CN101830936B - 一种制备固体木二糖的方法 - Google Patents
一种制备固体木二糖的方法 Download PDFInfo
- Publication number
- CN101830936B CN101830936B CN2010101748384A CN201010174838A CN101830936B CN 101830936 B CN101830936 B CN 101830936B CN 2010101748384 A CN2010101748384 A CN 2010101748384A CN 201010174838 A CN201010174838 A CN 201010174838A CN 101830936 B CN101830936 B CN 101830936B
- Authority
- CN
- China
- Prior art keywords
- xylobiose
- component
- bioses
- xylo
- preparing solid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
- LGQKSQQRKHFMLI-SJYYZXOBSA-N (2s,3r,4s,5r)-2-[(3r,4r,5r,6r)-4,5,6-trihydroxyoxan-3-yl]oxyoxane-3,4,5-triol Chemical compound O[C@@H]1[C@@H](O)[C@H](O)CO[C@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O)OC1 LGQKSQQRKHFMLI-SJYYZXOBSA-N 0.000 title claims abstract description 25
- LGQKSQQRKHFMLI-UHFFFAOYSA-N 4-O-beta-D-xylopyranosyl-beta-D-xylopyranose Natural products OC1C(O)C(O)COC1OC1C(O)C(O)C(O)OC1 LGQKSQQRKHFMLI-UHFFFAOYSA-N 0.000 title claims abstract description 25
- SQNRKWHRVIAKLP-UHFFFAOYSA-N D-xylobiose Natural products O=CC(O)C(O)C(CO)OC1OCC(O)C(O)C1O SQNRKWHRVIAKLP-UHFFFAOYSA-N 0.000 title claims abstract description 25
- 238000000034 method Methods 0.000 title claims abstract description 16
- 239000007787 solid Substances 0.000 title claims abstract description 15
- 239000011347 resin Substances 0.000 claims abstract description 9
- 229920005989 resin Polymers 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 7
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims abstract description 6
- 230000002378 acidificating effect Effects 0.000 claims abstract description 6
- 229910052791 calcium Inorganic materials 0.000 claims abstract description 6
- 239000011575 calcium Substances 0.000 claims abstract description 6
- 238000001704 evaporation Methods 0.000 claims abstract description 6
- 230000008020 evaporation Effects 0.000 claims abstract description 6
- 150000003740 xylobioses Chemical class 0.000 claims description 22
- 238000000926 separation method Methods 0.000 claims description 9
- GMWTXQKKRDUVQG-WOPPDYDQSA-N 4-amino-5-bromo-1-[(2r,3s,4s,5r)-4-hydroxy-5-(hydroxymethyl)-3-methyloxolan-2-yl]pyrimidin-2-one Chemical compound C[C@H]1[C@H](O)[C@@H](CO)O[C@H]1N1C(=O)N=C(N)C(Br)=C1 GMWTXQKKRDUVQG-WOPPDYDQSA-N 0.000 claims description 7
- 238000004108 freeze drying Methods 0.000 claims description 4
- 239000003480 eluent Substances 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- 230000008014 freezing Effects 0.000 abstract description 4
- 238000007710 freezing Methods 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 238000009777 vacuum freeze-drying Methods 0.000 abstract description 4
- 238000013375 chromatographic separation Methods 0.000 abstract 2
- 125000002091 cationic group Chemical group 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 238000011033 desalting Methods 0.000 abstract 1
- 238000002425 crystallisation Methods 0.000 description 5
- 230000008025 crystallization Effects 0.000 description 4
- 238000001035 drying Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 238000000108 ultra-filtration Methods 0.000 description 3
- 241000193830 Bacillus <bacterium> Species 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- SRBFZHDQGSBBOR-IOVATXLUSA-N D-xylopyranose Chemical compound O[C@@H]1COC(O)[C@H](O)[C@H]1O SRBFZHDQGSBBOR-IOVATXLUSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 229930006000 Sucrose Natural products 0.000 description 2
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 2
- 239000003610 charcoal Substances 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000002349 favourable effect Effects 0.000 description 2
- 229910017053 inorganic salt Inorganic materials 0.000 description 2
- 239000012528 membrane Substances 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 239000005720 sucrose Substances 0.000 description 2
- 229960003487 xylose Drugs 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 208000031226 Hyperlipidaemia Diseases 0.000 description 1
- 208000008589 Obesity Diseases 0.000 description 1
- 241000194019 Streptococcus mutans Species 0.000 description 1
- LPQOADBMXVRBNX-UHFFFAOYSA-N ac1ldcw0 Chemical compound Cl.C1CN(C)CCN1C1=C(F)C=C2C(=O)C(C(O)=O)=CN3CCSC1=C32 LPQOADBMXVRBNX-UHFFFAOYSA-N 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- SRBFZHDQGSBBOR-LECHCGJUSA-N alpha-D-xylose Chemical compound O[C@@H]1CO[C@H](O)[C@H](O)[C@H]1O SRBFZHDQGSBBOR-LECHCGJUSA-N 0.000 description 1
- PYMYPHUHKUWMLA-UHFFFAOYSA-N arabinose Natural products OCC(O)C(O)C(O)C=O PYMYPHUHKUWMLA-UHFFFAOYSA-N 0.000 description 1
- 230000008953 bacterial degradation Effects 0.000 description 1
- SRBFZHDQGSBBOR-UHFFFAOYSA-N beta-D-Pyranose-Lyxose Natural products OC1COC(O)C(O)C1O SRBFZHDQGSBBOR-UHFFFAOYSA-N 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 238000004440 column chromatography Methods 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 208000002925 dental caries Diseases 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 210000004907 gland Anatomy 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 210000000214 mouth Anatomy 0.000 description 1
- 235000020824 obesity Nutrition 0.000 description 1
- 210000001819 pancreatic juice Anatomy 0.000 description 1
- 230000000505 pernicious effect Effects 0.000 description 1
- 230000001766 physiological effect Effects 0.000 description 1
- 229920002401 polyacrylamide Polymers 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 210000003296 saliva Anatomy 0.000 description 1
- 235000019605 sweet taste sensations Nutrition 0.000 description 1
- 230000003245 working effect Effects 0.000 description 1
Landscapes
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Saccharide Compounds (AREA)
Abstract
Description
Claims (3)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2010101748384A CN101830936B (zh) | 2010-05-18 | 2010-05-18 | 一种制备固体木二糖的方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2010101748384A CN101830936B (zh) | 2010-05-18 | 2010-05-18 | 一种制备固体木二糖的方法 |
Publications (2)
Publication Number | Publication Date |
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CN101830936A CN101830936A (zh) | 2010-09-15 |
CN101830936B true CN101830936B (zh) | 2012-07-18 |
Family
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Family Applications (1)
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CN2010101748384A Active CN101830936B (zh) | 2010-05-18 | 2010-05-18 | 一种制备固体木二糖的方法 |
Country Status (1)
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CN (1) | CN101830936B (zh) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103319545B (zh) * | 2013-07-15 | 2015-07-08 | 山东绿健生物技术有限公司 | 一种木二糖联产木糖的生产方法 |
CN106046066B (zh) * | 2016-05-25 | 2018-08-24 | 广西大学 | 一种纯化制备高纯度木二糖的方法 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1847254A (zh) * | 2005-08-30 | 2006-10-18 | 南京林业大学 | 一种聚合度为2~8的低聚木糖各组分的制备分离方法 |
CN101632877A (zh) * | 2009-08-17 | 2010-01-27 | 山东龙力生物科技有限公司 | 一种低聚木糖各组分的分离纯化方法 |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FI20020675A0 (fi) * | 2002-04-09 | 2002-04-09 | Danisco Sweeteners Oy | Puhtaan disakkaridiliuoksen puhdistaminen |
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2010
- 2010-05-18 CN CN2010101748384A patent/CN101830936B/zh active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1847254A (zh) * | 2005-08-30 | 2006-10-18 | 南京林业大学 | 一种聚合度为2~8的低聚木糖各组分的制备分离方法 |
CN101632877A (zh) * | 2009-08-17 | 2010-01-27 | 山东龙力生物科技有限公司 | 一种低聚木糖各组分的分离纯化方法 |
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CN101830936A (zh) | 2010-09-15 |
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C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C53 | Correction of patent for invention or patent application | ||
CB02 | Change of applicant information |
Address after: 251200 Yucheng high tech Development Zone, Shandong Applicant after: Shandong Lvjian Biological Technology Co., Ltd. Address before: 251200 Yucheng high tech Development Zone, Shandong Applicant before: Yucheng Lujian Biological Technology Co.,Ltd. |
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CB03 | Change of inventor or designer information |
Inventor after: Xin Chengfu Inventor after: Jing Wenli Inventor after: Yu Li Inventor after: Ren Shangmei Inventor before: Xin Chengfu Inventor before: Jing Wenli Inventor before: Ren Shangmei |
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COR | Change of bibliographic data |
Free format text: CORRECT: INVENTOR; FROM: XIN CHENGFU JING WENLI REN SHANGMEI TO: XIN CHENGFU JING WENLI YU LI REN SHANGMEI Free format text: CORRECT: APPLICANT; FROM: YUCHENG LVJIAN BIOLOGICAL TECHNOLOGY CO., LTD. TO: SHANDONG LUJIAN BIOLOGICAL TECHNOLOGY CO., LTD. |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Method for preparing solid xylobiose Effective date of registration: 20180109 Granted publication date: 20120718 Pledgee: Yucheng Shandong rural commercial bank Limited by Share Ltd Pledgor: Shandong Lvjian Biological Technology Co., Ltd. Registration number: 2018370000010 |
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Effective date of registration: 20180426 Granted publication date: 20120718 |
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Date of cancellation: 20210426 Granted publication date: 20120718 |
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Effective date of registration: 20210426 Granted publication date: 20120718 |
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