CN101565581A - Reflective heat-insulation coating and preparation method thereof - Google Patents
Reflective heat-insulation coating and preparation method thereof Download PDFInfo
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Abstract
The embodiment of the invention provides a reflective heat-insulation coating and a preparation method thereof. The reflective heat-insulation coating comprises the following raw materials of aqueous pure crylic acid resin, aqueous elastic resin, titanium dioxide, ceramic hollow microspheres, infrared powder, a flame retardant, water, an organic dispersant, a film-forming additive, an antifreeze, a thickener, an anti-foaming agent, a wetting agent, a preservative and a pH value regulator. The coating is a single-component aqueous coating, has no toxicity and good weatherability; extremely fine hollow microsheres are closely arranged by multi-stage in the coating to form a vacuum layer so as to have extremely strong reflection and obstruction function to the solar radiation heat and can effectively reduce the radiation heat transfer and convection heat transfer, thus reducing the heat balance temperature on the surface of the article. The reflective heat-insulation coating leads the building space and the facility container to be warm in winter and cool in summer, reduces the heat island effect and energy consumption of the air conditioner, has obvious energy-saving effect, and reduces the surface temperature by 20 DEG C to a maximum extent and reduces the internal temperature by 5-10 DEG C compared to the normal coating.
Description
Technical field
The present invention relates to building coating, relate in particular to a kind of reflective heat-insulation paint and preparation method thereof.
Background technology
Proportion is 30～40% in the whole energy consumption of the mankind for building energy consumption, and the overwhelming majority is the energy consumption of heating and air-conditioning, so thermal insulation technology is applied in the building more and more, as various wall heat insulation materials, reflective heat-insulation paint etc.Traditional heat preserving and insulating material is that it is main reducing thermal conductivity and transmissibility factor with raising gas phase voidage.The fiber-like lagging material will make transmission of heat by convection and radiative transfer raise in environment for use, and thicker coating must be arranged; And section bar class inorganic heat insulation material will carry out assembling construction, exist seam many, diminish defectives such as attractive in appearance, that water-repellancy is poor, work-ing life is short.
Now also be useful on heat insulation thermal insulating coating, the problem that there is function singleness in this thermal insulating coating, effect is limited and validity period is short, and constructional method complexity are used for industrial aspect more, use very few aspect construction work, dwelling construction.And do not have now a kind of thermal insulating coating that can be applied in construction work, dwelling construction aspect fully.
Summary of the invention
The purpose of the embodiment of the invention is to overcome the deficiencies in the prior art part, provides a kind of solar heat that can reflect with reflective heat-insulation paint of reducing room temp and preparation method thereof.
The purpose of the embodiment of the invention is achieved through the following technical solutions:
The embodiment of the invention provides a kind of reflective heat-insulation paint, and this thermal insulating coating comprises following each raw material by weight percentage:
Constituent mass per-cent
Water-based pure acrylic resin 5～15%
The pure elastic resin 40～45% of water-based
Titanium dioxide 20～30%
Pottery hollow beads 2～8%
Infrared powder 2～3%
Fire retardant 1～3%
Water 10～15%
Organic dispersing agent 0.4～0.8%
Film coalescence aid 0.2～1.4%
Frostproofer 1～1.5%
Thickening material 12～0.15%
Defoamer 0.1～0.3
Wetting agent 0.1～0.2
Sanitas 0.1～0.2
PH value conditioning agent 0.05～0.1.
The water-based pure acrylic resin that described water-based pure acrylic resin adopts soap-free polymerization to make.
The pure elastic resin of described water-based adopts UV-light self-crosslinking elastic pure acrylic acid resin.
Described titanium dioxide adopts Rutile type Titanium Dioxide.
Described infrared powder adopts the nano-far-infrared powder.
Described organic dispersing agent adopts polycarboxylic acid salt's organic dispersing agent.
Described film coalescence aid adopts Yi Shiman alcohol ester 12; Described frostproofer adopts propylene glycol; Described thickening material adopts alkali swelling class thickening material.
Described defoamer adopts silicone based defoamer; Described wetting agent adopts nonionic surface active agent.
Described sanitas adopts the isothiazolinone sanitas; Described pH value conditioning agent adopts organic amine pH value to regulate.
The embodiment of the invention also provides a kind of making method of reflective heat-insulation paint, comprising:
Get each raw material by each described prescription in above-mentioned;
To account for earlier water gross weight 5% water, organic dispersing agent, film coalescence aid, frostproofer, thickening material, account for half defoamer, wetting agent, sanitas, pH value conditioning agent of defoamer gross weight and join in the dispersion cylinder of dispersion machine, under 300～400 rev/mins rotating speed state, stirred evenly 20～30 minutes;
Add titanium dioxide again, under 800～1000 rev/mins rotating speed, system is dispersed to fineness≤40 μ m, add remainder water and remaining second half defoamer then, add water-based pure acrylic resin, the pure elastic resin of water-based again, add ceramic hollow beads, infrared powder, fire retardant under 100～300 rev/mins rotating speed, continuing to disperse did not have bubble to system in 8～12 minutes;
Add viscosity to the 98 ± 2KU of thickening material regulation system at last, promptly obtain reflective heat-insulation paint.
The technical scheme that is provided by the invention described above embodiment as can be seen, the invention process forms the water-borne coatings of single-component, nontoxic, weathering resistance is good, the superfine little cenosphere vacuum layer that tight multistage arrangement forms in coating has extremely strong reflection and iris action to solar radiant heat in the coating, can effectively reduce radiative transfer and transmission of heat by convection, thereby reduce the thermal equilibrium temperature of body surface.Use the space of this coating and facility container to have to be reflected in, heat insulation effect, reduce " tropical island effect ", reduce air conditioning energy consumption, energy-saving effect is remarkable.
Embodiment
Below in conjunction with respective embodiments, the invention will be further described.
Embodiment one
The embodiment of the invention provides a kind of reflective heat-insulation paint, is applied in architecturally, has the function of reflective insulation, and this thermal insulating coating comprises following each raw material by weight percentage:
Constituent mass per-cent
Water-based pure acrylic resin 5～15%
The pure elastic resin 40～45% of water-based
Titanium dioxide 20～30%
Pottery hollow beads 2～8%
Infrared powder 2～3%
Fire retardant 1～3%
Water 10～15%
Organic dispersing agent 0.4～0.8%
Film coalescence aid 0.2～1.4%
Frostproofer 1～1.5%
Thickening material 12～0.15%
Defoamer 0.1～0.3
Wetting agent 0.1～0.2
Sanitas 0.1～0.2
PH value conditioning agent 0.05～0.1.
The water-based pure acrylic resin that water-based pure acrylic resin in the above-mentioned coating adopts the soap-free polymerization technology to make, concrete
Can adopt the pure acrylic resin of national starch water-based.
The pure elastic resin of water-based in the above-mentioned coating adopts UV-light self-crosslinking elastic pure acrylic acid resin, specifically can adopt ROHM AND HAAS UV-light self-crosslinking elastic pure acrylic acid resin.
Titanium dioxide in the above-mentioned coating adopts Rutile type Titanium Dioxide, specifically can adopt Dupont rutile-type R902 titanium dioxide.
Infrared powder in the above-mentioned coating adopts the nano-far-infrared powder, specifically can adopt Minnesota Mining and Manufacturing Company's pottery hollow beads.
Organic dispersing agent in the above-mentioned coating adopts polycarboxylic acid salt's organic dispersing agent.
Film coalescence aid in the above-mentioned coating adopts alcohol ester 12, the alcohol ester 12 that can adopt Yi Shiman to produce; Frostproofer adopts propylene glycol, the propylene glycol that can adopt Yanshan Petrochemical to produce; Thickening material adopts alkali swelling class thickening material; Defoamer adopts silicone based defoamer, the silicone based defoamer that can adopt Japanese Nuo Puke to produce; Wetting agent adopts nonionic surface active agent, can adopt the nonionic surface active agent of Japanese Nuo Puke; Sanitas adopts the isothiazolinone sanitas; PH value conditioning agent adopts organic amine pH value to regulate.
The making method of the reflective heat-insulation paint of the embodiment of the invention, undertaken by following step:
Get each raw material by the prescription in above-mentioned;
Water, organic dispersing agent, film coalescence aid, frostproofer, thickening material, the defoamer that accounts for defoamer gross weight 1/2, wetting agent, sanitas, the pH value conditioning agent that will account for water gross weight 5% earlier join in the dispersion cylinder of dispersion machine, under 300～400rpm/ rotating speed state, stirred 20～30 minutes, stir;
Add titanium dioxide again, under 800～1000 rev/mins rotating speed, high speed dispersion makes system chat fineness≤40 μ m, add remainder water and the remaining defoamer that accounts for defoamer gross weight 1/2 then, add water-based pure acrylic resin, the pure elastic resin of water-based again, add ceramic hollow beads, infrared powder, fire retardant under 100～300 rev/mins rotating speeds stir, continuing to disperse did not have bubble to system in 8～12 minutes;
Add thickening material at last and be adjusted to viscosity to 98 ± 2KU, promptly obtain reflective heat-insulation paint.
Embodiment two
Present embodiment provides a kind of reflective heat-insulation paint, is used in various architecturally, is used for reflected sunlight to play heat insulation effect, and this thermal insulating coating forms by following formulated:
Constituent mass per-cent (%)
Water-based pure acrylic resin 5%
The pure elastic resin 45% of water-based
Titanium dioxide 25%
Pottery hollow beads 6%
Infrared powder 2%
Fire retardant 1%
Water 13.2%
Organic dispersing agent 0.2%
Organic dispersing agent 0.2%
Film coalescence aid 0.2%
Frostproofer propylene glycol 1.5%
Thickening material 0.12%
Defoamer 0.23%
Wetting agent 0.1%
Sanitas 0.2%
PH value conditioning agent 0.05%.
In each raw material of above-mentioned reflective heat-insulation paint prescription, used water-borne acrylic resin is a high molecular synthetic resin, can select pure third resin of the national starch of internationally renowned brand company for use, and the aqueous elastic resin can adopt the pure elastic resin of U.S. Rhom and Hass; Titanium dioxide can adopt the titanium dioxide of du pont company; The pottery hollow beads can adopt the ceramic hollow beads of Minnesota Mining and Manufacturing Company; Wherein, organic dispersing agent, film coalescence aid, frostproofer, thickening material, defoamer, wetting agent, sanitas and pH value conditioning agent etc. are auxiliary agent for 8 kinds; Polycarboxylic acid salt's dispersion agent, polycarboxylic acid salt's dispersion agent that can adopt German BASF AG and Ciba to provide are provided dispersion agent; Film coalescence aid can adopt the film coalescence aid of U.S. Yi Shi Man, can be used for reducing the film-forming temperature of acrylic resin; Thickening material adopts alkali swelling class thickening material, can select the product of U.S. Hai Mingsi company for use; Sanitas can be selected the sanitas product of U.S. Rhom and Hass for use; The pH value is adjusted and is adopted organic amine pH value to adjust.
The manufacture method of above-mentioned reflective heat-insulation paint:
(1) water, organic dispersing agent, film coalescence aid, frostproofer, thickening material, defoamer, wetting agent, sanitas, the pH value conditioning agent that will account for water gross weight 5% earlier joins in the dispersion cylinder of dispersion machine, under 300～400 rev/mins state, stirred 20～30 minutes, system is stirred;
(2) add titanium dioxide again, under 800～1000 rev/mins high-speed stirring, system is dispersed to fineness≤40 μ m, add remainder water and remaining defoamer then, add water-based pure acrylic resin, the pure elastic resin of water-based again, under 100～300 rev/mins whipped state, add ceramic hollow beads, infrared powder, fire retardant, continue to disperse 10min not have bubble to system;
(3) adding thickening material at last is adjusted to suitable viscosity (98 ± 2KU) promptly obtains this reflective heat-insulation paint.
Embodiment three
Present embodiment provides a kind of reflective heat-insulation paint, is used in various architecturally, is used for reflected sunlight to play heat insulation effect, and this thermal insulating coating forms by following formulated:
Constituent mass per-cent (%)
Import water-based pure acrylic resin 2,800 15%
The pure elastic resin 2,848 38% of import water-based
Import titanium dioxide 20%
Import pottery hollow beads 8%
Infrared powder 2%
Fire retardant 2%
Water 10.35%
Organic dispersing agent PA30 0.4%
Organic dispersing agent 4,585 0.4%
Film coalescence aid Texanol 1.4%
Frostproofer propylene glycol 1.5%
Thickening material 420 0.15%
Defoamer NXZ 0.3%
Wetting agent X-405 0.2%
Sanitas LXZ 0.2%
PH value conditioning agent AMP-95 0.1%.
The preparation method of the preparation method of the reflective heat-insulation paint in the present embodiment and embodiment two is basic identical, in this no longer repeat specification.
Embodiment four
Present embodiment provides a kind of reflective heat-insulation paint, is used in various architecturally, is used for reflected sunlight to play heat insulation effect, and this thermal insulating coating forms by following formulated:
Constituent mass per-cent (%)
Import water-based pure acrylic resin 2,800 10%
The pure elastic resin 2,848 42% of import water-based
Import titanium dioxide 25%
Import pottery hollow beads 5%
Infrared powder 2.5%
Fire retardant 1.5%
Water 10.69%
Organic dispersing agent PA30 0.3%
Organic dispersing agent 4,585 0.3%
Film coalescence aid Texanol 0.8%
Frostproofer propylene glycol 1.2%
Thickening material 420 0.13%
Defoamer NXZ 0.2%
Wetting agent X-405 0.15%
Sanitas LXZ 0.15%
PH value conditioning agent AMP-95 0.08%.
The preparation method of the preparation method of the reflective heat-insulation paint in the present embodiment and embodiment two is basic identical, in this no longer repeat specification.
The paint film fundamental property of the reflective heat-insulation paint of the embodiment of the invention sees Table 1
Table 1
The construction technology of the reflective heat-insulation paint that the embodiment of the invention makes is as follows:
Construction process is: metope base treatment → scrape (smearing) be coated with flexible waterproof putty 2-3 all over → roller coating exterior wall seal coat → snap the line, lattice, tape → roller coating reflective heat-insulation paint → spraying coating varnish.
The concrete operations step is:
(1) processing base level: before base treatment, body of wall needs the maintenance of certain hour, and the curing time in general new cement wall surface winter is 28 days, and the curing time in summer is 14 days.Maintenance is arrived the pH value of basic unit less than 10, and water ratio carries out processing base level again after 10%;
Should thoroughly remove loose, peeling, hollowing, atomizing basic unit before the base treatment, then, remove pollutents such as dust, greasy dirt;
(2) blade coating flexible waterproof putty:
Repair metope with flexible waterproof putty, the local levelling in first road is filled up big hole and slit with putty or gap-filling glue, treat the putty drying after, detail sanding is completely criticized putty again and is made basic unit smooth.One time blade coating thickness should not surpass 0.5mm, divides twice above construction; Per pass was not less than 5 hours pitch time; (general 4-6 hour) polishing was in time revised after per pass putty blade coating finished.The flexible putty total thickness is controlled at 1.0～1.5mm;
Flexible waterproof putty is a cement system, need carry out maintenance equally, and general curing time is 14 days, to the pH value less than 10, water ratio can carry out the construction of next process after 10%.
(3) brushing seal coat:
After treating that putty reaches requirement, basic unit should be polished flat before the brushing, the cleaning floating dust, hair rolls and should keep clean, and brushes watersoluble closed priming paint one time, brushes evenly, and the brush of leakage phenomenon never can be arranged.Forbid converting water when watersoluble closed priming paint is constructed, guarantee that simultaneously seal coat is not subjected to any pollution, is not with any color;
(4) roller coating reflective heat-insulation paint:
Treat can adopt after the abundant maintenance of putty layer method of roll coating to divide all over the construction thermal insulating coating, treat next time of constructing again after the first pass thorough drying, converting the water yield during construction is 10-20%, and generally constructing just can survive about 3 times;
(5) spraying coating varnish:
(general fine day kept 3 days at least) can spray coating varnish after treating the thermal insulating coating complete drying, notes keeping viscosity during construction, air pressure, and the spout size is consistent, notes pre-sag prevention phenomenon;
The coating varnish construction time is not converted any thinner, must spray evenly and comprehensively, generally will spray twice, and phenomenons such as the spray of leakage never can be arranged;
(6) construction precautions
Construction environment: guarantee that envrionment temperature should be greater than 5 ℃, relative humidity is less than 70%, and the weather of no strong wind is construction down, and rainy day or the weather that will soon rain also must not be constructed, and pay close attention to weather-forecast during construction more;
(7) accumulating requires:
1. condition of storage: coating ventilate, dry, temperature stores under 5～35 ℃ environment;
2. quality guaranteed period: effective shelf lives of product is 1 year;
3. transport condition: transportation is handled by " non-dangerous goods transportation rule ".
In sum, the reflective heat-insulation paint of the embodiment of the invention, it is a kind of water-borne coatings of single-component, the superfine little cenosphere vacuum layer that tight multistage arrangement forms in coating has extremely strong reflection and iris action to solar radiant heat in the coating, can effectively reduce radiative transfer and transmission of heat by convection, thereby reduce the thermal equilibrium temperature of body surface.This coating is nontoxic, and weathering resistance is good, has waterproof, anti-flaming function concurrently, has high wear resistance and cohesive strength and excellent toughness.Compare with common coating; be not only for realizing a certain protection function; coat a protective layer for material requested (or fender), but from modernized demand quality, with multifunctional protection, energy-efficiently, long-acting the functional coat that modern coating complex art merges such as continue.Its coating is the functional layer that is rich in elasticity, ductility and ventilation property after the operation.Be coated in architectural after, have the function that flashes back the sunlight, can form a protective layer, be a kind of multifunctional protection, energy-efficient, long-acting lasting functional coat, the coating of formation is a kind of functional coating that is rich in elasticity, ductility and ventilation property.Make space and facility container cool in summer and warm in winter, reduce " tropical island effect ", reduce air conditioning energy consumption, energy-saving effect is remarkable.Compare with common coating, 20 ℃ of the highest reductions of surface temperature, internal temperature reduces by 5～10 ℃.
The above; only be the preferable embodiment of the present invention; but protection scope of the present invention is not limited thereto; the present invention is not caused any restriction because of the succession of each embodiment yet; anyly be familiar with those skilled in the art in the technical scope that the present invention discloses; the variation that can expect easily or replacement all should be encompassed within protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with the protection domain of claim.
Claims (10)
1, a kind of reflective heat-insulation paint is characterized in that, this thermal insulating coating comprises following each raw material by weight percentage:
Constituent mass per-cent
Water-based pure acrylic resin 5～15%
The pure elastic resin 40～45% of water-based
Titanium dioxide 20～30%
Pottery hollow beads 2～8%
Infrared powder 2～3%
Fire retardant 1～3%
Water 10～15%
Organic dispersing agent 0.4～0.8%
Film coalescence aid 0.2～1.4%
Frostproofer 1～1.5%
Thickening material 0.15～12%
Defoamer 0.1～0.3
Wetting agent 0.1～0.2
Sanitas 0.1～0.2
PH value conditioning agent 0.05～0.1.
2, reflective heat-insulation paint according to claim 1 is characterized in that, the water-based pure acrylic resin that described water-based pure acrylic resin adopts soap-free polymerization to make.
3, reflective heat-insulation paint according to claim 1 is characterized in that, the pure elastic resin of described water-based adopts UV-light self-crosslinking elastic pure acrylic acid resin.
4, reflective heat-insulation paint according to claim 1 is characterized in that, described titanium dioxide adopts Rutile type Titanium Dioxide.
5, reflective heat-insulation paint according to claim 1 is characterized in that, described infrared powder adopts the nano-far-infrared powder.
6, reflective heat-insulation paint according to claim 1 is characterized in that, described organic dispersing agent adopts polycarboxylic acid salt's organic dispersing agent.
7, reflective heat-insulation paint according to claim 1 is characterized in that, described film coalescence aid adopts Yi Shiman alcohol ester 12; Described frostproofer adopts propylene glycol; Described thickening material adopts alkali swelling class thickening material.
8, reflective heat-insulation paint according to claim 1 is characterized in that, described defoamer adopts silicone based defoamer; Described wetting agent adopts nonionic surface active agent.
9, reflective heat-insulation paint according to claim 1 is characterized in that, described sanitas adopts the isothiazolinone sanitas; Described pH value conditioning agent adopts organic amine pH value to regulate.
10, a kind of making method of reflective heat-insulation paint is characterized in that, comprising:
Get each raw material by each described prescription in the aforesaid right requirement 1～9;
To account for earlier water gross weight 5% water, organic dispersing agent, film coalescence aid, frostproofer, thickening material, account for half defoamer, wetting agent, sanitas, pH value conditioning agent of defoamer gross weight and join in the dispersion cylinder of dispersion machine, under 300～400 rev/mins rotating speed state, stirred evenly 20～30 minutes;
Add titanium dioxide again, under 800～1000 rev/mins rotating speed, system is dispersed to fineness≤40 μ m, add remainder water and remaining second half defoamer then, add water-based pure acrylic resin, the pure elastic resin of water-based again, add ceramic hollow beads, infrared powder, fire retardant under 100～300 rev/mins rotating speed, continuing to disperse did not have bubble to system in 8～12 minutes;
Add viscosity to the 98 ± 2KU of thickening material regulation system at last, promptly obtain reflective heat-insulation paint.
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