2015-06-24 | 2015-11-04 | 李云军 | Ball bearing anti-rust oil preparation method |
| CN105018197A (en) * | 2015-06-24 | 2015-11-04 | 李云军 | Manufacturing method of anti-rust oil for part processing |
| CN105038920A (en) * | 2015-06-24 | 2015-11-11 | 李云军 | Method for manufacturing antirust oil of instrument |
| CN112574798A (en) * | 2020-12-08 | 2021-03-30 | 苏州安科霖化工环保科技有限公司 | Guide rail oil manufacturing process |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102719304A (en) * | 2012-06-21 | 2012-10-10 | 浙江丹弗王力润滑油有限公司 | Low-carbon lubricating oil for diesel locomotive and production method thereof |
| CN103266001A (en) * | 2013-05-22 | 2013-08-28 | 江苏紫石化工科技有限公司 | Engine oil |
| CN104031723A (en) * | 2014-05-15 | 2014-09-10 | 山东力牌石油化学有限公司 | Engineering machinery dedicated lubricating oil formula and production process thereof |
| CN104109573A (en) * | 2014-07-01 | 2014-10-22 | 山东力牌石油化学有限公司 | Formula and production process for special lubricating oil for turbosupercharged engine |
| CN104109572A (en) * | 2014-07-01 | 2014-10-22 | 山东力牌石油化学有限公司 | Formula and production technology of special lubricating oil for high-pressure common rail diesel engine |
| CN104119992A (en) * | 2014-07-01 | 2014-10-29 | 山东力牌石油化学有限公司 | Formula as well as production technology of special lubricating oil for dual-fuel engine |
| CN104893793A (en) * | 2015-05-14 | 2015-09-09 | 浙江工贸职业技术学院 | Production process of engine oil |
| CN104974830A (en) * | 2015-06-24 | 2015-10-14 | 李云军 | Preparation method for concentrated type anti-rust oil |
| CN105001951A (en) * | 2015-06-24 | 2015-10-28 | 李云军 | Manufacturing method for anti-rust oil used for processing of precision components |
| CN105018196A (en) * | 2015-06-24 | 2015-11-04 | 李云军 | Ball bearing anti-rust oil preparation method |
| CN105018197A (en) * | 2015-06-24 | 2015-11-04 | 李云军 | Manufacturing method of anti-rust oil for part processing |
| CN105038920A (en) * | 2015-06-24 | 2015-11-11 | 李云军 | Method for manufacturing antirust oil of instrument |
| CN112574798A (en) * | 2020-12-08 | 2021-03-30 | 苏州安科霖化工环保科技有限公司 | Guide rail oil manufacturing process |
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Effective date of registration: 20180605 Address after: 321300 East, 22 floor, Jinji building, Yongkang headquarters, Jinhua, Zhejiang Patentee after: Zhejiang Denver green Polytron Technologies Inc Address before: 321300 No. 9 South Avenue, Yongkang famous hardware and Technology Industrial Park, Jinhua, Zhejiang Patentee before: Zhejiang Danfer Wangli Lubricants Co.,Ltd. |