CN101919453B - Medium carbon chain fatty acid powder grease and preparation method thereof - Google Patents
Medium carbon chain fatty acid powder grease and preparation method thereof Download PDFInfo
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- CN101919453B CN101919453B CN 201010254268 CN201010254268A CN101919453B CN 101919453 B CN101919453 B CN 101919453B CN 201010254268 CN201010254268 CN 201010254268 CN 201010254268 A CN201010254268 A CN 201010254268A CN 101919453 B CN101919453 B CN 101919453B
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Abstract
The invention discloses medium carbon chain fatty acid powder grease and a preparation method thereof. The medium carbon chain fatty acid powder grease comprises the following components in percentage by weight: 40%-60% of MCT (Medium Chain Fatty Acid) grease, 4%-6% of sodium caseinate, 0.5%-2.0% of monoglyceride, 0.3%-0.7% of sodium stearoyl lactylate, 1%-2% of dipotassium hydrogen phosphate, 0.2%-0.4% of silicon dioxide and the balance of glucose syrup. The invention greatly enhances the stability of the MCT grease, extends the application of the MCT grease in the field of foods, prevents the risk of excessive grease intake and also reduces the potential hazards of excessive antioxidant intake.
Description
Technical field
The present invention relates to a kind of powdered oil and preparation method thereof, relate in particular to a kind of medium-chain fatty acid powdered oil and preparation method thereof.
Background technology
Powdered oil claims again cream, fatty powder, is take refining hydrogenated vegetable oil and numerous food auxiliary material as raw material, forms through allotment, emulsification, sterilization, spray-drying.This product has good dispersiveness, water-soluble, stable, is used for various food and can improves nutritive value and caloric value, raising instant capacity and brew, improve mouthfeel, makes product tastier.
Powdered oil has good water-soluble, and the many loose property of many breasts form in water that milk is aqueous uniformly.Powdered oil can improve the interior tissue of food, and flavouring increases fat, is delicate mouthfeel, and is lubricated abundant, therefore be again the good companion of coffee product, can be used for instant oatmeal, cake, biscuit etc., makes the cake tissue fine and smooth, improves elasticity.Biscuit can improve shortening property, is difficult for walking wet goods.
The powdered oil instant capacity is good, sees through the approximate milk of essence seasoning local flavor, can replace milk powder or reduce the milk amount of using in food processing, thereby under the prerequisite that keeps product with stable quality, can reduce production costs.
Studies show that, the aliphatic acid of moderate-length carbochain can reduce the levels of accumulation of low density fat acid in human body, reduce the risk that people suffer from angiocardiopathy, therefore contain more median chain triglyceride oil (being called for short miglyol 812 fat) and have preferably health care, but it is the liquid fat form owing to miglyol 812 fat, and its application has been subject to certain restriction.
Miglyol 812 fat capsule is owing to wherein containing other more edible oil and fat, the problem that can bring the grease intake to increase, and because it is liquid, other edible oil and fat such as soybean oil as main adapted mostly are greatly consaturated oil, putrid and deteriorated problem extremely easily occurs, so can add therein some antioxidants such as vitamin E, and the excessive absorption of antioxidant is proved to be to be harmful to, this potential harm risk with regard to bringing for the health of human body.
Summary of the invention
For solving the prior art above shortcomings, one of technical problem to be solved by this invention provides a kind of medium-chain fatty acid powdered oil, improved greatly the stability of liquid miglyol 812 fat, not only can directly reconstitute use, simultaneously can also as the batching in the formula powder, greatly expand its application.
Two of technical problem to be solved by this invention provides a kind of preparation method of above-mentioned medium-chain fatty acid powdered oil.
Concrete, the present invention is implemented by following technical proposals:
A kind of medium-chain fatty acid powdered oil is comprised of following compositions in weight percentage:
Miglyol 812 fat 40～60%;
Casein sodium 4～6%;
Monoglyceride 0.5～2.0%;
Stearoyl lactate 0.3～0.7%;
Dipotassium hydrogen phosphate 1～2%;
Silica 0.2～0.4%;
The glucose syrup surplus.
Preferably, described medium-chain fatty acid powdered oil is comprised of following compositions in weight percentage:
Miglyol 812 fat 50%;
Casein sodium 5%;
Monoglyceride 1.5%;
Stearoyl lactate 0.5%;
Dipotassium hydrogen phosphate 1.5%;
Silica 0.3%;
Glucose syrup 41.2%.
Concrete, in the present invention:
Miglyol 812 fat is called again median chain triglyceride oil.It is a kind of functional grease of absorption easy to digest, is a kind of saturated fatty acid, and the general character of existing long chain triglycerides (LCT) has again self characteristics.Median chain triglyceride oil only is made of saturated fatty acid, and freezing point is low, is liquid under the room temperature, and viscosity is little.With soybean oil relatively, be odorless, colourless transparency liquid fully.Compare with hydrogenated oil and fat with common grease, the content of unrighted acid is extremely low in the median chain triglyceride oil, and oxidation stability is very good, and its iodine number is no more than 0.5.Miglyol 812 fat is stable especially under high temperature and low temperature.
Miglyol 812 fat is a kind of product that obtains by chemical method, is widely used in preparation and the processing of numerous food.The saturated fatty acid that contains 8 carbon atoms is sad with the saturated fatty acid aliphatic acid that contains 10 carbon atoms and certain herbaceous plants with big flowers acid, is commonly referred to be medium chain fatty acid.
Miglyol 812 fat extracts from coconut oil or from palm oil.They are mixtures of saturated triglycerides, and that main is sad (C
8H
16O
2) and certain herbaceous plants with big flowers acid (C
10H
20O
2), their content is not less than 95%.
The characteristic of miglyol 812 fat is as follows: fabulous cooling stability, low-viscosity, preferably dissolubility, good lubricity and unique metabolic pathway.
More and more about the research of MCT in recent years.The miglyol 812 fat character is colorless and odorless, transparent as the water free-pouring liquid.Because the molecular weight of miglyol 812 fat is little, solubility is high, easily digested and assimilated by pancreatic lipase, and do not cause the secretion of pancreatic juice; Do not need when transporting in the body and other lipid material formation chylomicron, be difficult for and protein bound; And directly enter liver through portal vein, synthctic fat not in liver is difficult for forming fatty liver.Can be used for fat splitting, absorption and the defective patient in transportation aspect.
Casein sodium, in food industry, have moisturizing, fresh-keeping, protect fragrant and the effects such as improvement quality.Casein sodium united state food and agricultural organization and the food additives committee of the World Health Organization are defined as the food additives of endless use, therefore be widely used in the industries such as meat products, bakery, beverage, medicine, tobacco, cosmetics and daily-use chemical industry.
Monoglyceride is a kind of food emulsifier, adds this emulsifying agent in the powdered oil and can improve its wetability, dispersiveness in the aqueous solution.
Stearoyl lactate, English name Sodium stearyl lactate is called for short SSL.For white to light yellow brittle solid or powder, slightly the caramel smell slightly has hygroscopicity.Can be used as anion surfactant; Food emulsifying agent; Cosmetic emulsifier and thickener.
Dipotassium hydrogen phosphate acts on buffer in food industry, chelating agent, yeast food, emulsification salt, anti-oxidant synergist.
Silica has large specific area, makes it can play the effect of interval dose between the particle of powdered rubber, has promoted simultaneously flowing freely of powdered rubber, and its moisture pick-up properties is very big, has also strengthened agglomeration resistance effect and suction-operated.
Glucose syrup is a kind of a kind of starch syrup that produces in the effect of enzyme or acid take starch as raw material, Main Ingredients and Appearance be glucose, maltose, maltotriose, maltotetraose and tetrose with first-class, be called again liquid glucose or Portugal's wheat syrup.
The present invention also provides the preparation method of above-mentioned medium-chain fatty acid powdered oil, is comprised of following step:
(1) water is dipotassium hydrogen phosphate dissolving preparation aqueous dibasic potassium phosphate solution, with the water of 60～70 ℃ of temperature the casein sodium dissolving prepared the caseinic acid sodium water solution;
(2) above-mentioned aqueous dibasic potassium phosphate solution and above-mentioned caseinic acid sodium water solution are mixed,
(3) miglyol 812 fat is heated to 60～70 ℃, adds monoglyceride and stearoyl lactate and mix;
(4) solution of the solution of glucose syrup, step (2) preparation and step (3) preparation injected emulsion tank simultaneously fully carry out emulsification after, the slip that emulsification is good injects the homogenizer emulsifying homogeneous, carry out spray-drying in the slip spray injection drying tower behind the homogeneous, obtain powder;
(5) powder with step (4) preparation utilizes Antitackiness agent adding device to add silica in fluid bed, mixes and can obtain medium-chain fatty acid powdered oil of the present invention.
Above-mentioned related equipment is the conventional general equipment of the industry.
It is further preferred,
In the step (4), the Chinese patent application number 201020022379.0 a kind of spray drying towers that provide are provided described spray drying tower.
In the step (5), the Chinese patent application number 201020022378.9 a kind of Antitackiness agent adding devices that provide are provided described Antitackiness agent adding device.
The present invention has improved the stability of miglyol 812 fat greatly, has enlarged its application in field of food, the risk of having avoided excess grease to take in, and the while has also reduced the potential hazard of some antioxidants of excessive absorption such as vitamin E.
The specific embodiment
Embodiment 1
Take by weighing successively according to corresponding embodiment 1 each raw material components of table 1.
(1) water is dipotassium hydrogen phosphate dissolving preparation aqueous dibasic potassium phosphate solution, with the water of 65 ℃ of temperature the casein sodium dissolving prepared the caseinic acid sodium water solution;
(2) above-mentioned aqueous dibasic potassium phosphate solution and above-mentioned caseinic acid sodium water solution are mixed,
(3) miglyol 812 fat is heated to 65 ℃, adds monoglyceride and stearoyl lactate and mix;
(4) solution of the solution of glucose syrup, step (2) preparation and step (3) preparation injected emulsion tank simultaneously fully carry out emulsification after, the slip that emulsification is good injects the homogenizer emulsifying homogeneous, carry out spray-drying in the slip spray injection drying tower behind the homogeneous, obtain powder;
(5) powder with step (4) preparation utilizes Antitackiness agent adding device to add silica in fluid bed, mixes and can obtain medium-chain fatty acid powdered oil of the present invention.
Wherein,
In the step (4), the Chinese patent application number 201020022379.0 a kind of spray drying towers that provide are provided described spray drying tower.
In the step (5), the Chinese patent application number 201020022378.9 a kind of Antitackiness agent adding devices that provide are provided described Antitackiness agent adding device.
Table 1: medium-chain fatty acid powdered oil raw material proportioning list position: kilogram
| Material name | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 |
| Miglyol 812 fat | 40 | 55 | 60 | 45 | 50 |
| Casein sodium | 4 | 6 | 4.5 | 5.5 | 5 |
| Monoglyceride | 2 | 1.5 | 0.5 | 1 | 1.5 |
| Stearoyl lactate | 0.3 | 0.7 | 0.4 | 0.6 | 0.5 |
| Dipotassium hydrogen phosphate | 1.3 | 1.6 | 2 | 1 | 1.5 |
| Silica | 0.4 | 0.2 | 0.3 | 0.25 | 0.3 |
| Glucose syrup | 52 | 35 | 32.3 | 46.65 | 41.2 |
Embodiment 2
Take by weighing successively according to corresponding embodiment 2 each raw material components of table 1.Adopt embodiment 1 described method to be prepared, can make medium-chain fatty acid powdered oil of the present invention.
Embodiment 3
Take by weighing successively according to corresponding embodiment 3 each raw material components of table 1.Adopt embodiment 1 described method to be prepared, can make medium-chain fatty acid powdered oil of the present invention.
Embodiment 4
Take by weighing successively according to corresponding embodiment 4 each raw material components of table 1.Adopt embodiment 1 described method to be prepared, can make medium-chain fatty acid powdered oil of the present invention.
Wherein, also can adopt the general spray drying tower of the industry to carry out drying in the step (4), step (5) also can adopt the Antitackiness agent adding device of industry routine that powder and the silica that step (4) prepares is mixed, be prepared medium-chain fatty acid powdered oil of the present invention, certainly, adopt prescription of the present invention also can adopt existing conventional method to be prepared fully, just the preparation method's effect with respect to embodiment 1 descends to some extent.
Embodiment 5
Take by weighing successively according to corresponding embodiment 5 each raw material components of table 1.Adopt embodiment 1 described method to be prepared, can make medium-chain fatty acid powdered oil of the present invention.
The present invention has improved the stability of miglyol 812 fat greatly, has enlarged its application in field of food, the risk of having avoided excess grease to take in, and the while has also reduced the potential hazard of some antioxidants of excessive absorption such as vitamin E.
Claims (3)
1. a medium-chain fatty acid powdered oil is characterized in that, its raw material is comprised of following compositions in weight percentage:
Miglyol 812 fat 40～60%;
Casein sodium 4～6%;
Monoglyceride 0.5～2.0%;
Stearoyl lactate 0.3～0.7%;
Dipotassium hydrogen phosphate 1～2%;
Silica 0.2～0.4%;
The glucose syrup surplus.
2. medium-chain fatty acid powdered oil as claimed in claim 1 is characterized in that, its raw material is comprised of following compositions in weight percentage:
Miglyol 812 fat 50%;
Casein sodium 5%;
Monoglyceride 1.5%;
Stearoyl lactate 0.5%;
Dipotassium hydrogen phosphate 1.5%;
Silica 0.3%;
Glucose syrup 41.2%.
3. the preparation method of medium-chain fatty acid powdered oil as claimed in claim 1 is characterized in that, is comprised of following step:
(1) water is dipotassium hydrogen phosphate dissolving preparation aqueous dibasic potassium phosphate solution, with the water of 60～70 ℃ of temperature the casein sodium dissolving prepared the caseinic acid sodium water solution;
(2) above-mentioned aqueous dibasic potassium phosphate solution and above-mentioned caseinic acid sodium water solution are mixed,
(3) miglyol 812 fat is heated to 60～70 ℃, adds monoglyceride and stearoyl lactate and mix;
(4) solution of the solution of glucose syrup, step (2) preparation and step (3) preparation injected emulsion tank simultaneously fully carry out emulsification after, the slip that emulsification is good injects the homogenizer emulsifying homogeneous, carry out spray-drying in the slip spray injection drying tower behind the homogeneous, obtain powder;
(5) powder with step (4) preparation utilizes Antitackiness agent adding device to add silica in fluid bed, mixes and namely obtains described medium-chain fatty acid powdered oil.
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| CN 201010254268 CN101919453B (en) | 2010-08-16 | 2010-08-16 | Medium carbon chain fatty acid powder grease and preparation method thereof |
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|---|---|---|---|
| CN 201010254268 CN101919453B (en) | 2010-08-16 | 2010-08-16 | Medium carbon chain fatty acid powder grease and preparation method thereof |
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| CN101919453B true CN101919453B (en) | 2013-04-10 |
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Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102771581A (en) * | 2011-12-19 | 2012-11-14 | 天津科技大学 | Process for preparing powdered oil with modified starch and alcohol soluble protein as wall materials |
| CN102696788A (en) * | 2012-06-26 | 2012-10-03 | 杭州博多工贸有限公司 | Zero-trans fatty acid non-dairy creamer and preparation method thereof |
| CN103005006B (en) * | 2012-12-14 | 2014-10-15 | 孟松林 | Microencapsulated powder grease and production method thereof |
| CN105283079B (en) * | 2013-04-27 | 2020-01-21 | 荷兰联合利华有限公司 | Powdered composition for instant milk tea powder |
| CN103404615B (en) * | 2013-07-26 | 2015-08-19 | 山东天骄生物技术有限公司 | A kind of preparation method of cold cut type non-dairy creamer |
| CN103518920A (en) * | 2013-10-16 | 2014-01-22 | 苏州市佳禾食品工业有限公司 | Instant white chocolate solid beverage and preparation method thereof |
| CN105764497A (en) * | 2013-11-14 | 2016-07-13 | 奥特吉尼克斯制药公司 | Solid compositions of triglycerides and uses thereof |
| JP5892295B2 (en) * | 2013-11-19 | 2016-03-23 | 日清オイリオグループ株式会社 | Powdered oil and fat composition and method for producing the same |
| CN104054849A (en) * | 2014-05-21 | 2014-09-24 | 上海英莱腾医药研究有限公司 | High-content medium chain triglyceride powdered oil and preparation method thereof |
| CN104522188B (en) * | 2015-01-07 | 2017-11-21 | 广州倚德生物科技有限公司 | Powdered oil rich in middle low carbon acid and preparation method thereof |
| WO2018170235A1 (en) | 2017-03-15 | 2018-09-20 | Accera, Inc. | Pharmaceutical compositions having high drug loadings of medium chain triglycerides and methods related thereto |
| CN107373508B (en) * | 2017-09-05 | 2021-01-15 | 中科特膳（天津）医用食品有限公司 | Fat powder for controlling body weight and preparation method thereof |
| CN114668050A (en) * | 2020-12-24 | 2022-06-28 | 丰益(上海)生物技术研发中心有限公司 | Powdered oil |
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Address after: 215200 Wufang Road 127, Friendship Industrial Zone, Songling Town, Wujiang District, Suzhou City, Jiangsu Province Patentee after: Jiahe Food Industry Co., Ltd. Address before: 215222 Square Road, Friendship Industrial Zone, Songling Town, Wujiang City, Jiangsu Province Patentee before: Suzhou Jiahe Foods Industry Co., Ltd. |