CN110495632A - A kind of preparation method and application of cigarette celery oil resin - Google Patents
A kind of preparation method and application of cigarette celery oil resin Download PDFInfo
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- CN110495632A CN110495632A CN201910909301.9A CN201910909301A CN110495632A CN 110495632 A CN110495632 A CN 110495632A CN 201910909301 A CN201910909301 A CN 201910909301A CN 110495632 A CN110495632 A CN 110495632A
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- celery
- cigarette
- oil resin
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- 235000015849 Apium graveolens Dulce Group Nutrition 0.000 title claims abstract description 40
- 235000010591 Appio Nutrition 0.000 title claims abstract description 40
- 239000011347 resin Substances 0.000 title claims abstract description 30
- 229920005989 resin Polymers 0.000 title claims abstract description 30
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 24
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 244000101724 Apium graveolens Dulce Group Species 0.000 title 1
- 240000007087 Apium graveolens Species 0.000 claims abstract description 39
- 239000001387 apium graveolens Substances 0.000 claims abstract description 30
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 20
- 239000000706 filtrate Substances 0.000 claims abstract description 16
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 11
- 235000019441 ethanol Nutrition 0.000 claims abstract description 8
- 238000004140 cleaning Methods 0.000 claims abstract description 6
- 239000012535 impurity Substances 0.000 claims abstract description 6
- 239000000843 powder Substances 0.000 claims abstract description 6
- 230000008961 swelling Effects 0.000 claims abstract description 6
- 239000000284 extract Substances 0.000 claims abstract description 4
- 239000003921 oil Substances 0.000 claims description 34
- 235000019198 oils Nutrition 0.000 claims description 34
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 15
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 12
- OCWLYWIFNDCWRZ-UHFFFAOYSA-N Methyl (S)-2-Methylbutanoate Chemical compound CCC(C)C(=O)OC OCWLYWIFNDCWRZ-UHFFFAOYSA-N 0.000 claims description 10
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 10
- 238000002156 mixing Methods 0.000 claims description 8
- 238000005119 centrifugation Methods 0.000 claims description 7
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 claims description 5
- NPFVOOAXDOBMCE-PLNGDYQASA-N (3Z)-hex-3-en-1-yl acetate Chemical compound CC\C=C/CCOC(C)=O NPFVOOAXDOBMCE-PLNGDYQASA-N 0.000 claims description 5
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 claims description 5
- UFLHIIWVXFIJGU-ARJAWSKDSA-N (Z)-hex-3-en-1-ol Chemical compound CC\C=C/CCO UFLHIIWVXFIJGU-ARJAWSKDSA-N 0.000 claims description 5
- 241000219000 Populus Species 0.000 claims description 5
- 235000021028 berry Nutrition 0.000 claims description 5
- 239000001072 coriandrum sativum l. fruit oil Substances 0.000 claims description 5
- 229930007744 linalool Natural products 0.000 claims description 5
- POIARNZEYGURDG-FNORWQNLSA-N beta-damascenone Chemical compound C\C=C\C(=O)C1=C(C)C=CCC1(C)C POIARNZEYGURDG-FNORWQNLSA-N 0.000 claims description 3
- 229930007850 β-damascenone Natural products 0.000 claims description 3
- 230000008719 thickening Effects 0.000 claims description 2
- 244000061176 Nicotiana tabacum Species 0.000 claims 2
- 125000002485 formyl group Chemical class [H]C(*)=O 0.000 claims 1
- 241000208125 Nicotiana Species 0.000 abstract description 18
- 239000003205 fragrance Substances 0.000 abstract description 14
- 238000000034 method Methods 0.000 abstract description 8
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract description 6
- 239000003546 flue gas Substances 0.000 abstract description 6
- 239000000463 material Substances 0.000 abstract description 5
- 238000002137 ultrasound extraction Methods 0.000 abstract description 5
- 230000000638 stimulation Effects 0.000 abstract description 4
- 238000000605 extraction Methods 0.000 abstract description 3
- 235000016709 nutrition Nutrition 0.000 abstract description 2
- 230000035764 nutrition Effects 0.000 abstract description 2
- 239000008601 oleoresin Substances 0.000 description 7
- 239000002904 solvent Substances 0.000 description 6
- 239000000341 volatile oil Substances 0.000 description 6
- 150000001299 aldehydes Chemical class 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 238000002604 ultrasonography Methods 0.000 description 4
- 244000147058 Derris elliptica Species 0.000 description 3
- 230000008859 change Effects 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000001914 filtration Methods 0.000 description 3
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 238000010298 pulverizing process Methods 0.000 description 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 2
- 208000024756 faint Diseases 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 150000002561 ketenes Chemical class 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 239000002304 perfume Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 206010042772 syncope Diseases 0.000 description 2
- 241000208173 Apiaceae Species 0.000 description 1
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 240000008881 Oenanthe javanica Species 0.000 description 1
- 235000000365 Oenanthe javanica Nutrition 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 235000013559 Schnittsellerie Nutrition 0.000 description 1
- 241000238370 Sepia Species 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 238000007792 addition Methods 0.000 description 1
- DTOSIQBPPRVQHS-PDBXOOCHSA-N alpha-linolenic acid Chemical compound CC\C=C/C\C=C/C\C=C/CCCCCCCC(O)=O DTOSIQBPPRVQHS-PDBXOOCHSA-N 0.000 description 1
- 235000020661 alpha-linolenic acid Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910052796 boron Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000010642 eucalyptus oil Substances 0.000 description 1
- 229940044949 eucalyptus oil Drugs 0.000 description 1
- 235000019197 fats Nutrition 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002213 flavones Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- 230000008676 import Effects 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 150000002596 lactones Chemical class 0.000 description 1
- 229960004488 linolenic acid Drugs 0.000 description 1
- KQQKGWQCNNTQJW-UHFFFAOYSA-N linolenic acid Natural products CC=CCCC=CCC=CCCCCCCCC(O)=O KQQKGWQCNNTQJW-UHFFFAOYSA-N 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- -1 methoxyl group Chemical group 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/20—Biochemical treatment
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
- A24B15/303—Plant extracts other than tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/305—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances of undetermined constitution characterised by their preparation
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Agronomy & Crop Science (AREA)
- Botany (AREA)
- Biochemistry (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention relates to tobacco aromaticss technical field more particularly to a kind of preparation method and applications of cigarette celery oil resin.The preparation method of this cigarette celery oil resin, comprising the following steps: (1) by celery seed cleaning, removal of impurities；(2) it is crushed after celery seed being carried out high pressure swelling processing；(3) obtained celery seed powder is mixed, and under the conditions of 40-45 DEG C of temperature with ethyl alcohol, extracts 40-50min, is then centrifuged for, collect filtrate.The present invention uses the extracting method of pure physics, expanding treatment realizes the crushing to celery seed, the cell interior of the deep enough material of ultrasonic extraction energy, so that effective component extraction rate be greatly improved, remain the nutrition and fragrance of celery seed itself, and less pollution.Meanwhile celery oil resin produced by the present invention being used in pipe tobacco, flue gas can be made more soft, reduce suction stimulation.
Description
Technical field
The present invention relates to the preparation method of tobacco aromaticss technical field more particularly to a kind of cigarette celery oil resin and answer
With.
Background technique
Currently, the tobacco aromaticss of China's cigarettes plus, generally use two major classes: one kind is natural extraction fragrance, utilizes day
The natural component coordinated with flue gas contain in right fragrance or potential；Another kind of is exactly synthetic perfume, using synthesis and cigarette
Gas is coordinated, and has the perfume monomer of certain effect to flue gas.This two major classes fragrance is independent or deploys manufactured tobacco aromaticss, although work
Skill is simple, but there are fragrance dullness, stimulation, the single problem of the effect to flue gas.Research of the China on tobacco aromaticss is always
Relatively backward, most fragrance rely on import, and therefore, exploitation can make the soft exquisiteness of flue gas, and the cigarette that can reduce stimulation is used
Fragrance is necessary.
Celery is divided into Chinese celery and celery, is the full name of umbelliferae, belongs to food and medicament dual-purpose plant.Celery seed is derived from celery
In the slight flower of dish, thus the bodily form of seed is also very small, and in oval, color is mostly sepia or dark-brown, contains eucalyptus oil
Alcohol, phosphorus methoxyl group phenol, umbrella flower lactone, apiolin, linolenic acid, volatility grease, flavones, boron, minerals such as: calcium, magnesium, sodium, zinc.
Celery seed essential oil have pleasant enhanced aroma, taste micro-pungent and it is bitter, can be widely used for food, blending etc..The tune of celery seed
Taste, health care and blending effect all with its fragrance ingredient close relation.
Oleoresin is a kind of important fragrance very widely used at present, is from raw material that it is fragrant using solvent appropriate
Taste and taste ingredient extract, then solvent is distilled to recover, and are finally made sticky, color is slightly deep, the tree containing essential oil
Lipid product.Oleoresin baseset has suffered the effective component including essential oil in raw material, and fragrance and taste compare balance, and
And than more complete.Compared to essential oil class product, oleoresin does not also have containing essential oil not only containing the volatile component of essential oil
Standby flavor component, although fragrance is slightly weaker, fragrance is richer.Oleoresin in storage because active constituent by fat surround and
Containing natural, keep its oxidation deterioration chance few.
Therefore how effectively to extract celery seed and obtain oleoresin product is current urgent problem.
Summary of the invention
The invention solves the above problems, provide a kind of preparation method and application of cigarette celery oil resin.
The technical solution that the present invention solves the problems, such as is to provide a kind of preparation method of cigarette celery oil resin, including with
Lower step:
(1) by celery seed cleaning, removal of impurities；
(2) it is crushed after celery seed being carried out high pressure swelling processing；
(3) obtained celery seed powder is mixed, and under the conditions of 40-45 DEG C of temperature with ethyl alcohol, extracts 40-50min, then
Filtrate is collected in centrifugation.
Preferably, further include step (4), by filtrate under the conditions of cryogenic vacuum, be concentrated into the 1/8-1/6 of original volume, obtain
To celery oil resin paste.
Preferably, before concentration, filtrate is filtered again.
Preferably, in step (2), the expanding treatment 10- under conditions of temperature is 35-40 DEG C, pressure is 3-10Mpa
15min。
Preferably, in step (2), it is crushed to 60-100 mesh.
Preferably, it in step (3), is extracted using hypervelocity.
Preferably, in step (3), under conditions of centrifugal rotational speed is 800-1000r/min, centrifugation power is 150-200W
It is centrifuged 10-15min.
Preferably, in step (4), thickening temperature is 40-50 DEG C.
It is a further object to provide a kind of applications of celery oil resin of cigarette, according to mass parts, by celery
7.3-7.5 parts and ethyl acetate 0.2-0.3 parts of seed oleoresin, 0.2-0.3 parts of methyl 2-methylbutyrate, 0.5-0.6 parts of poplar certain kind of berries aldehyde,
0.6-0.7 parts of Leaf Acetate, 0.6-0.7 parts of 1wt% Damascenone, 0.02-0.03 parts of oil of badian, leaf-alcohol 0.5-0.6
Part, 0.3-0.5 parts of coriander seed oil, 0.5-0.7 parts of linalool, 88.70-89.50 parts of propylene glycol mixing, obtained mixture is added
In pipe tobacco.
Preferably, mixture accounts for the 1-100ppm of pipe tobacco weight.
Beneficial effects of the present invention:
1. expanding treatment realizes the crushing to celery seed using the extracting method of pure physics, ultrasonic extraction can deep enough object
The cell interior of material, is greatly improved effective component extraction rate, and less pollution.
2, the extracting method of celery seed can carry out under the conditions of relatively mild in the application, to avoid effective component broken
It is bad, to retain the nutrition and fragrance of celery seed itself to the maximum extent.
3, it is extracted in the application using alcohol solvent, avoids the use of organic solvent, to avoid organic solvent
Oleoresin product is polluted.
4. passing through the mixing match of various other combinations and celery oil resin, enable to be used in pipe tobacco, not only not
The original natural fragrance of celery oil resin can be lost, and enables to flue gas more soft, reduces suction stimulation.
Specific embodiment
It is a specific embodiment of the invention below, and technical scheme of the present invention will be further described, but this hair
It is bright to be not limited to these examples.
Embodiment 1
A kind of cigarette preparation method of celery oil resin, its step are as follows:
(1) by celery seed cleaning, removal of impurities.
(2) clean celery seed is put into pressure vessel, setting bulking pressure is 3Mpa, and swelling temperature is 35 DEG C, swollen
Change 10 min of processing.
(3) then by the celery seed pulverization process after extruding to 60 mesh.
(4) obtained celery seed powder is placed in Vltrasonic device, alcohol solvent, solid-liquid ratio 1:6 is added.Ultrasonic function is set
Rate 200W, under the conditions of 40 DEG C of temperature, ultrasonic extraction 40min.
(5) material after ultrasound is centrifuged, centrifugal rotational speed 800r/min is set, be centrifuged power 150W, centrifugation time
10min collects filtrate.
(6) after filtering again using the filtrate that Buchner funnel obtains, obtained secondary filtrate is placed in cryogenic vacuum concentration
To the 1/8 of original volume, the pure paste celery oil naval stores of quality is obtained.
Obtained celery oil resin can be applied in pipe tobacco, concrete operations are as follows: according to mass parts, by celery oil tree
7.3 parts and 0.2 part of ethyl acetate of rouge, 0.2 part of methyl 2-methylbutyrate, 0.5 part of poplar certain kind of berries aldehyde, 0.6 part of Leaf Acetate, 1wt% is prominent
It faints 0.6 part of ketenes, 0.02 part of oil of badian, 0.5 part of leaf-alcohol, 0.3 part of coriander seed oil, 0.5 part of linalool, propylene glycol 88.70
Part mixing, obtained mixture is added in pipe tobacco, and mixture accounts for the 1ppm of pipe tobacco weight.
Embodiment 2
A kind of cigarette preparation method of celery oil resin, its step are as follows:
(1) by celery seed cleaning, removal of impurities.
(2) clean celery seed is put into pressure vessel, setting bulking pressure is 10Mpa, and swelling temperature is 40 DEG C, swollen
Change 15 min of processing.
(3) then by the celery seed pulverization process after extruding to 100 mesh.
(4) obtained celery seed powder is placed in Vltrasonic device, alcohol solvent, solid-liquid ratio 1:10 is added.Setting ultrasound
Power 250W, under the conditions of 50 DEG C of temperature, ultrasonic extraction 50min.
(5) material after ultrasound is centrifuged, centrifugal rotational speed 1000r/min is set, be centrifuged power 200W, centrifugation time
15min collects filtrate.
(6) after filtering again using the filtrate that Buchner funnel obtains, obtained secondary filtrate is placed in cryogenic vacuum concentration
To the 1/6 of original volume, the pure paste celery oil naval stores of quality is obtained.
Obtained celery oil resin can be applied in pipe tobacco, concrete operations are as follows: according to mass parts, by celery oil tree
7.5 parts and 0.3 part of ethyl acetate of rouge, 0.3 part of methyl 2-methylbutyrate, 0.6 part of poplar certain kind of berries aldehyde, 0.7 part of Leaf Acetate, 1wt% is prominent
It faints 0.7 part of ketenes, 0.03 part of oil of badian, 0.6 part of leaf-alcohol, 0.5 part of coriander seed oil, 0.7 part of linalool, propylene glycol 89.50
Part mixing, obtained mixture is added in pipe tobacco, and mixture accounts for the 100ppm of pipe tobacco weight.
Embodiment 3
A kind of cigarette preparation method of celery oil resin, its step are as follows:
(1) by celery seed cleaning, removal of impurities.
(2) clean celery seed is put into pressure vessel, setting bulking pressure is 8Mpa, and swelling temperature is 38 DEG C, swollen
Change 12 min of processing.
(3) then by the celery seed pulverization process after extruding to 80 mesh.
(4) obtained celery seed powder is placed in Vltrasonic device, alcohol solvent, solid-liquid ratio 1:8 is added.Ultrasonic function is set
Rate 230W, under the conditions of 45 DEG C of temperature, ultrasonic extraction 45min.
(5) material after ultrasound is centrifuged, centrifugal rotational speed 900r/min is set, be centrifuged power 170W, centrifugation time
13min collects filtrate.
(6) after filtering again using the filtrate that Buchner funnel obtains, obtained secondary filtrate is placed in cryogenic vacuum concentration
To the 1/7 of original volume, the pure paste celery oil naval stores of quality is obtained.
Obtained celery oil resin can be applied in pipe tobacco, concrete operations are as follows: according to mass parts, by celery oil tree
7.4 parts and 0.25 part of ethyl acetate of rouge, 0.25 part of methyl 2-methylbutyrate, 0.55 part of poplar certain kind of berries aldehyde, 0.65 part of Leaf Acetate,
0.65 part of 1wt% Damascenone, 0.025 part of oil of badian, 0.55 part of leaf-alcohol, 0.4 part of coriander seed oil, 0.6 part of linalool, third
89 parts of glycol mixing, obtained mixture is added in pipe tobacco, and mixture accounts for the 50ppm of pipe tobacco weight.
Specific embodiment described herein is only an example for the spirit of the invention.The neck of technology belonging to the present invention
The technical staff in domain can make various modifications or additions to the described embodiments or replace by a similar method
In generation, however, it does not deviate from the spirit of the invention or beyond the scope of the appended claims.
Claims (10)
1. a kind of cigarette preparation method of celery oil resin, it is characterised in that: the following steps are included:
(1) by celery seed cleaning, removal of impurities；
(2) it is crushed after celery seed being carried out high pressure swelling processing；
(3) obtained celery seed powder is mixed, and under the conditions of 40-45 DEG C of temperature with ethyl alcohol, extracts 40-50min, then
Filtrate is collected in centrifugation.
2. a kind of preparation method of cigarette celery oil resin according to claim 1, it is characterised in that: further include step
(4), by filtrate under the conditions of cryogenic vacuum, it is concentrated into the 1/8-1/6 of original volume, obtains celery oil resin paste.
3. a kind of preparation method of cigarette celery oil resin according to claim 2, it is characterised in that: before concentration,
Filtrate is filtered again.
4. a kind of preparation method of cigarette celery oil resin according to claim 1, it is characterised in that: in step (2),
The expanding treatment 10-15min under conditions of temperature is 35-40 DEG C, pressure is 3-10Mpa.
5. a kind of preparation method of cigarette celery oil resin according to claim 1, it is characterised in that: in step (2),
It is crushed to 60-100 mesh.
6. a kind of preparation method of cigarette celery oil resin according to claim 1, it is characterised in that: in step (3),
It is extracted using hypervelocity.
7. a kind of preparation method of cigarette celery oil resin according to claim 1, it is characterised in that: in step (3),
10-15min is centrifuged under conditions of centrifugal rotational speed is 800-1000r/min, centrifugation power is 150-200W.
8. a kind of preparation method of cigarette celery oil resin according to claim 2, it is characterised in that: in step (4),
Thickening temperature is 40-50 DEG C.
9. a kind of application of cigarette according to any one of claims 1 to 8 celery oil resin, it is characterised in that: according to
Mass parts, by 7.3-7.5 parts of celery oil resin and ethyl acetate 0.2-0.3 parts, 0.2-0.3 parts of methyl 2-methylbutyrate, poplar
0.5-0.6 parts of certain kind of berries aldehyde, 0.6-0.7 parts of Leaf Acetate, 0.6-0.7 parts of 1wt% Damascenone, oil of badian 0.02-0.03
Part, 0.5-0.6 parts of leaf-alcohol, 0.3-0.5 parts of coriander seed oil, 0.5-0.7 parts of linalool, 88.70-89.50 parts of propylene glycol mixing obtain
To mixture be added pipe tobacco in.
10. a kind of application of cigarette celery oil resin according to claim 9, it is characterised in that: mixture accounts for pipe tobacco
The 1-100ppm of weight.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910909301.9A CN110495632B (en) | 2019-09-25 | 2019-09-25 | Preparation method and application of celery seed oil resin for cigarettes |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910909301.9A CN110495632B (en) | 2019-09-25 | 2019-09-25 | Preparation method and application of celery seed oil resin for cigarettes |
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| CN114377044A (en) * | 2021-12-01 | 2022-04-22 | 山东省农业科学院 | Preparation method of celery seed extract |
| CN115211492A (en) * | 2022-06-07 | 2022-10-21 | 圣道生物技术(山东)有限公司 | Stress relieving medicine for resisting stress and promoting growth of livestock and poultry and preparation method and application thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114377044A (en) * | 2021-12-01 | 2022-04-22 | 山东省农业科学院 | Preparation method of celery seed extract |
| CN115211492A (en) * | 2022-06-07 | 2022-10-21 | 圣道生物技术(山东)有限公司 | Stress relieving medicine for resisting stress and promoting growth of livestock and poultry and preparation method and application thereof |
| CN115211492B (en) * | 2022-06-07 | 2024-04-19 | 圣道生物技术(山东)有限公司 | Stress-resistant growth-promoting stress-relieving medicine for livestock and poultry, and preparation method and application thereof |
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| CN110495632B (en) | 2021-09-17 |
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