CN101878870A - Preparation method of propolis all-components soft capsule - Google Patents
Preparation method of propolis all-components soft capsule Download PDFInfo
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- CN101878870A CN101878870A CN2010102066791A CN201010206679A CN101878870A CN 101878870 A CN101878870 A CN 101878870A CN 2010102066791 A CN2010102066791 A CN 2010102066791A CN 201010206679 A CN201010206679 A CN 201010206679A CN 101878870 A CN101878870 A CN 101878870A
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Abstract
The invention discloses a preparation method of a propolis all-components soft capsule, which takes a propolis supercritical extract and an ethanol extract as main functional raw materials, natural beewax, octyl and decyl glycerate, lecithin and soybean oil are matched to prepare a kind of health food, a supercritical extraction technology and an ethanol extraction technology are applied to treat the propolis, then bioactive substances in the raw materials are greatly maintained via the advanced technologies of dissolution, emulsification, degasification, pelleting preparation and the like, heavy metal is removed, and the capsule has the functions of strengthening immunity, resisting inflammation, resisting tumor, assisting blood fat reduction and blood pressure reduction and the like.
Description
Technical field
The present invention relates to a kind of preparation method of propolis product, especially a kind of preparation method of propolis all-components soft capsule.
Background technology
Propolis is a kind of natural precious resources, and domestic only have more than 350 ton, and 50,000 honeybees were gathered the propolis that raw material only can be produced 0.21 gram in one day, were called " purple gold " on the international market.The major function of propolis has: immunological regulation, improvement sleep, adjusting blood fat, adjusting blood sugar, protection liver, inhibition tumour etc.
Since 1996, propolis research was listed in " 95 " national key scientific and technological project and " key industry promotion project and honeybee resources effective utilization and industrialization development " problem Program for Tackling Key Problems by the Ministry of Science and Technology, the Ministry of Agriculture, forestry bureau etc., and program for tackling key problems in science and technology was also listed in Jiangxi Province in 2005 years.Propolis deep process technology research at present and industrialization development production and application have been subjected to the unprecedented attention of country.
China starts from the sixties in last century to propolis research and development, and starting but makes much progress a little later, grasps the technology such as collection, storage, fabricated product of propolis at present substantially, possesses development and production capacity.The propolis composition Study is finished substantially existing effective bee glue components physiologically active and pharmacological research thereof, the development function product of mainly carrying out at present both at home and abroad.The propolis health food is safe and effective, and consumption is few, instant effect, obvious health-care efficacy.
Domestic enterprise uses the alcohol extract propolis; but often active ingredient is carried unclean; not only wasted valuable propolis resource; and lost the part active principle of liposoluble in the propolis; influenced the curative effect of propolis,, carried out Agricultural recycling economy in order to protect national limited resources; make precious natural resources obtain comprehensive utilization, and bee product (propolis) deep process technology research and product development are state key tackling of key scientific and technical problems and promotion project.Meet national industry development policies and high technology industry technical policy.
Present most of corporate boss will develop the propolis of alcohol extract, and has had many products selling.Perhaps there are some enterprises also only to develop the product of supercritical extract propolis.
Wang Shi honeybee garden Co., Ltd initiates at home and adopts two kinds of extracting methods to extract propolis, be respectively earlier propolis to be carried out supercritical extract, and then extract (perhaps carry out earlier alcohol extract after supercritical extract) with ethanol, adopt capsule technique to make the full constituent propolis product then and put on market, and obtained effect preferably.
Summary of the invention
The object of the present invention is to provide a kind of preparation method of propolis all-components soft capsule, this product makes pure soluble components and the liposoluble constituent in the propolis obtain best reservation, can play better auxiliary antilipemic, aided blood pressure-lowering, auxiliary hyperglycemic and strengthen immunity, anti-inflammatory, function such as antitumor.
Technical scheme of the present invention is: a kind of preparation method of propolis all-components soft capsule, this propolis all-components soft capsule formula for a product composition by weight: 10-15 part supercritical extract propolis, 20-30 part propolis ethanol extract, 0.5-5 part lecithin, 0.5-6.5 part beeswax, 2-5 part Glycerin, mixed triester with caprylic acid capric acid, 40-58 part soybean oil.Soybean oil can substitute with the olive oil or the camellia oil of same component in this propolis all-components soft capsule formula for a product composition by weight.
The preparation method of this propolis all-components soft capsule:
(1) preparation of propolis raw material:
The preparation of supercritical extract propolis: with propolis removal of impurities, dewaxing, freezing, pulverize, sieve, add that carrier is handled, extraction, obtain the propolis supercritical extract, standby; The extraction of propolis: with the remaining slag of supercritical extract, adopt the alcohol-pickled extraction of 4 times of quality, concentrate and obtain the propolis alcohol-extracted extract, standby.
The preparation another kind method of propolis raw material: a, with after the propolis raw material removal of impurities, adopt 4 times alcohol-pickled extraction, concentrate and to obtain the propolis alcohol-extracted extract, standby; The preparation of b, supercritical extract propolis: with the propolis slag behind propolis alcohol extract dewaxing, freezing, pulverize, sieve, add that carrier is handled, extraction, obtain the propolis supercritical extract, standby.
(2) preparation process:
A, fusing: soybean oil, beeswax, propolis supercritical extract are required weighing in proportion, in material-compound tank, be heated to 65～70 ℃ and after beeswax melts fully, stop heating, be cooled to 40～50 ℃ then; B, stirring: continue to be cooled to 30～40 ℃ after stirring; C, emulsification: carried out emulsification 15～20 minutes with stirring in lecithin and the Glycerin, mixed triester with caprylic acid capric acid adding material-compound tank; D, fusing: 60～65 ℃ of heat fused, make propolis be flow-like extractive of propolis alcohol; E, be mixed, polish, outgas: will melt good extractive of propolis alcohol and add and continue the emulsification mixing preparation in the material-compound tank after 30 minutes, crossing the colloid mill back of milling crosses 120 order nylon filter clothes and filters, carry out the vacuum stirring degassing then, there is not bubble to material, material after the degassing can be placed 22-26 hour in 20～25 ℃ environment, simultaneously the sealing of material is preserved, prevent suction; F, change glue, the degassing: pour glycerine, gelatin and water into material-compound tank, and add and use ethylparaben, do not stop to mix, and adopt recirculated water chuck heatingization glue.Simultaneously the vacuum of maintenanceization glue jar-0.085～-0.090MPa outgases, glue temperature is controlled at 60～70 ℃, the time is controlled at was advisable in 1～1.5 hour, finally not having bubble with gelatin solution serves as to judge terminal point, the degassing fully; G, insulation: the gelatin solution after will outgasing is fully put into heat-preserving container, and 56～65 ℃ of temperature are incubated 15～20 hours; H, pelleting: pour content into hopper, carry out pelleting according to required weight, the environment temperature between pelleting is controlled at 18～24 ℃, and relative humidity is controlled at 45～60%; The content temperature is controlled at 20～30 ℃; I, rotating cage moulding: the ball rotating cage moulding of extrusion 1 hour; I, once wash ball, primary drying: the ball after the moulding divides 2 times cleanings, whenever all is immersed in the ethanol all over all being to adopt 95% ethanol, and the time was controlled at 10～20 seconds.Pull a ball after washing out and carry out primary drying; Adopt the method for rotating cage drying, 22～24 ℃ of the temperature of drying room, relative humidity 50～60%, the time was controlled at 16～20 hours; K, once choose ball, sterilization: a dried ball adopts hand picked method that a defective ball in all balls is picked out, and the ball of defective is for having bubble, impurity is arranged, different in nature ball, leaking ball; A qualified ball adopts 75% ethanol disinfection cleaning, and method is with reference to the technological operation of once washing ball; 1, redrying: the ball after the sterilization continues drying and moulding, 24～26 ℃ of the temperature of drying room, and relative humidity 40～50%, the time was controlled at 4～8 hours, was dry the end until the rubber water content 13～14%; M, secondary are chosen ball: continue to select a ball of once choosing choosing that ball leaks; N, detection: the random sampling of QC department is carried out subjective inspection and is delivered to quality testing department and detect, and can pack after qualified; O, packing: be packaged to be finished product on demand.
The invention has the advantages that: the leaching process of propolis adopted for two steps extracted, and mainly was to be divided into nonpolar extraction and polar solvent extraction, almost all extracted the active ingredient in the propolis clean.The omnidistance low-temperature extraction of supercritical extract propolis keeps a large amount of active material and heat-sensitive substances, and the extractant carbon dioxide is nonpoisonous and tasteless, and is stable.Supercritical extract contains multiple volatile ingredient, and terpenoid substance wherein obtains increasing.Physics deleading technology is adopted in the alcohol extracting of propolis, and the lead in the propolis is almost all removed.Can select for use the kind of diluent soybean oil, olive oil, camellia oil to make that the effect of product is further strengthened in some aspects.
This bee glue soft capsule product adopts the nonpolar part and the partially mixed best proportioning that reaches active ingredient in the raw material propolis of polarity of propolis, adopt technology such as emulsification, homogeneous make polarity in the propolis and nonpolarity element can be in dispersant stable existence, do not separate out, not stratified.Also adopt the soft capsule preparation technology, avoided tastes such as hardship that propolis directly takes, suffering, be convenient for carrying and take.
The suitable crowd of this product is the higher person of blood fat, the higher person of blood pressure, hypoglycemic higher person and strengthens immunocompromised person and tumor patient.
The specific embodiment
Example 1:
A kind of preparation method of propolis all-components soft capsule, this propolis all-components soft capsule formula for a product composition by weight: 10 kilograms of supercritical extract propolis, 20 kilograms of propolis ethanol extracts, 0.5 kilogram of lecithin, 0.5 kilogram of beeswax, 2 kilograms of Glycerin, mixed triester with caprylic acid capric acid, 40 kilograms of soybean oils.
(1) preparation of propolis raw material:
The preparation of supercritical extract propolis: with propolis removal of impurities, dewaxing, freezing, pulverize, sieve, add that carrier is handled, extraction, obtain the propolis supercritical extract, standby; The extraction of propolis: with the remaining slag of supercritical extract, adopt the alcohol-pickled extraction of 4 times of quality, concentrate and obtain the propolis alcohol-extracted extract, standby.
(2) preparation process:
A, fusing: soybean oil, beeswax, propolis supercritical extract are required weighing in proportion, in material-compound tank, be heated to 65～70 ℃ and after beeswax melts fully, stop heating, be cooled to 40～50 ℃ then; B, stirring: continue to be cooled to 30～40 ℃ after stirring; C, emulsification: carried out emulsification 15～20 minutes with stirring in lecithin and the Glycerin, mixed triester with caprylic acid capric acid adding material-compound tank; D, fusing: 60～65 ℃ of heat fused, make propolis be flow-like extractive of propolis alcohol; E, be mixed, polish, outgas: will melt good extractive of propolis alcohol and add and continue the emulsification mixing preparation in the material-compound tank after 30 minutes, crossing the colloid mill back of milling crosses 120 order nylon filter clothes and filters, carry out the vacuum stirring degassing then, there is not bubble to material, material after the degassing can be placed 24 hours in 20～25 ℃ environment, simultaneously the sealing of material is preserved, prevent suction; F, change glue, the degassing: pour glycerine, gelatin and water into material-compound tank, and add and use ethylparaben, do not stop to mix, and adopt recirculated water chuck heatingization glue.Simultaneously the vacuum of maintenanceization glue jar-0.085～-0.090MPa outgases, glue temperature is controlled at 60～70 ℃, the time is controlled at was advisable in 1～1.5 hour, finally not having bubble with gelatin solution serves as to judge terminal point, the degassing fully; G, insulation: the gelatin solution after will outgasing is fully put into heat-preserving container, and 56～65 ℃ of temperature are incubated 15～20 hours; H, pelleting: pour content into hopper, carry out pelleting according to required weight, the environment temperature between pelleting is controlled at 18～24 ℃, and relative humidity is controlled at 45～60%; The content temperature is controlled at 20～30 ℃; I, rotating cage moulding: the ball rotating cage moulding of extrusion 1 hour; J, once wash ball, primary drying: the ball after the moulding divides 2 times cleanings, whenever all is immersed in the ethanol all over all being to adopt 95% ethanol, and the time was controlled at 10～20 seconds.Pull a ball after washing out and carry out primary drying; Adopt the method for rotating cage drying, 22～24 ℃ of the temperature of drying room, relative humidity 50～60%, the time was controlled at 16～20 hours; K, once choose ball, sterilization: a dried ball adopts hand picked method that a defective ball in all balls is picked out, and the ball of defective is for having bubble, impurity is arranged, different in nature ball, leaking ball; A qualified ball adopts 75% ethanol disinfection cleaning, and method is with reference to the technological operation of once washing ball; 1, redrying: the ball after the sterilization continues drying and moulding, 24～26 ℃ of the temperature of drying room, and relative humidity 40～50%, the time was controlled at 4～8 hours, was dry the end until the rubber water content 13～14%; M, secondary are chosen ball: continue to select a ball of once choosing choosing that ball leaks; N, detection: the random sampling of QC department is carried out subjective inspection and is delivered to quality testing department and detect, and can pack after qualified; O, packing:
Be packaged to be finished product on demand.
Example 2:
15 kilograms of supercritical extract propolis, 30 kilograms of propolis ethanol extracts, 6.5 kilograms of beeswaxs, 5 kilograms of Glycerin, mixed triester with caprylic acid capric acid, 58 kilograms of olive oil, 5 kilograms of lecithin, other procedure of processing is with example 1.
Example 3:
12 kilograms, 25 kilograms propolis ethanol extracts of supercritical extract propolis, 3 kilograms of beeswaxs, 3 kilograms of Glycerin, mixed triester with caprylic acid capric acid, 49 kilograms of camellia oils, 2.5 kilograms of lecithin, the preparation of propolis raw material: after the propolis raw material removal of impurities, adopt the alcohol-pickled extraction of 4 times of quality, concentrate and obtain the propolis alcohol-extracted extract, standby; The preparation of supercritical extract propolis: with the propolis slag behind propolis alcohol extract dewaxing, freezing, pulverize, sieve, add that carrier is handled, extraction, obtain the propolis supercritical extract, standby.Other procedure of processing is with example 1.
Claims (4)
1. the preparation method of a propolis all-components soft capsule is characterized in that: this propolis all-components soft capsule formulation weight component:
Supercritical extract propolis 10-15 propolis ethanol extract 20-30 lecithin 0.5-5
Beeswax 0.5-6.5 Glycerin, mixed triester with caprylic acid capric acid 2-5 soybean oil 40-58;
The preparation method of this propolis all-components soft capsule:
(1) preparation of propolis raw material:
The preparation of supercritical extract propolis: with propolis removal of impurities, dewaxing, freezing, pulverize, sieve, add that carrier is handled, extraction, obtain the propolis supercritical extract, standby; The extraction of propolis: with the remaining slag of supercritical extract, adopt the alcohol-pickled extraction of 4 times of quality, concentrate and obtain propolis alcohol extract medicinal extract, standby;
(2) preparation process:
A, fusing: soybean oil, beeswax, propolis supercritical extract are required weighing in proportion, in material-compound tank, be heated to 65～70 ℃ and after beeswax melts fully, stop heating, be cooled to 40～50 ℃ then; B, stirring: continue to be cooled to 30～40 ℃ after stirring; C, emulsification: carried out emulsification 15～20 minutes with stirring in lecithin and the Glycerin, mixed triester with caprylic acid capric acid adding material-compound tank; D, fusing: 60～65 ℃ of heat fused, make propolis be flow-like extractive of propolis alcohol; E, be mixed, polish, outgas: will melt good extractive of propolis alcohol and add and continue the emulsification mixing preparation in the material-compound tank after 30 minutes, crossing the colloid mill back of milling crosses 120 order nylon filter clothes and filters, carry out the vacuum stirring degassing then, there is not bubble to material, material after the degassing can be placed 22-26 hour in 20～25 ℃ environment, simultaneously the sealing of material is preserved, prevent suction; F, change glue, the degassing: pour glycerine, gelatin and water into material-compound tank, and add and use ethylparaben, do not stop to mix, and adopt recirculated water chuck heatingization glue; Simultaneously the vacuum of maintenanceization glue jar-0.085～-0.090MPa outgases, glue temperature is controlled at 60～70 ℃, the time is controlled at was advisable in 1～1.5 hour, finally not having bubble with gelatin solution serves as to judge terminal point, the degassing fully; G, insulation: the gelatin solution after will outgasing is fully put into heat-preserving container, and 56～65 ℃ of temperature are incubated 15～20 hours; H, pelleting: pour content into hopper, carry out pelleting according to required weight, the environment temperature between pelleting is controlled at 18～24 ℃, and relative humidity is controlled at 45～60%; The content temperature is controlled at 20～30 ℃; I, rotating cage moulding: the ball rotating cage moulding of extrusion 1 hour; I, once wash ball, primary drying: the ball after the moulding divides 2 times cleanings, whenever all is immersed in the ethanol all over all being to adopt 95% ethanol, and the time was controlled at 10～20 seconds; Pull a ball after washing out and carry out primary drying; Adopt the method for rotating cage drying, 22～24 ℃ of the temperature of drying room, relative humidity 50～60%, the time was controlled at 16～20 hours; K, once choose ball, sterilization: a dried ball adopts hand picked method that a defective ball in all balls is picked out, and the ball of defective is for having bubble, impurity is arranged, different in nature ball, leaking ball; A qualified ball adopts 75% ethanol disinfection cleaning, and method is with reference to the technological operation of once washing ball; 1, redrying: the ball after the sterilization continues drying and moulding, 24～26 ℃ of the temperature of drying room, and relative humidity 40～50%, the time was controlled at 4～8 hours, was dry the end until the rubber water content 13～14%; M, secondary are chosen ball: continue to select a ball of once choosing choosing that ball leaks; N, detection: the random sampling of QC department is carried out subjective inspection and is delivered to quality testing department and detect, and can pack after qualified; O, packing: be packaged to be finished product on demand.
2. the preparation method of propolis all-components soft capsule according to claim 1 is characterized by: the preparation another kind method of propolis raw material: after the propolis raw material removal of impurities, adopts the alcohol-pickled extraction of 4 times of quality, concentrates and obtain the propolis alcohol-extracted extract, and standby; The preparation of supercritical extract propolis: with the propolis slag behind propolis alcohol extract dewaxing, freezing, pulverize, sieve, add that carrier is handled, extraction, obtain the propolis supercritical extract, standby.
3. the preparation method of propolis all-components soft capsule according to claim 1 and 2, it is characterized in that: soybean oil can substitute with the olive oil of same component in this propolis all-components soft capsule formula for a product composition by weight.
4. the preparation method of propolis all-components soft capsule according to claim 1 and 2, it is characterized in that: soybean oil can substitute with the camellia oil of same component in this propolis all-components soft capsule formula for a product composition by weight.
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Cited By (8)
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| CN102188455A (en) * | 2011-05-13 | 2011-09-21 | 扬州三邦生物工程有限公司 | Method for extracting totipotent propolis |
| CN102429140A (en) * | 2011-10-27 | 2012-05-02 | 喀左县春蕾特产品开发中心 | Supercritical CO2 fluid extraction method of propolis |
| CN103637197A (en) * | 2013-12-03 | 2014-03-19 | 江苏江大源生态生物科技有限公司 | Propolis soft capsule and preparation method thereof |
| CN103859394A (en) * | 2014-01-16 | 2014-06-18 | 安徽工程大学 | Formula of geohiong mountain cordyceps mycelium propolis oral liquid and preparation method thereof |
| CN104489444A (en) * | 2014-12-22 | 2015-04-08 | 黑龙江农垦东北黑蜂开发有限公司 | Propolis-royal jelly soft capsule |
| CN107224445A (en) * | 2017-05-08 | 2017-10-03 | 西北大学 | Propolis active component and its compound product and application |
| CN108041589A (en) * | 2017-12-11 | 2018-05-18 | 江西省三抗保健品有限公司 | A kind of soft capsule of strengthen immunity auxiliary reducing blood lipid and preparation method thereof |
| CN109645414A (en) * | 2019-02-22 | 2019-04-19 | 江西汪氏蜜蜂园有限公司 | A kind of royal jelly selenium soft capsule and its preparation process |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102188455A (en) * | 2011-05-13 | 2011-09-21 | 扬州三邦生物工程有限公司 | Method for extracting totipotent propolis |
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| CN103637197A (en) * | 2013-12-03 | 2014-03-19 | 江苏江大源生态生物科技有限公司 | Propolis soft capsule and preparation method thereof |
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| CN103859394B (en) * | 2014-01-16 | 2016-05-25 | 安徽工程大学 | Formula of mountain, a kind of Kaohsiung cordyceps mycelia propolis oral liquid and preparation method thereof |
| CN104489444A (en) * | 2014-12-22 | 2015-04-08 | 黑龙江农垦东北黑蜂开发有限公司 | Propolis-royal jelly soft capsule |
| CN107224445A (en) * | 2017-05-08 | 2017-10-03 | 西北大学 | Propolis active component and its compound product and application |
| CN107224445B (en) * | 2017-05-08 | 2020-05-15 | 西北大学 | Propolis effective part and compound product and application thereof |
| CN108041589A (en) * | 2017-12-11 | 2018-05-18 | 江西省三抗保健品有限公司 | A kind of soft capsule of strengthen immunity auxiliary reducing blood lipid and preparation method thereof |
| CN109645414A (en) * | 2019-02-22 | 2019-04-19 | 江西汪氏蜜蜂园有限公司 | A kind of royal jelly selenium soft capsule and its preparation process |
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Application publication date: 20101110 |