CN101982517A - Modified asphalt adhesive and preparation method thereof - Google Patents
Modified asphalt adhesive and preparation method thereof Download PDFInfo
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- CN101982517A CN101982517A CN2010105481122A CN201010548112A CN101982517A CN 101982517 A CN101982517 A CN 101982517A CN 2010105481122 A CN2010105481122 A CN 2010105481122A CN 201010548112 A CN201010548112 A CN 201010548112A CN 101982517 A CN101982517 A CN 101982517A
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Abstract
The invention discloses a modified asphalt adhesive and a preparation method thereof. The preparation method comprises the following steps: pumping fused asphalt in a stirring kettle; starting a stirring paddle, wherein, the stirring speed is 60-200 revolutions/min, and the material temperature is 120-150 DEG C; stirring for 10-30min; adding styrene-butadiene block copolymer (SBS) and styrene butadiene rubber (SBR) and continuously stirring; heating to 160-180 DEG C; stirring for 1-2h; keeping the stirring temperature and the stirring speed; adding tackifier; continuously stirring for 30-60min; adding rubber powder and filler in sequence; continuously stirring for 30-60min; and grinding by a colloid mill to obtain the modified asphalt adhesive with good performance.
Description
Technical field
The present invention relates to field of waterproof materials, a kind of modifying asphalt sizing agent of saying so more specifically with good adhesion, good high temperature resistant and resistance to low temperature.
Background technology
Along with greatly developing of national large foundation Facilities Construction and public works, waterproofing work becomes the most important thing in these engineerings, and waterproof problem receives much concern.Various waterproof materials emerge in an endless stream, and the quality of water-proof material performance directly has influence on the success or failure of waterproofing work, and then have influence on the functional quality of whole engineering, and therefore, the user is in waterproof construction, and is very prudent to the selection of water-proof material.Along with the requirement to waterproofing quality is more and more higher, simultaneously, also excited the development potentiality of field of waterproof materials, the development of water-proof material enters flourishing high-speed development period, at present, main waterproof roll is divided into asphalt felt class, high-polymer modified pitch base waterproof roll class and polymer membranes class on the market, and pitch class waterproof roll is withdrawn from the market gradually owing to environmental issue; Polymer modified bituminous waterproof sheet material is with its cheap cost, good performance and become the main flow in market; High score subclass waterproof roll mechanical property is very good, but cost is higher, and the commercial market is difficult to be popularized.Present all tabula rasa waterproof rolls, what realize in waterproofing work all is " raincoat formula " waterproof, and the fatal shortcoming that this waterproof roll exists is " string water " problem, and leak is easy-to-search not, is difficult for repairing; In order to realize " skin-type " waterproof, waterproof roll and base material are realized good applying, thoroughly solve " string water " problem, this waterproof roll surface needs compound one deck sizing agent, thereby realize the comprehensive excellent bonds of waterproof roll and base material, and become " skin " of base material, realize " skin-type " waterproof.At present, the shortcoming such as the cost height that exist of some sizing agents, bond properties is poor, high temperature is easy " trickling ", low temperature easy " embrittlement " etc.
Summary of the invention
The object of the invention is to overcome the shortcoming and defect of prior art, and a kind of modifying asphalt sizing agent with good bond properties, resistance to elevated temperatures, resistance to low temperature and cheap advantages such as cost is provided.
The technical scheme that the present invention solves described modifying asphalt sizing agent technical problem is: design a kind of modifying asphalt sizing agent, it is characterized in that this modifying asphalt sizing agent is made up of the following portions by weight material:
Pitch 45-65 part
Tackifier 10-30 part
SBS 3-15 part
SBR 1-10 part
Filler 5-20 part
Rubber powder 5-15 part
Described pitch is 90# pitch or 100# pitch or two kinds of asphalt mixtures;
Described tackifier are one or more compounds in terpine resin, aromatic hydrocarbon oil, the rosin;
Described SBS is a kind of among trade mark KTR-101, LG411, GF-6, YH-791 and the YH-792;
Described SBR is a kind of powder styrene butadiene rubber or several different trade mark powder styrene butadiene rubber compound;
Described filler is one or more compounds in talcum powder, lime carbonate, mica powder and the barium sulfate;
Described rubber powder is a using rubber powder of waste tire.
The technical scheme that the present invention solves described preparation method's technical problem is: design a kind of preparation method of modifying asphalt sizing agent, this preparation method is a foundation with the sizing agent of parts by weight material of the present invention, and adopts following technology:
Under the normal temperature, composition according to described sizing agent parts by weight, earlier fused pitch is got in the stirring tank by pump, stirring tank is the chuck stainless steel cauldron, heat by thermal oil, open stirring rake, stirring velocity is 60-200 rev/min, temperature of charge is 120-150 ℃, stirs 10-30 minute; Adding SBS, SBR continues to stir, and temperature is raised to 160-180 ℃, stirred 1-2 hour, keep whipping temp and stirring velocity, add tackifier, continue to stir 30-60 minute, add rubber powder and filler then successively, continue to stir 30-60 minute, after colloidal mill grinds, the modifying asphalt sizing agent that obtained performance is good.
Compared with prior art, modifying asphalt sizing agent of the present invention and preparation method thereof has following advantage:
1 with macromolecular material have excellent adhesion performance;
2 good high temperature resistant and resistance to low temperatures;
3 cheap costs, excellent performance has the stronger market competitiveness;
The employing of 4 waste Crumb rubbers has positive environmental protection and energy saving meaning.
Figure of description
Fig. 1 modifying asphalt sizing agent technological process of production figure
Embodiment:
Below in conjunction with embodiment the present invention is done further explaination.
Modifying asphalt sizing agent of the present invention (abbreviation sizing agent) is characterized in that the mixture that this sizing agent is made up of the following portions by weight material:
Pitch 45-65 part
Tackifier 10-30 part
SBS 3-15 part
SBR 1-10 part
Filler 5-20 part
Rubber powder 5-15 part
Described pitch is 90# pitch;
Described tackifier are the compound of the aromatic hydrocarbon oil of the terpine resin of 3-10 part and 10-20 part;
Described SBS is trade mark LG411;
Described SBR is a kind of powder styrene butadiene rubber GS-1;
Described filler is the talcum powder of 5-10 part and the compound of 1-10 part lime carbonate;
Described rubber powder is 60 order using rubber powder of waste tire.
The present invention has designed the preparation method (abbreviation preparation method) of described modifying asphalt sizing agent simultaneously.This preparation method is a foundation with the sizing agent of parts by weight material of the present invention, earlier the 90# pitch of fused 45-65 part is got in the stirring tank by pump, stirring tank is the chuck stainless steel cauldron, heat by thermal oil, open stirring rake, stirring velocity is 60-200 rev/min, and temperature of charge is 120-150 ℃, stirs 10-30 minute; Adding the LG411SBS of 3-15 part, the powder styrene butadiene rubber GS-1SBR of 1-10 part continues to stir, and temperature is raised to 160-180 ℃, stirred 1-2 hour, keep whipping temp and stirring velocity, add terpine resin of 3-10 part and the aromatic hydrocarbon oil of 10-20 part, continue to stir 30-60 minute, add the 60 order rubber powders of 5-15 part, the talcum powder of 5-10 part and the lime carbonate of 1-10 part then successively, continue to stir 30-60 minute, after colloidal mill grinds, the modifying asphalt sizing agent that obtained performance is good.
Provide specific embodiments of the invention below, these embodiment further specify of the present invention, do not constitute the restriction to claim protection domain of the present invention.
Embodiment 1:
Prescription and preparation method:
1, prescription:
Pitch 450kg
Tackifier 200kg
SBS 30kg
SBR 10kg
Filler 150kg
Rubber powder 100kg
2, preparation method:
Earlier the 90# pitch of fused 450kg is got in the stirring tank by pump, stirring tank is the chuck stainless steel cauldron, heats by thermal oil, opens stirring rake, and stirring velocity is 100 rev/mins, and temperature of charge is 130 ℃, stirs 20 minutes; The powder styrene butadiene rubber GS-1SBR that adds LG411SBS, the 10kg of 30kg continues to stir, and temperature is raised to 170 ℃, stirred 1.5 hours, keep whipping temp and stirring velocity, add the terpine resin of 50kg and the aromatic hydrocarbon oil of 150kg, continue to stir 40 minutes, add the 60 order rubber powders of 100kg, the talcum powder of 50kg and the lime carbonate of 100kg then successively, continue to stir 50 minutes, after colloidal mill grinds, the modifying asphalt sizing agent that obtained performance is good.
The salient features of the sizing agent that the present invention is prepared
Embodiment 2:
Prescription and preparation method:
1, prescription:
Pitch 450kg
Tackifier 180kg
SBS 50kg
SBR 20kg
Filler 150kg
Rubber powder 100kg
2, preparation method:
Earlier the 90# pitch of fused 450kg is got in the stirring tank by pump, stirring tank is the chuck stainless steel cauldron, heats by thermal oil, opens stirring rake, and stirring velocity is 120 rev/mins, and temperature of charge is 130 ℃, stirs 30 minutes; The powder styrene butadiene rubber GS-1SBR that adds LG411SBS, the 20kg of 50kg continues to stir, and temperature is raised to 170 ℃, stirred 1.5 hours, keep whipping temp and stirring velocity, add the terpine resin of 80kg and the aromatic hydrocarbon oil of 100kg, continue to stir 40 minutes, add the 60 order rubber powders of 100kg, the talcum powder of 50kg and the lime carbonate of 100kg then successively, continue to stir 50 minutes, after colloidal mill grinds, the modifying asphalt sizing agent that obtained performance is good.
Embodiment 3:
Prescription and preparation method:
1, prescription:
Pitch 450kg
Tackifier 250kg
SBS 80kg
SBR 30kg
Filler 120kg
Rubber powder 80kg
2, preparation method:
Earlier the 90# pitch of fused 450kg is got in the stirring tank by pump, stirring tank is the chuck stainless steel cauldron, heats by thermal oil, opens stirring rake, and stirring velocity is 100 rev/mins, and temperature of charge is 130 ℃, stirs 20 minutes; The powder styrene butadiene rubber GS-1SBR that adds LG411SBS, the 30kg of 80kg continues to stir, and temperature is raised to 170 ℃, stirred 1.5 hours, keep whipping temp and stirring velocity, add the terpine resin of 100kg and the aromatic hydrocarbon oil of 150kg, continue to stir 40 minutes, add the 60 order rubber powders of 80kg, the talcum powder of 50kg and the lime carbonate of 70kg then successively, continue to stir 50 minutes, after colloidal mill grinds, the modifying asphalt sizing agent that obtained performance is good.
The performance comparison sheet
Project | Embodiment 1 | Embodiment 2 | Embodiment 3 |
High thermal resistance | 65 ℃, 8h do not trickle | 80 ℃, 8h do not trickle | 90 ℃, 8h do not trickle |
Lower temperature resistance | -20 ℃, 24h bend flawless | -25 ℃, 24h bend flawless | -35 ℃, 24h bend flawless |
With the aluminium sheet cutting performance | 3.8N/mm | 4.6N/mm | 6.1N/mm |
With the aluminium sheet stripping performance | 4.0N/mm | 4.9N/mm | 6.2N/mm |
The present invention is not limited to the foregoing description, more than a part in the shown just preferred embodiment of the present invention, can not once limit the present invention's interest field, therefore, equivalent variations so that the present patent application claim is done still belongs to the scope that the present invention is contained.
Claims (2)
1. modifying asphalt sizing agent is characterized in that the mixture that this sizing agent is made up of the following portions by weight material:
Pitch 45-65 part
Tackifier 10-30 part
SBS 3-15 part
SBR 1-10 part
Filler 5-20 part
Rubber powder 5-15 part
Described pitch is 90# pitch or 100# pitch or two kinds of asphalt mixtures;
Described tackifier are one or more compounds in terpine resin, aromatic hydrocarbon oil, the rosin;
Described SBS is a kind of among trade mark KTR-101, LG411, GF-6, YH-791 and the YH-792;
Described SBR is a kind of powder styrene butadiene rubber or several different trade mark powder styrene butadiene rubber compound;
Described filler is one or more compounds in talcum powder, lime carbonate, mica powder and the barium sulfate;
Described rubber powder is a using rubber powder of waste tire.
2. preparation method according to the described sizing agent of claim 1, this preparation method is a foundation with the parts by weight ratio of sizing agent of the present invention, and adopts following technology:
Under the normal temperature, composition according to described sizing agent parts by weight, earlier fused pitch is got in the stirring tank by pump, stirring tank is the chuck stainless steel cauldron, heat by thermal oil, open stirring rake, stirring velocity is 60-200 rev/min, temperature of charge is 120-150 ℃, stirs 10-30 minute; Adding SBS, SBR continues to stir, and temperature is raised to 160-180 ℃, stirred 1-2 hour, keep whipping temp and stirring velocity, add tackifier, continue to stir 30-60 minute, add rubber powder and filler then successively, continue to stir 30-60 minute, after colloidal mill grinds, the modifying asphalt sizing agent that obtained performance is good.
Priority Applications (1)
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CN2010105481122A CN101982517A (en) | 2010-11-18 | 2010-11-18 | Modified asphalt adhesive and preparation method thereof |
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CN2010105481122A CN101982517A (en) | 2010-11-18 | 2010-11-18 | Modified asphalt adhesive and preparation method thereof |
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CN101982517A true CN101982517A (en) | 2011-03-02 |
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Cited By (24)
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CN102504756A (en) * | 2011-09-29 | 2012-06-20 | 广东辛美来亚科技实业有限公司 | Road gap-filling cement and preparation method thereof |
CN102604589A (en) * | 2012-03-22 | 2012-07-25 | 云南光电辅料有限公司 | Rubber for processing small lens, and preparation method of the rubber |
CN102690629A (en) * | 2011-03-22 | 2012-09-26 | 闫炳润 | Rapid-welding self-curing crack pouring adhesive and application method thereof |
CN102827572A (en) * | 2012-09-17 | 2012-12-19 | 山东建筑大学 | Rubber and plastic waterproof bonding modification asphalt mastic and preparation method of rubber and plastic waterproof bonding modification asphalt mastic |
CN103013142A (en) * | 2011-09-22 | 2013-04-03 | 北京嘉格伟业筑路科技有限公司 | Waste tire rubber powder plant asphalt material and preparation method thereof |
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2010
- 2010-11-18 CN CN2010105481122A patent/CN101982517A/en active Pending
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Addressee: Zhang Zhiqiu Document name: Notification that Application Deemed to be Withdrawn |
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WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20110302 |