CN102260170B - 微波管道化生产乙酸正t酯的方法 - Google Patents
微波管道化生产乙酸正t酯的方法 Download PDFInfo
- Publication number
- CN102260170B CN102260170B CN201110147117.9A CN201110147117A CN102260170B CN 102260170 B CN102260170 B CN 102260170B CN 201110147117 A CN201110147117 A CN 201110147117A CN 102260170 B CN102260170 B CN 102260170B
- Authority
- CN
- China
- Prior art keywords
- butyl acetate
- mixed solution
- pipeline reactor
- reaction
- volume pump
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Abstract
Description
Claims (3)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201110147117.9A CN102260170B (zh) | 2011-06-02 | 2011-06-02 | 微波管道化生产乙酸正t酯的方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201110147117.9A CN102260170B (zh) | 2011-06-02 | 2011-06-02 | 微波管道化生产乙酸正t酯的方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN102260170A CN102260170A (zh) | 2011-11-30 |
CN102260170B true CN102260170B (zh) | 2014-10-15 |
Family
ID=45007040
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201110147117.9A Active CN102260170B (zh) | 2011-06-02 | 2011-06-02 | 微波管道化生产乙酸正t酯的方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN102260170B (zh) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109608332A (zh) * | 2019-01-18 | 2019-04-12 | 西安优耐特容器制造有限公司 | 利用微波-微反应器催化连续合成丙烯酸十四酯的方法 |
CN114315658B (zh) * | 2021-12-29 | 2023-06-30 | 宁波南大光电材料有限公司 | 一种磺酸盐烷烃酯的制备方法 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0021242A1 (en) * | 1979-06-20 | 1981-01-07 | BASF Canada Inc. | Use of microwave energy in the production of plasticizer esters |
US5387397A (en) * | 1988-10-10 | 1995-02-07 | Commonwealth Scientific And Industrial Research Organisation | Method and apparatus for continuous chemical reactions |
CN1931980A (zh) * | 2006-09-29 | 2007-03-21 | 陈必昌 | 一种制备五金加工润滑剂的方法 |
WO2011000464A2 (de) * | 2009-06-30 | 2011-01-06 | Clariant International Ltd | Kontinuierliches verfahren zur herstellung von estern aromatischer carbonsäuren |
CN101973873A (zh) * | 2010-10-09 | 2011-02-16 | 东北石油大学 | 一种微波辐射催化合成羧酸酯的方法 |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH07330667A (ja) * | 1994-06-10 | 1995-12-19 | Koichi Shinozaki | マイクロ波を加熱に用いるエステル類の製造方法 |
-
2011
- 2011-06-02 CN CN201110147117.9A patent/CN102260170B/zh active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0021242A1 (en) * | 1979-06-20 | 1981-01-07 | BASF Canada Inc. | Use of microwave energy in the production of plasticizer esters |
US5387397A (en) * | 1988-10-10 | 1995-02-07 | Commonwealth Scientific And Industrial Research Organisation | Method and apparatus for continuous chemical reactions |
CN1931980A (zh) * | 2006-09-29 | 2007-03-21 | 陈必昌 | 一种制备五金加工润滑剂的方法 |
WO2011000464A2 (de) * | 2009-06-30 | 2011-01-06 | Clariant International Ltd | Kontinuierliches verfahren zur herstellung von estern aromatischer carbonsäuren |
CN101973873A (zh) * | 2010-10-09 | 2011-02-16 | 东北石油大学 | 一种微波辐射催化合成羧酸酯的方法 |
Non-Patent Citations (6)
Title |
---|
Development and Application of a Continuous Microwave Reactor for Organic Synthesis;Teresa Cablewski et al;《J. Org. Chem》;19941015;第59卷(第12期);3408-3412 * |
Teresa Cablewski et al.Development and Application of a Continuous Microwave Reactor for Organic Synthesis.《J. Org. Chem》.1994,第59卷(第12期),3408-3412. |
孟庆华等.面向化学研究的微波反应器.《实验室研究与探索》.2003,第22卷(第3期),第94-97页. |
微波辐射催化合成乙酸正丁酯;邓斌等;《化学工程师》;20070930(第9期);第2页左栏第3-7行、左栏倒数第13-11行 * |
邓斌等.微波辐射催化合成乙酸正丁酯.《化学工程师》.2007,(第9期),第2页左栏第3-7行、左栏倒数第13-11行. |
面向化学研究的微波反应器;孟庆华等;《实验室研究与探索》;20030630;第22卷(第3期);第94-97页 * |
Also Published As
Publication number | Publication date |
---|---|
CN102260170A (zh) | 2011-11-30 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN102000559B (zh) | 一种采用负载氧化铌催化剂制备甲缩醛的方法 | |
CN107501042B (zh) | 一种通过乙酸异丙酯水解制备异丙醇的方法 | |
CN104557801A (zh) | 一种金属/固体酸催化剂上由糠醛制备γ-戊内酯的方法 | |
CN107311868B (zh) | 一种制备对叔丁基苯甲酸甲酯的方法 | |
CN101121625B (zh) | 乙醇脱水制备乙烯的方法 | |
CN103394370A (zh) | 一种硅胶负载磺酸双核离子液体催化剂、制备方法以及应用 | |
CN102557932A (zh) | 醋酸异丁酯的生产方法 | |
CN104557524B (zh) | 一种乙酸乙酯的生产方法 | |
CN102260170B (zh) | 微波管道化生产乙酸正t酯的方法 | |
CN108043456B (zh) | 一种多酸类离子液体催化剂、制备方法及用其催化乙酸环己酯水解制备环己醇的方法 | |
CN101704733B (zh) | 一种醋酸甲酯水解耦合工艺及其专用设备 | |
CN110950760B (zh) | 一种合成丙烯酸叔丁酯的工艺 | |
CN102807500A (zh) | 一种液相制备n,n-二甲基乙酰胺的方法 | |
CN102617522A (zh) | 一种合成γ-壬内酯的方法 | |
CN101676252A (zh) | 一种乙二醛制备缩醛的方法 | |
CN102757341A (zh) | 一种醋酸乙酯和/或醋酸异丙酯的制备方法 | |
CN102219679B (zh) | Co气相偶联生产草酸酯的方法 | |
CN101747156A (zh) | 2,4-二特戊基苯酚的新制备方法 | |
CN105585468B (zh) | 一种以环戊烯为原料制备环戊酮的方法 | |
CN107952479B (zh) | 一种功能化多酸类离子液体催化剂、制备方法及用其催化环己烯直接酯化的方法 | |
CN107033000A (zh) | 一种固定床连续液固催化制备乳酸酯的方法 | |
CN102276459B (zh) | 采用co气相法制备草酸酯的方法 | |
CN102557877A (zh) | 一种近均相的两相反应体系中提高松油醇产率的方法 | |
CN101502806B (zh) | 一种合成醋酐的负载型非贵金属催化剂及制法和应用 | |
CN114539026B (zh) | 一种以乙醇和1,2-丙二醇为原料合成1,2-戊二醇的方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CI01 | Correction of invention patent gazette |
Correction item: Denomination of Invention Correct: Method for producing n-butyl acetate by microwave pipeline False: Method for producing acetic acid positive T ester by microwave pipeline Number: 42 Volume: 30 |
|
CI03 | Correction of invention patent |
Correction item: Denomination of Invention Correct: Method for producing n-butyl acetate by microwave pipeline False: Method for producing acetic acid positive T ester by microwave pipeline Number: 42 Volume: 30 |
|
ERR | Gazette correction |
Free format text: CORRECT: INVENTION NAME; FROM: METHOD FOR PRODUCING N-T ESTER BY MICROWAVE PIPELINE TO: METHOD FOR PRODUCING N-BUTYL ACETATE BY MICROWAVE PIPELINE |
|
RECT | Rectification | ||
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20171215 Address after: 311604, No. 48, Fu Fu West Road, Mei Town, Hangzhou, Zhejiang, Jiande Patentee after: Zhejiang Jianye Chemical Co., Ltd. Address before: 310027 Hangzhou, Zhejiang Province, Xihu District, Zhejiang Road, No. 38, No. Co-patentee before: Zhejiang Jianye Chemical Co., Ltd. Patentee before: Zhejiang University |