CN102191689A - Fogging surface silky wax feel finishing agent for synthetic leather and preparation method thereof - Google Patents
Fogging surface silky wax feel finishing agent for synthetic leather and preparation method thereof Download PDFInfo
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- CN102191689A CN102191689A CN2010105693997A CN201010569399A CN102191689A CN 102191689 A CN102191689 A CN 102191689A CN 2010105693997 A CN2010105693997 A CN 2010105693997A CN 201010569399 A CN201010569399 A CN 201010569399A CN 102191689 A CN102191689 A CN 102191689A
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Abstract
The invention relates to a fogging surface silky wax feel finishing agent for synthetic leather and a preparation method thereof. The finishing agent comprises modified polyurethane resins, DMF (dimethyl formamide), butyl acetate, silica matting powder, modified amino siloxane, dimethicone, erucyl amide, polyurethane color beads and an organosilicon leveling agent. The finishing agent has the following advantages: the fogging surface matting effect is excellent, the silky wax feel is unique and the real leather effect of the leather surface is strong; and the synthetic leather applying the finishing agent has silky handfeel and excellent general effect.
Description
Technical field
The present invention relates to the sliding wax sense of a kind of use for synthetic leather cloudy surface silk finishing agent, particularly be applied to the sliding wax sense of the use for synthetic leather silk finishing agent of synthetic leather rear section technology, belong to innovative back segment material.The invention still further relates to the preparation method of the sliding wax sense of a kind of use for synthetic leather cloudy surface silk finishing agent.
Background technology
Synthetic leather is divided into PU leather (polyurethane leather) and PVC leather (polyvinyl chloride leather) usually.For the PVC leather, in order to obtain in manufacture process, needing PVC is carried out surface treatment at different product, different pliability, the brightness that requires.In practice, PVC obtains good leather effect through being difficult in after the surface treatment on natural, the soft basis of gloss.
Summary of the invention
The purpose of this invention is to provide the sliding wax sense of a kind of use for synthetic leather cloudy surface silk finishing agent.
The sliding wax sense of use for synthetic leather cloudy surface silk of the present invention finishing agent is achieved through the following technical solutions:
The sliding wax sense of use for synthetic leather cloudy surface silk disclosed in this invention finishing agent, composed of the following components: modified polyurethane resin, DMF, butyl acetate, silica flatting silica, modified amido siloxanes, dimethicone, erucyl amide, polyurethane look pearl and organosilicon levelling agent.
The proportioning of each component of the sliding wax sense of use for synthetic leather cloudy surface silk provided by the invention finishing agent can be modified polyurethane resin 30～40 weight portions, DMF 20～30 weight portions, butyl acetate 20～30 weight portions, silica flatting silica 4～5 weight portions, modified amido siloxanes 1～4 weight portion, dimethicone 1～3 weight portion, erucyl amide 1～3 weight portion, polyurethane look pearl 3～5 weight portions, organosilicon levelling agent 1～2 weight portion.
In one embodiment of the invention, the proportioning of each component of the sliding wax sense of use for synthetic leather cloudy surface silk finishing agent is as follows: modified polyurethane resin 40 weight portions, DMF 20 weight portions, butyl acetate 20 weight portions, silica flatting silica 4 weight portions, modified amido siloxanes 2 weight portions, dimethicone 2 weight portions, erucyl amide 3 weight portions, polyurethane look pearl 3 weight portions, organosilicon levelling agent 1 weight portion.
In another embodiment of the present invention, the proportioning of each component of the sliding wax sense of use for synthetic leather cloudy surface silk finishing agent is as follows: modified polyurethane resin 30 weight portions, DMF 30 weight portions, butyl acetate 30 weight portions, silica flatting silica 5 weight portions, modified amido siloxanes 1 weight portion, dimethicone 3 weight portions, erucyl amide 1 weight portion, polyurethane look pearl 5 weight portions, organosilicon levelling agent 2 weight portions.
In another embodiment of the present invention, the proportioning of each component of the sliding wax sense of use for synthetic leather cloudy surface silk finishing agent is as follows: modified polyurethane resin 35 weight portions, DMF 25 weight portions, butyl acetate 25 weight portions, silica flatting silica 4.5 weight portions, modified amido siloxanes 4 weight portions, dimethicone 1 weight portion, erucyl amide 2 weight portions, polyurethane look pearl 4 weight portions, organosilicon levelling agent 1.5 weight portions.
The present invention also provides the preparation method of the sliding wax sense of a kind of use for synthetic leather cloudy surface silk finishing agent, comprises following steps:
1) partially modified polyurethane resin and DMF, butyl acetate, silica flatting silica are stirred the back and grind and filter, discard filter residue;
2) adding modified amido siloxanes, dimethicone, erucyl amide, polyurethane look pearl evenly stir in the mixture that step 1) obtains;
3) in step 2) add remaining polyurethane resin and organosilicon levelling agent in the mixture that obtains, filter the back that stirs, and discards filter residue, promptly get described use for synthetic leather cloudy surface silk and slide wax sense finishing agent.
The proportioning of each component among the preparation method of the sliding wax sense of use for synthetic leather cloudy surface silk provided by the invention finishing agent can be as follows: modified polyurethane resin 30～40 weight portions, DMF 20～30 weight portions, butyl acetate 20～30 weight portions, silica flatting silica 4～5 weight portions, modified amido siloxanes 1～4 weight portion, dimethicone 1～3 weight portion, erucyl amide 1～3 weight portion, polyurethane look pearl 3～5 weight portions, organosilicon levelling agent 1～2 weight portion.
In one embodiment of the invention, the step 1), 2 among the preparation method of the sliding wax sense of use for synthetic leather cloudy surface silk finishing agent), 3) all carry out at normal temperatures and pressures.
Because adopt above technical scheme, the present invention compared with prior art has following advantage:
1, the sliding wax sense of cloudy surface silk finishing agent is an ep-type material, meets the environmental protection standard of European Union;
2, each component of forming the sliding wax sense of silk finishing agent coordinate mutually, acting in conjunction, the cloudy surface extinction effect is good, the sliding wax sense of unique silk, the leather surface leather effect is strong, uses the synthetic leather of this sliding wax sense finishing agent, the sliding feel of its silk, resultant effect is good;
3, the sliding wax sense of this cloudy surface silk finishing agent is used on existing synthetic leather production line, technology is simple, is a kind of new material of back segment printing, and need not to change production equipment increases cost.
The specific embodiment
Below by embodiment, technical solution of the present invention is elaborated, but protection scope of the present invention is not limited to described embodiment.
Embodiment 1
The sliding wax sense of use for synthetic leather cloudy surface silk finishing agent is by modified polyurethane resin 40 weight portions, DMF 20 weight portions, butyl acetate 20 weight portions, silica flatting silica 4 weight portions, modified amido siloxanes 2 weight portions, dimethicone 2 weight portions, erucyl amide 3 weight portions, polyurethane look pearl 3 weight portions, organosilicon levelling agent 1 weight portion is formed.
The preparation method of the sliding wax sense of above-mentioned use for synthetic leather cloudy surface silk finishing agent is: at normal temperatures and pressures, 10 weight portion modified polyurethane resins, 20 weight portion DMF, 20 weight portion butyl acetates and 4 weight portion silica flatting silicas are fully mixed, stir and grind filtration after at least 30 minutes, discard filter residue.In the mixture that obtains, add 2 weight portion modified amido siloxanes, 2 weight portion dimethicones, 3 weight portion erucyl amides, 3 weight portion polyurethane look pearls, stirred at least 30 minutes.Add 30 weight portion modified polyurethane resins and 1 weight portion organosilicon levelling agent after waiting to stir, stir after at least 30 minutes and filter, discard filter residue, promptly get the sliding wax sense of use for synthetic leather cloudy surface silk of the present invention finishing agent.The performance indications of the sliding wax sense of resulting use for synthetic leather cloudy surface silk finishing agent see Table 1.
Methods such as the stirring of being adopted in the above-mentioned preparation process, filtration are customary way in this area.
Embodiment 2
The sliding wax sense of use for synthetic leather cloudy surface silk finishing agent is by modified polyurethane resin 30 weight portions, DMF 30 weight portions, butyl acetate 30 weight portions, silica flatting silica 5 weight portions, modified amido siloxanes 1 weight portion, dimethicone 3 weight portions, erucyl amide 1 weight portion, polyurethane look pearl 5 weight portions, organosilicon levelling agent 2 weight portions are formed.
The preparation method of the sliding wax sense of above-mentioned use for synthetic leather cloudy surface silk finishing agent is: at normal temperatures and pressures, 12 weight portion modified polyurethane resins, 30 weight portion DMF, 30 weight portion butyl acetates and 5 weight portion silica flatting silicas are fully mixed, stir and grind filtration after at least 30 minutes, discard filter residue.In the mixture that obtains, add 1 weight portion modified amido siloxanes, 3 weight portion dimethicones, 1 weight portion erucyl amide, 5 weight portion polyurethane look pearls, stirred at least 30 minutes.Add 18 weight portion modified polyurethane resins and 2 weight portion organosilicon levelling agents after waiting to stir, stir after at least 30 minutes and filter, discard filter residue, promptly get the sliding wax sense of use for synthetic leather cloudy surface silk of the present invention finishing agent.The performance indications of the sliding wax sense of resulting use for synthetic leather cloudy surface silk finishing agent see Table 1.
Methods such as the stirring of being adopted in the above-mentioned preparation process, filtration are customary way in this area.
Embodiment 3
The sliding wax sense of use for synthetic leather cloudy surface silk finishing agent is by modified polyurethane resin 35 weight portions, DMF 25 weight portions, butyl acetate 25 weight portions, silica flatting silica 4.5 weight portions, modified amido siloxanes 4 weight portions, dimethicone 1 weight portion, erucyl amide 2 weight portions, polyurethane look pearl 4 weight portions, organosilicon levelling agent 1.5 weight portions are formed.
The preparation method of the sliding wax sense of above-mentioned use for synthetic leather cloudy surface silk finishing agent is: at normal temperatures and pressures, 20 weight portion modified polyurethane resins, 25 weight portion DMF, 25 weight portion butyl acetates and 4.5 weight portion silica flatting silicas are fully mixed, stir and grind filtration after at least 30 minutes, discard filter residue.In the mixture that obtains, add 4 weight portion modified amido siloxanes, 1 weight portion dimethicone, 2 weight portion erucyl amides, 4 weight portion polyurethane look pearls, stirred at least 30 minutes.Add 15 weight portion modified polyurethane resins and 1.5 weight portion organosilicon levelling agents after waiting to stir, stir after at least 30 minutes and filter, discard filter residue, promptly get the sliding wax sense of use for synthetic leather cloudy surface silk of the present invention finishing agent.The performance indications of the sliding wax sense of resulting use for synthetic leather cloudy surface silk finishing agent see Table 1.
Methods such as the stirring of being adopted in the above-mentioned preparation process, filtration are customary way in this area.
Table 1
The above is preferred embodiment of the present invention only, is not to be used for limiting practical range of the present invention; If do not break away from the spirit and scope of the present invention, the present invention is made amendment or is equal to replacement, all should be encompassed in the middle of the protection domain of claim of the present invention.
Claims (8)
1. a use for synthetic leather cloudy surface silk is slided wax sense finishing agent, it is characterized in that, composed of the following components: modified polyurethane resin, DMF, butyl acetate, silica flatting silica, modified amido siloxanes, dimethicone, erucyl amide, polyurethane look pearl and organosilicon levelling agent.
2. the sliding wax sense of use for synthetic leather cloudy surface silk according to claim 1 finishing agent, it is characterized in that, the proportioning of described each component is as follows: modified polyurethane resin 30～40 weight portions, DMF 20～30 weight portions, butyl acetate 20～30 weight portions, silica flatting silica 4～5 weight portions, modified amido siloxanes 1～4 weight portion, dimethicone 1～3 weight portion, erucyl amide 1～3 weight portion, polyurethane look pearl 3～5 weight portions, organosilicon levelling agent 1～2 weight portion.
3. the sliding wax sense of use for synthetic leather cloudy surface silk according to claim 2 finishing agent, it is characterized in that, the proportioning of described each component is as follows: modified polyurethane resin 40 weight portions, DMF 20 weight portions, butyl acetate 20 weight portions, silica flatting silica 4 weight portions, modified amido siloxanes 2 weight portions, dimethicone 2 weight portions, erucyl amide 3 weight portions, polyurethane look pearl 3 weight portions, organosilicon levelling agent 1 weight portion.
4. the sliding wax sense of use for synthetic leather cloudy surface silk according to claim 2 finishing agent, it is characterized in that, the proportioning of described each component is as follows: modified polyurethane resin 30 weight portions, DMF 30 weight portions, butyl acetate 30 weight portions, silica flatting silica 5 weight portions, modified amido siloxanes 1 weight portion, dimethicone 3 weight portions, erucyl amide 1 weight portion, polyurethane look pearl 5 weight portions, organosilicon levelling agent 2 weight portions.
5. the sliding wax sense of use for synthetic leather cloudy surface silk according to claim 2 finishing agent, it is characterized in that, the proportioning of described each component is as follows: modified polyurethane resin 35 weight portions, DMF 25 weight portions, butyl acetate 25 weight portions, silica flatting silica 4.5 weight portions, modified amido siloxanes 4 weight portions, dimethicone 1 weight portion, erucyl amide 2 weight portions, polyurethane look pearl 4 weight portions, organosilicon levelling agent 1.5 weight portions.
6. the preparation method of the sliding wax sense of each described use for synthetic leather cloudy surface silk of claim 1-5 finishing agent is characterized in that, comprises following steps:
1) partially modified polyurethane resin and DMF, butyl acetate, silica flatting silica are stirred the back and grind and filter, discard filter residue;
2) adding modified amido siloxanes, dimethicone, erucyl amide, polyurethane look pearl evenly stir in the mixture that step 1) obtains;
3) in step 2) add remaining polyurethane resin and organosilicon levelling agent in the mixture that obtains, filter the back that stirs, and discards filter residue, promptly get described use for synthetic leather cloudy surface silk and slide wax sense finishing agent.
7. the preparation method of the sliding wax sense of use for synthetic leather cloudy surface silk according to claim 6 finishing agent, it is characterized in that, the proportioning of each component is as follows: modified polyurethane resin 30～40 weight portions, DMF20～30 weight portions, butyl acetate 20～30 weight portions, silica flatting silica 4～5 weight portions, modified amido siloxanes 1～4 weight portion, dimethicone 1～3 weight portion, erucyl amide 1～3 weight portion, polyurethane look pearl 3～5 weight portions, organosilicon levelling agent 1～2 weight portion.
8. the preparation method of the sliding wax sense of use for synthetic leather cloudy surface silk according to claim 6 finishing agent is characterized in that institute all carries out in steps at normal temperatures and pressures.
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| CN2010105693997A CN102191689A (en) | 2010-12-01 | 2010-12-01 | Fogging surface silky wax feel finishing agent for synthetic leather and preparation method thereof |
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| CN2010105693997A CN102191689A (en) | 2010-12-01 | 2010-12-01 | Fogging surface silky wax feel finishing agent for synthetic leather and preparation method thereof |
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102587145A (en) * | 2012-01-09 | 2012-07-18 | 浙江禾欣实业集团股份有限公司 | Manufacturing method of oil-wax feel Yangbuck |
| CN103031728A (en) * | 2012-08-22 | 2013-04-10 | 江苏宝泽高分子材料股份有限公司 | Skin-touch matte washing and brightening treatment agent for synthetic leather and preparation method thereof |
| CN103031727A (en) * | 2012-08-22 | 2013-04-10 | 江苏宝泽高分子材料股份有限公司 | Water rubbing soft and smooth additive for synthetic leather and preparation method thereof |
| CN103046377A (en) * | 2012-12-28 | 2013-04-17 | 苏州鼎润复合材料有限公司 | Cloudy-surface skin touch-feeling finishing agent for synthetic leather and surface treatment method of synthetic leather |
| CN103255628A (en) * | 2013-05-21 | 2013-08-21 | 江苏宝泽高分子材料股份有限公司 | Matte wet and unsmooth feeling treating agent for synthetic leather and preparation method of treating agent |
| WO2014029057A1 (en) * | 2012-08-21 | 2014-02-27 | 江苏宝泽高分子材料股份有限公司 | Eco-solvent soft and smooth treating agent for yangbuck leather and preparation method thereof |
| CN104032580A (en) * | 2014-06-26 | 2014-09-10 | 江苏宝泽高分子材料股份有限公司 | Crystal haze waxy resin for synthetic leather and preparation method of waxy resin |
| CN104032583A (en) * | 2014-06-30 | 2014-09-10 | 江苏宝泽高分子材料股份有限公司 | Yangbuck matt surface unsmooth wax feeling treating agent for synthetic leather and preparation method thereof |
| CN104047179A (en) * | 2014-06-26 | 2014-09-17 | 江苏宝泽高分子材料股份有限公司 | Injection molding and blow molding treating agent for synthetic leather, and preparation method thereof |
| WO2017088698A1 (en) * | 2015-11-27 | 2017-06-01 | 江苏宝泽高分子材料股份有限公司 | Bright lustering treatment agent for synthetic leather and preparation method for same |
| CN107326681A (en) * | 2017-08-18 | 2017-11-07 | 江苏宝泽高分子材料股份有限公司 | A kind of use for synthetic leather cloudy surface slides waxy-feeling treatment agent and preparation method thereof again |
| CN111040183A (en) * | 2019-12-30 | 2020-04-21 | 江苏领瑞新材料科技有限公司 | Preparation method of resin for stab-resistant coating |
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Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102587145A (en) * | 2012-01-09 | 2012-07-18 | 浙江禾欣实业集团股份有限公司 | Manufacturing method of oil-wax feel Yangbuck |
| WO2014029057A1 (en) * | 2012-08-21 | 2014-02-27 | 江苏宝泽高分子材料股份有限公司 | Eco-solvent soft and smooth treating agent for yangbuck leather and preparation method thereof |
| CN103031727B (en) * | 2012-08-22 | 2014-12-10 | 江苏宝泽高分子材料股份有限公司 | Water rubbing soft and smooth additive for synthetic leather and preparation method thereof |
| CN103031728A (en) * | 2012-08-22 | 2013-04-10 | 江苏宝泽高分子材料股份有限公司 | Skin-touch matte washing and brightening treatment agent for synthetic leather and preparation method thereof |
| CN103031727A (en) * | 2012-08-22 | 2013-04-10 | 江苏宝泽高分子材料股份有限公司 | Water rubbing soft and smooth additive for synthetic leather and preparation method thereof |
| CN103031728B (en) * | 2012-08-22 | 2015-05-13 | 江苏宝泽高分子材料股份有限公司 | Skin-touch matte washing and brightening treatment agent for synthetic leather and preparation method thereof |
| CN103046377A (en) * | 2012-12-28 | 2013-04-17 | 苏州鼎润复合材料有限公司 | Cloudy-surface skin touch-feeling finishing agent for synthetic leather and surface treatment method of synthetic leather |
| CN103255628A (en) * | 2013-05-21 | 2013-08-21 | 江苏宝泽高分子材料股份有限公司 | Matte wet and unsmooth feeling treating agent for synthetic leather and preparation method of treating agent |
| CN104047179A (en) * | 2014-06-26 | 2014-09-17 | 江苏宝泽高分子材料股份有限公司 | Injection molding and blow molding treating agent for synthetic leather, and preparation method thereof |
| CN104032580A (en) * | 2014-06-26 | 2014-09-10 | 江苏宝泽高分子材料股份有限公司 | Crystal haze waxy resin for synthetic leather and preparation method of waxy resin |
| CN104047179B (en) * | 2014-06-26 | 2016-09-07 | 江苏宝泽高分子材料股份有限公司 | A kind of use for synthetic leather injection, blow process agent and preparation method thereof |
| CN104032583A (en) * | 2014-06-30 | 2014-09-10 | 江苏宝泽高分子材料股份有限公司 | Yangbuck matt surface unsmooth wax feeling treating agent for synthetic leather and preparation method thereof |
| WO2017088698A1 (en) * | 2015-11-27 | 2017-06-01 | 江苏宝泽高分子材料股份有限公司 | Bright lustering treatment agent for synthetic leather and preparation method for same |
| CN107326681A (en) * | 2017-08-18 | 2017-11-07 | 江苏宝泽高分子材料股份有限公司 | A kind of use for synthetic leather cloudy surface slides waxy-feeling treatment agent and preparation method thereof again |
| CN111040183A (en) * | 2019-12-30 | 2020-04-21 | 江苏领瑞新材料科技有限公司 | Preparation method of resin for stab-resistant coating |
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Application publication date: 20110921 |