CN101309945A - 低表面能烯键式不饱和多异氰酸酯加成化合物及其在涂料组合物中的应用 - Google Patents
低表面能烯键式不饱和多异氰酸酯加成化合物及其在涂料组合物中的应用 Download PDFInfo
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- CN101309945A CN101309945A CNA2006800428728A CN200680042872A CN101309945A CN 101309945 A CN101309945 A CN 101309945A CN A2006800428728 A CNA2006800428728 A CN A2006800428728A CN 200680042872 A CN200680042872 A CN 200680042872A CN 101309945 A CN101309945 A CN 101309945A
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- CN
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- Prior art keywords
- thing
- addition compounds
- compounds based
- polyisocyanate addition
- lysine triisocyanate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/2805—Compounds having only one group containing active hydrogen
- C08G18/288—Compounds containing at least one heteroatom other than oxygen or nitrogen
- C08G18/289—Compounds containing at least one heteroatom other than oxygen or nitrogen containing silicon
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/67—Unsaturated compounds having active hydrogen
- C08G18/671—Unsaturated compounds having only one group containing active hydrogen
- C08G18/672—Esters of acrylic or alkyl acrylic acid having only one group containing active hydrogen
- C08G18/6725—Esters of acrylic or alkyl acrylic acid having only one group containing active hydrogen containing ester groups other than acrylate or alkylacrylate ester groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/77—Polyisocyanates or polyisothiocyanates having heteroatoms in addition to the isocyanate or isothiocyanate nitrogen and oxygen or sulfur
- C08G18/78—Nitrogen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/77—Polyisocyanates or polyisothiocyanates having heteroatoms in addition to the isocyanate or isothiocyanate nitrogen and oxygen or sulfur
- C08G18/78—Nitrogen
- C08G18/79—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates
- C08G18/791—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates containing isocyanurate groups
- C08G18/792—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates containing isocyanurate groups formed by oligomerisation of aliphatic and/or cycloaliphatic isocyanates or isothiocyanates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/81—Unsaturated isocyanates or isothiocyanates
- C08G18/8141—Unsaturated isocyanates or isothiocyanates masked
- C08G18/815—Polyisocyanates or polyisothiocyanates masked with unsaturated compounds having active hydrogen
- C08G18/8158—Polyisocyanates or polyisothiocyanates masked with unsaturated compounds having active hydrogen with unsaturated compounds having only one group containing active hydrogen
- C08G18/8175—Polyisocyanates or polyisothiocyanates masked with unsaturated compounds having active hydrogen with unsaturated compounds having only one group containing active hydrogen with esters of acrylic or alkylacrylic acid having only one group containing active hydrogen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L75/00—Compositions of polyureas or polyurethanes; Compositions of derivatives of such polymers
- C08L75/04—Polyurethanes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
- C09D175/14—Polyurethanes having carbon-to-carbon unsaturated bonds
- C09D175/16—Polyurethanes having carbon-to-carbon unsaturated bonds having terminal carbon-to-carbon unsaturated bonds
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Polyurethanes Or Polyureas (AREA)
- Paints Or Removers (AREA)
- Macromonomer-Based Addition Polymer (AREA)
Abstract
Description
实施例 | 1 | 2 | 3 | 4(对比例) | 5(对比例) | 6 | 7 | 8 | 9 |
原料多异氰酸酯 | 3600 | 3600 | 3600 | 3600 | 3600 | 3400 | 2410 | 4470 | 4470 |
醇 | 0411 | 0411 | 4411 | 异丁醇 | 异丁醇 | 0411 | 0411 | 0411 | 0411 |
重量%-OH | 1 | 10 | 1 | 0.1 | 0.8 | 1 | 1 | 1 | 10 |
当量%-OH | 0.2 | 1.9 | 0.4 | 0.2 | 1.9 | 0.2 | 0.2 | 0.3 | 2.7 |
%NCO | 22.3 | 19.8 | 22.5 | 22.8 | 22.1 | 21.3 | 23.3 | 17.0 | 15.1 |
%SiO | 0.5 | 4.6 | 0.5 | 0.0 | 0.0 | 0.5 | 0.5 | 0.5 | 4.8 |
粘度,mPa.s,(25℃) | 1195 | 1310 | 1218 | 1242 | 1353 | 136 | 670 | 510 | 598 |
表面张力,达因/厘米 | 23 | 23 | 25 | 45 | 44 | 23 | 23 | 27 | 24 |
实施例 | 10 | 11 | 12 | 13(对比例) | 14(对比例) | 15 | 16 | 17 | 18 |
多异氰酸酯所来自的实施例号 | 1 | 2 | 3 | 4 | 5 | 6 | 7 | 8 | 9 |
原料多异氰酸酯 | 3600 | 3600 | 3600 | 3600 | 3600 | 3400 | 2410 | 4470 | 4470 |
醇 | 0411 | 0411 | 4411 | 异丁醇 | 异丁醇 | 0411 | 0411 | 0411 | 0411 |
多异氰酸酯的当量 | 1 | 1 | 1 | 1 | 1 | 1 | 1 | 1 | 1 |
丙烯酸酯M 100的当量 | 1 | 1 | 1 | 1 | 1 | 1 | 1 | 1 | 1 |
多异氰酸酯加成化合物中的%SiO | 0.2 | 1.8 | 0.2 | 0.0 | 0.0 | 0.2 | 0.2 | 0.2 | 2.2 |
多异氰酸酯加成化合物中的%C=C | 4.5 | 4.3 | 4.5 | 4.6 | 4.5 | 4.4 | 4.6 | 4.1 | 3.9 |
粘度,mPa.s(25℃) | 21,335 | 18,228 | 14,277 | 20,734 | 18,534 | 6,980 | 19,895 | 15,012 | 59,324 |
表面张力,达因/厘米 | 24 | 22 | 26 | 44 | 44 | 23 | 24 | 22 | 18 |
实施例 | 19 | 20 | 21(对比例) | 22(对比例) | 23 | 24 |
多异氰酸酯加成化合物所来自的实施例号 | 10 | 11 | 13 | 14 | 11 | 11 |
原料多异氰酸酯 | 3600 | 3600 | 3600 | 3600 | 3600 | 3600 |
醇 | 0411 | 0411 | 异丁醇 | 异丁醇 | 0411 | 0411 |
多异氰酸酯加成化合物,克 | 1 | 1 | 1 | 1 | 1 | 1 |
丙烯酸酯稀释剂 | 2513 | 2513 | 2513 | 2513 | 238 | 256 |
重量,克 | 9 | 9 | 9 | 9 | 9 | 9 |
混合物的%SiO | 0.02 | 0.2 | 0.0 | 0.0 | 0.2 | 0.2 |
混合物的%C=C | 4.6 | 4.6 | 4.6 | 4.6 | 19.5 | 12.0 |
表面张力,达因/厘米 | 28 | 23 | 44 | 45 | 23 | 23 |
Claims (17)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US11/281,232 | 2005-11-17 | ||
US11/281,232 US20070112161A1 (en) | 2005-11-17 | 2005-11-17 | Low surface energy, ethylenically unsaturated polyisocyanate addition compounds and their use in coating compositions |
PCT/US2006/043977 WO2007061663A2 (en) | 2005-11-17 | 2006-11-13 | Low surface energy, ethylenically unsaturated polyisocyanate addition compounds and their use in coating compositions |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101309945A true CN101309945A (zh) | 2008-11-19 |
CN101309945B CN101309945B (zh) | 2012-01-11 |
Family
ID=37891927
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2006800428728A Active CN101309945B (zh) | 2005-11-17 | 2006-11-13 | 低表面能烯键式不饱和多异氰酸酯加成化合物及其在涂料组合物中的应用 |
Country Status (6)
Country | Link |
---|---|
US (1) | US20070112161A1 (zh) |
EP (1) | EP1963391B8 (zh) |
JP (1) | JP2009516057A (zh) |
KR (1) | KR20080075119A (zh) |
CN (1) | CN101309945B (zh) |
WO (1) | WO2007061663A2 (zh) |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102414240A (zh) * | 2009-04-30 | 2012-04-11 | 道康宁东丽株式会社 | 聚氨酯及其制造方法、母料、油墨用粘合剂、油墨组合物、成形用热塑性聚合物组合物、成形体、复合成形体及其制造方法 |
CN101885849B (zh) * | 2009-05-15 | 2012-05-09 | 欧阳允亮 | 生物医学材料的预聚物 |
CN101712842B (zh) * | 2009-11-09 | 2013-10-16 | 深圳市广田环保涂料有限公司 | 一种防粘贴防涂鸦涂料 |
CN105051012A (zh) * | 2012-10-23 | 2015-11-11 | 巴斯夫欧洲公司 | 含有聚合物稳定剂基团的烯属不饱和低聚物 |
CN107541176A (zh) * | 2016-06-27 | 2018-01-05 | 赢创德固赛有限公司 | 烷氧基硅烷官能化的脲基甲酸酯 |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7989074B2 (en) | 2006-06-09 | 2011-08-02 | Ndsu Research Foundation | Thermoset siloxane-urethane fouling release coatings |
US8372384B2 (en) * | 2007-01-08 | 2013-02-12 | Ndsu Research Foundation | Quaternary ammonium functionalized cross-linked polyalkylsiloxanes with anti-fouling activity |
CN101679705B (zh) | 2007-06-08 | 2013-12-11 | 3M创新有限公司 | 含氟烷基的酯低聚物与聚碳二亚胺的共混物 |
US8053535B2 (en) * | 2007-07-11 | 2011-11-08 | Ndsu Research Foundation | Polysiloxanes with anti-fouling activity |
US8709394B2 (en) * | 2007-09-28 | 2014-04-29 | Ndsu Research Foundation | Antimicrobial polysiloxane materials containing metal species |
US8071706B2 (en) | 2008-02-13 | 2011-12-06 | Ndsu Research Foundation | Siloxane polymer containing tethered levofloxacin |
US10174220B2 (en) * | 2014-08-06 | 2019-01-08 | Mitsubishi Chemical Corporation | Coated film |
WO2023099995A1 (en) * | 2021-12-03 | 2023-06-08 | 3M Innovative Properties Company | Free-radically polymerizable compounds, compositions including the same, polymerized compounds, methods of making and articles including the same |
Family Cites Families (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP3167229B2 (ja) * | 1993-09-27 | 2001-05-21 | 株式会社メニコン | 眼用レンズ材料 |
US5576411A (en) * | 1994-09-14 | 1996-11-19 | Bayer Corporation | Low surface energy polyisocyanates and their use in one-or two component coating compositions |
US5541281A (en) * | 1994-12-20 | 1996-07-30 | Bayer Corporation | Low surface energy polyisocyanates and their use in one- or two-component coating compositions |
US5574122A (en) * | 1995-09-29 | 1996-11-12 | Bayer Corporation | Low surface energy polyisocyanates and their use in one- or two-component coating compositions |
US5646227A (en) * | 1996-02-01 | 1997-07-08 | Bayer Corporation | Low surface energy polyisocyanates and their use in one- or two-component coating compositions |
US5747629A (en) * | 1996-12-16 | 1998-05-05 | Bayer Corporation | Low surface energy polyisocyanates and their use in one-or two-component coating compositions |
US5691439A (en) * | 1996-12-16 | 1997-11-25 | Bayer Corporation | Low surface energy polyisocyanates and their use in one- or two-component coating compositions |
JPH10231341A (ja) * | 1997-02-20 | 1998-09-02 | Jsr Corp | 液状硬化性樹脂組成物 |
US5767220A (en) * | 1997-08-25 | 1998-06-16 | Bayer Corporation | Low viscosity, ethylenically unsaturated polyurethanes containing allophanate groups |
JPH11228643A (ja) * | 1998-02-17 | 1999-08-24 | Menicon Co Ltd | 眼用レンズ材料およびその製法 |
CN1145660C (zh) * | 1998-08-26 | 2004-04-14 | Basf公司 | 滋发剂组合物及其用途 |
DE60013702T2 (de) * | 1999-06-30 | 2005-09-29 | Menicon Co., Ltd., Nagoya | Verfahren zum Herstellen einer Urethanverbindung für medizinische Instrumente |
US7459167B1 (en) * | 2000-07-27 | 2008-12-02 | 3M Innovative Properties Company | Biocidal polyurethane compositions and methods of use |
ATE329976T1 (de) * | 2002-08-22 | 2006-07-15 | Du Pont | Verfahren zum beschichten von faserverstärkten kunststoffsubstraten mit einem primer |
US7211621B2 (en) * | 2004-02-11 | 2007-05-01 | E. I. Du Pont De Nemours And Company | Polyurethaneurea resins with trialkoxysilane groups and processes for the production thereof |
-
2005
- 2005-11-17 US US11/281,232 patent/US20070112161A1/en not_active Abandoned
-
2006
- 2006-11-13 KR KR1020087011794A patent/KR20080075119A/ko not_active Application Discontinuation
- 2006-11-13 CN CN2006800428728A patent/CN101309945B/zh active Active
- 2006-11-13 WO PCT/US2006/043977 patent/WO2007061663A2/en active Application Filing
- 2006-11-13 JP JP2008541248A patent/JP2009516057A/ja not_active Withdrawn
- 2006-11-13 EP EP06837433.9A patent/EP1963391B8/en active Active
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102414240A (zh) * | 2009-04-30 | 2012-04-11 | 道康宁东丽株式会社 | 聚氨酯及其制造方法、母料、油墨用粘合剂、油墨组合物、成形用热塑性聚合物组合物、成形体、复合成形体及其制造方法 |
CN102414240B (zh) * | 2009-04-30 | 2014-09-17 | 道康宁东丽株式会社 | 聚氨酯及其制造方法、母料、油墨用粘合剂、油墨组合物、成形用热塑性聚合物组合物、成形体、复合成形体及其制造方法 |
CN101885849B (zh) * | 2009-05-15 | 2012-05-09 | 欧阳允亮 | 生物医学材料的预聚物 |
CN101712842B (zh) * | 2009-11-09 | 2013-10-16 | 深圳市广田环保涂料有限公司 | 一种防粘贴防涂鸦涂料 |
CN105051012A (zh) * | 2012-10-23 | 2015-11-11 | 巴斯夫欧洲公司 | 含有聚合物稳定剂基团的烯属不饱和低聚物 |
CN105051012B (zh) * | 2012-10-23 | 2019-01-04 | 巴斯夫欧洲公司 | 含有聚合物稳定剂基团的烯属不饱和低聚物 |
CN107541176A (zh) * | 2016-06-27 | 2018-01-05 | 赢创德固赛有限公司 | 烷氧基硅烷官能化的脲基甲酸酯 |
Also Published As
Publication number | Publication date |
---|---|
EP1963391B1 (en) | 2014-02-26 |
EP1963391B8 (en) | 2014-04-02 |
EP1963391A2 (en) | 2008-09-03 |
US20070112161A1 (en) | 2007-05-17 |
WO2007061663A8 (en) | 2008-08-21 |
JP2009516057A (ja) | 2009-04-16 |
KR20080075119A (ko) | 2008-08-14 |
WO2007061663A3 (en) | 2008-01-10 |
WO2007061663A2 (en) | 2007-05-31 |
CN101309945B (zh) | 2012-01-11 |
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