CN102167610A - 氮化硼纤维织物增强氮化硅陶瓷材料的制备方法 - Google Patents
氮化硼纤维织物增强氮化硅陶瓷材料的制备方法 Download PDFInfo
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- CN102167610A CN102167610A CN 201110005941 CN201110005941A CN102167610A CN 102167610 A CN102167610 A CN 102167610A CN 201110005941 CN201110005941 CN 201110005941 CN 201110005941 A CN201110005941 A CN 201110005941A CN 102167610 A CN102167610 A CN 102167610A
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- Prior art keywords
- boron nitride
- silicon nitride
- preparation
- fibre fabric
- ceramic material
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- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 title claims abstract description 55
- 229910052582 BN Inorganic materials 0.000 title claims abstract description 54
- 239000000835 fiber Substances 0.000 title claims abstract description 49
- 229910052581 Si3N4 Inorganic materials 0.000 title claims abstract description 36
- HQVNEWCFYHHQES-UHFFFAOYSA-N silicon nitride Chemical compound N12[Si]34N5[Si]62N3[Si]51N64 HQVNEWCFYHHQES-UHFFFAOYSA-N 0.000 title claims abstract description 36
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 229910010293 ceramic material Inorganic materials 0.000 title claims abstract description 17
- 239000004744 fabric Substances 0.000 claims abstract description 35
- 238000001035 drying Methods 0.000 claims abstract description 15
- 238000005336 cracking Methods 0.000 claims abstract description 14
- 239000002243 precursor Substances 0.000 claims abstract description 7
- 239000002002 slurry Substances 0.000 claims abstract description 3
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims description 14
- 230000002378 acidificating effect Effects 0.000 claims description 9
- 229920001709 polysilazane Polymers 0.000 claims description 9
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 claims description 9
- 238000007711 solidification Methods 0.000 claims description 7
- 230000008023 solidification Effects 0.000 claims description 7
- 238000001132 ultrasonic dispersion Methods 0.000 claims description 7
- 238000002203 pretreatment Methods 0.000 claims description 5
- 238000005470 impregnation Methods 0.000 claims description 3
- 239000012298 atmosphere Substances 0.000 claims description 2
- 229910052757 nitrogen Inorganic materials 0.000 claims description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N nitrogen Substances N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 2
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 claims description 2
- 239000002904 solvent Substances 0.000 claims description 2
- 238000002679 ablation Methods 0.000 abstract description 10
- 239000000463 material Substances 0.000 abstract description 6
- 239000002131 composite material Substances 0.000 abstract description 5
- 238000000034 method Methods 0.000 abstract description 4
- 238000011065 in-situ storage Methods 0.000 abstract description 2
- 238000002791 soaking Methods 0.000 abstract 3
- 239000011248 coating agent Substances 0.000 abstract 1
- 238000000576 coating method Methods 0.000 abstract 1
- 238000000626 liquid-phase infiltration Methods 0.000 abstract 1
- 229910052755 nonmetal Inorganic materials 0.000 abstract 1
- 239000000758 substrate Substances 0.000 abstract 1
- 239000011159 matrix material Substances 0.000 description 9
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 8
- 238000007598 dipping method Methods 0.000 description 8
- 238000005482 strain hardening Methods 0.000 description 6
- 238000000498 ball milling Methods 0.000 description 5
- QFXZANXYUCUTQH-UHFFFAOYSA-N ethynol Chemical group OC#C QFXZANXYUCUTQH-UHFFFAOYSA-N 0.000 description 5
- 238000007676 flexural strength test Methods 0.000 description 5
- 239000012299 nitrogen atmosphere Substances 0.000 description 5
- 239000000919 ceramic Substances 0.000 description 4
- 239000000377 silicon dioxide Substances 0.000 description 4
- 239000012780 transparent material Substances 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- HPNSNYBUADCFDR-UHFFFAOYSA-N chromafenozide Chemical compound CC1=CC(C)=CC(C(=O)N(NC(=O)C=2C(=C3CCCOC3=CC=2)C)C(C)(C)C)=C1 HPNSNYBUADCFDR-UHFFFAOYSA-N 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 229960000935 dehydrated alcohol Drugs 0.000 description 1
- YGANSGVIUGARFR-UHFFFAOYSA-N dipotassium dioxosilane oxo(oxoalumanyloxy)alumane oxygen(2-) Chemical compound [O--].[K+].[K+].O=[Si]=O.O=[Al]O[Al]=O YGANSGVIUGARFR-UHFFFAOYSA-N 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 229960004756 ethanol Drugs 0.000 description 1
- 230000008595 infiltration Effects 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 229910052627 muscovite Inorganic materials 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- 238000009738 saturating Methods 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
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CN 201110005941 CN102167610B (zh) | 2011-01-12 | 2011-01-12 | 氮化硼纤维织物增强氮化硅陶瓷材料的制备方法 |
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Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103664191A (zh) * | 2012-09-13 | 2014-03-26 | 南京航空航天大学 | 一种氮化硼纤维增韧的氮化硼-氮化硅基透波复合材料的制备方法 |
CN103664213A (zh) * | 2012-09-13 | 2014-03-26 | 南京航空航天大学 | 一种混编纤维增韧的高温透波复合材料的制备方法 |
CN104261850A (zh) * | 2014-09-10 | 2015-01-07 | 航天材料及工艺研究所 | 一种耐高温透波氮化硅纤维增强复合材料及其制备方法 |
CN109400173A (zh) * | 2018-10-30 | 2019-03-01 | 山东工业陶瓷研究设计院有限公司 | 一种氮化硼纤维增强氮化物复合材料及其制备方法 |
CN111041819A (zh) * | 2019-12-13 | 2020-04-21 | 武汉纺织大学 | 一种SiC-Si3N4-碳纤维复合的防弹衣面料及其制备方法 |
CN111205097A (zh) * | 2020-01-14 | 2020-05-29 | 中国人民解放军国防科技大学 | 一种具有双透波陶瓷涂层的纤维预制体及其制备方法 |
CN112010654A (zh) * | 2020-09-11 | 2020-12-01 | 航天特种材料及工艺技术研究所 | 一种纤维增强氮化硅复合材料及其制备方法 |
CN114773082A (zh) * | 2022-03-30 | 2022-07-22 | 西北工业大学 | 一种对称连续梯度结构氮化硅陶瓷天线罩及制备方法 |
CN114874016A (zh) * | 2022-04-26 | 2022-08-09 | 滁州用朴新材料科技有限公司 | 一种高韧性高硬度氮化硅陶瓷刀具及其制备方法 |
CN116354736A (zh) * | 2023-03-27 | 2023-06-30 | 中国人民解放军国防科技大学 | 一种纤维增强氧化铝陶瓷基复合材料的制备方法 |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109400193B (zh) * | 2018-10-30 | 2021-08-03 | 山东工业陶瓷研究设计院有限公司 | 一种耐高温抗烧蚀透波端头及其制备方法 |
Citations (4)
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CN85104097A (zh) * | 1985-05-24 | 1986-11-19 | 中国科学院上海硅酸盐研究所 | 氮化硼纤维补强反应烧结氮化硅陶瓷 |
EP0222960A1 (en) * | 1985-11-18 | 1987-05-27 | Battelle Memorial Institute | Method and apparatus for the on-line coating of silica based fibers with boron-nitride |
CN101224989A (zh) * | 2008-01-29 | 2008-07-23 | 中国人民解放军国防科学技术大学 | 二维纤维布增强陶瓷基复合材料及其制备方法 |
CN101555156A (zh) * | 2009-05-15 | 2009-10-14 | 山东大学 | 一种氮化硼晶须/氮化硅陶瓷复合材料及其制备方法 |
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2011
- 2011-01-12 CN CN 201110005941 patent/CN102167610B/zh active Active
Patent Citations (4)
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CN85104097A (zh) * | 1985-05-24 | 1986-11-19 | 中国科学院上海硅酸盐研究所 | 氮化硼纤维补强反应烧结氮化硅陶瓷 |
EP0222960A1 (en) * | 1985-11-18 | 1987-05-27 | Battelle Memorial Institute | Method and apparatus for the on-line coating of silica based fibers with boron-nitride |
CN101224989A (zh) * | 2008-01-29 | 2008-07-23 | 中国人民解放军国防科学技术大学 | 二维纤维布增强陶瓷基复合材料及其制备方法 |
CN101555156A (zh) * | 2009-05-15 | 2009-10-14 | 山东大学 | 一种氮化硼晶须/氮化硅陶瓷复合材料及其制备方法 |
Cited By (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103664191A (zh) * | 2012-09-13 | 2014-03-26 | 南京航空航天大学 | 一种氮化硼纤维增韧的氮化硼-氮化硅基透波复合材料的制备方法 |
CN103664213A (zh) * | 2012-09-13 | 2014-03-26 | 南京航空航天大学 | 一种混编纤维增韧的高温透波复合材料的制备方法 |
CN103664213B (zh) * | 2012-09-13 | 2016-06-08 | 南京航空航天大学 | 一种混编纤维增韧的高温透波复合材料的制备方法 |
CN104261850A (zh) * | 2014-09-10 | 2015-01-07 | 航天材料及工艺研究所 | 一种耐高温透波氮化硅纤维增强复合材料及其制备方法 |
CN104261850B (zh) * | 2014-09-10 | 2015-12-30 | 航天材料及工艺研究所 | 一种耐高温透波氮化硅纤维增强复合材料及其制备方法 |
CN109400173B (zh) * | 2018-10-30 | 2021-09-10 | 山东工业陶瓷研究设计院有限公司 | 一种氮化硼纤维增强氮化物复合材料及其制备方法 |
CN109400173A (zh) * | 2018-10-30 | 2019-03-01 | 山东工业陶瓷研究设计院有限公司 | 一种氮化硼纤维增强氮化物复合材料及其制备方法 |
CN111041819A (zh) * | 2019-12-13 | 2020-04-21 | 武汉纺织大学 | 一种SiC-Si3N4-碳纤维复合的防弹衣面料及其制备方法 |
CN111205097A (zh) * | 2020-01-14 | 2020-05-29 | 中国人民解放军国防科技大学 | 一种具有双透波陶瓷涂层的纤维预制体及其制备方法 |
CN111205097B (zh) * | 2020-01-14 | 2022-03-29 | 中国人民解放军国防科技大学 | 一种具有双透波陶瓷涂层的纤维预制体及其制备方法 |
CN112010654A (zh) * | 2020-09-11 | 2020-12-01 | 航天特种材料及工艺技术研究所 | 一种纤维增强氮化硅复合材料及其制备方法 |
CN114773082A (zh) * | 2022-03-30 | 2022-07-22 | 西北工业大学 | 一种对称连续梯度结构氮化硅陶瓷天线罩及制备方法 |
CN114874016A (zh) * | 2022-04-26 | 2022-08-09 | 滁州用朴新材料科技有限公司 | 一种高韧性高硬度氮化硅陶瓷刀具及其制备方法 |
CN116354736A (zh) * | 2023-03-27 | 2023-06-30 | 中国人民解放军国防科技大学 | 一种纤维增强氧化铝陶瓷基复合材料的制备方法 |
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