AU2009322861B2 - Systems and methods for improving ammonia synthesis efficiency - Google Patents

Systems and methods for improving ammonia synthesis efficiency Download PDF

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AU2009322861B2
AU2009322861B2 AU2009322861A AU2009322861A AU2009322861B2 AU 2009322861 B2 AU2009322861 B2 AU 2009322861B2 AU 2009322861 A AU2009322861 A AU 2009322861A AU 2009322861 A AU2009322861 A AU 2009322861A AU 2009322861 B2 AU2009322861 B2 AU 2009322861B2
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syngas
temperature
mol
effluent
carbon dioxide
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AU2009322861A1 (en
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Israr Ul Haque
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Kellogg Brown and Root LLC
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/025—Preparation or purification of gas mixtures for ammonia synthesis
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/32—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air
    • C01B3/34—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents
    • C01B3/38—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents using catalysts
    • C01B3/382—Multi-step processes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/32—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air
    • C01B3/34—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents
    • C01B3/38—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents using catalysts
    • C01B3/384—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents using catalysts the catalyst being continuously externally heated
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/32—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air
    • C01B3/34—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents
    • C01B3/48—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents followed by reaction of water vapour with carbon monoxide
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02—Processes for making hydrogen or synthesis gas
    • C01B2203/0205—Processes for making hydrogen or synthesis gas containing a reforming step
    • C01B2203/0227—Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step
    • C01B2203/0233—Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step the reforming step being a steam reforming step
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02—Processes for making hydrogen or synthesis gas
    • C01B2203/025—Processes for making hydrogen or synthesis gas containing a partial oxidation step
    • C01B2203/0261—Processes for making hydrogen or synthesis gas containing a partial oxidation step containing a catalytic partial oxidation step [CPO]
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02—Processes for making hydrogen or synthesis gas
    • C01B2203/0283—Processes for making hydrogen or synthesis gas containing a CO-shift step, i.e. a water gas shift step
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0435—Catalytic purification
    • C01B2203/044—Selective oxidation of carbon monoxide
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0435—Catalytic purification
    • C01B2203/0445—Selective methanation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465—Composition of the impurity
    • C01B2203/0475—Composition of the impurity the impurity being carbon dioxide
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/06—Integration with other chemical processes
    • C01B2203/068—Ammonia synthesis
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/12—Feeding the process for making hydrogen or synthesis gas
    • C01B2203/1205—Composition of the feed
    • C01B2203/1211—Organic compounds or organic mixtures used in the process for making hydrogen or synthesis gas
    • C01B2203/1235—Hydrocarbons
    • C01B2203/1241—Natural gas or methane
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/14—Details of the flowsheet
    • C01B2203/146—At least two purification steps in series
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Hydrogen, Water And Hydrids (AREA)
AU2009322861A 2008-12-03 2009-10-19 Systems and methods for improving ammonia synthesis efficiency Active AU2009322861B2 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US12/327,249 2008-12-03
US12/327,249 US8617270B2 (en) 2008-12-03 2008-12-03 Systems and methods for improving ammonia synthesis efficiency
PCT/US2009/061155 WO2010065202A1 (en) 2008-12-03 2009-10-19 Systems and methods for improving ammonia synthesis efficiency

Publications (2)

Publication Number Publication Date
AU2009322861A1 AU2009322861A1 (en) 2011-07-21
AU2009322861B2 true AU2009322861B2 (en) 2015-02-12

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AU2009322861A Active AU2009322861B2 (en) 2008-12-03 2009-10-19 Systems and methods for improving ammonia synthesis efficiency

Country Status (9)

Country Link
US (1) US8617270B2 (ja)
EP (1) EP2364270B1 (ja)
JP (1) JP2012510427A (ja)
CN (2) CN102239110A (ja)
AU (1) AU2009322861B2 (ja)
BR (1) BRPI0922143B1 (ja)
CA (1) CA2744477C (ja)
RU (1) RU2503613C2 (ja)
WO (1) WO2010065202A1 (ja)

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US9321655B2 (en) * 2009-08-20 2016-04-26 Kellogg Brown & Root Llc Systems and methods for producing syngas and products therefrom
DE102010044939C5 (de) * 2010-09-10 2015-11-19 Thyssenkrupp Industrial Solutions Ag Verfahren und Vorrichtung zur Erzeugung von Prozessdampf und Kesselspeisewasserdampf in einem beheizbaren Reformierreaktor zur Herstellung von Synthesegas
WO2012142084A1 (en) 2011-04-11 2012-10-18 ADA-ES, Inc. Fluidized bed method and system for gas component capture
JP6328611B2 (ja) 2012-04-16 2018-05-23 シーアストーン リミテッド ライアビリティ カンパニー 非鉄触媒で炭素酸化物を還元するための方法および構造
CN104302575B (zh) 2012-04-16 2017-03-22 赛尔斯通股份有限公司 通过还原二氧化碳来产生固体碳的方法
NO2749379T3 (ja) 2012-04-16 2018-07-28
MX354526B (es) 2012-04-16 2018-03-07 Seerstone Llc Metodos y sistemas para capturar y secuestrar carbono y para reducir la masa de oxidos de carbono en una corriente de gas de desechos.
CN104284861A (zh) 2012-04-16 2015-01-14 赛尔斯通股份有限公司 处理含有碳氧化物的废气的方法
US9896341B2 (en) 2012-04-23 2018-02-20 Seerstone Llc Methods of forming carbon nanotubes having a bimodal size distribution
CA2875696C (en) 2012-06-27 2020-09-01 Grannus, Llc Polygeneration production of power and fertilizer through emissions capture
US10815124B2 (en) 2012-07-12 2020-10-27 Seerstone Llc Solid carbon products comprising carbon nanotubes and methods of forming same
JP6284934B2 (ja) 2012-07-12 2018-02-28 シーアストーン リミテッド ライアビリティ カンパニー カーボンナノチューブを含む固体炭素生成物およびそれを形成する方法
MX2015000580A (es) * 2012-07-13 2015-08-20 Seerstone Llc Metodos y sistemas para formar productos de carbono solido y amoniaco.
US9779845B2 (en) 2012-07-18 2017-10-03 Seerstone Llc Primary voltaic sources including nanofiber Schottky barrier arrays and methods of forming same
AU2013317997B2 (en) 2012-09-20 2016-04-07 ADA-ES, Inc. Method and system to reclaim functional sites on a sorbent contaminated by heat stable salts
JP6389824B2 (ja) 2012-11-29 2018-09-12 シーアストーン リミテッド ライアビリティ カンパニー 固体炭素材料を製造するための反応器および方法
EP3129133A4 (en) 2013-03-15 2018-01-10 Seerstone LLC Systems for producing solid carbon by reducing carbon oxides
WO2014151144A1 (en) 2013-03-15 2014-09-25 Seerstone Llc Carbon oxide reduction with intermetallic and carbide catalysts
EP2801550A1 (en) * 2013-05-10 2014-11-12 Ammonia Casale S.A. A process for producing ammonia synthesis gas with high temperature shift and low steam-to-carbon ratio
US9561968B2 (en) 2013-08-07 2017-02-07 Kellogg Brown & Root Llc Methods and systems for producing and processing syngas in a pressure swing adsorption unit and making ammonia therefrom
DE102014003392A1 (de) * 2014-03-06 2015-09-10 Linde Aktiengesellschaft Verfahren zum Betrieb einer Dampfreformierungsanlage
EP2993158A1 (en) * 2014-09-05 2016-03-09 Casale SA Process for production of ammonia and derivatives, in particular urea
EP3050849A1 (en) * 2015-01-27 2016-08-03 Casale SA A process for the synthesis of ammonia
CA3007124A1 (en) 2015-12-04 2017-06-08 Grannus, Llc Polygeneration production of hydrogen for use in various industrial processes
AR106923A1 (es) * 2015-12-07 2018-02-28 Haldor Topsoe As Control de la temperatura de entrada para el paso de conversión
RU2616942C1 (ru) * 2016-05-24 2017-04-18 Андрей Владиславович Курочкин Установка получения водорода высокого давления
WO2018022999A1 (en) 2016-07-28 2018-02-01 Seerstone Llc. Solid carbon products comprising compressed carbon nanotubes in a container and methods of forming same
EP3333124B1 (de) * 2016-12-09 2019-06-26 L'air Liquide, Société Anonyme Pour L'Étude Et L'exploitation Des Procédés Georges Claude Anlage und verfahren zur erzeugung von synthesegas
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RU2653034C9 (ru) * 2017-06-01 2019-04-11 Общество с ограниченной ответственностью "Новые химические продукты" Способ извлечения фторида водорода из его водных растворов
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JPWO2021230045A1 (ja) * 2020-05-14 2021-11-18
CN114804149B (zh) * 2022-05-27 2023-10-31 中国能源建设集团广东省电力设计研究院有限公司 一种光催化合成氨反应器及光催化合成氨反应***

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Also Published As

Publication number Publication date
CN105329854A (zh) 2016-02-17
US8617270B2 (en) 2013-12-31
US20100132259A1 (en) 2010-06-03
RU2503613C2 (ru) 2014-01-10
EP2364270A1 (en) 2011-09-14
BRPI0922143A2 (pt) 2016-06-21
CN102239110A (zh) 2011-11-09
BRPI0922143B1 (pt) 2020-10-20
JP2012510427A (ja) 2012-05-10
EP2364270A4 (en) 2013-09-18
CA2744477C (en) 2018-06-12
WO2010065202A1 (en) 2010-06-10
CA2744477A1 (en) 2010-06-10
RU2011127224A (ru) 2013-01-10
EP2364270B1 (en) 2023-01-18
AU2009322861A1 (en) 2011-07-21

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