BR112015006162A8 - método - Google Patents

método Download PDF

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Publication number
BR112015006162A8
BR112015006162A8 BR112015006162A BR112015006162A BR112015006162A8 BR 112015006162 A8 BR112015006162 A8 BR 112015006162A8 BR 112015006162 A BR112015006162 A BR 112015006162A BR 112015006162 A BR112015006162 A BR 112015006162A BR 112015006162 A8 BR112015006162 A8 BR 112015006162A8
Authority
BR
Brazil
Prior art keywords
xylose
exchange resins
optionally
recovery
separation system
Prior art date
Application number
BR112015006162A
Other languages
English (en)
Other versions
BR112015006162B1 (pt
BR112015006162A2 (pt
Inventor
Lewandowski Jari
Mattila Jari
Laiho Kari
Kekäläinen Kati
Nurmi Nina
Original Assignee
Dupont Nutrition Biosci Aps
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dupont Nutrition Biosci Aps filed Critical Dupont Nutrition Biosci Aps
Publication of BR112015006162A2 publication Critical patent/BR112015006162A2/pt
Publication of BR112015006162A8 publication Critical patent/BR112015006162A8/pt
Publication of BR112015006162B1 publication Critical patent/BR112015006162B1/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
    • C13K13/00—Sugars not otherwise provided for in this class
    • C13K13/002—Xylose
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B01D15/1814—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns recycling of the fraction to be distributed
    • B01D15/1821—Simulated moving beds
    • B01D15/185—Simulated moving beds characterized by the components to be separated
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/36—Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction
    • B01D15/361—Ion-exchange
    • B01D15/362—Cation-exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/36—Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction
    • B01D15/361—Ion-exchange
    • B01D15/363—Anion-exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J39/00—Cation exchange; Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
    • B01J39/04—Processes using organic exchangers
    • B01J39/05—Processes using organic exchangers in the strongly acidic form
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J39/00—Cation exchange; Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
    • B01J39/04—Processes using organic exchangers
    • B01J39/07—Processes using organic exchangers in the weakly acidic form
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J39/00—Cation exchange; Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
    • B01J39/26—Cation exchangers for chromatographic processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J41/00—Anion exchange; Use of material as anion exchangers; Treatment of material for improving the anion exchange properties
    • B01J41/04—Processes using organic exchangers
    • B01J41/07—Processes using organic exchangers in the weakly basic form
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J41/00—Anion exchange; Use of material as anion exchangers; Treatment of material for improving the anion exchange properties
    • B01J41/08—Use of material as anion exchangers; Treatment of material for improving the anion exchange properties
    • B01J41/12—Macromolecular compounds
    • B01J41/14—Macromolecular compounds obtained by reactions only involving unsaturated carbon-to-carbon bonds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J41/00—Anion exchange; Use of material as anion exchangers; Treatment of material for improving the anion exchange properties
    • B01J41/20—Anion exchangers for chromatographic processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J47/00—Ion-exchange processes in general; Apparatus therefor
    • B01J47/011—Ion-exchange processes in general; Apparatus therefor using batch processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J47/00—Ion-exchange processes in general; Apparatus therefor
    • B01J47/02—Column or bed processes
    • B01J47/04—Mixed-bed processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J47/00—Ion-exchange processes in general; Apparatus therefor
    • B01J47/10—Ion-exchange processes in general; Apparatus therefor with moving ion-exchange material; with ion-exchange material in suspension or in fluidised-bed form
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B20/00—Purification of sugar juices
    • C13B20/14—Purification of sugar juices using ion-exchange materials
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B20/00—Purification of sugar juices
    • C13B20/14—Purification of sugar juices using ion-exchange materials
    • C13B20/146—Purification of sugar juices using ion-exchange materials using only anionic ion-exchange material
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B20/00—Purification of sugar juices
    • C13B20/14—Purification of sugar juices using ion-exchange materials
    • C13B20/148—Purification of sugar juices using ion-exchange materials for fractionating, adsorption or ion exclusion processes combined with elution or desorption of a sugar fraction

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Sustainable Development (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Saccharide Compounds (AREA)

Abstract

método de separação e recuperação de xilose a presente invenção se refere a um método para separar e recuperar xilose a partir de uma solução à base de plantas contendo xilose. o método é realizado em um sistema de separação cromatográfica, o qual compreende uma ou mais resinas de troca aniônica de base fraca e, opcionalmente, uma ou mais resinas selecionadas entre as resinas de troca catiônica de ácidos fortes e as resinas de troca catiônica de ácidos fracos, em que a solução passa através do sistema de separação, seguida por recuperação de, pelo menos, uma fração enriquecida em xilose. opcionalmente, uma fração de ramnose também pode ser recuperada.
BR112015006162-1A 2012-09-20 2013-09-19 Método cromatográfico de separação para separação e recuperação de xilose BR112015006162B1 (pt)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US201261703322P 2012-09-20 2012-09-20
GB1216764.9 2012-09-20
US61/703,322 2012-09-20
GBGB1216764.9A GB201216764D0 (en) 2012-09-20 2012-09-20 Separation and recovery of xylose
PCT/EP2013/069473 WO2014044753A1 (en) 2012-09-20 2013-09-19 Separation and recovery of xylose using weakly basic anion exchange resins

Publications (3)

Publication Number Publication Date
BR112015006162A2 BR112015006162A2 (pt) 2017-07-04
BR112015006162A8 true BR112015006162A8 (pt) 2019-09-03
BR112015006162B1 BR112015006162B1 (pt) 2021-09-28

Family

ID=47144552

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112015006162-1A BR112015006162B1 (pt) 2012-09-20 2013-09-19 Método cromatográfico de separação para separação e recuperação de xilose

Country Status (8)

Country Link
US (1) US9777342B2 (pt)
EP (1) EP2897704B1 (pt)
CN (1) CN104661718A (pt)
BR (1) BR112015006162B1 (pt)
DK (1) DK2897704T3 (pt)
GB (1) GB201216764D0 (pt)
WO (1) WO2014044753A1 (pt)
ZA (1) ZA201501811B (pt)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PL3401410T3 (pl) 2010-06-26 2021-11-29 Virdia, Llc Sposoby wytwarzania mieszanek cukrów
IL206678A0 (en) 2010-06-28 2010-12-30 Hcl Cleantech Ltd A method for the production of fermentable sugars
IL207329A0 (en) 2010-08-01 2010-12-30 Robert Jansen A method for refining a recycle extractant and for processing a lignocellulosic material and for the production of a carbohydrate composition
IL207945A0 (en) 2010-09-02 2010-12-30 Robert Jansen Method for the production of carbohydrates
EP2694594A4 (en) 2011-04-07 2015-11-11 Virdia Ltd METHODS AND PRODUCTS FOR LIGNOCELLULOSE CONVERSION
US9617608B2 (en) 2011-10-10 2017-04-11 Virdia, Inc. Sugar compositions
US9493851B2 (en) 2012-05-03 2016-11-15 Virdia, Inc. Methods for treating lignocellulosic materials
GB2523234B (en) 2012-05-03 2016-03-30 Virdia Ltd A method of fractionating a liquid sample
EP3242871B1 (en) 2015-01-07 2019-11-06 Virdia, Inc. Methods for extracting and converting hemicellulose sugars
GB201600161D0 (en) * 2016-01-05 2016-02-17 Bayer As Isotope purification method
CN110229195B (zh) * 2019-06-14 2022-11-04 广西福仪生物技术有限公司 一种从蔗渣中提取鼠李糖的方法
CN112340707B (zh) * 2020-12-01 2022-02-18 南京工业大学 一种利用三区式顺序模拟移动床连续色谱技术分离废酸的方法
CN114307252B (zh) * 2021-12-30 2022-09-20 南京工业大学 一种利用准二维色谱法分离糖和酸的工艺

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4075406A (en) 1974-04-22 1978-02-21 Suomen Sokeri Osakeyhtio Process for making xylose
CA1230348A (en) * 1985-02-22 1987-12-15 Akira Matsumoto Process for purifying aqueous solution of non- electrolytic organic substance to high purity
WO1991003574A1 (en) * 1989-09-01 1991-03-21 The Dow Chemical Company Process for purifying sugar solutions
US5084104A (en) 1989-12-05 1992-01-28 Cultor, Ltd. Method for recovering xylose
FI102962B (fi) 1996-06-24 1999-03-31 Xyrofin Oy Menetelmä ksylitolin valmistamiseksi
FI962609A (fi) * 1996-06-24 1997-12-25 Xyrofin Oy Menetelmä ksylitolin valmistamiseksi
US6451123B1 (en) 1999-01-14 2002-09-17 Board Of Supervisors Of Louisiana State University And Agricultural And Mechanical College Process for the separation of sugars
FI20002148A (fi) * 2000-09-29 2002-03-30 Xyrofin Oy Menetelmä tuotteiden talteenottamiseksi
FI20002149A (fi) 2000-09-29 2002-03-30 Xyrofin Oy Sakkaridien puhdistaminen kromatografisella erotuksella
DE60206487T3 (de) * 2001-04-12 2013-03-21 Mitsubishi Shoji Foodtech Co., Ltd. Verfahren zur entsalzung einer zuckerlösung und anionenaustauscher
FI20020592A (fi) * 2002-03-27 2003-09-28 Danisco Sweeteners Oy Menetelmä sokereiden, sokerialkoholien, hiilihydraattien ja niiden seosten erottamiseksi niitä sisältävistä liuoksista
US7037378B2 (en) 2003-09-24 2006-05-02 Danisco Sweetners Oy Separation of sugars
BRPI0715755A2 (pt) 2006-08-18 2013-02-26 Iogen Energy Corp processo para obter um sal orgÂnico ou Ácido orgÂnico a partir de uma corrente de aÇécar aquosa
CA2728726A1 (en) * 2008-06-26 2009-12-30 Danisco A/S Process for separation of ca- or mg-sulfite spent liquor to yield crystalline xylose

Also Published As

Publication number Publication date
BR112015006162B1 (pt) 2021-09-28
GB201216764D0 (en) 2012-10-31
BR112015006162A2 (pt) 2017-07-04
WO2014044753A1 (en) 2014-03-27
CN104661718A (zh) 2015-05-27
ZA201501811B (en) 2016-11-30
EP2897704A1 (en) 2015-07-29
DK2897704T3 (da) 2020-01-27
US9777342B2 (en) 2017-10-03
EP2897704B1 (en) 2019-10-23
US20150247211A1 (en) 2015-09-03

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B06F Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette]
B06F Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette]
B06I Publication of requirement cancelled [chapter 6.9 patent gazette]

Free format text: ANULADA A PUBLICACAO CODIGO 6.6.1 NA RPI NO 2462 DE 13/03/2018 POR TER SIDO INDEVIDA.

B06U Preliminary requirement: requests with searches performed by other patent offices: procedure suspended [chapter 6.21 patent gazette]
B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B06I Publication of requirement cancelled [chapter 6.9 patent gazette]

Free format text: ANULADA A PUBLICACAO CODIGO 6.1 NA RPI NO 2619 DE 16/03/2021 POR TER SIDO INDEVIDA.

B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 19/09/2013, OBSERVADAS AS CONDICOES LEGAIS.