CN101671952A - Anion finishing liquor and preparation method and anion functional seamless underwear - Google Patents
Anion finishing liquor and preparation method and anion functional seamless underwear Download PDFInfo
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- CN101671952A CN101671952A CN200910306006A CN200910306006A CN101671952A CN 101671952 A CN101671952 A CN 101671952A CN 200910306006 A CN200910306006 A CN 200910306006A CN 200910306006 A CN200910306006 A CN 200910306006A CN 101671952 A CN101671952 A CN 101671952A
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Abstract
The invention belongs to the field of after-finishing of costume products. First of all, an anion finishing liquor is provided and obtained from 2 to 3 parts of electrical stone superfine powder, 0.5to 1.5 parts of polyacrylic acid amine,1 to 3 parts of laurel acid sodium, 1 to 3 parts of triethanolamine and 1000 parts of water in parts by weight through emulsion and ultrasonic treatment; the anion finishing liquor preparation method comprises: treating pretreated products for 30 to 50 min through emulsion at the emulsion speed of 5000 to 6000 rpm, then treating the products for 8 to 15 min through ultrasound with the power of 1100 w to 1300 w; adding a binding agent to the anion finishing liquor to obtain an anion finishing agent,, immersing the seamless underwear in the anion finishingagent for more than 20 min with the weight ratio between the seamless underwear and the anion sorting agent being 1:8 to 12; and finally obtaining the anion functional seamless underwear through dehydration, sizing and drying. The anion release concentration of the obtained seamless underwear is more than 4000 anions per cm<3>.
Description
Technical field
The invention belongs to the back finishing field of dress-goods, specifically relate to a kind of anion finishing liquor and preparation method thereof and anion functional seamless underwear.
Background technology
Along with the raising of living standard, people more and more pay close attention to the healthy and health care of human body.The textile fabric of various health cares and textile fabrics emerge in multitude thereof, wherein, the underwear with health care more and more is subjected to people's attention, and it also becomes one of the research focus in clothing item field.
Negative ion concentration is one of sign of weighing the air quality quality in the air.World Health Organization's regulation: the anion normal concentration of fresh air is to be lower than 1000～1500 in every cc of air.How many negative ion concentrations is not only indicating the quality of air quality in the air, and the atmospheric environment of high-negative ion concentration has certain medical care effect to human beings'health simultaneously.How textiles increases anion generation concentration and becomes one of major subjects of health textile area research.The researcher is arranged from textile material, developed the fiber of novel negative ion health care, such as publication number is that the Chinese patent of CN1294208 has been introduced a kind of synthetic negative-ion far infrared fibre, but its fiber anion emission number is less and fragile eedle in the manufacturing procedure after weaving, increase processing cost widely, limited the development and the utilization of this fiber; Publication number provides a kind of negative-ion fiber and preparation method thereof for the Chinese patent of CN1827868, what it adopted is to add anion to urge the effect element to make tencel in fibrous material, and then be applied to garment industry, as underwear, wherein said ionic Cuixiaoshu is mainly by opal 40-60%; Diatomite 15-25%; Aethiops vegetabilis 5-10%; Bamboo charcoal 2-4%; Medical stone 2-4%; Shell 3-6%; Titanium dioxide 4-10%; Aluminium oxide 3% is formed, and its fibrous composition is various, and cost is than higher.
The researcher is also arranged from product structure, bring into play the functional of anion, such as notification number is that the Chinese utility model patent of CN200966348 discloses a kind of infrared negative ion health-care clothes, it comprises the clothes body, acupuncture point or joint corresponding to the wearer on the clothes body are provided with infrared negative ion health-care cloth sheet, and described infrared negative ion health-care cloth sheet is formed by natural fabric and the fiber blend that has added infrared nano-ceramic powder and negative ion powder.The content that does not have anion seamless underwear functional finishing agent and finishing technique in this background technology.
Also there is the researcher to pass through mode to the dress-goods post processing, make fabric have the functional of anion, provide a kind of treatment technology that can make the fabric stability capacity produce negative oxygen ion as publication number for the invention of China of CN101139800, earlier chemical ﹠ blended fabric is handled through cationic surfactant, use water washing again less than 20 ℃, because the cationic surfactant on the fabric is wash clean all, allow about the residual 0.3-3.0% of the relative fiber quality of cationic surfactant on the fabric, last fabric carries out surface treatment with quaternary ammonium salt, can constantly stablize emitting negative oxygen ion by the fabric after this technical finesse, reach about 4200ML, can quantitatively stablize emitting negative oxygen ion, function can not increase with washing times and reduce, and can make underwear with this kind fabric, articles for use etc. spin in nightwear and family.But the method is more loaded down with trivial details.
Seamless underwear is the one-shot forming underwear that adopts novel special equipment to produce, make positions such as neck, waist, stern need not seam, it is with comfortable, consideration, fashion, variation is rolled into one, not only make the consumer be so fond that will not let out of one's hand, simultaneously also move many designers deeply, become the trend of underwear.Anion function is incorporated in the seamless underwear product the functional target that has become the researcher and pursued that has seamless underwear and anion concurrently.
Summary of the invention
At above-mentioned existing in prior technology shortcoming and defect, first purpose of inventor provides a kind of anion finishing liquor, second purpose provides the preparation method of described anion finishing liquor, and the 3rd purpose provides with described anion finishing liquor post processing seamless underwear to obtain a kind of anion functional seamless underwear.
For realizing purpose of the present invention, the inventor provides following technical proposals:
The various factors that the inventor fully disperses by analyzing influence tourmaline ultrafine powder in theory, on this basis, method by mathematics is more specific with these influence factors, summarize the dispersion scheme that a cover can instruct practical application, it comprises determine (the comprising factors such as decentralized medium, temperature, emulsifying manner and time) of selecting suitable dispersant and optimum dispersion technology, the anionic finishing agent of final preparation has satisfied requirement preferably, and its anion release concentration of seamless underwear of using described anionic finishing agent post processing acquisition has surpassed 4000/cm
3
At first, the inventor provides a kind of anion finishing liquor, and its raw material by following weight parts prepares through Over emulsfication and sonicated:
Tourmaline ultra micro powder 2-3 part,
Poly amic acid 0.5-1.5 part,
Sodium laurate 1-3 part,
Triethanolamine 1-3 part,
1000 parts in water.
As preferably, according to anion finishing liquor of the present invention, wherein, the granularity of described tourmaline ultra micro powder is at 100-200nm.
The present invention also provides the preparation method of above-mentioned anion finishing liquor, comprises the steps:
(1) preliminary treatment: load weighted water is put into container, and slowly add poly amic acid, sodium laurate and triethanolamine then and constantly stir, and then slowly add the tourmaline micro mist and continuous the stirring,
(2) emulsification treatment: pretreated product is 5000-6000 rev/min of following emulsification treatment 30-50 minute at the emulsification rotating speed,
(3) sonicated: the product after the emulsification treatment is under the 1100-1300w sonicated 8-15 minute at power, can obtain described anion finishing liquor.
As preferably, according to preparation method of the present invention, wherein, adopt high-shear emulsion machine in described step (2) emulsification treatment, emulsifying rate accelerates to 5000-6000 rev/min with 90-110 rev/min.It should be noted that the mulser continuous operation should not surpass 50 minutes, rotating speed should not surpass 6000 rev/mins, and continuous operation is shut down at least after 50 minutes and can be used in 30 minutes, so that mulser fully dispels the heat.
The present invention also provides the anion functional seamless underwear that is obtained by above-mentioned anion finishing liquor post processing.Anion functional method for sorting for garment material need be considered several aspects: at first, the method that is provided need satisfy not only suitable enterprise scale production but also anionic finishing agent fully is adsorbed on the garment material, and absorption needs evenly; Secondly the seamless underwear after the arrangement of anion functional finishing agent can discharge anion continually and steadily.For this reason, the characteristics of the characteristics of anion finishing liquor and seamless underwear according to the present invention, anion functional seamless underwear of the present invention prepares as follows:
A, seamless underwear is immersed in the anionic finishing agent at least 20 minutes, take out then and do processed, wherein, seamless underwear and anionic finishing agent weight ratio=1: 8-12, anionic finishing agent mixes acquisition by above-mentioned anion finishing liquor with adhesive, binder dosage is the 0.7-1.2% of seamless underwear weight
B, the seamless underwear that the A step is obtained are done shaping and drying and are handled.
As preferably, according to anion functional seamless underwear of the present invention, wherein, described adhesive adopts the polyacrylate adhesive, as GD-6 type polyacrylate adhesive etc.
As preferably, according to anion functional seamless underwear of the present invention, wherein, the temperature of anionic finishing agent is at 30-35 ℃ during described the immersion.
As preferably, according to anion functional seamless underwear of the present invention, wherein, need do following processing earlier when described anionic finishing agent uses every other day: anionic finishing agent is warming up to 35 ± 2 ℃, and stirs at least 30 minutes.
The present invention has following beneficial effect:
Seamless underwear by technology arrangement of the present invention has obtained anion releasing effect preferably, and the release concentration of its anion surpasses 4000/cm
3, fastness to washing can reach more than 3 grades, and feel, the appearance style of fabric do not had influence.
Method of the present invention is simple to operate, is easy to suitability for industrialized production, can guarantee the stable of performance between product batches.
Anion can make cerebral cortex function and mental activity strengthen, in high spirits, operating efficiency improves, sleep quality is improved, the effect of obvious hemangiectasis is arranged,, can remove the arteries spasm to improve people's lung capacity, reach the purpose that brings high blood pressure down, the state of an illness that helps high blood pressure and cardiovascular and cerebrovascular patient is recovered.The tourmaline ultrafine powder that adopts in this technology has pyroelectricity and piezoelectricity, therefore under the situation that temperature and pressure variation (even small variation) is arranged, can cause the electrical potential difference between the anion crystal, this static is up to 1,000,000 electron volts, thereby formation electric field, high voltage makes the air generation ionization in the electric field, the electron attachment of being hit is near water and oxygen molecule and make them be converted into negative aeroion, i.e. anion.By back of the present invention Collator Mode anion functional and seamless underwear are combined, make product have better health-care effect and low production cost.
The specific embodiment
Below in conjunction with embodiment, be described more specifically content of the present invention.Should be appreciated that enforcement of the present invention is not limited to the following examples, also can carry out certain pro forma accommodation and change the present invention.
In the present invention, if not refer in particular to, all equipment and raw material etc. all can be buied from market or the industry is commonly used.
Embodiment 1
1, gets the raw materials ready
Weigh up the seamless underwear weight M (weight before the washing) that will put in order, prepare other raw materials according to tourmaline ultra micro powder (100-200nm) weight=0.025M, water weight=10M, poly amic acid weight=0.01M, sodium laurate weight=0.02M, triethanolamine weight=0.02M, GD-6 type polyacrylate binder wt=0.01M.
2, preparation anion finishing liquor
A, preliminary treatment: load weighted water is poured in the middle of the container, slowly adds poly amic acid, sodium laurate, triethanolamine and ceaselessly stir; Slowly the tourmaline ultrafine powder is added container again, and ceaselessly stir;
B, emulsification treatment: container is installed on the high speed shear mulser, plug high speed shear mulser power supply, and open switch, after treating that the automatic check and correction of mulser is made zero, beginning is quickened from low to high, adopts crawl during acceleration, quickens 100 rev/mins at every turn, till 5000 rev/mins, keep the emulsification rotating speed to carry out emulsification treatment 50 minutes for 5000 rev/mins;
C, sonicated: the emulsification product re-uses ultrasonic cell disruptor finishing agent sonicated 10min with emulsification under the ultrasonic power of 1200W, obtains anion finishing liquor, and is standby.
3, the preparation of anion functional seamless underwear
A, the anion finishing liquor of step 2 preparation is poured in the unscrambled containers, added load weighted adhesive and stir, obtain anionic finishing agent;
B, the seamless underwear after will washing and dry are evenly put into unscrambled containers and are soaked (30 ℃), require all seamless underwears liquid that all submerges, and soak after 20 minutes, and the taking-up seamless underwear carries out processed.
C, the seamless underwear after will dewatering carry out shaping and drying by the difference of its raw material according to normal shaping and drying technique requirement to be handled and gets final product.
After testing, its anion release concentration of seamless underwear product of present embodiment acquisition is 4300/cm
3, fastness to washing reaches 3 grades.
During batch process, in one day, anionic finishing agent is used up as far as possible.If failed to use up the same day, second angel's time spent, should earlier anionic finishing agent be warming up to about 35 ℃, stir with stirring rifle (industrial) then and can use after 30 minutes.
Embodiment 2
1, gets the raw materials ready
Weigh up the seamless underwear weight M (weight before the washing) that will put in order, prepare other raw materials according to tourmaline ultra micro powder (100-200nm) weight=0.02M, water weight=10M, poly amic acid weight=0.005M, sodium laurate weight=0.01M, triethanolamine weight=0.01M, GD-6 type polyacrylate binder wt=0.007M.
2, preparation anion finishing liquor
A, preliminary treatment: load weighted water is poured in the middle of the container, slowly adds poly amic acid, sodium laurate, triethanolamine and ceaselessly stir; Slowly the tourmaline ultrafine powder is added container again, and ceaselessly stir;
B, emulsification treatment: container is installed on the high speed shear mulser, plug high speed shear mulser power supply, and open switch, after treating that the automatic check and correction of mulser is made zero, beginning is quickened from low to high, adopts crawl during acceleration, quickens 90 rev/mins at every turn, till 5400 rev/mins, keep the emulsification rotating speed to carry out emulsification treatment 30 minutes for 5400 rev/mins;
C, sonicated: the emulsification product re-uses ultrasonic cell disruptor finishing agent sonicated 8min with emulsification under the ultrasonic power of 1100W, obtains anion finishing liquor, and is standby.
3, the preparation of anion functional seamless underwear
A, the anion finishing liquor of step 2 preparation is poured in the unscrambled containers, added load weighted adhesive and stir, obtain anionic finishing agent;
B, the seamless underwear after will washing and dry are evenly put into unscrambled containers and are soaked (35 ℃), require all seamless underwears liquid that all submerges, and soak after 20 minutes, and the taking-up seamless underwear carries out processed.
C, the seamless underwear after will dewatering carry out shaping and drying by the difference of its raw material according to normal shaping and drying technique requirement to be handled and gets final product.
After testing, its anion release concentration of seamless underwear product of present embodiment acquisition is 4010/cm
3, fastness to washing reaches 3 grades.
Embodiment 3
1, gets the raw materials ready
Weigh up the seamless underwear weight M (weight before the washing) that will put in order, prepare other raw materials according to tourmaline ultra micro powder (100-200nm) weight=0.03M, water weight=10M, poly amic acid weight=0.015M, sodium laurate weight=0.03M, triethanolamine weight=0.03M, GD-6 type polyacrylate binder wt=0.012M.
2, preparation anion finishing liquor
A, preliminary treatment: load weighted water is poured in the middle of the container, slowly adds poly amic acid, sodium laurate, triethanolamine and ceaselessly stir; Slowly the tourmaline ultrafine powder is added container again, and ceaselessly stir;
B, emulsification treatment: container is installed on the high speed shear mulser, plug high speed shear mulser power supply, and open switch, after treating that the automatic check and correction of mulser is made zero, beginning is quickened from low to high, adopts crawl during acceleration, quickens 110 rev/mins at every turn, till 5500 rev/mins, keep the emulsification rotating speed to carry out emulsification treatment 45 minutes for 5500 rev/mins;
C, sonicated: the emulsification product re-uses ultrasonic cell disruptor finishing agent sonicated 15min with emulsification under the ultrasonic power of 1300W, obtains anion finishing liquor, and is standby.
3, the preparation of anion functional seamless underwear
A, the anion finishing liquor of step 2 preparation is poured in the unscrambled containers, added load weighted adhesive and stir, obtain anionic finishing agent;
B, the seamless underwear after will washing and dry are evenly put into unscrambled containers and are soaked (32 ℃), require all seamless underwears liquid that all submerges, and soak after 20 minutes, and the taking-up seamless underwear carries out processed.
C, the seamless underwear after will dewatering carry out shaping and drying by the difference of its raw material according to normal shaping and drying technique requirement to be handled and gets final product.
After testing, its anion release concentration of seamless underwear product of present embodiment acquisition is 4600/cm
3, fastness to washing reaches 3 grades.
The foregoing description just is used for description and interpretation content of the present invention, can not constitute limitation of the scope of the invention.Although the inventor has done in more detail the present invention and has enumerated, but, the content that those skilled in the art is disclosed according to summary of the invention part and embodiment can be made various modifications or/and additional or to adopt similar mode to substitute be obvious to described specific embodiment.
Claims (8)
1. an anion finishing liquor is characterized in that, its raw material by following weight parts prepares through Over emulsfication and sonicated:
Tourmaline ultra micro powder 2-3 part,
Poly amic acid 0.5-1.5 part,
Sodium laurate 1-3 part,
Triethanolamine 1-3 part,
1000 parts in water.
2] anion finishing liquor as claimed in claim 1 is characterized in that, the granularity of described tourmaline ultra micro powder is at 100-200nm.
3. the preparation method of claim 1 or 2 described anion finishing liquors is characterized in that, described method comprises the steps:
(1) preliminary treatment: load weighted water is put into container, and slowly add poly amic acid, sodium laurate and triethanolamine then and constantly stir, and then slowly add the tourmaline micro mist and continuous the stirring,
(2) emulsification treatment: pretreated product is 5000-6000 rev/min of following emulsification treatment 30-50 minute at the emulsification rotating speed,
(3) sonicated: the product after the emulsification treatment is under the 1100-1300w sonicated 8-15 minute at power, can obtain described anion finishing liquor.
4. preparation method as claimed in claim 3 is characterized in that, adopts high-shear emulsion machine in described step (2) emulsification treatment, and emulsifying rate accelerates to 5000-6000 rev/min with 90-110 rev/min.
5. anion functional seamless underwear is characterized in that, described seamless underwear prepares as follows:
A, seamless underwear is immersed in the anionic finishing agent at least 20 minutes, take out then and do processed, wherein, seamless underwear and anionic finishing agent weight ratio=1: 8-12, anionic finishing agent mixes acquisition by claim 1 or 2 described anion finishing liquors with adhesive, binder dosage is the 0.7-1.2% of seamless underwear weight
B, the seamless underwear that the A step is obtained are done shaping and drying and are handled.
6. anion functional seamless underwear as claimed in claim 5 is characterized in that, described adhesive adopts the polyacrylate adhesive.
7. anion functional seamless underwear as claimed in claim 5 is characterized in that, the temperature of anionic finishing agent is at 30-35 ℃ during described the immersion.
8. as claim 5 or 7 described anion functional seamless underwears, it is characterized in that, need do following processing earlier when described anionic finishing agent uses every other day: anionic finishing agent is warming up to 35 ± 2 ℃, and stirs at least 30 minutes.
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| CN2009103060060A CN101671952B (en) | 2009-08-25 | 2009-08-25 | Anion finishing liquor and preparation method and anion functional seamless underwear |
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| CN2009103060060A CN101671952B (en) | 2009-08-25 | 2009-08-25 | Anion finishing liquor and preparation method and anion functional seamless underwear |
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| CN101671952B CN101671952B (en) | 2011-06-29 |
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| CN104562653A (en) * | 2014-12-23 | 2015-04-29 | 常熟市海虞富盛经纬编织造厂 | Fabric finishing liquor |
| CN105177856A (en) * | 2015-08-29 | 2015-12-23 | 福建鑫华股份有限公司 | Environment-friendly antibacterial composite material and manufacturing method thereof |
| CN106012259A (en) * | 2016-06-01 | 2016-10-12 | 佛山市航宇针织有限公司 | Seamless knitting method |
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| CN106283616A (en) * | 2016-08-29 | 2017-01-04 | 徐杭婷 | A kind of preparation method of fabric anion finishing liquor |
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| CN106618010A (en) * | 2016-12-29 | 2017-05-10 | 郑州德惠纺织科技有限公司 | Degradable milk fiber quilt containing negative ions and preparation method of milk fiber quilt |
| CN106724474A (en) * | 2016-12-29 | 2017-05-31 | 郑州德惠纺织科技有限公司 | Containing anion and washable fibre and soya quilt and preparation method thereof |
| CN106884272A (en) * | 2017-03-23 | 2017-06-23 | 浙江绿龙新材料有限公司 | The preparation method of nano-negative ion vehicle inside decoration fabric |
| CN107130427A (en) * | 2017-05-18 | 2017-09-05 | 浙江宏都寝具有限公司 | A kind of negative-ion fiber and its manufacturing process |
| CN107164946A (en) * | 2017-05-25 | 2017-09-15 | 海盐派特普科技有限公司 | A kind of clothing anion finishing liquor |
| CN107190501A (en) * | 2017-05-25 | 2017-09-22 | 兰溪市拜瑞珂科技服务有限公司 | A kind of preparation method of clothing anion finishing liquor |
| CN110409169A (en) * | 2019-09-12 | 2019-11-05 | 河北森雅环保新材料科技有限公司 | The production method for inducing the pure cotton and its functional powders and auxiliary agent of negative oxygen ion |
| CN111287005A (en) * | 2020-02-12 | 2020-06-16 | 常德集智生物科技有限公司 | Green antibacterial and bactericidal negative oxygen ion releasing garment |
| CN112342796A (en) * | 2020-11-10 | 2021-02-09 | 西安工程大学 | Preparation method of negative ion 3D printing flexible garment fabric |
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| CN104562653A (en) * | 2014-12-23 | 2015-04-29 | 常熟市海虞富盛经纬编织造厂 | Fabric finishing liquor |
| CN105177856A (en) * | 2015-08-29 | 2015-12-23 | 福建鑫华股份有限公司 | Environment-friendly antibacterial composite material and manufacturing method thereof |
| CN106012259A (en) * | 2016-06-01 | 2016-10-12 | 佛山市航宇针织有限公司 | Seamless knitting method |
| CN106283670A (en) * | 2016-08-29 | 2017-01-04 | 徐杭婷 | A kind of preparation method of antibiotic finish of the fabric liquid |
| CN106283616A (en) * | 2016-08-29 | 2017-01-04 | 徐杭婷 | A kind of preparation method of fabric anion finishing liquor |
| CN106381716A (en) * | 2016-08-29 | 2017-02-08 | 徐杭婷 | Preparation method of fabric photochromic finishing liquid |
| CN106618010A (en) * | 2016-12-29 | 2017-05-10 | 郑州德惠纺织科技有限公司 | Degradable milk fiber quilt containing negative ions and preparation method of milk fiber quilt |
| CN106724474A (en) * | 2016-12-29 | 2017-05-31 | 郑州德惠纺织科技有限公司 | Containing anion and washable fibre and soya quilt and preparation method thereof |
| CN106884272A (en) * | 2017-03-23 | 2017-06-23 | 浙江绿龙新材料有限公司 | The preparation method of nano-negative ion vehicle inside decoration fabric |
| CN106884272B (en) * | 2017-03-23 | 2019-04-12 | 浙江绿龙新材料有限公司 | The production method of nano-negative ion vehicle inside decoration fabric |
| CN107130427A (en) * | 2017-05-18 | 2017-09-05 | 浙江宏都寝具有限公司 | A kind of negative-ion fiber and its manufacturing process |
| CN107130427B (en) * | 2017-05-18 | 2020-06-23 | 浙江宏都寝具有限公司 | Anion fiber and manufacturing process thereof |
| CN107164946A (en) * | 2017-05-25 | 2017-09-15 | 海盐派特普科技有限公司 | A kind of clothing anion finishing liquor |
| CN107190501A (en) * | 2017-05-25 | 2017-09-22 | 兰溪市拜瑞珂科技服务有限公司 | A kind of preparation method of clothing anion finishing liquor |
| CN110409169A (en) * | 2019-09-12 | 2019-11-05 | 河北森雅环保新材料科技有限公司 | The production method for inducing the pure cotton and its functional powders and auxiliary agent of negative oxygen ion |
| CN111287005A (en) * | 2020-02-12 | 2020-06-16 | 常德集智生物科技有限公司 | Green antibacterial and bactericidal negative oxygen ion releasing garment |
| CN112342796A (en) * | 2020-11-10 | 2021-02-09 | 西安工程大学 | Preparation method of negative ion 3D printing flexible garment fabric |
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