CN102114216A - Externally applied antibacterial and antiphlogistic medicament and preparation method thereof - Google Patents
Externally applied antibacterial and antiphlogistic medicament and preparation method thereof Download PDFInfo
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Abstract
The invention discloses an externally applied antibacterial and antiphlogistic medicament and a preparation method thereof, and relates to an antiphlogistic medicament and the preparation method thereof. The antiphlogistic medicament is processed and prepared by the following raw materials: peppermint, fineleaf schizonepeta herb, divaricate saposhnikovia root, rhubarb, amur corktree bark, common andrographis herb, fructus forsythiae, baical skullcap root, Philippine violet herb, radix salviae miltiorrhizae, lightyellow sophora root, dahurian angelica root, tree peony bark, aloe, membranous milkvetch root, indigowoad leaf, sweet wormwood herb, Chinese gentian, sinkiang arnebia root, liquoric root, Chinese gall, golden thread, cassia seed, indigowoad root, honeysuckle flower, chrysanthemum, hawthorn fruit, sessile stemona root, argy wormwood leaf, common cnidium fruit, borneol powder, borax powder, honey, propanetriol, propanediol, Tween-60, OP10, castor oil and turpentine oil. The product has good antibacterial and antiphlogistic effects, bacteria can not generate an antibody and can not generate the resistance to the medicament, the bacteria can be prevented from being mutated to superbacteria, and the antiphlogistic medicament has no toxicity or side effects and is safe to use.
Description
Technical field
The present invention relates to a kind of antiphlogistic medicament and preparation method thereof, say it is a kind of external application anti-inflammation medicament and preparation method thereof in detail.
Background technology
In daily life, human health usually is subjected to the threat of various diseases, and in these various diseases, modal is exactly various types of inflammation, and inflammation causes because of various bacterial infections.All in people's brains have the inflammation disease must use antibiotic, and the toxic and side effects of these medicines is big.China is one of country of abuse of antibiotics in the world, and abuse of antibiotics has brought Drug resistance, pathogenicity, sequela, the variability of antibacterial and virus.The present age is annual in the whole world, and nearly 50% antibiotic is abused, and China in this ratio on the one hand near 80%.Exactly because antibiotic abuse makes pathogenic bacteria adapt to antibiotic environment rapidly, various superbug are born in succession.Because drug-fast bacterial infection, antibiotic is uncontrollable, finally causes patient death.In the sixties in last century, it is about 7,000,000 that the number of infectious disease is died from the whole world every year, and this numeral to the beginning of this century rise to 2,000 ten thousand, the number of dying from septicemia has risen 80%, most people die from the medication difficulty that superbacteria brings.
Summary of the invention
The technical problem that the present invention solves is, provides a kind of anti-inflammation effective, and antibacterial can not produce antibody, no Drug resistance, avoids bacterial dissociation to become superbacteria, has no side effect, external application anti-inflammation medicament safe in utilization and preparation method thereof.
Technical scheme of the present invention is:
A kind of external application anti-inflammation medicament is by raw material (pressing proportion by weight) Herba Menthae 5-15 part, Herba Schizonepetae 5-15 part, Radix Saposhnikoviae 5-15 part, Radix Et Rhizoma Rhei 5-15 part, Cortex Phellodendri 5-15 part, Herba Andrographis 5-15 part, Fructus Forsythiae 5-15 part, Radix Scutellariae 5-15 part, bavin flower Herba Violae 5-15 part, Radix Salviae Miltiorrhizae 5-15 part, Radix Sophorae Flavescentis 5-15 part, Radix Angelicae Dahuricae 5-15 part, Cortex Moutan 5-15 part, Aloe 5-15 part, Radix Astragali 5-15 part, Folium Isatidis 5-15 part, Herba Artemisiae Annuae 5-15 part, Radix Gentianae 5-15 part, Radix Arnebiae (Radix Lithospermi) 5-15 part, Radix Glycyrrhizae 5-15 part, Galla Chinensis 5-15 part, Rhizoma Coptidis 5-15 part, Semen Cassiae 5-15 part, Radix Isatidis 5-15 part, Flos Lonicerae 5-15 part, Flos Chrysanthemi 5-15 part, Fructus Crataegi 5-15 part, Radix Stemonae 5-15 part, Folium Artemisiae Argyi 5-15 part, Fructus Cnidii 5-15 part, Borneolum Syntheticum powder 5-15 part, Borax powder 5-15 part, Mel 80-120 part, glycerol 400-600 part, propylene glycol 150-250 part, tween
6080-120 part, OP
1080-120 part, Oleum Ricini 40-60 part, Oleum Terebinthinae 40-60 part are processed into.
A kind of preparation method of external application anti-inflammation medicament is (pressing proportion by weight):
1, chooses raw material by proportion by weight;
2, Herba Menthae, Herba Schizonepetae, Herba Andrographis, Aloe, Folium Isatidis, Herba Artemisiae Annuae, Radix Gentianae, Radix Arnebiae (Radix Lithospermi), Radix Glycyrrhizae, Flos Lonicerae, Flos Chrysanthemi, Fructus Crataegi, Folium Artemisiae Argyi 13 flavor medicines are shredded to 30 orders, the concentration that immerses 10 times of own wts is in 45% the ethanol, room temperature soaks 4 days after-filtration down and removes slag, the boiled water that adds its weight 20% in filtrate precipitates 48 hours, remove precipitate, it is stand-by to get extracting solution;
3, Radix Saposhnikoviae, Radix Et Rhizoma Rhei, Cortex Phellodendri, Fructus Forsythiae, Radix Scutellariae, Herba Violae, Radix Salviae Miltiorrhizae, Radix Sophorae Flavescentis, the Radix Angelicae Dahuricae, Cortex Moutan, the Radix Astragali, Galla Chinensis, Rhizoma Coptidis, Semen Cassiae, Radix Isatidis, the Radix Stemonae, Fructus Cnidii 17 flavor medicated powder are broken to 40 orders, immerse in the clear water of 20 times of own wts, decoct to boiling 20 minutes, the decoction after-filtration removes slag, in filtrate, added its weight 20% concentration and be 40% ethanol precipitation 24 hours, remove precipitate, it is stand-by to get extracting solution;
4, the extracting solution and the 3rd that the 2nd step was made goes on foot the extracting solution mixing that makes, and adds Borneolum Syntheticum powder, Borax powder, Mel, glycerol, propylene glycol, tween
60, OP
10, Oleum Ricini, Oleum Terebinthinae mix together, heat to 40 ℃ of emulsifyings 8 hours;
5, the 4th step gained emulsion is ground 2 times with colloid mill, put into the sterilization of high temperature sterilize pot, be filled into bottle and irradiation-sterilize after the sterilization, get product.
The invention has the beneficial effects as follows the pharmacology foundation of main component in the crude drug: 1, Herba Menthae: inhibited to staphylococcus aureus, Staphylococcus albus, alpha streptococcus, group B streptococcus, enteritis coccus, shigella flexneri, anthrax bacillus, diphtheria corynebacterium, Bacillus typhi, bacillus pyocyaneus, escherichia coli etc.2, Herba Schizonepetae: staphylococcus aureus and diphtheria corynebacterium are had stronger antibacterial action.3, Radix Saposhnikoviae: bacillus pyocyaneus and staphylococcus aureus are had certain antibacterial action.4, Radix Et Rhizoma Rhei: staphylococcus, Hemolytic streptococcus, micrococcus gonococcus, Bacillus typhi, dysentery bacterium are had antibacterial action.5, Cortex Phellodendri:, also Diplococcus pneumoniae, comma bacillus, bacillus subtilis, meningococcus are had inhibitory action except that above-mentioned antibacterial is had the inhibition.6, Herba Andrographis: all effective in cure to multiple trauma infection contamination furuncle, carbuncle, erysipelas, upper respiratory tract infection, chronic tonsillitis, pharyngolaryngitis, bacillary dysentery, gastroenteritis, urinary tract infection, endometritis, otitis media, periodontitis etc.7, Fructus Forsythiae: can suppress typhoid fever and Salmonella paratyphi, escherichia coli, dysentery bacterium, diphtheria corynebacterium, comma bacillus, staphylococcus, streptococcus.8, Radix Scutellariae: cure mainly epidemic febrile disease, inflammation of upper respiratory tract, pneumonia, jaundice, dysentery etc., antibacterial action is better than Rhizoma Coptidis, does not develop immunity to drugs.9, bavin flower Herba Violae: tubercule bacillus and hook end spiral shell family body are had inhibitory action.10, Radix Salviae Miltiorrhizae: staphylococcus, escherichia coli, degeneration bacillus are had inhibitory action.11, Radix Sophorae Flavescentis: staphylococcus aureus and trichophyton, Trichophyton concentricunm, trichophyton etc. are had inhibitory action.12, the Radix Angelicae Dahuricae: escherichia coli, dysentery bacterium, Bacillus proteus and gram positive bacteria are all had inhibitory action.13, Cortex Moutan: bacillus subtilis, escherichia coli, Bacillus typhi etc. are had inhibitory action.14, Aloe: fungus, mycete, diphtheria bacterium, tetanolysin, Bubonic plague bacterium etc. are had inhibitory action.15, the Radix Astragali: chronic nephritis, rhinitis, digestive tract, ulcer, HIV (human immunodeficiency virus) are had antiinflammatory action.16, Folium Isatidis: staphylococcus aureus, alpha streptococcus, meningococcus, streptococcus pneumoniae, card ground coccus, Bacillus typhi, hemophilus influenza, diphtheria corynebacterium are had certain inhibitory action.17, Herba Artemisiae Annuae: staphylococcus epidermidis, card ground coccus, anthrax bacillus are had stronger bacteriostasis.18, Radix Gentianae: trichophyton gypseum, star nocardia, dermatophytes are had the effect of inhibition.19, Radix Arnebiae (Radix Lithospermi): gold-coloured staphylococci, escherichia coli, bacillus subtilis are had inhibitory action.20, Radix Glycyrrhizae: staphylococcus aureus, bacillus subtilis, yeast, streptococcus etc. are had inhibitory action.21, Galla Chinensis: gold-coloured staphylococci, streptococcus, streptococcus pneumoniae, typhoid fever and Salmonella paratyphi etc. are had the obvious sterilization effect.22, Rhizoma Coptidis: gold-coloured staphylococci, Hemolytic streptococcus, streptococcus pneumoniae, meningococcus, anthrax bacillus are had inhibitory action.23, Semen Cassiae: staphylococcus, diphtheria corynebacterium, Bacillus typhi, Salmonella paratyphi, escherichia coli are all had inhibitory action.24, Radix Isatidis: bacillus subtilis, staphylococcus aureus, sarcine, escherichia coli, typhoid fever and Salmonella paratyphi, dysentery bacterium, bacillus enteritidis are all had inhibitory action.25, Flos Lonicerae: Bacillus proteus, bordetella pertussis and the Cao Lanshi positive, negative bacterium such as gold-coloured staphylococci, Staphylococcus albus, Hemolytic streptococcus, pneumobacillus, meningococcus, Bacillus typhi are all had inhibitory action.26, Flos Chrysanthemi: inhibited to Song Shi dysentery bacterium, Bacillus proteus, typhoid fever Salmonella paratyphi, bacillus pyocyaneus, escherichia coli and comma bacillus etc.27, Fructus Crataegi: shigella flexneri, Song Shi dysentery bacterium, Bacillus proteus, escherichia coli are all had antibacterial action.28, the Radix Stemonae: golden yellow and Staphylococcus albus, beta hemolytic streptococcus, anthrax bacillus, pneumobacillus etc. and bacillus pestis are had bacteriostasis.29, Folium Artemisiae Argyi: 10 kinds of Cao Lanshi positive bacterias such as anthrax bacillus, alpha-Hemolytic streptococcus, beta hemolytic streptococcus, diphtheria corynebacterium, bacillus pseudodiphthericus, Diplococcus pneumoniae, staphylococcus aureus, Staphylococcus citreus, Staphylococcus albus, bacillus subtilis are had antibacterial action.30, Fructus Cnidii: acrothesium floccosum, Gypsum Fibrosum sample microspore bacterium, ulotrichy microspore bacterium are all had inhibitory action.By above-mentioned material is that the external application anti-inflammation medicament anti-inflammation made of the mutual compatibility of primary raw material is effective, antibacterial can not produce antibody during medication, and the long-term prescription antibacterial does not have Drug resistance, avoids bacterial dissociation to become superbacteria, this product has no side effect, and is safe in utilization.
The specific embodiment
Embodiment 1
A kind of external application anti-inflammation medicament is by raw material (pressing proportion by weight) Herba Menthae 5-15 part, Herba Schizonepetae 5-15 part, Radix Saposhnikoviae 5-15 part, Radix Et Rhizoma Rhei 5-15 part, Cortex Phellodendri 5-15 part, Herba Andrographis 5-15 part, Fructus Forsythiae 5-15 part, Radix Scutellariae 5-15 part, bavin flower Herba Violae 5-15 part, Radix Salviae Miltiorrhizae 5-15 part, Radix Sophorae Flavescentis 5-15 part, Radix Angelicae Dahuricae 5-15 part, Cortex Moutan 5-15 part, Aloe 5-15 part, Radix Astragali 5-15 part, Folium Isatidis 5-15 part, Herba Artemisiae Annuae 5-15 part, Radix Gentianae 5-15 part, Radix Arnebiae (Radix Lithospermi) 5-15 part, Radix Glycyrrhizae 5-15 part, Galla Chinensis 5-15 part, Rhizoma Coptidis 5-15 part, Semen Cassiae 5-15 part, Radix Isatidis 5-15 part, Flos Lonicerae 5-15 part, Flos Chrysanthemi 5-15 part, Fructus Crataegi 5-15 part, Radix Stemonae 5-15 part, Folium Artemisiae Argyi 5-15 part, Fructus Cnidii 5-15 part, Borneolum Syntheticum powder 5-15 part, Borax powder 5-15 part, Mel 80-120 part, glycerol 400-600 part, propylene glycol 150-250 part, tween
6080-120 part, OP
1080-120 part, Oleum Ricini 40-60 part, Oleum Terebinthinae 40-60 part are processed into.
Its preparation method is (pressing proportion by weight):
1, choose raw material: 5 parts of Herba Menthaes, 15 parts of Herba Schizonepetae, 5 parts of Radix Saposhnikoviaes, 15 parts of Radix Et Rhizoma Rhei, 5 parts of Cortex Phellodendris, 15 parts of Herba Andrographis, 5 parts of Fructus Forsythiaes, 15 parts of Radix Scutellariaes, 5 parts of bavin flower Herba Violaes, 15 parts of Radix Salviae Miltiorrhizaes, 5 parts of Radix Sophorae Flavescentiss, 15 parts of the Radixs Angelicae Dahuricae, 5 parts of Cortex Moutans, 15 parts of Aloes, 5 parts of the Radixs Astragali, 15 parts of Folium Isatidiss, 5 parts of Herba Artemisiae Annuaes, 15 parts of Radix Gentianaes, 5 parts of Radix Arnebiae (Radix Lithospermi)s, 15 parts in Radix Glycyrrhizae, 5 parts of Galla Chinensiss, 15 parts of Rhizoma Coptidis, 5 parts of Semen Cassiaes, 15 parts of Radix Isatidis, 5 parts of Flos Loniceraes, 15 parts of Flos Chrysanthemis, 5 parts of Fructus Crataegis, 15 parts of the Radixs Stemonae, 5 parts of Folium Artemisiae Argyis, 15 parts of Fructus Cnidiis, 5 parts of Borneolum Syntheticum powder, 15 parts in Borax powder, 80 parts of Mel, 600 parts of glycerol, 150 parts of propylene glycol, tween
60120 parts, OP
1080 parts, 60 parts of Oleum Ricini, 40 parts of Oleum Terebinthinaes;
2, Herba Menthae, Herba Schizonepetae, Herba Andrographis, Aloe, Folium Isatidis, Herba Artemisiae Annuae, Radix Gentianae, Radix Arnebiae (Radix Lithospermi), Radix Glycyrrhizae, Flos Lonicerae, Flos Chrysanthemi, Fructus Crataegi, Folium Artemisiae Argyi 13 flavor medicines are shredded to 30 orders, the concentration that immerses 10 times of own wts is in 45% the ethanol, room temperature soaks 4 days after-filtration down and removes slag, the boiled water that adds its weight 20% in filtrate precipitates 48 hours, remove precipitate, it is stand-by to get extracting solution;
3, Radix Saposhnikoviae, Radix Et Rhizoma Rhei, Cortex Phellodendri, Fructus Forsythiae, Radix Scutellariae, Herba Violae, Radix Salviae Miltiorrhizae, Radix Sophorae Flavescentis, the Radix Angelicae Dahuricae, Cortex Moutan, the Radix Astragali, Galla Chinensis, Rhizoma Coptidis, Semen Cassiae, Radix Isatidis, the Radix Stemonae, Fructus Cnidii 17 flavor medicated powder are broken to 40 orders, immerse in the clear water of 20 times of own wts, decoct to boiling 20 minutes, the decoction after-filtration removes slag, in filtrate, added its weight 20% concentration and be 40% ethanol precipitation 24 hours, remove precipitate, it is stand-by to get extracting solution;
4, the extracting solution and the 3rd that the 2nd step was made goes on foot the extracting solution mixing that makes, with Borneolum Syntheticum powder, Borax powder, Mel, glycerol, propylene glycol, tween
60, OP
10, Oleum Ricini, Oleum Terebinthinae mix together, heat to 40 ℃ of emulsifyings 8 hours;
5, the 4th step gained emulsion is ground 2 times with colloid mill, put into the sterilization of high temperature sterilize pot, be filled into bottle and irradiation-sterilize after the sterilization, get product.
Embodiment 2:
A kind of preparation method of external application anti-inflammation medicament is (pressing proportion by weight):
1, choose raw material: 10 parts of Herba Menthaes, 10 parts of Herba Schizonepetae, 10 parts of Radix Saposhnikoviaes, 10 parts of Radix Et Rhizoma Rhei, 10 parts of Cortex Phellodendris, 10 parts of Herba Andrographis, 10 parts of Fructus Forsythiaes, 10 parts of Radix Scutellariaes, 10 parts of bavin flower Herba Violaes, 10 parts of Radix Salviae Miltiorrhizaes, 10 parts of Radix Sophorae Flavescentiss, 10 parts of the Radixs Angelicae Dahuricae, 10 parts of Cortex Moutans, 10 parts of Aloes, 10 parts of the Radixs Astragali, 10 parts of Folium Isatidiss, 10 parts of Herba Artemisiae Annuaes, 10 parts of Radix Gentianaes, 10 parts of Radix Arnebiae (Radix Lithospermi)s, 10 parts in Radix Glycyrrhizae, 10 parts of Galla Chinensiss, 10 parts of Rhizoma Coptidis, 10 parts of Semen Cassiaes, 10 parts of Radix Isatidis, 10 parts of Flos Loniceraes, 10 parts of Flos Chrysanthemis, 10 parts of Fructus Crataegis, 10 parts of the Radixs Stemonae, 10 parts of Folium Artemisiae Argyis, 10 parts of Fructus Cnidiis, 10 parts of Borneolum Syntheticum powder, 10 parts in Borax powder, 100 parts of Mel, 500 parts of glycerol, 200 parts of propylene glycol, tween
60100 parts, OP
10100 parts, 50 parts of Oleum Ricini, 50 parts of Oleum Terebinthinaes;
Other steps are identical with embodiment 1, repeat no more.
Embodiment 3:
A kind of preparation method of external application anti-inflammation medicament is (pressing proportion by weight):
1, choose raw material: 15 parts of Herba Menthaes, 5 parts of Herba Schizonepetae, 15 parts of Radix Saposhnikoviaes, 5 parts of Radix Et Rhizoma Rhei, 15 parts of Cortex Phellodendris, 5 parts of Herba Andrographis, 15 parts of Fructus Forsythiaes, 5 parts of Radix Scutellariaes, 15 parts of bavin flower Herba Violaes, 5 parts of Radix Salviae Miltiorrhizaes, 15 parts of Radix Sophorae Flavescentiss, 5 parts of the Radixs Angelicae Dahuricae, 15 parts of Cortex Moutans, 5 parts of Aloes, 15 parts of the Radixs Astragali, 5 parts of Folium Isatidiss, 15 parts of Herba Artemisiae Annuaes, 5 parts of Radix Gentianaes, 15 parts of Radix Arnebiae (Radix Lithospermi)s, 5 parts in Radix Glycyrrhizae, 15 parts of Galla Chinensiss, 5 parts of Rhizoma Coptidis, 15 parts of Semen Cassiaes, 5 parts of Radix Isatidis, 15 parts of Flos Loniceraes, 5 parts of Flos Chrysanthemis, 15 parts of Fructus Crataegis, 5 parts of the Radixs Stemonae, 15 parts of Folium Artemisiae Argyis, 5 parts of Fructus Cnidiis, 15 parts of Borneolum Syntheticum powder, 5 parts in Borax powder, 120 parts of Mel, 400 parts of glycerol, 250 parts of propylene glycol, tween
6080 parts, OP
10120 parts, 40 parts of Oleum Ricini, 60 parts of Oleum Terebinthinaes;
Other steps are identical with embodiment 1, repeat no more.
During use, medicament is spread upon on the gauze, bundle is rolled in chest and back or waist and belly, with thin film externally package tightly get final product, once a day, can take off in each 4-6 hour.Indication: the inflammatory of each internal organs infects in the body, and the various infection of skin are to fever, tic, inflammatory pain, coughing, pant all can be effective.Local inflammation can wrap up part or upper body.Symptom changes with injection equally fast, no pain, non-stimulated, have no side effect, do not have Drug resistance.
Through clinical statistics, use example surplus this external application anti-inflammation medicament treatment patient 300, effective percentage reaches 95%, cure rate 72%.
Claims (2)
1. an external application anti-inflammation medicament is characterized in that: by raw material (pressing proportion by weight) Herba Menthae 5-15 part, Herba Schizonepetae 5-15 part, Radix Saposhnikoviae 5-15 part, Radix Et Rhizoma Rhei 5-15 part, Cortex Phellodendri 5-15 part, Herba Andrographis 5-15 part, Fructus Forsythiae 5-15 part, Radix Scutellariae 5-15 part, bavin flower Herba Violae 5-15 part, Radix Salviae Miltiorrhizae 5-15 part, Radix Sophorae Flavescentis 5-15 part, Radix Angelicae Dahuricae 5-15 part, Cortex Moutan 5-15 part, Aloe 5-15 part, Radix Astragali 5-15 part, Folium Isatidis 5-15 part, Herba Artemisiae Annuae 5-15 part, Radix Gentianae 5-15 part, Radix Arnebiae (Radix Lithospermi) 5-15 part, Radix Glycyrrhizae 5-15 part, Galla Chinensis 5-15 part, Rhizoma Coptidis 5-15 part, Semen Cassiae 5-15 part, Radix Isatidis 5-15 part, Flos Lonicerae 5-15 part, Flos Chrysanthemi 5-15 part, Fructus Crataegi 5-15 part, Radix Stemonae 5-15 part, Folium Artemisiae Argyi 5-15 part, Fructus Cnidii 5-15 part, Borneolum Syntheticum powder 5-15 part, Borax powder 5-15 part, Mel 80-120 part, glycerol 400-600 part, propylene glycol 150-250 part, tween
6080-120 part, OP
1080-120 part, Oleum Ricini 40-60 part, Oleum Terebinthinae 40-60 part are processed into.
2. the preparation method of a kind of external application anti-inflammation medicament according to claim 1 is characterized in that (pressing proportion by weight):
(1), chooses raw material by proportion by weight;
(2), Herba Menthae, Herba Schizonepetae, Herba Andrographis, Aloe, Folium Isatidis, Herba Artemisiae Annuae, Radix Gentianae, Radix Arnebiae (Radix Lithospermi), Radix Glycyrrhizae, Flos Lonicerae, Flos Chrysanthemi, Fructus Crataegi, Folium Artemisiae Argyi 13 flavor medicines are shredded to 30 orders, the concentration that immerses 10 times of own wts is in 45% the ethanol, room temperature soaks 4 days after-filtration down and removes slag, the boiled water that adds its weight 20% in filtrate precipitates 48 hours, remove precipitate, it is stand-by to get extracting solution;
(3), Radix Saposhnikoviae, Radix Et Rhizoma Rhei, Cortex Phellodendri, Fructus Forsythiae, Radix Scutellariae, Herba Violae, Radix Salviae Miltiorrhizae, Radix Sophorae Flavescentis, the Radix Angelicae Dahuricae, Cortex Moutan, the Radix Astragali, Galla Chinensis, Rhizoma Coptidis, Semen Cassiae, Radix Isatidis, the Radix Stemonae, Fructus Cnidii 17 flavor medicated powder are broken to 40 orders, immerse in the clear water of 20 times of own wts, decoct to boiling 20 minutes, the decoction after-filtration removes slag, in filtrate, added its weight 20% concentration and be 40% ethanol precipitation 24 hours, remove precipitate, it is stand-by to get extracting solution;
(4), the extracting solution and the 3rd that the 2nd step was made goes on foot the extracting solution mixing that makes, adding Borneolum Syntheticum powder, Borax powder, Mel, glycerol, propylene glycol, tween
60, OP
10, Oleum Ricini, Oleum Terebinthinae mix together, heat to 40 ℃ of emulsifyings 8 hours;
(5), the 4th step gained emulsion is ground 2 times with colloid mill, put into the sterilization of high temperature sterilize pot, be filled into bottle and irradiation-sterilize after the sterilization, get product.
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