CN101514302A - Method for comprehensively utilizing peanut shell - Google Patents
Method for comprehensively utilizing peanut shell Download PDFInfo
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- CN101514302A CN101514302A CNA2008100469080A CN200810046908A CN101514302A CN 101514302 A CN101514302 A CN 101514302A CN A2008100469080 A CNA2008100469080 A CN A2008100469080A CN 200810046908 A CN200810046908 A CN 200810046908A CN 101514302 A CN101514302 A CN 101514302A
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- Prior art keywords
- arachidis hypogaeae
- pericarppium arachidis
- extract
- extracting solution
- comprehensive utilization
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- 235000017060 Arachis glabrata Nutrition 0.000 title abstract description 10
- 235000010777 Arachis hypogaea Nutrition 0.000 title abstract description 10
- 235000018262 Arachis monticola Nutrition 0.000 title abstract description 10
- 235000020232 peanut Nutrition 0.000 title abstract description 10
- 241001553178 Arachis glabrata Species 0.000 title abstract 7
- 239000000284 extract Substances 0.000 claims abstract description 59
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 32
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Abstract
The invention discloses a method for comprehensively utilizing a peanut shell, which relates to a method for extracting active ingredients from the peanut shell for preparing cigarette flavor and preparing filter residue of the extracted peanut shell into a disposable product. The method comprises the following steps: (1) extracting effective ingredients in the peanut shell by an ultrasonic wave extraction method, and filtering the effective ingredients to obtain an original extracting solution; (2) concentrating, refrigerating and filtering the original extracting solution to obtain a clear rufous liquid; (3) directly flavoring the cigarette by the extracting solution of the peanut shell or using the extracting solution into an essence formulation of the cigarette; (4) adding a toughness adhesion agent into the filter residue of the peanut shell and mixing the toughness adhesion agent and the filter residue into even granular materials; (5) feeding the materials into a forming machine and feeding the materials into a food package vessel or dishware; and (6) air drying and disinfecting the vessel or the dishware. The method has good coordination of the extract and cigarette flavor without residue, can obviously soften smoke gas and enrich cigarette flavor, and has wide range of application. The filter residue manufactures the disposable product by a method of aggregated compaction and addition of edible glue, so that waste materials are not generated in the whole process.
Description
Technical field
The invention belongs to a kind of technology that the depleted Pericarppium arachidis hypogaeae is fully utilized, relate to and from Pericarppium arachidis hypogaeae, extract activeconstituents, be used to prepare the method for tobacco aromatics using, and the Pericarppium arachidis hypogaeae filter residue after will extracting is processed into the method for disposable product.
Background technology
Peanut is a leguminous plants, is one of main oil variety of high-quality edible oil, and Pericarppium arachidis hypogaeae is a depleted shell behind the removal peanut fruit.In the prior art, generally be to compress making sheet, can not make full use of effective constituent wherein as feed or with other plant crude fiber to the utilization of Pericarppium arachidis hypogaeae.Though the research of following bibliographical information is arranged, the utility value of Pericarppium arachidis hypogaeae also is far from developing.
Document " extraction, purifying and the research of bacteriostatic active ingredients such as luteolin in the Pericarppium arachidis hypogaeae " report, slightly carry, solvent gradient extraction, cooperate bacteriostatic activity to follow the tracks of to detect with methyl alcohol, obtained the Pericarppium arachidis hypogaeae ethyl acetate component that bacteriostatic activity is strong, be rich in flavonoid, and obtain three kinds of compounds (1# with method purifying such as acid-base precipitation, column chromatographies, 2#, 3#), wherein 2# streptococcus aureus and Bacillus subtilus have certain inhibition effect, and 3# has certain bacteriostatic activity to streptococcus aureus, yeast saccharomyces cerevisiae; 1# then has wider antimicrobial spectrum, and streptococcus aureus, yeast saccharomyces cerevisiae, Bacillus subtilus and mould are all had stronger restraining effect.
Document " Pericarppium arachidis hypogaeae comprehensive utilizating research---Pericarppium arachidis hypogaeae is to the adsorption of Cr (IV) " has been inquired into the comprehensive utilization to Pericarppium arachidis hypogaeae, investigated absorption and desorption and the influence factor of Pericarppium arachidis hypogaeae to Cr (IV), studied the recovery of the Cr (IV) that is adsorbed by Pericarppium arachidis hypogaeae, find to use the high chloro acid dissolution after the ashing, the rate of recovery reaches more than 95%.
The japanese food expert studies and uses Pericarppium arachidis hypogaeae with methanol extraction, and the extract that obtains contains luteolin, and its anti-Oxidation of Fat and Oils surpasses BHA (BHA) commonly used.
Ultrasonic wave extraction is to grow up nineteen nineties.Originally aspect industrial application, utilize usually that the excusing from death ripple cleans, drying, sterilization, atomizing and nondestructive testing etc.Ultrasonic wave is meant that frequency is 20 kilo hertzs about-50,000,000 a hertzian wave, is a kind of mechanical wave, needs medium to propagate, and has characteristics such as frequency height, wavelength is short, power is big, penetration power is strong.Ultrasonic wave extraction is the strong longitudinal vibration that utilizes ultrasonic wave special, the high speed impact fragmentation, physicalies such as cavitation effect stirring and heating, between solvent and extract, produce the sound wave cavatition, cause the formation of bubble in the solution, increase and the explosion compression, thereby dispersible solid extract, destroy the extract cellularstructure, make solvent can infiltrate cell interior, thereby quicken the dissolving of effective constituent, improve extraction ratio of effective constituents, experiment comparative analysis proof ultrasonic wave extraction can shorten extraction time greatly, improves extraction yield, and does not change the structure of effective constituent.
Summary of the invention
Above-mentioned situation at prior art, the technical problem to be solved in the present invention provides a kind of method of comprehensive utilization of Pericarppium arachidis hypogaeae, it extracts Pericarppium arachidis hypogaeae with ultrasonic wave, extract is used for tobacco aromatics using, filter residue after again Pericarppium arachidis hypogaeae being extracted adds binding agent and makes disposable food container or tableware; Pericarppium arachidis hypogaeae is utilized completely, and solved environmental issue.
Technical scheme of the present invention is achieved in that a kind of method of comprehensive utilization of Pericarppium arachidis hypogaeae carries out according to the following steps:
(1) with ultrasonic extraction the effective constituent in the Pericarppium arachidis hypogaeae is extracted earlier, filtering gained filtrate is first extract, and the Pericarppium arachidis hypogaeae filter residue is left subsequent step and uses;
(2) first extract is concentrated into the 1/3-1/8 of its original volume, places 0 ℃ to-5 ℃ to locate to refrigerate 1-7 days, filter the throw out of removing wherein, the Pericarppium arachidis hypogaeae extracting solution that obtains is clarifying sorrel liquid, has light peanut fragrance;
(3) the Pericarppium arachidis hypogaeae extracting solution is used for the direct perfuming of cigarette or be used for cigarette perfume formulation;
(4) with the Pericarppium arachidis hypogaeae filter residue dryness in the sun of step (1), add the toughness binding agent, stir and be single-size shape material;
(5) above-mentioned single-size shape material is sent into shaper and be shaped to food container or tableware;
(6) in type food container or tableware are carried out air-dry, sterilization.
The step of the described ultrasonic extraction of step (1) is:
1) Pericarppium arachidis hypogaeae is broken into powdered, crosses 80 mesh sieves;
2) with the Pericarppium arachidis hypogaeae powder: the ratio of ethanol=1: 3-7 places container, soaks 1-3 hour;
3) the above-mentioned material after will soaking is put into the ultrasonic wave container and is carried out ultrasonic extraction, and ultrasonic frequency 45-65Hz extracted 30-180 minute; Filtration obtains extract just.
Described ethanol is 50～95% ethanol.
Step (1) or 3) the described ultrasonic extraction of carrying out is an extract at room temperature or extract down at 40 ℃-50 ℃.
The described toughness binding agent of step (4) is the food grade sodium alginate of safety non-toxic.
Described toughness binding agent, its add-on are the 5-15% of Pericarppium arachidis hypogaeae filter residue gross weight.
Step (3) is described when the Pericarppium arachidis hypogaeae extracting solution is used for direct perfuming, and the ratio that extracting solution accounts for pipe tobacco weight is 1 ‰-5 ‰.
Step (3) is described when the Pericarppium arachidis hypogaeae extracting solution is used for perfume formulation, and the ratio that extracting solution accounts for the perfume formulation gross weight is 0.5%-3%.
The described Pericarppium arachidis hypogaeae filter residue of step (4) dryness in the sun, dried moisture content is 5-15%.
The described shaper moulding of step (5) is the die cavity that the single-size shape amount of anticipating is transported to shaper, compression moulding behind vibration 10-30 second, the uniform distribution, and the unit pressure of compacting is 250-450kg/cm
2, temperature is 140～200 ℃, keeps under this temperature and pressure 30～80 seconds.
Method of the present invention has the following advantages:
1, the Pericarppium arachidis hypogaeae extract of prior art only stays in the research aspect, does not bring economic benefit as yet, and the present invention has possessed the condition that Workshop Production transforms, can create economic worth.
2, extraction raw material Pericarppium arachidis hypogaeae is cheap and easy to get, and raw material sources are not limited to yet.
3, extraction process simple, extract and fully, do not destroy effective constituent, and have easy handling, the simple advantage of aftertreatment, be beneficial to produce and transform.
4, the waste residue of Ti Quing, the method for employing aggregated compaction adds food grade glue, is processed into disposable product, and whole process does not have waste material.
5, the present invention combines Pericarppium arachidis hypogaeae and cigarette first, adopt the Pericarppium arachidis hypogaeae extract of method of the present invention preparation good, noresidue, the obvious soft flue gas of energy, enrich cigarette perfume (or spice) with the fragrant Harmony of cigarette, applied range can directly feed in raw material and use and use in the perfume formulation.
6, the extract that adopts method preparation of the present invention is as tobacco aromatics using, stability is strong, overcome extract that the common solvent refluxing extraction obtains to cigarette bring residual, can obviously reduce stimulation, the oral cavity pleasant impression is clean.
7, the present invention has prepared a kind of spices that can comprehensively promote the cigarette quality, and is natural harmless, and with low cost, opened up the new way of preparation tobacco aromatics using.
Description of drawings
Accompanying drawing 2 is that gas phase-GC-MS is analyzed Pericarppium arachidis hypogaeae extract split product total ion current figure;
Accompanying drawing 3 is flavones content stability superpotential figure in the Pericarppium arachidis hypogaeae extract.
Embodiment
Below in conjunction with accompanying drawing the specific embodiment of the present invention and relevant technologies problem are described in further detail.The present invention is achieved through the following technical measures:
At first the ethanolic soln of usefulness 50-95% is used the effective constituent in the ultrasonic extraction Pericarppium arachidis hypogaeae under room temperature or heating condition, extraction time is 0.5-3 hour, extracting solution is concentrated into the 1/3-1/8 of its original volume, put into 0 ℃ to-5 ℃ refrigeration of refrigerator, elimination insolubles (mainly being wax and robust fibre) is clarified, transparent brown liquid is the Pericarppium arachidis hypogaeae extract.Directly be added on extract in the cigarette again or be used in the perfume formulation, the result shows that the Pericarppium arachidis hypogaeae extract has tangible fine and smooth cigarette perfume (or spice), soft flue gas, covers the effect of assorted gas.The applicant analyzes the split product of extract and extract, and the extract main active ingredient is a Flavonoid substances, mainly is the heterocyclic flavor matter after the cracking.The results are shown in Figure 1 and Fig. 2.
Fig. 1 is the aroma component total ion current figure that adopts in gas phase-GC-MS analysis Pericarppium arachidis hypogaeae extract; Adopt the method for dichloromethane extraction to carry out pre-treatment to the Pericarppium arachidis hypogaeae extract.
GC-MS analysis condition: GC conditions: chromatographic column: 30m * 0.25mm * 0.25 μ mVF-5 post; Carrier gas: helium; Column temperature: temperature programming, 40 ℃-260 ℃, 10 ℃/min of temperature rise rate, constant temperature 10min; 220 ℃ of injector temperatures; Split stream sampling, splitting ratio are 10: 1.
The mass spectrum condition: ionization mode EI, transmitter current 150 μ A, detector voltage 350V, 250 ℃ of ion source temperatures, 250 ℃ of transmission line temperature, electron energy 70eV, sweep limit 50-650 (relative atomic mass unit) diagramatic content sees Table 1 with the form display result.
Aroma component table in table 1, the Pericarppium arachidis hypogaeae extract
| Sequence number | Retention time | Title | SI | RSI | Matching degree (%) | Peak area per-cent (%) |
| 1 | 8.15 | Propylene glycol | 895 | 900 | 92.9 | 0.88 |
| 2 | 14.03 | Octanal | 847 | 850 | 83.3 | 0.98 |
| 3 | 14.85 | Trimethylammonium-2-furfuralcohol | 900 | 920 | 85.2 | 13.88 |
| 4 | 21.56 | 3-methoxyl group-d-glucose | 859 | 812 | 80.5 | 2.07 |
| 5 | 21.89 | The folium eucalypti enol | 849 | 888 | 83.2 | 7.20 |
| 6 | 22.53 | Eucalyptol | 793 | 905 | 75.6 | 23.41 |
| 7 | 26.40 | The n-palmitic acid | 752 | 732 | 77.3 | 4.01 |
| 8 | 30.43 | Quercitroside | 700 | 732 | 69.5 | 9.20 |
| 9 | 35.53 | Three heptadecyl alcohol | 860 | 810 | 82.1 | 2.10 |
| 10 | 38.58 | (Z, Z)-9,12 octadecadienoic acid | 786 | 898 | 79.8 | 0.58 |
| 11 | 39.54 | Stearic acid | 793 | 846 | 72.6 | 0.82 |
| 12 | 40.72 | Uniphat A60 | 735 | 879 | 68.2 | 2.55 |
| 13 | 41.91 | Meraneine | 775 | 888 | 75.4 | 3.03 |
| 14 | 45.88 | The Herba Astragali Melilotoidis (Herba Astragali Sinici) glycosides | 798 | 802 | 78.6 | 3.15 |
Accompanying drawing 2 is gas phase-GC-MS branch Pericarppium arachidis hypogaeae extract split product total ion current figure that extract; Diagram is the result show as table 2 with form.
Table 2, Pericarppium arachidis hypogaeae extract split product component list
| Sequence number | Retention time | Title | SI | RSI | Matching degree (%) | Peak area per-cent (%) |
| 1 | 4.31 | Propylene glycol | 821 | 816 | 86.9 | 0.48 |
| 2 | 7.59 | 1-(2-carboxyl-4,4-diformazan basic ring | 815 | 812 | 83.3 | 0.99 |
| Butenyl)-1-butylene-3 |
||||||
| 3 | 9.79 | Myrcene | 799 | 785 | 75.2 | 3.02 |
| 4 | 15.05 | Trimethylammonium-2-furfuralcohol | 843 | 812 | 85.5 | 0.91 |
| 5 | 15.52 | The folium eucalypti enol | 892 | 865 | 83.2 | 0.80 |
| 6 | 20.61 | Furfural | 905 | 905 | 95.6 | 8.32 |
| 7 | 30.8 | Eucalyptol | 721 | 732 | 75.3 | 4.99 |
| 8 | 32.42 | 2,3-dihydro-3,5-dihydroxyl-6-methyl-4H-pyrans-4-ketone | 785 | 702 | 62.5 | 6.20 |
| 9 | 37.56 | 1-(2,6,6-trimethylammonium-1,3-cyclohexadiene) 2-butylene-1-ketone | 895 | 900 | 82.1 | 1.98 |
| 10 | 37.92 | Duryl aldehyde | 847 | 917 | 79.8 | 2.54 |
| 11 | 39.37 | Phantol | 793 | 846 | 79.6 | 2.99 |
| 12 | 39.95 | Linalool oxide | 654 | 754 | 66.2 | 10.22 |
| 13 | 40.06 | 1-oxyethyl group pentanone | 859 | 888 | 81.4 | 10.35 |
| 14 | 41.03 | 1-hexanaphthene-1-alkynes-1-phenylethyl alcohol | 786 | 791 | 80.6 | 4.28 |
| 15 | 44.21 | Methyl palmitate | 855 | 731 | 70.1 | 3.35 |
| 16 | 44.44 | Tetrahydrochysene-trimethylammonium benzo furanone | 853 | 823 | 75.9 | 12.14 |
| 17 | 44.96 | Pentadecylic acid | 799 | 716 | 72.8 | 6.35 |
| 18 | 45.84 | Margaric acid | 890 | 713 | 70.3 | 3.26 |
Accompanying drawing 3 is that general flavone content changes superpotential in the extract.This is the result that the applicant carries out the stability test of extract.In the prior art, common fault of ubiquity when the natural plant extracts of employing solvent extraction is used in cigarette, some extract is after placing for some time, and effective function can weaken, or occur stimulating shortcomings such as increase, residual increase, give the unsettled sensation of quality.In order to verify the stability of Pericarppium arachidis hypogaeae extract, we are measurement index with the general flavone content, the extract room temperature was placed 60 days, every sampling in 7 days once, with general flavone content in the determined by ultraviolet spectrophotometry extract; And prepare cigarette with perfuming commonly used and reinforced experimental technique and smoke panel test, smoking result shows the effect that the Pericarppium arachidis hypogaeae extract has soft flue gas, fine and smooth cigarette perfume (or spice), Hui Tian to promote the production of body fluid in cigarette, very stable, does not change over time.
Pericarppium arachidis hypogaeae extract of the present invention has two purposes in cigarette, and the one, direct perfuming uses; The 2nd, can use in the perfume formulation.
The perfuming experiment: the ratio that accounts for pipe tobacco weight 1 ‰ in extract is added in the pipe tobacco, put the baking of 50 ℃ in baking oven after 30 minutes, 22 ± 1 ℃ of temperature, humidity is balance 2 hours under 60 ± 1% environment, roll into cigarette then and prop up, do contrast with the blank cigarette that does not add extract and smoke panel test.
Being applied in the perfume formulation reinforced experiment: essence 1008 be with flavouring, to improve the flue gas fullness ratio be the perfume formulation of target design, though the flavouring effect is arranged, slightly puckery sense and residual is added the Pericarppium arachidis hypogaeae extract in 0.5% ratio in 1008 prescriptions, after stirring, do reinforced experiment.The ratio that accounts for pipe tobacco weight 1 ‰ in essence 1008 is added in the pipe tobacco, and 80 ℃ of sealings are after 30 minutes, and 22 ± 1 ℃ of temperature, humidity is balance 2 hours under 60 ± 1% environment, rolls into cigarette then and props up, and does contrast with the cigarette that adds essence 1008 and smokes panel test.
Form the group of smokeing panel test by 7 people, the national level Shi Yiming that smokes panel test wherein, two of provincial teacher of the smokeing panel test.Smoking result shows, the Pericarppium arachidis hypogaeae extract can soft flue gas and is applicable in the cigarette of different class, is a kind of tobacco aromatics using of novel excellence.
Table 3. smoking result table
Smoking result shows the effect that the Pericarppium arachidis hypogaeae extract has soft flue gas, fine and smooth cigarette perfume (or spice), Hui Tian to promote the production of body fluid in cigarette, and is applicable in the cigarette of different class.
The present invention also is that the Pericarppium arachidis hypogaeae filter residue utilizes with the extract waste residue, because the Pericarppium arachidis hypogaeae filter residue is by the extraction using alcohol mistake, ethanol accounts for 20～40% of extract waste residue material, only need dryness in the sun, volatilize ethanol and get final product, because by the extraction using alcohol mistake, it is soft that powder becomes, and is easy to very much processing; The adding ductile adhesive is put into stirrer and is stirred to the single-size shape in the Pericarppium arachidis hypogaeae filter residue; To become the Pericarppium arachidis hypogaeae filter residue of single-size shape quantitatively to be transported to the die cavity of shaper more, compression moulding behind vibration 10-30 second, the uniform distribution, the unit pressure of compacting is 250-450kg/cm
2, temperature is 140～200 ℃, keeps under this temperature and pressure 30～80 seconds; Utilize ozone to carry out disinfection after the demoulding.In addition, can also utilize surface treatment agent and tap water after on the existing installation of the sector moulding product being done surface treatment, to be finished product.
The advantage that the Pericarppium arachidis hypogaeae filter residue utilizes is:
(1), the waste residue after utilize extracting further processes, not only cost is low, the soft easy processing of powder, has also solved the waste disposal problem of extract;
(2), used binding agent and the surface treatment agent of the present invention be safe and harmless material, so the disposable product safety that obtains, pollution-free, can degrade fully under field conditions (factors);
(3), complete processing is simple, practical.
Several embodiment are described below.
Get 500 gram Pericarppium arachidis hypogaeaes, be crushed to powdery, the ethanol with 70% is carrying out ultrasonic extraction, extracted 2 hours, extracting solution is concentrated into 1/5 of original volume in Rotary Evaporators, filters, filtrate is filtered after 0 ℃ of refrigeration one week of sedimentation once more, obtains clear filtrate and is the Pericarppium arachidis hypogaeae extract.
This extracting solution is added in the cigarette by 1 ‰.
The Pericarppium arachidis hypogaeae filter residue 11kg that concentrate multiple extraction back, air-dry back is 9.4kg, hung 2 hours in the ventilation, the solution of 0.6kg ductile adhesive (sodium alginate) with pure water furnishing 25% is added in the Pericarppium arachidis hypogaeae filter residue, putting into stirrer together stirs, rotating speed is 800 commentaries on classics/min, stir 5min, make to be the single-size shape, get 50g by quantitative disk and be transported to die cavity, vibrated for 10 seconds, compression moulding behind the uniform distribution, the unit pressure of compacting is 250kg/cm2, and temperature is 150 ℃, keeps 60 seconds under this temperature and pressure, release then, the demoulding carries out disinfection with ozone.It is that 20% solution is sent into surface treatment chamber by paint feeding system that the 0.1kg surface treatment agent is diluted with water to concentration, makes moulding product surface form even, the fine and close Elastic Film of one deck.
Embodiment 2
Get 500 gram Pericarppium arachidis hypogaeaes, be crushed to powdery, the ethanol with 75% extracted 1 hour under the ultrasonic wave condition, and extracting solution is concentrated into 1/6 of original volume in Rotary Evaporators, filtration, and filtrate low temperature-2 ℃ is deposited filtration once more after three days, promptly gets the Pericarppium arachidis hypogaeae extract.
This Pericarppium arachidis hypogaeae extract is used for cigarette carries out perfuming.
The Pericarppium arachidis hypogaeae filter residue 10.7kg that concentrate multiple extraction back, air-dry back is 9.1kg, hung 2 hours in the ventilation, the solution of 0.8kg ductile adhesive (sodium alginate) with pure water furnishing 40% is added in the Pericarppium arachidis hypogaeae slag, putting into stirrer together stirs, rotating speed is 800 commentaries on classics/min, stir 5min, make to be the single-size shape, get 50g by quantitative disk and be transported to die cavity, vibrated for 10 seconds, compression moulding behind the uniform distribution, the unit pressure of compacting is 300kg/cm2, and temperature is 180 ℃, keeps 60 seconds under this temperature and pressure, release then, the demoulding carries out disinfection with ozone.It is that 20% solution is sent into surface treatment chamber by paint feeding system that the 0.1kg surface treatment agent is diluted with water to concentration, makes moulding product surface form even, the fine and close Elastic Film of one deck.
Get 500 gram Pericarppium arachidis hypogaeaes, directly under the ultrasonic wave condition, extracted 1 hour with 70% ethanol, extracting solution is concentrated into 1/4 of original volume in Rotary Evaporators, filter, filtrate is put refrigerator-5 ℃ sedimentation and is taken out after one day, filter once more, promptly get the Pericarppium arachidis hypogaeae extract, this Pericarppium arachidis hypogaeae extract is used for cigarette carries out perfuming.
The Pericarppium arachidis hypogaeae filter residue 11kg that concentrate multiple extraction back, hung 2 hours in the ventilation, the solution of 0.6kg ductile adhesive (sodium alginate) with pure water furnishing 25% is added in the Pericarppium arachidis hypogaeae slag, put into stirrer together and stir, rotating speed is 800 commentaries on classics/min, stir 5min, make to be the single-size shape, get 50g by quantitative disk and be transported to die cavity, vibrate compression moulding behind 10 seconds, the uniform distribution, the unit pressure of compacting is 400kg/cm2, and temperature is 120 ℃, keeps 60 seconds under this temperature and pressure.Release then, the demoulding carry out disinfection with ozone.It is that 20% solution is sent into surface treatment chamber by paint feeding system that the 0.1kg surface treatment agent is diluted with water to concentration, makes moulding product surface form even, the fine and close Elastic Film of one deck.
Claims (10)
1, a kind of method of comprehensive utilization of Pericarppium arachidis hypogaeae is characterized in that described method of comprehensive utilization carries out according to the following steps:
(1) with ultrasonic extraction the effective constituent in the Pericarppium arachidis hypogaeae is extracted earlier, filtering gained filtrate is first extract, and the Pericarppium arachidis hypogaeae filter residue is left subsequent step and uses;
(2) first extract is concentrated into the 1/3-1/8 of its original volume, places 0 ℃ to-5 ℃ to locate to refrigerate 1-7 days, filter the throw out of removing wherein, the Pericarppium arachidis hypogaeae extracting solution that obtains is clarifying sorrel liquid;
(3) the Pericarppium arachidis hypogaeae extracting solution is used for the direct perfuming of cigarette or be used for cigarette perfume formulation;
(4) with the Pericarppium arachidis hypogaeae filter residue dryness in the sun of step (1), add the toughness binding agent, stir and be single-size shape material;
(5) above-mentioned single-size shape material Pericarppium arachidis hypogaeae filter residue is sent into shaper and be shaped to food container or tableware;
(6) in type food container or tableware are carried out air-dry, sterilization.
2, the method for comprehensive utilization of a kind of Pericarppium arachidis hypogaeae according to claim 1 is characterized in that: the step of the described ultrasonic extraction of step (1) is:
1) Pericarppium arachidis hypogaeae is broken into powdered, crosses 80 mesh sieves;
2) with the Pericarppium arachidis hypogaeae powder: the ratio of ethanol=1: 3-7 places container, soaks 1-3 hour;
3) the above-mentioned material after will soaking is put into the ultrasonic wave container and is carried out ultrasonic extraction, and ultrasonic frequency 45-65Hz extracted 30-180 minute; Filtration obtains extract just.
3, the method for comprehensive utilization of a kind of Pericarppium arachidis hypogaeae according to claim 2 is characterized in that: described ethanol is 50～95% ethanol.
4, the method for comprehensive utilization of a kind of Pericarppium arachidis hypogaeae according to claim 1 and 2 is characterized in that: step (1) or 3) the described ultrasonic extraction of carrying out is an extract at room temperature or extract down at 40 ℃-50 ℃.
5, the method for comprehensive utilization of a kind of Pericarppium arachidis hypogaeae according to claim 1 is characterized in that: the described toughness binding agent of step (4) is the food grade sodium alginate of safety non-toxic.
6, a kind of method of comprehensive utilization of Pericarppium arachidis hypogaeae according to claim 1 or 5, it is characterized in that: described toughness binding agent, its add-on are the 5-15% of Pericarppium arachidis hypogaeae filter residue gross weight.
7, the method for comprehensive utilization of a kind of Pericarppium arachidis hypogaeae according to claim 1 is characterized in that: step (3) is described when the Pericarppium arachidis hypogaeae extracting solution is used for direct perfuming, and the ratio that extracting solution accounts for pipe tobacco weight is 1 ‰-5 ‰.
8, the method for comprehensive utilization of a kind of Pericarppium arachidis hypogaeae according to claim 1 is characterized in that: step (3) is described when the Pericarppium arachidis hypogaeae extracting solution is used for perfume formulation, and the ratio that extracting solution accounts for the perfume formulation gross weight is 0.5%-3%.
9, the method for comprehensive utilization of a kind of Pericarppium arachidis hypogaeae according to claim 1 is characterized in that: the described Pericarppium arachidis hypogaeae filter residue of step (4) dryness in the sun, dried moisture content is 5-15%.
10, the method for comprehensive utilization of a kind of Pericarppium arachidis hypogaeae according to claim 1, it is characterized in that: the described shaper moulding of step (5), it is the die cavity that the single-size shape amount of anticipating is transported to shaper, compression moulding behind vibration 10-30 second, the uniform distribution, the unit pressure of compacting is 250-450kg/cm
2, temperature is 140～200 ℃, keeps under this temperature and pressure 30～80 seconds.
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