AU2001246497A1 - Producing liquid crystals with cf2o bond - Google Patents

Producing liquid crystals with cf2o bond

Info

Publication number
AU2001246497A1
AU2001246497A1 AU2001246497A AU4649701A AU2001246497A1 AU 2001246497 A1 AU2001246497 A1 AU 2001246497A1 AU 2001246497 A AU2001246497 A AU 2001246497A AU 4649701 A AU4649701 A AU 4649701A AU 2001246497 A1 AU2001246497 A1 AU 2001246497A1
Authority
AU
Australia
Prior art keywords
cf2o
bond
liquid crystals
producing liquid
bridge
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
AU2001246497A
Inventor
Matthias Bremer
Peer Kirsch
Detlef Pauluth
Andreas Taugerbeck
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Merck Patent GmbH
Original Assignee
Merck Patent GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE2000110537 external-priority patent/DE10010537A1/en
Priority claimed from DE10027102A external-priority patent/DE10027102A1/en
Application filed by Merck Patent GmbH filed Critical Merck Patent GmbH
Publication of AU2001246497A1 publication Critical patent/AU2001246497A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K19/00—Liquid crystal materials
    • C09K19/04—Liquid crystal materials characterised by the chemical structure of the liquid crystal components, e.g. by a specific unit
    • C09K19/06—Non-steroidal liquid crystal compounds
    • C09K19/08—Non-steroidal liquid crystal compounds containing at least two non-condensed rings
    • C09K19/30—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing saturated or unsaturated non-aromatic rings, e.g. cyclohexane rings
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K19/00—Liquid crystal materials
    • C09K19/04—Liquid crystal materials characterised by the chemical structure of the liquid crystal components, e.g. by a specific unit
    • C09K19/06—Non-steroidal liquid crystal compounds
    • C09K19/08—Non-steroidal liquid crystal compounds containing at least two non-condensed rings
    • C09K19/30—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing saturated or unsaturated non-aromatic rings, e.g. cyclohexane rings
    • C09K19/3001—Cyclohexane rings
    • C09K19/3066—Cyclohexane rings in which the rings are linked by a chain containing carbon and oxygen atoms, e.g. esters or ethers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B41/00—Formation or introduction of functional groups containing oxygen
    • C07B41/04—Formation or introduction of functional groups containing oxygen of ether, acetal or ketal groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D339/00—Heterocyclic compounds containing rings having two sulfur atoms as the only ring hetero atoms
    • C07D339/08—Six-membered rings
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K19/00—Liquid crystal materials
    • C09K19/04—Liquid crystal materials characterised by the chemical structure of the liquid crystal components, e.g. by a specific unit
    • C09K19/06—Non-steroidal liquid crystal compounds
    • C09K19/08—Non-steroidal liquid crystal compounds containing at least two non-condensed rings
    • C09K19/30—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing saturated or unsaturated non-aromatic rings, e.g. cyclohexane rings
    • C09K19/3001—Cyclohexane rings
    • C09K19/3003—Compounds containing at least two rings in which the different rings are directly linked (covalent bond)
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K2323/00—Functional layers of liquid crystal optical display excluding electroactive liquid crystal layer characterised by chemical composition

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Heterocyclic Compounds Containing Sulfur Atoms (AREA)
  • Liquid Crystal Substances (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)

Abstract

The invention relates to a process for the preparation of compounds having at least one -CF2O- bridge in the molecule, which comprises initially reacting a bis(alkylthio)carbenium salt with a compound containing at least one hydroxyl group in the presence of a base followed by oxidative fluorination, preferably in situ, with a fluorinating agent and an oxidizing agent to form the compound having at least one -CF2O- bridge in the molecule.
AU2001246497A 2000-03-03 2001-03-02 Producing liquid crystals with cf2o bond Abandoned AU2001246497A1 (en)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
DE10010537 2000-03-03
DE2000110537 DE10010537A1 (en) 2000-03-03 2000-03-03 Production of compounds having at least one -CF2-O- bridge, useful for liquid crystal displays, comprises reaction of a bis(alkylthio)carbenium salt with a hydroxyl group containing compound.
DE10027102A DE10027102A1 (en) 2000-05-31 2000-05-31 Production of compounds having at least one -CF2-O- bridge, useful for liquid crystal displays, comprises reaction of a bis(alkylthio)carbenium salt with a hydroxyl group containing compound.
DE10027102 2000-05-31
PCT/EP2001/002402 WO2001064667A1 (en) 2000-03-03 2001-03-02 Producing liquid crystals with cf2o bond

Publications (1)

Publication Number Publication Date
AU2001246497A1 true AU2001246497A1 (en) 2001-09-12

Family

ID=26004680

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2001246497A Abandoned AU2001246497A1 (en) 2000-03-03 2001-03-02 Producing liquid crystals with cf2o bond

Country Status (11)

Country Link
US (1) US6787062B2 (en)
EP (1) EP1259503B1 (en)
JP (2) JP4132818B2 (en)
KR (1) KR100760562B1 (en)
CN (1) CN100467460C (en)
AT (1) ATE372996T1 (en)
AU (1) AU2001246497A1 (en)
DE (1) DE50113003D1 (en)
HK (1) HK1054040A1 (en)
TW (1) TW538117B (en)
WO (1) WO2001064667A1 (en)

Families Citing this family (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AU2002213983A1 (en) * 2000-10-20 2002-05-06 Merck Patent G.M.B.H Method for producing cyclic carboxylic orthoester fluorides and corresponding compounds
US7105708B2 (en) * 2000-12-12 2006-09-12 Merck Patentgesellschaft Method for producing compounds having a CF2O bridge
DE10065218B4 (en) * 2000-12-27 2014-04-10 Merck Patent Gmbh Preparation of disubstituted tetrafluoroethylene derivatives
JP4972826B2 (en) * 2001-04-10 2012-07-11 Ｊｎｃ株式会社 Difluoroalkoxy-terminated compound, liquid crystal composition, and liquid crystal display device
KR101052420B1 (en) * 2002-12-03 2011-07-29 메르크 파텐트 게엠베하 Method for preparing naphthalene derivative
DE102004021334B4 (en) 2003-05-27 2019-05-16 Merck Patent Gmbh Aldehydes with difluoroxymethylene bridge
JP4379623B2 (en) * 2004-02-02 2009-12-09 ダイキン工業株式会社 Method for producing fluorine-containing unsaturated sulfonyl fluoride
DE102005004055B4 (en) * 2004-02-25 2016-10-20 Merck Patent Gmbh synthesis method
JP5015774B2 (en) 2004-07-29 2012-08-29 メルク パテント ゲゼルシャフト ミット ベシュレンクテル ハフツング Difluoro-substituted heterocyclic compounds and their use as building blocks in liquid crystal media
US8777967B2 (en) * 2005-06-09 2014-07-15 Xlumena, Inc. Methods and devices for anchoring to tissue
DE502007004625D1 (en) * 2006-09-13 2010-09-16 Merck Patent Gmbh Fluorophenyl compounds for liquid crystalline mixtures
WO2009139330A1 (en) 2008-05-15 2009-11-19 チッソ株式会社 Optically isotropic liquid crystalline medium, and optical element
EP2319897B1 (en) 2009-11-04 2012-06-20 Merck Patent GmbH Liquid crystal compounds
CN101735822B (en) * 2009-12-14 2015-04-29 武汉工业学院 Preparation and use of low-temperature low-viscosity liquid crystal compositions
DE102013005820A1 (en) 2012-05-05 2013-11-07 Merck Patent Gmbh New phenol compounds, useful as intermediate for the preparation of polysubstituted benzene compounds
JP5850023B2 (en) * 2012-11-27 2016-02-03 Jnc株式会社 Liquid crystal compound, liquid crystal composition and liquid crystal display element having CF2OCF3 at terminal
CN103058947B (en) * 2012-12-24 2015-07-29 石家庄诚志永华显示材料有限公司 Liquid crystalline cpd containing the sub-methoxyl group bridge of benzoxazole and difluoro and preparation method thereof and application
CN103087038B (en) * 2012-12-24 2015-07-29 石家庄诚志永华显示材料有限公司 Liquid crystalline cpd containing the sub-methoxyl group bridge of benzo 1,3-dioxolane and difluoro
KR101524570B1 (en) * 2013-04-05 2015-06-01 디아이씨 가부시끼가이샤 Method for producing compound
CN103254903B (en) * 2013-04-27 2016-04-06 石家庄诚志永华显示材料有限公司 Liquid crystalline cpd containing difluoro methylene key bridge and preparation method thereof and composition
JP5975081B2 (en) 2013-09-30 2016-08-23 ダイキン工業株式会社 Method for producing fluorine-containing biaryl compound
CN103787845A (en) * 2014-01-21 2014-05-14 石家庄诚志永华显示材料有限公司 Deuterium-substituted difluoro-oxymethane derivative
JP5910776B2 (en) 2014-03-20 2016-04-27 ダイキン工業株式会社 Method for producing compound having oxydifluoromethylene skeleton
CN108251127A (en) * 2014-11-20 2018-07-06 北京八亿时空液晶科技股份有限公司 Liquid crystal compound containing difluoromethoxy bridge bond and application thereof
CN104560060A (en) * 2014-12-16 2015-04-29 石家庄诚志永华显示材料有限公司 Novel liquid crystal medium containing deuterated difluoromethoxy-bridge compound and application thereof
CN104531167B (en) * 2014-12-29 2017-02-22 石家庄诚志永华显示材料有限公司 Liquid crystal medium

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4119639A (en) 1977-06-27 1978-10-10 Mcneil Laboratories, Incorporated Preparation of 5-aroylpyrrole-2-acetic acid derivatives
DE3437935A1 (en) * 1984-10-17 1986-04-24 Merck Patent Gmbh, 6100 Darmstadt HETEROCYCLIC COMPOUNDS
JPS61227563A (en) 1985-03-30 1986-10-09 Nippon Chemiphar Co Ltd Production of tolmetin
JP3287288B2 (en) * 1996-11-22 2002-06-04 チッソ株式会社 Polyhaloalkyl ether derivatives, liquid crystal compositions containing them and liquid crystal display devices

Also Published As

Publication number Publication date
EP1259503A1 (en) 2002-11-27
WO2001064667A1 (en) 2001-09-07
KR20030041857A (en) 2003-05-27
HK1054040A1 (en) 2003-11-14
JP2007262069A (en) 2007-10-11
JP5037999B2 (en) 2012-10-03
TW538117B (en) 2003-06-21
JP2003525286A (en) 2003-08-26
US20030069433A1 (en) 2003-04-10
JP4132818B2 (en) 2008-08-13
DE50113003D1 (en) 2007-10-25
US6787062B2 (en) 2004-09-07
KR100760562B1 (en) 2007-10-04
ATE372996T1 (en) 2007-09-15
EP1259503B1 (en) 2007-09-12
CN100467460C (en) 2009-03-11
CN1411455A (en) 2003-04-16

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