CN101390658B - Cigarette composite tip containing plant saponin extract - Google Patents
Cigarette composite tip containing plant saponin extract Download PDFInfo
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- CN101390658B CN101390658B CN2008102335413A CN200810233541A CN101390658B CN 101390658 B CN101390658 B CN 101390658B CN 2008102335413 A CN2008102335413 A CN 2008102335413A CN 200810233541 A CN200810233541 A CN 200810233541A CN 101390658 B CN101390658 B CN 101390658B
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Abstract
The invention relates to plant material processing method and the application of the plant material in tobacco, particularly the application of saponin in tobacco, belonging to tobacco filter tip additive processing technique. The processing method makes use of saponin extracted from different plants and arranges the saponin in a proper carrier through technical treatment to make the saponin into modified adsorbent material grains. The modified adsorbent material grains are added into composite filter tips in an amount of 10-30mg per one filter tip and have the function of improving the quality of the cigarette and removing harmful components of the cigarette. With the advantages of cheap and easy material, low production cost, simple synthesizing technique, excellent performance and being suitable for industrial production, the saponin has strong market competitiveness and great popularization value and application value.
Description
Technical field
The present invention relates to plant material treating method and the application in tobacco, the particularly saponin application in tobacco thereof.Belong to tobacco mouth rod additive treating technology.
Background technology
Saponin is the complicated glycosides compound of a class, can generate persistent like soap lather shape thing during with water mixing jolting.It is very wide to distribute in plant kingdom, and many Chinese medicines for example genseng, pseudo-ginseng, the wind-weed, polygala root, Radix Glycyrrhizae, balloonflower root, radix bupleuri etc. all contain saponin(e.Saponin(e is made up of sapogenin and sugar, uronic acid or other organic acids.That forms saponin(e sugared common has D-glucose, L-rhamnose, D-galactolipin, L-arabinose, a L-wood sugar.Common uronic acid has glucuronic acid, galacturonic acid, these sugar or uronic acid often are combined into the compound sugar sugar chain earlier, then with the sapogenin molecule in C3-OH condensation mutually, or by two sugar chains respectively with the sapogenin molecule in OH condensation mutually on two diverse locations, in the sapogenin molecule-COOH also may be connected with sugar, forms the ester glycosidic bond.
Saponin(e is divided into two classes by the structure of sapogenin: 1. steroid saponin(e.Its sapogenin is the derivative of spirostan, how to be formed (as Dioscin) by 27 carbon atoms.This saponins is present in Liliaceae and the Dioscoreaceae plant more.2. triterpenoid saponin.Its sapogenin is the derivative of triterpene (seeing terpene), is made up of 30 carbon atoms mostly.Triterpenoid saponin is divided into tetracyclic triterpene and pentacyclic triterpene.This saponins is present in the plants such as Araliaceae and Umbelliferae more.
Saponin extensively is present in the plant, is the main active ingredient of many Chinese herbal medicines.The many Chinese medicine of saponin component such as effects that polygala root, balloonflower root etc. have expelling phlegm and arresting coughing of containing are arranged; Some saponin(e also has antibiotic valuable biologically active such as active or analgesic, calm, anticancer.Indivedual saponin(es have special physiologically active, can promote the biosynthesis of DNA and protein as ginsenoside, improve the immunocompetence of body.Glycyrrhizic acid has the effect that promotes cortex hormone of aadrenaline, and the effect of cough-relieving and treatment gastric ulcer is arranged.Genseng contains about 4 % of total saponin, is the mixture of saponin more than 12 kinds; It is about 6.4%～7.3% that American Ginseng contains total saponin, with the panaxoside structural similarity; Gynostemma pentaphylla contains total saponin 2%～4%, and tens kinds of isomers are arranged, and wherein also has several identical with the panaxoside structure; Rhodiola root contains total saponin 1%～2%.Source difference according to saponin is called panaxoside, gynosaponin etc. again.The pharmacological action of saponin:.
1. bidirectional modulation immunization;
2. anti-anoxic and antifatigue effect;
3. low-temperature resistance stress effect;
4. lipotropism matter oxidation;
5. to the effect of central nervous system;
6. anti-mutation effect.
Panaxoside is the main component of genseng.At present by science, advanced technology separation and the panaxoside made from extra care out, called after Ro, Ra1, Ra2, Rb1, Rb2, Rb3, Rc, Rd, Rf, Rg1, Rg2, Rg3, Rh1, Rh2, I, K, O-glaco, all form by glucoside unit and sugar, except that the glucoside unit of Ro is the oleanolic acid, other be protopanoxadiol and Protopanaxatriol.
Partial monosomy saponin in the panaxoside such as Rb1, Rb2, Rd, Rc, Re, Rg1, Rg2, Rh1 etc. can reduce interior free yl content to some extent.Panaxoside can delay the old and feeble and old memory impairment that takes place of reduction of nerve cell, and has the stabilising membrane structure and increase protein synthesis, can improve memory of elderly person power ability.
Saponin monomer Rg1 and Rb1 are the main components of nootropic effect in the genseng in the genseng.Pharmacological evaluation shows that panaxoside A and Rb1 all can promote young mouse body development, and facilitation mouse adult back diving tower method and darkness avoidance test memory procurement process, finds that with outstanding quantitative technique Rb1 and Rg1 can obviously increase mouse hippocampus CA3 district synapse cell number.This is the tectology basis that panaxoside promotes learning and memory.The nootropic effect of panaxoside is relevant with its raising nervous function.Panaxoside also has the activation Skin Cell except that having effects such as above-mentioned anti-ageing, antifatigue, enhancing memory, strengthen skin elasticity, reduces effects such as wrinkle.Can promote body immunity; and suppress the panaxoside Pd that cancer cell grows up and can protect cell membrane and prevent cell senescence, hemangiectasis brings high blood pressure down and blood sugar; it is synthetic to improve liver cell protein and DNA, significantly suppresses the saponin Ro that the ginsenoside Re of cervical cancer cell growth causes the people to get angry.
Be applied to by the saponin that will extract in the plant in the sorbing material such as active carbon, the sorbing material of preparation modification is applied in the cigarette filter and will will be with the better quality of material to enjoy and security to the smoker.The cigarette tipping filter tip is the effective means that improves the smoking property of cigarette security.Why filter tip cigarette can reduce the harmful substance in the flue gas, is because of its filter material can adsorb a part of T/N in the flue gas, thereby reaches the purpose of filtration.Along with becoming increasingly conspicuous of smoking and healthy contradiction, countries in the world are more and more paid attention to the exploitation of filter tip material and filter structures cigarette, and function of use mouth rod (all being different from the fine mouth rod of common vinegar on structure and material) will be the trend of tobacco business lowering harm and decreasing coking from now on.Wherein using more function mouth rod in the world is active carbon mouth rod.The general interpolation approach of handling is: select processing (quality of material is selected in assurance), pulverize (material is ground into fine particle), sieve (selecting satisfactory material).
Active carbon is as the additive of cigarette filter tip, and mainly there are two problems in the application in the Chinese style cigarette, and the one, active carbon is when effectively filtering the flue gas gaseous component, and " carbon " flavor to flue gas brings makes the smoker produce uncomfortable feeling; Secondly, active carbon causes environmental pollution easily in mouth rod processing and making process, pollute working environment and other auxiliary materials sometimes.
Along with the progress of material science, aspect filter tip material, made a large amount of developments at cigarette both at home and abroad, comprise various organic and inorganic material.But these materials are because self reason, or and flue gas inharmonious, or may bring new safety issue, be exactly the cost problem in addition.
Adopt the saponin that extracts in the natural plants,, can be applied in preferably and serve as sorbing material in the filter tip through being used in cigarette after certain PROCESS FOR TREATMENT with in the filter tip.At first since its from natural plants, and PROCESS FOR TREATMENT can not change its security; Secondly, absorbing material granules such as modified activated carbon can not pollute working environment and other auxiliary materials in the filter tip molding process.
Summary of the invention
Purpose of the present invention uses vegetable material as the cigarette filter tip additive at the defective of present cigarette filter tip additive and the vacancy of new material, adds in the cigarette filter tip, solves the versatility and the vacancy of cigarette filter tip additive.The saponin that utilization of the present invention is extracted from different vegetable materials is prepared into modified absorbing material granules by carrying after the PROCESS FOR TREATMENT in suitable carriers, be added in the composite filter tip, plays and improves the cigarette smoking quality, removes the purpose of harmful components.
The composite filter tip that contains modified absorbing material granules of the present invention is characterized in that described modified absorbing material granules is activated carbon granule, zeolite granular, cabo particle, charcoal fiber etc., preferably activated carbon granule.The preparation of modified absorbing material granules of the present invention, it is characterized in that saponin, comprise the saponin that extracts in genseng, pseudo-ginseng, the wind-weed, polygala root, Radix Glycyrrhizae, balloonflower root, the radix bupleuri, the sugar of forming saponin(e has D-glucose, L-rhamnose, D-galactolipin, L-arabinose, L-wood sugar etc., is applied on the sorbing material by certain operation.Described modified absorbing material granules preparation method is characterized in that saponin extract is dissolved in the water, sorbing material was soaked wherein 2-4 hour, and fully stir; Filter the back at 40-60 ℃ of following vacuum drying 24-48 hour.The described application of modified absorbing material granules in composite filter tip with adsorption function, it is characterized in that described modified absorbing material granules, its amount of adding in the composite filter tip to is that 10-30mg/ props up, and the binary composite filter tip is that 10-15mg/ props up, and the ternary composite filter tip is that 20-30mg/ props up.
Technical solution of the present invention is: utilize tobacco industry sorbing material commonly used, as a kind of in activated carbon granule, zeolite granular, cabo particle, the charcoal fiber etc., as activated carbon granule, select the particle of particle diameter between the 40-60 order for use; Select for use then natural extract saponin, comprise saponin, comprise the saponin that extracts in genseng, pseudo-ginseng, the wind-weed, polygala root, Radix Glycyrrhizae, balloonflower root, the radix bupleuri, the sugar of forming saponin(e has in D-glucose, L-rhamnose, D-galactolipin, L-arabinose, L-wood sugar or the like one or more, the saponin that extracts fully is dissolved in forms the aqueous solution in the water, the sorbing material that chooses is soaked wherein 2-4 hour then, adopt mechanical agitation fully to stir (unsuitable too fast) therebetween; After the filtration, with solid material 40-60 ℃ of following vacuum drying (vacuum degree control is at 10mm) 24-48 hour.Handle with the screening of 40～60 mesh sieves, make its fine particle that reaches the requirement size, so that it is added in the cigarette filter tip.The fine particle that reaches the requirement size is packed, for future use.The common active carbon of modified absorbing material granules being applied in composite filter tip uses identical, mainly is that its amount of adding in the composite filter tip to is that 10-30mg/ props up, and the binary composite filter tip is that 10-15mg/ props up, and the ternary composite filter tip is that 20-30mg/ props up.
The selected natural plant material of the present invention mainly is charcoal absorption material and saponin, still the activated carbon granule that is not limited to enumerate in the specification, zeolite granular, cabo particle, charcoal fiber etc., preferably activated carbon granule.The preparation of described modified absorbing material granules, it is characterized in that saponin, comprise the saponin that extracts in genseng, pseudo-ginseng, the wind-weed, polygala root, Radix Glycyrrhizae, balloonflower root, the radix bupleuri, the sugar of forming saponin(e has D-glucose, L-rhamnose, D-galactolipin, L-arabinose, L-wood sugar etc.
Beneficial effect of the present invention: the vegetable material saponin that additive of the present invention adopted is a green product, and is distributed more widely at occurring in nature, be easy to extract or preparation, and cost is lower, steady quality.Modified absorbing material granules is comparatively simple as the cigarette additive process, and process can not cause environmental pollution.Can not damage human body.Modified absorbing material granules does not after treatment have significant taste and darker primary colors.Add in the cigarette filter tip and can not influence cigarette quality.Modified absorbing material granules is widely applicable as cigarette additive, can use in various products, improves availability greatly and saves the processing cost that cigarette props up.Play after adding in the cigarette filter and improve the cigarette smoking quality, remove the purpose of harmful components.
The specific embodiment
Further specify flesh and blood of the present invention with example below, but content of the present invention is not limited to this.
Embodiment 1: select the activated carbon granule of particle diameter between the 40-60 order for use; The saponin of selecting natural extraction then for use or producing, this example is used the saponin class of extracting in the hay.1% (percentage by weight) by the active carbon dry weight takes by weighing saponin, the saponin that weighs up fully is dissolved in forms the aqueous solution in the water, and the water yield is 1.5 times of active carbon volume.Then the activated carbon granule that chooses was soaked wherein 4 hours, adopt therebetween mechanical agitation fully stir (2,000rmp); Filter then, solid material is transferred in the vacuum drying chamber, 40 ℃ of following vacuum drying (vacuum degree control is at 10mm Hg) 48 hours.Handle with the sub-rescreening of 40～60 mesh sieves, make its fine particle that reaches the requirement size, so that it is added in the cigarette filter tip.The fine particle that reaches the requirement size is packed, for future use.The common active carbon of modified absorbing material granules being applied in composite filter tip uses identical, mainly is that its amount of adding in the composite filter tip to is that 10-30mg/ props up, and the binary composite filter tip is that 15mg/ props up, and the ternary composite filter tip is that 30mg/ props up.
Adopt certain cloud to produce cigarette leaf group rolling cigarette, the flue gas analysis data of cigarette sample and organoleptic analysis's data see Table 1 and table 2, and are as follows.
Embodiment 2: select the activated carbon granule of particle diameter between the 40-60 order for use; The saponin of selecting natural extraction then for use or producing, this example is used the saponin that extracts in the pseudo-ginseng.2% (percentage by weight) by the active carbon dry weight takes by weighing saponin, the saponin that weighs up fully is dissolved in forms the aqueous solution in the water, and the water yield is 1.5 times of active carbon volume.Then the activated carbon granule that chooses was soaked wherein 6 hours, adopt therebetween mechanical agitation fully stir (2,000rmp); Filter then, solid material is transferred in the vacuum drying chamber, 60 ℃ of following vacuum drying (vacuum degree control is at 10mm Hg) 48 hours.Handle with the sub-rescreening of 40～60 mesh sieves, make its fine particle that reaches the requirement size, so that it is added in the cigarette filter tip.The fine particle that reaches the requirement size is packed, for future use.The common active carbon of modified absorbing material granules being applied in composite filter tip uses identical, mainly is that its amount of adding in the composite filter tip to is that 10-30mg/ props up, and the binary composite filter tip is that 20mg/ props up, and the ternary composite filter tip is that 25mg/ props up.
Embodiment 3: select the expanded granular offal of particle diameter between the 40-60 order for use; The saponin of selecting natural extraction then for use or producing, this example is used arasaponin.0.5% (percentage by weight) by expanded granular offal dry weight takes by weighing saponin, the reception that weighs up fully is dissolved in forms the aqueous solution in the water, and the water yield is 1/2nd of an expanded granular offal volume.Then the aqueous solution for preparing evenly is sprayed onto on the expanded granular offal that chooses, solid material is transferred in the vacuum drying chamber, 60 ℃ of following vacuum drying (vacuum degree control is at 10mm Hg) 72 hours.Handle with the sub-rescreening of 40～60 mesh sieves, make its fine particle that reaches the requirement size, so that it is added in the cigarette filter tip.The fine particle that reaches the requirement size is packed, for future use.The common active carbon of modified absorbing material granules being applied in composite filter tip uses identical, mainly is that its amount of adding in the composite filter tip to is that 10-30mg/ props up, and the binary composite filter tip is that 15mg/ props up, and the ternary composite filter tip is that 30mg/ props up.
Embodiment 4: select the expanded granular offal of particle diameter between the 40-60 order for use; The saponin of selecting natural extraction then for use or producing, this example is used panaxoside.0.5% (percentage by weight) by the active carbon dry weight takes by weighing saponin, the saponin that weighs up fully is dissolved in forms the aqueous solution in the water, and the water yield is 1/2nd of an expanded granular offal volume.Then the aqueous solution for preparing evenly is sprayed onto on the expanded granular offal that chooses, solid material is transferred in the vacuum drying chamber, 60 ℃ of following vacuum drying (vacuum degree control is at 10mm Hg) 72 hours.Handle with the sub-rescreening of 40～60 mesh sieves, make its fine particle that reaches the requirement size, so that it is added in the cigarette filter tip.The fine particle that reaches the requirement size is packed, for future use.The common active carbon of modified absorbing material granules being applied in composite filter tip uses identical, mainly is that its amount of adding in the composite filter tip to is that 10-30mg/ props up, and the binary composite filter tip is that 15mg/ props up, and the ternary composite filter tip is that 30mg/ props up.
The flue gas analysis result of table 1 part cigarette sample
| Numbering | Sample description | Cigarette weight g/ props up | TPM mg/ props up | Tarry matters in smoke amount mg/ props up | Nicotine content in smoke mg/ props up | Flue gas moisture mg/ props up |
| 1 | Active carbon, binary is compound | 0.910 | 14.71 | 13.47 | 1.09 | 0.90 |
| 2 | Active carbon, ternary is compound | 0.921 | 13.74 | 12.57 | 1.09 | 0.79 |
| 3 | Active carbon, ternary is compound | 0.890 | 14.84 | 13.60 | 1.09 | 0.92 |
| 4 | Granule peduncle, binary is compound | 0.920 | 13.80 | 12.81 | 0.99 | 0.72 |
| 5 | Active carbon, ternary is compound | 0.921 | 14.55 | 12.91 | 1.19 | 1.16 |
| 6 | Granule peduncle, binary is compound | 0.898 | 14.43 | 13.13 | 1.09 | 0.94 |
| 7 | Active carbon, ternary is compound | 0.901 | 14.68 | 13.37 | 1.09 | 0.96 |
| 8 | Granule peduncle, binary is compound | 0.921 | 15.48 | 13.79 | 1.09 | 1.34 |
| Contrast | Contrast, common cellulose acetate filter | 0.911 | 16.88 | 14.97 | 1.39 | 1.34 |
Table 2 part cigarette sample sensory evaluating smoking result (GB 5606.4-2005)
| Numbering | Gloss | Fragrance | Harmony | Assorted gas | Excitant | Pleasant impression | Total points |
| 1 | 5 | 29 | 5 | 10.5 | 17 | 22.5 | 84 |
| 2 | 5 | 29 | 5 | 11 | 17.5 | 22 | 84.5 |
| 3 | 5 | 29 | 5 | 10.5 | 17.5 | 22 | 84 |
| 4 | 5 | 28.5 | 5 | 11 | 18 | 22.5 | 85 |
| 5 | 5 | 28.5 | 5 | 10.5 | 17.5 | 22 | 83.5 |
| 6 | 5 | 29 | 5 | 11 | 18 | 22.5 | 85.5 |
| 7 | 5 | 29 | 5 | 10.5 | 17.5 | 22 | 84 |
| 8 | 5 | 28.5 | 5 | 11 | 18 | 22.5 | 85 |
| Contrast | 5 | 28 | 5 | 11 | 17 | 22 | 83 |
(annotate: participating in the personnel that smoke panel test is 11 people)
Claims (5)
1. a cigarette composite filter tip that contains plant saponin extract is with the preparation method of modified absorbing material, it is characterized in that the saponin that will extract is dissolved in to form the aqueous solution in the water, sorbing material soaked wherein 2-4 hour, and fully stir; Filter the back at 40-60 ℃ of following vacuum drying 24-48 hour, handle, obtain modified absorbing material granules with the screening of 40～60 mesh sieves;
Described saponin is made up of sapogenin and sugar, and the sugar of forming saponin(e has D-glucose, L-rhamnose, D-galactolipin, L-arabinose, L-wood sugar;
Described sorbing material is activated carbon granule, zeolite granular, cabo particle or charcoal fiber;
Described vacuum is 9～10mmHg;
Described abundant stirring is meant mechanical agitation.
2. the preparation method of modified absorbing material according to claim 1 is characterized in that described saponin is derived from genseng, pseudo-ginseng, the wind-weed, polygala root, Radix Glycyrrhizae, balloonflower root, radix bupleuri.
3. the preparation method of modified absorbing material according to claim 1 is characterized in that described sorbing material is an activated carbon granule, and the activated carbon granule particle diameter is between the 40-60 order.
4. the preparation method of modified absorbing material according to claim 1, it is characterized in that in cigarette filter, wrap up/contain modified absorbing material granules, contain saponin in the described modified absorbing material granules, the content of modified absorbing material granules is that 10-30mg/ props up.
5. the preparation method of modified absorbing material according to claim 4, it is characterized in that the content of modified absorbing material granules in cigarette filter: the binary composite filter tip is that 10-15mg/ props up, and the ternary composite filter tip is that 20-30mg/ props up.
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| CN102090719A (en) * | 2010-09-15 | 2011-06-15 | 张锐 | Cigarette filtering agent for protecting health, strengthening body, relieving cough and moisturizing throat |
| CN102090720A (en) * | 2010-09-15 | 2011-06-15 | 张锐 | Cigarette filtering agent for health care, body strengthening and cough relief |
| CN102090718A (en) * | 2010-09-15 | 2011-06-15 | 张锐 | Cigarette filtering agent for protecting health, relieving cough and refreshing |
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| CN104256889B (en) * | 2014-09-05 | 2015-10-28 | 云南中烟工业有限责任公司 | A kind of cigarette filter extract add tight extracting method |
| CN104705786B (en) * | 2015-01-14 | 2020-01-17 | 广西中烟工业有限责任公司 | Stem particles capable of improving cigarette taste and preparation method and application thereof |
| CN106263024A (en) * | 2016-08-12 | 2017-01-04 | 福建中烟工业有限责任公司 | A kind of reduce the method for phenol content in cigarette smoke |
| CN112841708B (en) * | 2019-12-26 | 2023-05-02 | 深圳市环球绿地新材料有限公司 | Application of spherical carbon in smoke adsorption generated by combustion of tobacco products |
| CN111802687B (en) * | 2020-07-27 | 2022-04-29 | 湖北中烟工业有限责任公司 | Atomizing agent containing conjugated linoleic acid and saponin and cigarette without burning during heating |
| CN112553004B (en) * | 2020-12-14 | 2022-06-21 | 湖北中烟工业有限责任公司 | Tobacco flavor and preparation method thereof |
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