CN101851868A - Ecological dyeing method for dyeing cotton fabric with mulberry red natural dye - Google Patents
Ecological dyeing method for dyeing cotton fabric with mulberry red natural dye Download PDFInfo
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- CN101851868A CN101851868A CN 201010119918 CN201010119918A CN101851868A CN 101851868 A CN101851868 A CN 101851868A CN 201010119918 CN201010119918 CN 201010119918 CN 201010119918 A CN201010119918 A CN 201010119918A CN 101851868 A CN101851868 A CN 101851868A
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- cotton fabric
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- natural dye
- soaping
- ecological
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- 239000004744 fabric Substances 0.000 title claims abstract description 51
- 229920000742 Cotton Polymers 0.000 title claims abstract description 41
- 238000004043 dyeing Methods 0.000 title claims abstract description 38
- 229930182559 Natural dye Natural products 0.000 title claims abstract description 25
- 239000000978 natural dye Substances 0.000 title claims abstract description 25
- 240000000249 Morus alba Species 0.000 title claims abstract description 22
- 235000008708 Morus alba Nutrition 0.000 title claims abstract description 21
- 238000000034 method Methods 0.000 title claims abstract description 13
- 238000005406 washing Methods 0.000 claims abstract description 20
- 239000007864 aqueous solution Substances 0.000 claims description 13
- 239000003153 chemical reaction reagent Substances 0.000 claims description 13
- 239000000975 dye Substances 0.000 claims description 11
- 239000000344 soap Substances 0.000 claims description 9
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 8
- 238000002360 preparation method Methods 0.000 claims description 8
- 239000000243 solution Substances 0.000 claims description 8
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 6
- 238000001035 drying Methods 0.000 claims description 6
- 238000007493 shaping process Methods 0.000 claims description 6
- 238000009736 wetting Methods 0.000 claims description 6
- 239000002253 acid Substances 0.000 claims description 4
- 239000006210 lotion Substances 0.000 claims description 4
- 239000001103 potassium chloride Substances 0.000 claims description 4
- 235000011164 potassium chloride Nutrition 0.000 claims description 4
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims description 3
- 239000001110 calcium chloride Substances 0.000 claims description 3
- 229910001628 calcium chloride Inorganic materials 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 229910052943 magnesium sulfate Inorganic materials 0.000 claims description 3
- 235000019341 magnesium sulphate Nutrition 0.000 claims description 3
- 238000002203 pretreatment Methods 0.000 claims description 3
- 238000009991 scouring Methods 0.000 claims description 3
- -1 alkane ketone Chemical class 0.000 claims description 2
- 235000011148 calcium chloride Nutrition 0.000 claims description 2
- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 claims description 2
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 2
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 2
- 229920000128 polypyrrole Polymers 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical compound [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 239000000049 pigment Substances 0.000 abstract description 3
- 230000008569 process Effects 0.000 abstract description 3
- 239000003086 colorant Substances 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 238000007781 pre-processing Methods 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 238000005516 engineering process Methods 0.000 description 6
- 239000002932 luster Substances 0.000 description 6
- 235000013399 edible fruits Nutrition 0.000 description 4
- 239000004753 textile Substances 0.000 description 4
- 238000010790 dilution Methods 0.000 description 3
- 239000012895 dilution Substances 0.000 description 3
- 239000003814 drug Substances 0.000 description 3
- 239000001054 red pigment Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 206010002198 Anaphylactic reaction Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 208000004880 Polyuria Diseases 0.000 description 1
- 208000031320 Teratogenesis Diseases 0.000 description 1
- 230000036783 anaphylactic response Effects 0.000 description 1
- 208000003455 anaphylaxis Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 210000004556 brain Anatomy 0.000 description 1
- 230000000711 cancerogenic effect Effects 0.000 description 1
- 231100000315 carcinogenic Toxicity 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000035619 diuresis Effects 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000002864 food coloring agent Nutrition 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
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Abstract
The invention relates to an ecological dyeing method for dyeing a cotton fabric with mulberry red natural dye, comprising the following steps: preprocessing the cotton fabric and then dyeing the preprocessed cotton fabric with the mulberry red natural dye; adding metal salt for fixation; and soaping the fabric after fixation and then fixing colors to obtain the dyed fabric with even color, wherein washing fastness can reach 3-4degrees. The ecological dyeing method has simple dyeing process, high dye-uptake, good pigment stability and wide market prospect.
Description
Technical field
The present invention relates to the application of natural dye, especially a kind of ecological dyeing method of dyeing cotton fabric with mulberry red natural dye.
Background technology
On human history, natural dye has been made indelible contribution for beautifying people's life.Since 19 end of the centurys, because developing rapidly of synthetic dyestuffs makes natural dye withdraw from the textile dyeing field basically.Along with the continuous enhancing of human environmental consciousness and to the growing interest of self health, the part synthetic dyestuffs are more and more noticeable to the harm that human health and ecological environment are produced.Under global green revolution tide, natural dye begins again to be paid attention to by people.The animals and plants dyestuff is by extracting in the organism in the natural dye, and is good, biodegradable with Environmental compatibility.Natural dye mostly is Chinese medicine greatly, and in dyeing course, its medicine and flavor component are absorbed by fabric with pigment, and except that the dyeing function, natural dye also has multiple functions such as medicine, spices, makes the fabric after the dyeing to human body special medicinal health-care function be arranged.
Mulberry fruit is the near ripe collective fruits of Moraceae Morus plant mulberry, and it contains abundant pigment, is one of important source of natural red colouring matter.Mulberry red pigment has enriching blood, moistens brain, diuresis and eliminate effect such as free radical.
Extract natural dye and be applied to textile dyeing from mulberry fruit, for increasing natural dye kind and chromatogram, improve the surcharge of textiles, construction economizing type, friendly environment society have crucial meaning.
Extracting method report about mulberry red pigment is more, and is mainly used in the food color aspect.Mulberry red pigment is applied to textile industry, and is applied to the dyeing aspect of pure cotton fabric with this as natural dye, not seeing at present has report.
Summary of the invention
The technical problem to be solved in the present invention is: proposing a kind of is the ecological dyeing method of the dyeing cotton fabric with mulberry red natural dye of raw material with the mulberry fruit, and its method comprises the pre-treatment of COTTON FABRIC, the dyeing and the fixation three process of soaping of processing back COTTON FABRIC.
The technical solution adopted in the present invention is: the pre-treatment that at first is COTTON FABRIC: preparation 5～20 grams per liter shitosan pretreating reagent aqueous solution, with COTTON FABRIC in the pretreating reagent aqueous solution after the complete wetting, two advance two and roll on padding machine, pick-up is 60～120%, bakes 3～10 minutes with 75～120 ℃ on shaping drying then.
In order to realize handling the purpose of the dyeing of COTTON FABRIC afterwards, dyeing of the present invention is: dye strength is 0.5～8%; bath raio is 1: 10～40; contaminated 30～90 minutes down at 70～100 ℃; the cooling back adds 3～10 grams per liter magnesium sulfate, potassium chloride or calcium chloride; after 15～40 minutes, take out washing 80～110 ℃ of following fixation, oven dry.
In order to realize keeping the purpose of the stability of color and luster behind the cotton fabric dyeing process, the present invention handles the back COTTON FABRIC that the dyes fixation of soaping, its technology of soaping is: prepare solution 3～10 grams per liters of soaping, after soaping 20～50 minutes under 50～100 ℃, take out washing, oven dry obtains pure cotton fabric and is celadon.The DYED FABRICS color and luster is even, and washing fastness can reach 3～4 grades.
In order to guarantee the quality of mulberry red natural dye dyed cotton fabric, improve its washability, the present invention uses acid scouring agent or basic soap lotion to the mulberry red natural dye dyed cotton fabric fixation of soaping.The acid soap dilution is 1～5: 1～3 for side chain polyoxyethylene ether and the water by Sodium Polyacrylate, polypyrrole alkane ketone, C13 with weight ratio: 5～15: 77～93 solution of forming, its pH are 5.5～6.8, and the basic soap lotion is conventional soap flakes or washing powder.
The invention has the beneficial effects as follows: help protecting environment; economize on resources; the clothes safety that DYED FABRICS makes does not have carcinogenic, teratogenesis or causes cutaneous anaphylaxis, and has effects such as sterilization; good with the ecological environment compatibility; biodegradable, dyeing of the present invention is simple, the dye-uptake height; fastness is good, and market prospects are wide.
The specific embodiment
Embodiment one
Prepare the 6 grams per liter shitosan pretreating reagent aqueous solution, in the pretreating reagent aqueous solution after the complete wetting, two advance two and roll on padding machine with COTTON FABRIC, and pick-up is 70%, bakes 8 minutes with 75 ℃ on shaping drying then.
Mulberry red natural dye is to handling the dyeing of back COTTON FABRIC, and its dyeing is a dye strength 1%, and bath raio 1: 10 was contaminated 80 minutes down at 80 ℃, and the cooling back adds 3 grams per liter magnesium sulfate, after 35 minutes, takes out washing 80 ℃ of following fixation, oven dry.
With the above-mentioned good COTTON FABRIC fixation of soaping that dyes, its technology of soaping is preparation acidity solution 3 grams per liters of soaping, and after soaping 70 minutes under 50 ℃, takes out washing, and oven dry obtains COTTON FABRIC and is celadon.The cloth cover color and luster is even, and the washing fastness test can reach 3～4 grades.
Embodiment two
Prepare the 8 grams per liter shitosan pretreating reagent aqueous solution, in the pretreating reagent aqueous solution after the complete wetting, two advance two and roll on padding machine with COTTON FABRIC, and pick-up is 80%, bakes 6 minutes with 85 ℃ on shaping drying then.
Mulberry red natural dye is to handling the dyeing of back COTTON FABRIC, and its dyeing is a dye strength 3%, and bath raio 1: 20 was contaminated 40 minutes down at 95 ℃, and the cooling back adds 5 grams per liter potassium chloride, after 20 minutes, takes out washing 90 ℃ of following fixation, oven dry.
With the above-mentioned good COTTON FABRIC fixation of soaping that dyes, its technology of soaping is preparation basic soap dilution 4 grams per liters, after soaping 50 minutes under 55 ℃, takes out washing, and oven dry obtains COTTON FABRIC and is celadon.The cloth cover color and luster is even, and the washing fastness test can reach 3～4 grades.
Embodiment three
Prepare the 15 grams per liter shitosan pretreating reagent aqueous solution, in the pretreating reagent aqueous solution after the complete wetting, two advance two and roll on padding machine with COTTON FABRIC, and pick-up is 90%, bakes 5 minutes with 100 ℃ on shaping drying then.
Mulberry red natural dye is to handling the dyeing of back COTTON FABRIC, and its dyeing is a dye strength 5%, and bath raio 1: 30 was contaminated 25 minutes down at 100 ℃, and the cooling back adds 7 grams per liter calcium chloride, after 15 minutes, takes out washing 100 ℃ of following fixation, oven dry.
With the above-mentioned good COTTON FABRIC fixation of soaping that dyes, its technology of soaping is preparation acidity solution 7 grams per liters of soaping, and after soaping 45 minutes under 70 ℃, takes out washing, and oven dry obtains COTTON FABRIC and is celadon.The cloth cover color and luster is even, and the washing fastness test can reach 3～4 grades.
Embodiment four
Prepare the 20 grams per liter shitosan pretreating reagent aqueous solution, in the pretreating reagent aqueous solution after the complete wetting, two advance two and roll on padding machine with COTTON FABRIC, and pick-up is 120%, bakes 3 minutes with 120 ℃ on shaping drying then.
Mulberry red natural dye is to handling the dyeing of back COTTON FABRIC, and its dyeing is a dye strength 8%, and bath raio 1: 40 was contaminated 40 minutes down at 100 ℃, and the cooling back adds 10 grams per liter potassium chloride, after 15 minutes, takes out washing 110 ℃ of following fixation, oven dry.
Above-mentioned material is dyed the good COTTON FABRIC fixation of soaping, and its technology of soaping is preparation basic soap dilution 10 grams per liters, after soaping 20 minutes under 100 ℃, takes out washing, and oven dry obtains COTTON FABRIC and is celadon.The cloth cover color and luster is even, and the washing fastness test can reach 3～4 grades.
With above-mentioned foundation desirable embodiment of the present invention is enlightenment, and by above-mentioned description, the related work personnel can carry out various change and modification fully in the scope that does not depart from this invention technological thought.The technical scope of this invention is not limited to the content on the specification, must determine its technical scope according to the claim scope.
Claims (2)
1. the ecological dyeing method of a dyeing cotton fabric with mulberry red natural dye is characterized in that: may further comprise the steps:
(1) the preparation pretreating reagent aqueous solution, COTTON FABRIC is carried out pre-treatment: preparation 5～20 grams per liter shitosan pretreating reagent aqueous solution, with COTTON FABRIC in the pretreating reagent aqueous solution after the complete wetting, two advance two and roll on padding machine, pick-up is 60～120%, bakes 3-10 minute with 75～120 ℃ on shaping drying then.
(2) mulberry red natural dye is to handling the dyeing of back COTTON FABRIC: dye strength is 0.5～8%; bath raio is 1: 10～40; contaminated 30～90 minutes down at 70～100 ℃; the cooling back adds 3～10 grams per liter magnesium sulfate, potassium chloride or calcium chloride; 80～110 ℃ of following fixation after 15～40 minutes; take out washing, oven dry.
(3) COTTON FABRIC after the dyeing in the step (2) is soaped fixation: preparation solution 3～10 grams per liters of soaping, after soaping 20～50 minutes under 50～100 ℃, take out washing, oven dry obtains COTTON FABRIC and is celadon.
2. the ecological dyeing method of dyeing cotton fabric with mulberry red natural dye as claimed in claim 1, it is characterized in that: the solution of soaping in the described step (3) comprises acid scouring agent or basic soap lotion, described acid scouring agent is 1～5: 1～3 for side chain polyoxyethylene ether and the water by Sodium Polyacrylate, polypyrrole alkane ketone, C13 with weight ratio: 5～15: 77～93 solution of forming, its pH is 5.5～6.8, and described basic soap lotion is conventional soap flakes or washing powder.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010119918XA CN101851868B (en) | 2010-03-09 | 2010-03-09 | Ecological dyeing method for dyeing cotton fabric with mulberry red natural dye |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010119918XA CN101851868B (en) | 2010-03-09 | 2010-03-09 | Ecological dyeing method for dyeing cotton fabric with mulberry red natural dye |
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| Publication Number | Publication Date |
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| CN101851868A true CN101851868A (en) | 2010-10-06 |
| CN101851868B CN101851868B (en) | 2011-11-09 |
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| CN201010119918XA Expired - Fee Related CN101851868B (en) | 2010-03-09 | 2010-03-09 | Ecological dyeing method for dyeing cotton fabric with mulberry red natural dye |
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| CN102168385A (en) * | 2011-03-03 | 2011-08-31 | 上海嘉麟杰纺织品股份有限公司 | Method for dyeing chitosan fabrics by vegetable dyes |
| CN102363925A (en) * | 2011-09-06 | 2012-02-29 | 江苏金辰针纺织有限公司 | Low-temperature soaping method |
| CN102400399A (en) * | 2011-09-27 | 2012-04-04 | 通亿（泉州）轻工有限公司 | Organic germanium function finishing method of pure cotton knitting underwear fabric with peppermint fragrance |
| CN102505533A (en) * | 2011-09-27 | 2012-06-20 | 通亿（泉州）轻工有限公司 | Dyeing and finishing method of dyed knitted cotton underwear fabric with tarragon delicate fragrance and mosquito-repelling and cleaning functions |
| CN102505534A (en) * | 2011-09-27 | 2012-06-20 | 通亿（泉州）轻工有限公司 | Dyeing and finishing method for dyed weaved pure-cotton underwear fabric with chrysanthemum flavor |
| CN102634993A (en) * | 2012-02-01 | 2012-08-15 | 常州美胜生物材料有限公司 | Method for dyeing cotton fibers by using natural dye |
| CN102926213A (en) * | 2012-11-12 | 2013-02-13 | 江苏金辰针纺织有限公司 | Process of low temperature pretreatment, colouration and aftertreatment of cotton fabrics |
| CN103046399A (en) * | 2012-12-17 | 2013-04-17 | 常州大学 | Natural dye transfer printing color paste as well as preparation method and printing method |
| CN103451963A (en) * | 2013-08-09 | 2013-12-18 | 常州纺织服装职业技术学院 | Method for dyeing cotton fabric with tea dye and finishing liquor used by method |
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| CN104088167A (en) * | 2014-07-04 | 2014-10-08 | 常州大学 | Method for improving color depth and light fastness of natural dye-dyed fabric |
| CN104233872A (en) * | 2013-06-17 | 2014-12-24 | 无锡市东新织造有限公司 | Dyeing process for real-silk fabrics pre-mordanted by iron salt by using lawsonia pigment |
| CN105133379A (en) * | 2015-09-16 | 2015-12-09 | 四川省丝绸科学研究院 | Cotton fabric ferric chloride cooling front medium and mulberry cold dyeing process |
| CN105386345A (en) * | 2015-12-22 | 2016-03-09 | 广州番禺职业技术学院 | Technology for printing and dyeing artificial leather through mulberry juice |
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| CN102168385B (en) * | 2011-03-03 | 2013-01-02 | 上海嘉麟杰纺织品股份有限公司 | Method for dyeing chitosan fabrics by vegetable dyes |
| CN102168385A (en) * | 2011-03-03 | 2011-08-31 | 上海嘉麟杰纺织品股份有限公司 | Method for dyeing chitosan fabrics by vegetable dyes |
| CN102363925A (en) * | 2011-09-06 | 2012-02-29 | 江苏金辰针纺织有限公司 | Low-temperature soaping method |
| CN102400399A (en) * | 2011-09-27 | 2012-04-04 | 通亿（泉州）轻工有限公司 | Organic germanium function finishing method of pure cotton knitting underwear fabric with peppermint fragrance |
| CN102505533A (en) * | 2011-09-27 | 2012-06-20 | 通亿（泉州）轻工有限公司 | Dyeing and finishing method of dyed knitted cotton underwear fabric with tarragon delicate fragrance and mosquito-repelling and cleaning functions |
| CN102505534A (en) * | 2011-09-27 | 2012-06-20 | 通亿（泉州）轻工有限公司 | Dyeing and finishing method for dyed weaved pure-cotton underwear fabric with chrysanthemum flavor |
| CN102634993B (en) * | 2012-02-01 | 2015-07-08 | 常州美胜生物材料有限公司 | Method for dyeing cotton fibers by using natural dye |
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| CN102926213A (en) * | 2012-11-12 | 2013-02-13 | 江苏金辰针纺织有限公司 | Process of low temperature pretreatment, colouration and aftertreatment of cotton fabrics |
| CN103046399A (en) * | 2012-12-17 | 2013-04-17 | 常州大学 | Natural dye transfer printing color paste as well as preparation method and printing method |
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