CN102274670B - Trapping device adopted in resin synthesis - Google Patents
Trapping device adopted in resin synthesis Download PDFInfo
- Publication number
- CN102274670B CN102274670B CN 201010208062 CN201010208062A CN102274670B CN 102274670 B CN102274670 B CN 102274670B CN 201010208062 CN201010208062 CN 201010208062 CN 201010208062 A CN201010208062 A CN 201010208062A CN 102274670 B CN102274670 B CN 102274670B
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- Prior art keywords
- pipeline
- valve
- medium
- control system
- control
- Prior art date
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Links
- 239000011347 resin Substances 0.000 title claims abstract description 12
- 229920005989 resin Polymers 0.000 title claims abstract description 12
- 230000015572 biosynthetic process Effects 0.000 title abstract 2
- 238000003786 synthesis reaction Methods 0.000 title abstract 2
- 238000006243 chemical reaction Methods 0.000 claims abstract description 18
- 238000004519 manufacturing process Methods 0.000 claims abstract description 18
- 238000011010 flushing procedure Methods 0.000 claims abstract description 10
- 239000000498 cooling water Substances 0.000 claims abstract description 4
- 238000000034 method Methods 0.000 claims description 9
- 238000005192 partition Methods 0.000 claims description 9
- 239000002351 wastewater Substances 0.000 claims description 8
- 230000001105 regulatory effect Effects 0.000 claims description 6
- 238000011144 upstream manufacturing Methods 0.000 claims description 5
- 238000005516 engineering process Methods 0.000 claims description 4
- 238000010079 rubber tapping Methods 0.000 claims description 4
- 230000008859 change Effects 0.000 claims description 3
- 238000005304 joining Methods 0.000 claims description 2
- 238000004140 cleaning Methods 0.000 abstract 1
- 239000002609 medium Substances 0.000 description 16
- 239000000047 product Substances 0.000 description 6
- 230000008569 process Effects 0.000 description 5
- 239000000126 substance Substances 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 230000009471 action Effects 0.000 description 2
- 238000013070 change management Methods 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000012120 mounting media Substances 0.000 description 2
- 238000004064 recycling Methods 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 229920002799 BoPET Polymers 0.000 description 1
- 239000005041 Mylar™ Substances 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000008065 acid anhydrides Chemical class 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 230000006978 adaptation Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- ANSXAPJVJOKRDJ-UHFFFAOYSA-N furo[3,4-f][2]benzofuran-1,3,5,7-tetrone Chemical compound C1=C2C(=O)OC(=O)C2=CC2=C1C(=O)OC2=O ANSXAPJVJOKRDJ-UHFFFAOYSA-N 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000008676 import Effects 0.000 description 1
- 239000003317 industrial substance Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000005405 multipole Effects 0.000 description 1
- 230000037361 pathway Effects 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000012465 retentate Substances 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Images
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- Other Resins Obtained By Reactions Not Involving Carbon-To-Carbon Unsaturated Bonds (AREA)
- Separation, Recovery Or Treatment Of Waste Materials Containing Plastics (AREA)
Abstract
The invention relates to a trapping device which is suitable for resin synthesis and production and comprises a body, a temperature adjusting system, a medium entrance and stop control system, a pressure adjusting system and a control system for preventing a medium from entering a tail gas treating part. The medium entrance and stop control system comprises a medium entrance and stop control valve and a flushing valve. The pressure adjusting system comprises a control valve on a pipeline connected with a vacuum pump station and an adjusting valve on an evacuation pipeline. The control system for preventing the medium from entering the tail gas treating part comprises a drain valve on a pipeline connected with the tail gas treating device. The body comprises a central clapboard and a series of wing plates. The temperature adjusting system consists of an enclosed pipeline system, a pipeline and a valve adaptively connected with the pipeline and used for realizing controllable conversion by connecting with external cooling water and a steam station supply system. The trapping device also comprises a bottom temperature adjuster and a product discharge device. The valves of the trapping device are manipulated in a control coordination way through a central controlling system according to programs; and the trapping device is switched among three states, such as reaction, evacuation and cleaning according to production process specifications.
Description
Technical field
The present invention relates generally to environment protection equipment, particularly the capturing device that adopts in synthetic of a kind of resin.
Background technology
In the production process of the mylar of one of chemical products, to use polyacid, polyalcohol etc. in the raw material; Course of reaction also has multiple byproduct and generates.Even the tail gas major part that generates in this process is steam, also can have the smell of dense industrial chemicals, offensive, bring adverse influence also for simultaneously the surrounding environment zone of Chemical Manufacture; In addition, wherein generating the part material that gas is taken away by process, also is a kind of waste if do not reclaim.Therefore need there be the gas of discharging in pair resin synthetic reaction to carry out integrated treatment, wherein uses and just include trap in the corresponding equipment.
The patent CN1136041A of trap aspect is entitled as " Rifinement of pyromellitic acid dianhydride by hot air carrying process " in the prior art, has wherein adopted the mode of multipole capture to make with extra care the polymer chemistry product.It is produced at equal acid anhydride.
Adopt the mixing chamber and the dust trapping chamber that are provided with sublimate bed and baffling structure in the production equipment that discloses among the patent CN 1388127A.
Vent gas treatment and comprehensive utilization aspect thereof in the Chemical Manufacture obtain all circles day by day and pay close attention to.But still lack processing method targetedly, also not fully up to expectations for the capturing device with comprehensive treatment capability, the sort of trap that multi-functional processing effectiveness can be arranged, can make adaptations by the process conditions requirement particularly, society gives very high expectation.
Summary of the invention
The present invention is intended to provide the core processing device that the product that can cause atmosphere pollution in the Chemical Manufacture is fully utilized at above-mentioned deficiency of the prior art.
A further object of the present invention provides a kind of trap that has the waste water effectiveness of storing the resin synthetic reaction simultaneously.
A kind of capturing device is applicable to the synthetic production of resin, and it includes one and is columnar body substantially, is positioned at a thermoregulating system at body middle part; A medium that is made of valve and pipeline that is positioned at bodies top advances only control system, and pressure regulating system and one are put the control system that medium is only gone to the vent gas treatment part.Its medium advance control system only include be positioned at import upstream side direction with the reactor flushing valve that a medium on the pipeline advances control valve only and join with the waste water pipeline of joining.
Its pressure regulating system also includes and Vacuum Pumps Station join by-pass valve control and a control valve on the emptying pipeline on the pipeline.
And its medium only put is gone to the control system of vent gas treatment part and has been comprised a drain valve on the pipeline that is connected with exhaust gas processing device.
Body also includes and is fixed in cover top portion and a central partition plate that extends downwards and is fixed in this outer casing inner wall and a series of wing-shaped plates that central partition plate, its free end stretch to oblique below.
Described thermoregulating system is a closing pipe line system that constitutes by a series of pipes that run through this series wing-shaped plate, with the connecting pipe of upper lower burrs row, it penetrate respectively should about body; Pipeline and form with the matched valve of this pipeline.
The valve matched with this pipeline includes two groups of valves, and they are by being connected the conversion that realizes controllable way with external cooling water with steam station feed system.
Described capturing device has also comprised a bottom thermosistor and a product tapping equipment.
The valve of capturing device is by central control system follow procedure control hormany operating, according to the production technology regulation realize this trap in reaction, find time and clear up to change between three kinds of states.
Capturing device of the present invention is by the setting conversion that multi-functional state is arranged, and can make to the greatest extent in the mounting medium of reaction the useful component enrichment so that its recycling; Also can make capturing device function in an acting capacity of waste water storage and to the effect of passage flushing by the intelligent change management of pipeline approach, thereby save the occupation of land space of equipment, improve efficient and reduced production cost.
Preferred embodiment below with reference to drawings attached is done further explanation to the present invention, and those skilled in the art can therefrom recognize other many purposes and advantages potential in the invention.
Description of drawings
Fig. 1 for by the capturing device schematic diagram of preferred embodiment of the present invention and
Fig. 2 is along the generalized section of B-B in Fig. 1 capturing device.
The specific embodiment
Describe by the synthetic a kind of capturing device that is suitable for of producing of resin of the present invention in more detailed mode now.
Schematically expressed the capturing device by preferred embodiment of the present invention among Fig. 1.It is suitable for, and resin is synthetic to be produced.
Be positioned at the middle part of this body 10, settled a thermoregulating system 20.
Be to advance only control system by the medium that valve and pipeline constitute on the top of body 10, the housing.Medium only advances, and control system has comprised the flushing valve 40 that medium advances to end control valve 51 and join with the waste water pipeline.
Medium advances upper left quarter that control valve 51 only is positioned at Fig. 1, is air inlet upstream side direction, is arranged on the reactor (not shown) to join on the pipeline.
40 of flushing valves and medium advance to end control valve 51 and adjoin, also in air inlet upstream side direction; Be in the left side top by a central partition plate 12 that is fixed in shell 10 tops and extends downwards.Flushing valve 40 will from the input of air inlet upstream side, be pooled to the bottom of trap subsequently via the waste water of a minute slide tower, cooling tower under reactiveness.
This capturing device makes capturing device function in an acting capacity of the waste water storage effect by the intelligent change management of pipeline approach; Meanwhile also play the flushing action to passage, thereby saved the occupation of land space of equipment, improved efficient greatly and reduced production cost.The flushing valve facility also is set on the body right side also is feasible certainly in order to enlarge its flushing action.
Two parts about central partition plate 12 is separated into the inside of body 10 because 12 on dividing plate extends to an intrinsic suitable height and position, so make trap constituted one from top to bottom, turn back after from bottom to top a passage.As shown in Figure 1, successively be furnished with on this passage respectively and tilt downwards from central partition plate 12 and outer cover body 11, play a series of wing-shaped plate 13 of barrier effect.Such layout be intended in the limited space to prolong institute by the path of medium in trap, it is had manyly contact and the chance that acts on and time with thermoregulating system 20 (hereinafter more detailed description will be arranged) efficient of medium temperature being controlled with raising.
Be positioned at Fig. 1 upper right quarter, be the downstream direction of air flue, also be the end of trap reentrant pathway, be provided with a pressure regulating system and one and put the control system that medium is only gone to the vent gas treatment part.
Pressure regulating system includes to be supplied with a by-pass valve control 321 that joins on the negative pressure line with Vacuum Pumps Station (not shown) and is arranged on a control valve 52 on the emptying pipeline.
That adjoins with it is one and puts the control system that medium is only gone to vent gas treatment part (not shown).It has comprised a drain valve 311, and drain valve 311 is provided in a side of on the pipeline that is connected with an exhaust gas processing device of downstream direction; And corresponding pipe-line system (not shown).Select as another kind, control valve 52 also can merge with drain valve 311.
As previously mentioned, body 10 also includes a central partition plate 12 that is fixed in cover top portion and extends downwards; Be fixed in a series of wing-shaped plate 13 that this outer casing inner wall and central partition plate, its free end stretch to oblique below.And the waste water quantity that a collection of synthetic operation cycle that feeds intake generates will be considered in dividing plate 12 downward position in body, need make in the body bottom and leave enough volumes.
Wing-shaped plate 13 can have influence on MEDIA FLOW the short long of path of flowing through in the corner dimension of horizontal direction in body 10 in crossing the center line longitudinal cross-section, in other words, angle is more little just may to make the path lengthening at the more wing-shaped plate 13 of layout on the effective vertical extension; But angle is more little, is unfavorable for that more the wing-shaped plate retentate flows to down the concentrated of body bottom by deadweight.General this angle is limited in 10 degree to 70 degree, and is more preferably 30 degree to about 45 degree.
As mentioned above, a closing pipe line system that run through a series of pipes 26 (seeing Fig. 2 for details) of this series wing-shaped plate 13, constitutes with the connecting pipe of upper lower burrs row (adopting schematically showing of simplifying among Fig. 1).It passes this body up and down again respectively.The valve matched with this pipeline includes two groups of valves 201,202; 203,204.They are by being connected the conversion that realizes controllable way with external cooling water with steam station feed system (not shown).Such conversion makes that the applicability of trap is expanded.
For example in the synthetic production process of resin, from the medium that reactor is discharged, can be entrained with the materials such as acids that do not reach reaction, the MEDIA FLOW of flowing through behind the fractionation cooler can be at trap along forming crystallization in the passage of warp, and it is not smooth that discharge medium is flowed, and causes production procedure to continue.This just need be by changing environment in the trap temperature regime so that crystals melt is pooled to the trap bottom further processes.
Capturing device has just comprised a bottom thermosistor 21 and a product tapping equipment 60.Can make the thing that compiles of bottom do property processing respectively.
What below list is each main valve event state list when being in reaction, finding time and clearing up three kinds of states about capturing device in the synthetic production process of vinyl unsaturated-resin, for your guidance.
In this example, each valve event of capturing device is by intelligent control system (not shown) follow procedure control hormany operating, and according to the production technology regulation realize this trap in reaction, find time and clear up to change between three kinds of states.The setting of this multi-functional state conversion can make to the greatest extent in the mounting medium of reaction the useful component enrichment so that its recycling.
Above content has shown and has described preferred embodiment of the present invention.The embodiment that this just shows by example, purpose is explanation, rather than will limit the invention.Self-evident, to one skilled in the art, under the situation that does not break away from aim of the present invention, can carry out numerous variations, variation and replacement to it.Content of the present invention is to be limited by the essence of additional claim and scope.
Claims (3)
1. a capturing device is suitable for the synthetic production of resin, and it includes
One is columnar body substantially;
Be positioned at a thermoregulating system at this body middle part;
A medium that is made of valve and pipeline that is positioned at this bodies top advances only control system, and pressure regulating system and one are put the control system that medium is only gone to the vent gas treatment part;
Wherein said medium advances control system only and includes the flushing valve that medium on the pipeline advances to end control valve and join with the waste water pipeline of joining of of being positioned at air inlet upstream side direction and reactor, described pressure regulating system then includes and Vacuum Pumps Station join by-pass valve control and a control valve on the emptying pipeline on the pipeline;
The wherein said medium only put is gone to the control system of vent gas treatment part and has been comprised a drain valve on the pipeline that is connected with exhaust gas processing device; It is characterized in that:
Described valve is by central control system follow procedure control hormany operating, according to the production technology regulation realize this trap in reaction, find time and clear up to change between three kinds of states;
Wherein said thermoregulating system is a closing pipe line system that constitutes by a series of pipes that run through this series wing-shaped plate, with the connecting pipe of upper lower burrs row, it penetrate respectively should about body; Pipeline and form with the matched valve of this pipeline;
The matched valve of wherein said and this pipeline includes two groups of valves, and they are by being connected the conversion that realizes controllable way with external cooling water with steam station feed system.
2. according to the described capturing device of claim 1, it is characterized in that wherein said body also includes is fixed in cover top portion and a central partition plate that extends downwards and is fixed in this outer casing inner wall and a series of wing-shaped plates that central partition plate, its free end stretch to oblique below.
3. according to the described capturing device of claim 1, it is characterized in that it has also comprised a bottom thermosistor and a product tapping equipment.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN 201010208062 CN102274670B (en) | 2010-06-10 | 2010-06-10 | Trapping device adopted in resin synthesis |
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Application Number | Priority Date | Filing Date | Title |
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CN 201010208062 CN102274670B (en) | 2010-06-10 | 2010-06-10 | Trapping device adopted in resin synthesis |
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CN102274670A CN102274670A (en) | 2011-12-14 |
CN102274670B true CN102274670B (en) | 2013-08-28 |
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CN 201010208062 Expired - Fee Related CN102274670B (en) | 2010-06-10 | 2010-06-10 | Trapping device adopted in resin synthesis |
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Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN2106645U (en) * | 1991-12-11 | 1992-06-10 | 王有德 | Condensing unit for oil smokes or chemical substances |
CN200963586Y (en) * | 2006-11-01 | 2007-10-24 | 徐友志 | Chemical industry waste material regenerating device |
CN101584944A (en) * | 2009-06-11 | 2009-11-25 | 许培圣 | The synthetic capturing device of discharging gas comprehensive utilization method and this gas of resin |
-
2010
- 2010-06-10 CN CN 201010208062 patent/CN102274670B/en not_active Expired - Fee Related
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN2106645U (en) * | 1991-12-11 | 1992-06-10 | 王有德 | Condensing unit for oil smokes or chemical substances |
CN200963586Y (en) * | 2006-11-01 | 2007-10-24 | 徐友志 | Chemical industry waste material regenerating device |
CN101584944A (en) * | 2009-06-11 | 2009-11-25 | 许培圣 | The synthetic capturing device of discharging gas comprehensive utilization method and this gas of resin |
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CN102274670A (en) | 2011-12-14 |
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