CA2660049C - Methods and apparatus for producing alkyl esters from lipid feed stocks and systems including same - Google Patents

Methods and apparatus for producing alkyl esters from lipid feed stocks and systems including same Download PDF

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Publication number
CA2660049C
CA2660049C CA2660049A CA2660049A CA2660049C CA 2660049 C CA2660049 C CA 2660049C CA 2660049 A CA2660049 A CA 2660049A CA 2660049 A CA2660049 A CA 2660049A CA 2660049 C CA2660049 C CA 2660049C
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CA
Canada
Prior art keywords
oil
reaction mixture
catalyst
metal oxide
zirconia
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CA2660049A
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English (en)
French (fr)
Other versions
CA2660049A1 (en
Inventor
Clayton V. Mcneff
Larry C. Mcneff
Arlin E. Gyberg
Bingwen Yan
Daniel Thomas Nowlan
Brian Krohn
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
MCNEFF RES CONSULTANTS Inc
Original Assignee
MCNEFF RESEARCH CONSULTANTS Inc
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Publication of CA2660049A1 publication Critical patent/CA2660049A1/en
Application granted granted Critical
Publication of CA2660049C publication Critical patent/CA2660049C/en
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/02—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
    • C10L1/026—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only for compression ignition
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Fats And Perfumes (AREA)
CA2660049A 2006-08-04 2007-08-03 Methods and apparatus for producing alkyl esters from lipid feed stocks and systems including same Active CA2660049C (en)

Applications Claiming Priority (7)

Application Number Priority Date Filing Date Title
US82149806P 2006-08-04 2006-08-04
US60/821,498 2006-08-04
US82557506P 2006-09-13 2006-09-13
US60/825,575 2006-09-13
US88973007P 2007-02-13 2007-02-13
US60/889,730 2007-02-13
PCT/US2007/075211 WO2008019325A2 (en) 2006-08-04 2007-08-03 Methods and apparatus for producing alkyl esters from lipid feed stocks and systems including same

Publications (2)

Publication Number Publication Date
CA2660049A1 CA2660049A1 (en) 2008-02-14
CA2660049C true CA2660049C (en) 2015-09-22

Family

ID=38924308

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2660049A Active CA2660049C (en) 2006-08-04 2007-08-03 Methods and apparatus for producing alkyl esters from lipid feed stocks and systems including same

Country Status (4)

Country Link
EP (1) EP2069465A2 (es)
CA (1) CA2660049C (es)
MX (1) MX2009001280A (es)
WO (1) WO2008019325A2 (es)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10239812B2 (en) 2017-04-27 2019-03-26 Sartec Corporation Systems and methods for synthesis of phenolics and ketones

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8445709B2 (en) * 2006-08-04 2013-05-21 Mcneff Research Consultants, Inc. Systems and methods for refining alkyl ester compositions
US9102877B2 (en) 2008-11-12 2015-08-11 Sartec Corporation Systems and methods for producing fuels from biomass
EP2462214A1 (en) * 2009-06-09 2012-06-13 Mcneff Research Consultants, Inc. Systems and methods for refining alkyl ester compositions
US8557001B2 (en) 2009-11-24 2013-10-15 Shell Oil Company Fuel formulations
US8663346B2 (en) 2009-11-24 2014-03-04 Shell Oil Company Fuel formulations
US10696923B2 (en) 2018-02-07 2020-06-30 Sartec Corporation Methods and apparatus for producing alkyl esters from lipid feed stocks, alcohol feedstocks, and acids
US10544381B2 (en) 2018-02-07 2020-01-28 Sartec Corporation Methods and apparatus for producing alkyl esters from a reaction mixture containing acidified soap stock, alcohol feedstock, and acid

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AU5225099A (en) * 1998-07-24 2000-02-14 Lockheed Martin Idaho Technologies Company A process for producing biodiesel, lubricants, and fuel and lubricant additives in a critical fluid medium
AU2003304018A1 (en) * 2003-03-26 2004-10-18 Japan Energy Corporation Process for producing ester through transesterification with solid acid catalyst
BRPI0414031A (pt) * 2003-08-29 2006-10-24 Nippon Catalytic Chem Ind método de produção de ésteres alquìlicos de ácidos graxos e/ou glicerina e composição contendo éster alquìlico de ácido graxo
JP4255823B2 (ja) * 2003-12-24 2009-04-15 花王株式会社 脂肪酸エステルの製造方法

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10239812B2 (en) 2017-04-27 2019-03-26 Sartec Corporation Systems and methods for synthesis of phenolics and ketones

Also Published As

Publication number Publication date
MX2009001280A (es) 2009-06-19
WO2008019325A2 (en) 2008-02-14
WO2008019325A3 (en) 2008-08-28
CA2660049A1 (en) 2008-02-14
EP2069465A2 (en) 2009-06-17

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