CN104611947B - Make natural plants dyed cloth or the method for silk goods - Google Patents
Make natural plants dyed cloth or the method for silk goods Download PDFInfo
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Abstract
Make dye liquor after the steps such as the present invention discloses a kind of method making natural plants dyed cloth or silk goods, uses plant material, size-reduced, then carry out contaminating thing pre-treatment, mordant dyeing, wash, dye, soap, dry in the shade after obtain plant dyeing fabric.Mordant dye adds slaine and also acts the effect of color development and fixation.Gained plant dyeing cloth of the present invention or silk goods color are vivid, and even dyeing, and dyeing color fastness is good, and colour-fast, nondiscolouring, color is many, and color and luster is soft, simple and unsophisticated, natural.And the plant material aboundresources of the present invention, easily expand plantation, nontoxic, harmless；There is not the synthetic dyestuffs pollution to environment and the injury to human body, also there is health care.The method that the present invention provides can apply to the cleaning of woolen industry and produces, it is achieved produce in a large number.
Description
Technical field
The present invention relates to a kind of method making natural plants dyed cloth or silk goods, belong to dyestuff and extract and fabrics printing and dyeing technical field.
Background technology
Using chemical dye in textile printing and dyeing industry in a large number, effect on environment is serious.The most conventional synthetic dyestuffs comprise carcinogenicity material, the most directly enable a wearer to or the producer is injured, have certain excitant and anaphylaxis to skin.For the aggravation that prevents the pollution of the environment, the most disabled chemical dye increases to hundreds of from tens kinds.
Compared with synthetic dyestuffs, natural colouring matter is natural, wears safety, and part natural colouring matter also has certain health care, is loved by the people.Vegetable colour is the dyestuff that in natural dye, applicating history is the longest, application surface is the widest.Vegetable colour mainly extracts from positions such as the stem of plant, leaf, flowers and obtains, and takes from nature, and therefore, vegetable colour is nontoxic with it, pollution-free, and tone elegance is advantage, is paid close attention to by people.
And the natural material that is currently used for vegetable colour is limited, people only commonly use several, and the fabric obtained currently with vegetable colour there is also the problems such as color fastness is low, color is few, and dyeing method is also difficult to industrialization.
Summary of the invention
Color fastness for overcoming plant printing and dyeing fabric is low, color is few, be difficult to the problems such as industrialization, and the present invention provides a kind of method making natural plants dyed cloth or silk goods, good to realize dyeing color fastness, dyeing equilibrium.
The present invention is realized by following technical proposal: a kind of method making natural plants dyed cloth or silk goods, through following each step:
(1) plant material is taken through water-boiling method, fermentation method, infusion method, the pigment dissolution in plant is made to make mill base, again in mill base by solid-to-liquid ratio kg/kg be calculated as 1:18000～22000 add potassium chloride to reach fully to extract the purpose of pigment, obtain dye liquor after filtering；
(2) by solid-to-liquid ratio kg/kg, biodiastase is calculated as 1:180～220 to be added to the water and be mixed to get treatment fluid, then puts in treatment fluid and wait to dye cloth material or silk goods carry out soaking 2～5 hours, then take out cloth or silk goods rinse 3 times after dehydration；
(3) cloth after step (2) process or silk goods are immersed in the dye liquor of step (1), and be heated at 50～70 DEG C insulation 8～15 minutes, be dehydrated after further taking out；
(4) preparation mordant dye；
(5) cloth after step (3) process or silk goods are immersed in the mordant dye of step (4), and be heated at 30～50 DEG C insulation 8～15 minutes, be dehydrated after rinsing with water after further taking out；
(6) dye liquor of step (1) adding 50～70 DEG C in cloth after step (5) processes or silk goods carries out contaminating 15～25 minutes, with rinsing 2 dehydrations after further taking out；
(7) step (6) gained cloth or silk goods neutral detergent or neutrality are soaped 1 time, then be dehydrated after rinsing with water, dry in the shade, obtain plant dyeing cloth or silk goods.
Above-mentioned plant material is herbaceous plant or xylophyta, such as purple stem pool indigo plant, Radix Isatidis, bush, Ma Liguo, madder, the chicken pin coptis, Asian puccoon, yellow pear tree skin, tealeaves, walnut shell etc.
The water-boiling method of described step (1) is to be pulverized by plant material, then is calculated as 1:3～4 by solid-to-liquid ratio kg/kg and adds water and carry out boiling 3～4 hours.
The fermentation method of described step (1) is that plant material takes its root, stem, leaf, takes the method banked up, and sprinkles lime above, seals and makes it rot, takes mill base.
The infusion method of described step (1) is by after the root of plant material, stem, leaf pulverizing, soaks 15～20 days.
The biodiastase of described step (2) is commercial BF7658 biodiastase.
The mordant dye of described step (4) is to choose slaine by required color to mix in proportion with water, i.e. obtains mordant dye.
When described slaine is frerrous chloride or ferric acetate, it is calculated as 1:180～220 by solid-to-liquid ratio kg/kg and is added to the water, i.e. obtain being dyed by cloth the mordant dye of taupe.
When described slaine is copper sulphate or copper acetate, being calculated as 1:200～220 by solid-to-liquid ratio kg/kg and be added to the water, i.e. obtaining can be by the mordant dye of cloth stained yellow.
When described slaine is aluminium chloride or aluminum acetate, it is calculated as 1:200～220 by solid-to-liquid ratio kg/kg and is added to the water, i.e. obtain cloth can be dyed flaxen mordant dye.
Advantage that the present invention possesses and effect: after the steps such as the present invention is to use plant material, size-reduced, make dye liquor, then carry out contaminating thing pre-treatment, mordant dyeing, wash, dye, soap, dry in the shade after obtain plant dyeing fabric.Carry out pre-treatment with biodiastase, the slurry etc. used when weaving cotton cloth can be removed, reach the effect well painted.Mordant dye adds slaine and also acts the effect of color development and fixation.Gained plant dyeing cloth of the present invention or silk goods color are vivid, and even dyeing, color fastness to washing reach 3～4 grades, color fastness to light reach 2～3 grades, dyeing color fastness good, colour-fast, nondiscolouring, color is many, and color and luster is soft, simple and unsophisticated, natural.And the plant material aboundresources of the present invention, easily expand plantation, nontoxic, harmless；There is not the synthetic dyestuffs pollution to environment and the injury to human body, also there is health care.The method that the present invention provides can apply to the cleaning of woolen industry and produces, it is achieved produce in a large number.
Detailed description of the invention
Below by embodiment, the present invention will be further described.
Embodiment 1
(1) take purple stem pool indigo plant to pulverize, it is calculated as 1:3 by solid-to-liquid ratio kg/kg again to add water and carry out boiling 4 hours, make the pigment dissolution in plant make mill base, then in mill base, be calculated as 1:20000 by solid-to-liquid ratio kg/kg add potassium chloride to reach fully to extract the purpose of pigment, obtain dye liquor after filtering；
(2) by solid-to-liquid ratio kg/kg, commercial BF7658 biodiastase is calculated as 1:200 to be added to the water and be mixed to get treatment fluid, then in treatment fluid, puts into material to be dyed cloth carry out soaking 3 hours, then take out after cloth rinses 3 times and be dehydrated；
(3) cloth after step (2) being processed immerses in the dye liquor of step (1), and is heated at 60 DEG C insulation 10 minutes, is dehydrated after further taking out；Now cloth is faint yellow；
(4) by solid-to-liquid ratio kg/kg, ferric acetate is calculated as 1:220 to be added to the water, i.e. obtains being dyed by cloth the mordant dye of taupe；
(5) cloth after step (3) being processed immerses in the mordant dye of step (4), and is heated at 50 DEG C insulation 8 minutes, is dehydrated after rinsing with water after further taking out；
(6) dye liquor of the step (1) adding 60 DEG C in the cloth after step (5) processes carries out contaminating 25 minutes, with rinsing 2 dehydrations after further taking out；
(7) step (6) gained cloth neutral detergent or neutrality are soaped 1 time, then be dehydrated with after water rinsing, dry in the shade, obtain the plant dyeing cloth of taupe.
Gained plant dyeing fabric color is vivid, and even dyeing, color fastness to washing reach 3 ~ 4 grades, color fastness to light reach 2 ~ 3 grades, dyeing color fastness good, colour-fast, nondiscolouring, color is many, and color and luster is soft, simple and unsophisticated, natural.
Embodiment 2
1) take purple stem pool indigo plant to pulverize, it is calculated as 1:3 by solid-to-liquid ratio kg/kg again to add water and carry out boiling 4 hours, make the pigment dissolution in plant make mill base, then in mill base, be calculated as 1:20000 by solid-to-liquid ratio kg/kg add potassium chloride to reach fully to extract the purpose of pigment, obtain dye liquor after filtering；
(2) by solid-to-liquid ratio kg/kg, commercial BF7658 biodiastase is calculated as 1:200 to be added to the water and be mixed to get treatment fluid, then in treatment fluid, puts into material to be dyed cloth carry out soaking 3 hours, then take out after cloth rinses 3 times and be dehydrated；
(3) cloth after step (2) being processed immerses in the dye liquor of step (1), and is heated at 60 DEG C insulation 10 minutes, is dehydrated after further taking out；Now cloth is faint yellow；
(4) by solid-to-liquid ratio kg/kg, copper acetate is calculated as 1:220 to be added to the water, i.e. obtains being dyed by cloth the mordant dye of buff；
(5) cloth after step (3) being processed immerses in the mordant dye of step (4), and is heated at 50 DEG C insulation 8 minutes, is dehydrated after rinsing with water after further taking out；
(6) dye liquor of the step (1) adding 60 DEG C in the cloth after step (5) processes carries out contaminating 25 minutes, with rinsing 2 dehydrations after further taking out；
(7) step (6) gained cloth neutral detergent or neutrality are soaped 1 time, then be dehydrated with after water rinsing, dry in the shade, obtain the plant dyeing cloth of taupe.
Further, the cloth that can will have contaminated, it is then added in indigo naturalis dye liquor, the green that vegetable colour is not directly dyed can be dyed.
Gained plant dyeing fabric color is vivid, and even dyeing, color fastness to washing reach 3 ~ 4 grades, color fastness to light reach 2 ~ 3 grades, dyeing color fastness good, colour-fast, nondiscolouring, color is many, and color and luster is soft, simple and unsophisticated, natural.
Embodiment 3
(1) root of Radix Isatidis, stem, leaf are taken, take the method banked up, lime is sprinkled above, sealing makes it rot, the pigment dissolution in plant is made to make mill base, again in mill base by solid-to-liquid ratio kg/kg be calculated as 1:18000 add potassium chloride to reach fully to extract the purpose of pigment, obtain dye liquor after filtering；
(2) by solid-to-liquid ratio kg/kg, commercial BF7658 biodiastase is calculated as 1:220 to be added to the water and be mixed to get treatment fluid, then in treatment fluid, puts into silk goods to be contaminated carry out soaking 5 hours, then take out after silk goods rinse 3 times and be dehydrated；
(3) silk goods after step (2) being processed immerse in the dye liquor of step (1), and are heated at 70 DEG C insulation 8 minutes, are dehydrated after further taking out；Now silk goods are light green；
(4) by solid-to-liquid ratio kg/kg, copper sulphate being calculated as 1:220 to be added to the water, i.e. obtaining can be by the mordant dye of cloth stained yellow；
(5) silk goods after step (3) being processed immerse in the mordant dye of step (4), and are heated at 40 DEG C insulation 10 minutes, are dehydrated after rinsing with water after further taking out；
(6) dye liquor of the step (1) adding 70 DEG C in the silk goods after step (5) processes carries out contaminating 20 minutes, with rinsing 2 dehydrations after further taking out；
(7) step (6) gained silk goods neutral detergent or neutrality are soaped 1 time, then be dehydrated with after water rinsing, dry in the shade, obtain blue plant dyeing silk goods.
Gained plant dyeing silk goods color is vivid, and even dyeing, color fastness to washing reach 3 ~ 4 grades, color fastness to light reach 4 ~ 5 grades, dyeing color fastness good, colour-fast, nondiscolouring, color is many, and color and luster is soft, simple and unsophisticated, natural.
Embodiment 4
(1) take the root of bush, stem, leaf after crushed, soak 15 days, make the pigment dissolution in plant make mill base, then in mill base, be calculated as 1:22000 by solid-to-liquid ratio kg/kg add potassium chloride to reach fully to extract the purpose of pigment, obtain dye liquor after filtering；
(2) by solid-to-liquid ratio kg/kg, commercial BF7658 biodiastase is calculated as 1:180 to be added to the water and be mixed to get treatment fluid, then puts in treatment fluid and wait to dye cloth material or silk goods carry out soaking 2 hours, then take out cloth or silk goods rinse 3 times after dehydration；
(3) cloth after step (2) process or silk goods are immersed in the dye liquor of step (1), and be heated at 50 DEG C insulation 15 minutes, be dehydrated after further taking out；Now cloth or silk goods are pale red；
(4) by solid-to-liquid ratio kg/kg, aluminium chloride is calculated as 1:200 to be added to the water, i.e. obtains cloth can be dyed flaxen mordant dye；
(5) cloth after step (3) process or silk goods are immersed in the mordant dye of step (4), and be heated at 30 DEG C insulation 15 minutes, be dehydrated after rinsing with water after further taking out；
(6) dye liquor of step (1) adding 50 DEG C in cloth after step (5) processes or silk goods carries out contaminating 15 minutes, with rinsing 2 dehydrations after further taking out；
(7) step (6) gained cloth or silk goods neutral detergent or neutrality are soaped 1 time, then be dehydrated after rinsing with water, dry in the shade, obtain mauve plant dyeing cloth or silk goods.
Gained plant dyeing cloth or silk goods color are vivid, and even dyeing, color fastness to washing reach 3 ~ 4 grades, color fastness to light reach 2 ~ 3 grades, dyeing color fastness good, colour-fast, nondiscolouring, color is many, and color and luster is soft, simple and unsophisticated, natural.
Embodiment 5
(1) take tealeaves to pulverize, it is calculated as 1:4 by solid-to-liquid ratio kg/kg again to add water and carry out boiling 3 hours, make the pigment dissolution in plant make mill base, then in mill base, be calculated as 1:19000 by solid-to-liquid ratio kg/kg add potassium chloride to reach fully to extract the purpose of pigment, obtain dye liquor after filtering；
(2) by solid-to-liquid ratio kg/kg, commercial BF7658 biodiastase is calculated as 1:190 to be added to the water and be mixed to get treatment fluid, then puts in treatment fluid and wait to dye cloth material or silk goods carry out soaking 4 hours, then take out cloth or silk goods rinse 3 times after dehydration；
(3) cloth after step (2) process or silk goods are immersed in the dye liquor of step (1), and be heated at 70 DEG C insulation 11 minutes, be dehydrated after further taking out；Now cloth or silk goods are light green；
(4) by solid-to-liquid ratio kg/kg, frerrous chloride is calculated as 1:180 to be added to the water, i.e. obtains being dyed by cloth the mordant dye of taupe；
(5) cloth after step (3) process or silk goods are immersed in the mordant dye of step (4), and be heated at 40 DEG C insulation 12 minutes, be dehydrated after rinsing with water after further taking out；
(6) dye liquor of step (1) adding 70 DEG C in cloth after step (5) processes or silk goods carries out contaminating 25 minutes, with rinsing 2 dehydrations after further taking out；
(7) step (6) gained cloth or silk goods neutral detergent or neutrality are soaped 1 time, then be dehydrated after rinsing with water, dry in the shade, obtain plant dyeing cloth or the silk goods of grey black.
Gained plant dyeing cloth or silk goods color are vivid, and even dyeing, color fastness to washing reach 3 ~ 4 grades, color fastness to light reach 3 ~ 4 grades, dyeing color fastness good, colour-fast, nondiscolouring, color is many, and color and luster is soft, simple and unsophisticated, natural.
Embodiment 6
(1) take alkanet, stem, leaf, take the method banked up, sprinkle lime above, sealing makes it rot, make the pigment dissolution in plant make mill base, then in mill base, be calculated as 1:22000 by solid-to-liquid ratio kg/kg add potassium chloride to reach fully to extract the purpose of pigment, obtain dye liquor after filtering；
(2) by solid-to-liquid ratio kg/kg, commercial BF7658 biodiastase is calculated as 1:200 to be added to the water and be mixed to get treatment fluid, then puts in treatment fluid and wait to dye cloth material or silk goods carry out soaking 5 hours, then take out cloth or silk goods rinse 3 times after dehydration；
(3) cloth after step (2) process or silk goods are immersed in the dye liquor of step (1), and be heated at 50 DEG C insulation 8 minutes, be dehydrated after further taking out；Now cloth or silk goods are lavender；
(4) by solid-to-liquid ratio kg/kg, copper acetate being calculated as 1:200 to be added to the water, i.e. obtaining can be by the mordant dye of cloth stained yellow；
(5) cloth after step (3) process or silk goods are immersed in the mordant dye of step (4), and be heated at 50 DEG C insulation 8 minutes, be dehydrated after rinsing with water after further taking out；
(6) dye liquor of step (1) adding 70 DEG C in cloth after step (5) processes or silk goods carries out contaminating 25 minutes, with rinsing 2 dehydrations after further taking out；
(7) step (6) gained cloth or silk goods neutral detergent or neutrality are soaped 1 time, then be dehydrated after rinsing with water, dry in the shade, obtain plant dyeing cloth or the silk goods of darkviolet.
Gained plant dyeing cloth or silk goods color are vivid, and even dyeing, color fastness to washing reach 3 ~ 4 grades, color fastness to light reach 3 ~ 4 grades, dyeing color fastness good, colour-fast, nondiscolouring, color is many, and color and luster is soft, simple and unsophisticated, natural.
Embodiment 7
(1) take after madder pulverizes, soak 20 days, make the pigment dissolution in plant make mill base, then in mill base, be calculated as 1:21000 by solid-to-liquid ratio kg/kg add potassium chloride to reach fully to extract the purpose of pigment, obtain dye liquor after filtering；
(2) by solid-to-liquid ratio kg/kg, commercial BF7658 biodiastase is calculated as 1:180 to be added to the water and be mixed to get treatment fluid, then puts in treatment fluid and wait to dye cloth material or silk goods carry out soaking 3 hours, then take out cloth or silk goods rinse 3 times after dehydration；
(3) cloth after step (2) process or silk goods are immersed in the dye liquor of step (1), and be heated at 70 DEG C insulation 12 minutes, be dehydrated after further taking out；Now cloth or silk goods are pale pink；
(4) by solid-to-liquid ratio kg/kg, aluminum acetate is calculated as 1:220 to be added to the water, i.e. obtains cloth can be dyed flaxen mordant dye；
(5) cloth after step (3) process or silk goods are immersed in the mordant dye of step (4), and be heated at 30～50 DEG C insulation 8～15 minutes, be dehydrated after rinsing with water after further taking out；
(6) dye liquor of step (1) adding 50～70 DEG C in cloth after step (5) processes or silk goods carries out contaminating 15～25 minutes, with rinsing 2 dehydrations after further taking out；
(7) step (6) gained cloth or silk goods neutral detergent or neutrality are soaped 1 time, then be dehydrated after rinsing with water, dry in the shade, obtain peach plant dyeing cloth or silk goods.
Gained plant dyeing cloth or silk goods color are vivid, and even dyeing, color fastness to washing reach 3 ~ 4 grades, color fastness to light reach 3 ~ 4 grades, dyeing color fastness good, colour-fast, nondiscolouring, color is many, and color and luster is soft, simple and unsophisticated, natural.
Claims (9)
1. the method making natural plants dyed cloth or silk goods, it is characterised in that through following each step:
(1) take plant material through water-boiling method, fermentation method, infusion method, make the pigment dissolution in plant make mill base, then in mill base, be calculated as 1:18000～22000 by solid-to-liquid ratio kg/kg add potassium chloride, obtain dye liquor after filtering；
(2) by solid-to-liquid ratio kg/kg, biodiastase is calculated as 1:180～220 to be added to the water and be mixed to get treatment fluid, then puts in treatment fluid and wait to dye cloth material or silk goods carry out soaking 2～5 hours, then take out cloth or silk goods rinse 3 times after be dehydrated；
(3) cloth after step (2) process or silk goods are immersed in the dye liquor of step (1), and be heated at 50～70 DEG C insulation 8～15 minutes, be dehydrated after further taking out；
(4) preparation mordant dye；
(5) cloth after step (3) process or silk goods are immersed in the mordant dye of step (4), and be heated at 30～50 DEG C insulation 8～15 minutes, be dehydrated after rinsing with water after further taking out；
(6) dye liquor of step (1) adding 50～70 DEG C in cloth after step (5) processes or silk goods carries out contaminating 15～25 minutes, is dehydrated after further taking out afterflush 2 times；
(7) by step (6) gained cloth or silk goods neutral detergent 1 time, then it is dehydrated after rinsing with water, dries in the shade, obtain plant dyeing cloth or silk goods.
Method the most according to claim 1, it is characterised in that: the water-boiling method of described step (1) is to be pulverized by plant material, then is calculated as 1:3～4 by solid-to-liquid ratio kg/kg and adds water and carry out boiling 3～4 hours.
Method the most according to claim 1, it is characterised in that: the fermentation method of described step (1) is that plant material takes its root, stem, leaf, takes the method banked up, and sprinkles lime above, seals and makes it rot, takes mill base.
Method the most according to claim 1, it is characterised in that: the infusion method of described step (1) is by after the root of plant material, stem, leaf pulverizing, soaks 15～20 days.
Method the most according to claim 1, it is characterised in that: the biodiastase of described step (2) is commercial BF7658 biodiastase.
Method the most according to claim 1, it is characterised in that: the mordant dye of described step (4) is to choose slaine by required color to mix in proportion with water, i.e. obtains mordant dye.
Method the most according to claim 6, it is characterised in that: when described slaine is frerrous chloride or ferric acetate, it is calculated as 1:180～220 by solid-to-liquid ratio kg/kg and is added to the water, i.e. obtain being dyed by cloth the mordant dye of taupe.
Method the most according to claim 6, it is characterised in that: when described slaine is copper sulphate or copper acetate, being calculated as 1:200～220 by solid-to-liquid ratio kg/kg and be added to the water, i.e. obtaining can be by the mordant dye of cloth stained yellow.
Method the most according to claim 6, it is characterised in that: when described slaine is aluminium chloride or aluminum acetate, it is calculated as 1:200～220 by solid-to-liquid ratio kg/kg and is added to the water, i.e. obtain cloth can be dyed flaxen mordant dye.
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| CN108116003A (en) * | 2017-12-19 | 2018-06-05 | 大连小萝莉服饰有限公司 | A kind of Multifunctional silk fabric and its preparation process |
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