ATE495205T1 - Unter scherwirkung verflüssigbare ethylen/alpha- olefin/dien polymere und ihre herstellung - Google Patents
Unter scherwirkung verflüssigbare ethylen/alpha- olefin/dien polymere und ihre herstellungInfo
- Publication number
- ATE495205T1 ATE495205T1 AT99971431T AT99971431T ATE495205T1 AT E495205 T1 ATE495205 T1 AT E495205T1 AT 99971431 T AT99971431 T AT 99971431T AT 99971431 T AT99971431 T AT 99971431T AT E495205 T1 ATE495205 T1 AT E495205T1
- Authority
- AT
- Austria
- Prior art keywords
- olefin
- ethylene
- fluffilizable
- sheer
- alpha
- Prior art date
Links
Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F210/00—Copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
- C08F210/16—Copolymers of ethene with alpha-alkenes, e.g. EP rubbers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
- C08L23/10—Homopolymers or copolymers of propene
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F10/00—Homopolymers and copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2/00—Processes of polymerisation
- C08F2/44—Polymerisation in the presence of compounding ingredients, e.g. plasticisers, dyestuffs, fillers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F210/00—Copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
- C08F210/16—Copolymers of ethene with alpha-alkenes, e.g. EP rubbers
- C08F210/18—Copolymers of ethene with alpha-alkenes, e.g. EP rubbers with non-conjugated dienes, e.g. EPT rubbers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F4/00—Polymerisation catalysts
- C08F4/42—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors
- C08F4/44—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides
- C08F4/60—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides together with refractory metals, iron group metals, platinum group metals, manganese, rhenium technetium or compounds thereof
- C08F4/62—Refractory metals or compounds thereof
- C08F4/64—Titanium, zirconium, hafnium or compounds thereof
- C08F4/659—Component covered by group C08F4/64 containing a transition metal-carbon bond
- C08F4/6592—Component covered by group C08F4/64 containing a transition metal-carbon bond containing at least one cyclopentadienyl ring, condensed or not, e.g. an indenyl or a fluorenyl ring
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
- C08L23/16—Elastomeric ethene-propene or ethene-propene-diene copolymers, e.g. EPR and EPDM rubbers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F4/00—Polymerisation catalysts
- C08F4/42—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors
- C08F4/44—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides
- C08F4/60—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides together with refractory metals, iron group metals, platinum group metals, manganese, rhenium technetium or compounds thereof
- C08F4/62—Refractory metals or compounds thereof
- C08F4/64—Titanium, zirconium, hafnium or compounds thereof
- C08F4/659—Component covered by group C08F4/64 containing a transition metal-carbon bond
- C08F4/65908—Component covered by group C08F4/64 containing a transition metal-carbon bond in combination with an ionising compound other than alumoxane, e.g. (C6F5)4B-X+
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F4/00—Polymerisation catalysts
- C08F4/42—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors
- C08F4/44—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides
- C08F4/60—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides together with refractory metals, iron group metals, platinum group metals, manganese, rhenium technetium or compounds thereof
- C08F4/62—Refractory metals or compounds thereof
- C08F4/64—Titanium, zirconium, hafnium or compounds thereof
- C08F4/659—Component covered by group C08F4/64 containing a transition metal-carbon bond
- C08F4/65912—Component covered by group C08F4/64 containing a transition metal-carbon bond in combination with an organoaluminium compound
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S526/00—Synthetic resins or natural rubbers -- part of the class 520 series
- Y10S526/903—Monomer polymerized in presence of transition metal containing catalyst and hydrocarbon additive affecting polymer properties of catalyst activity
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S526/00—Synthetic resins or natural rubbers -- part of the class 520 series
- Y10S526/943—Polymerization with metallocene catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)
- Manufacture Of Macromolecular Shaped Articles (AREA)
- Medicinal Preparation (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10656998P | 1998-11-02 | 1998-11-02 | |
| PCT/US1999/025637 WO2000026268A1 (en) | 1998-11-02 | 1999-11-02 | SHEAR THINNING ETHYLENE/α-OLEFIN INTERPOLYMERS AND THEIR PREPARATION |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE495205T1 true ATE495205T1 (de) | 2011-01-15 |
Family
ID=22312137
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT99971431T ATE495205T1 (de) | 1998-11-02 | 1999-11-02 | Unter scherwirkung verflüssigbare ethylen/alpha- olefin/dien polymere und ihre herstellung |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US7750104B2 (de) |
| EP (2) | EP2277928B1 (de) |
| JP (3) | JP5276757B2 (de) |
| KR (1) | KR100623106B1 (de) |
| CN (1) | CN1134467C (de) |
| AT (1) | ATE495205T1 (de) |
| AU (1) | AU1241600A (de) |
| BR (1) | BR9915199B1 (de) |
| CA (1) | CA2347501C (de) |
| DE (1) | DE69943133D1 (de) |
| ES (2) | ES2666708T3 (de) |
| MX (1) | MXPA01004337A (de) |
| WO (1) | WO2000026268A1 (de) |
Families Citing this family (53)
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|---|---|---|---|---|
| US7511104B2 (en) | 2001-06-20 | 2009-03-31 | Exxonmobil Chemical Patents Inc. | Polyolefins made by catalyst comprising a noncoordinating anion and articles comprising them |
| DE50207018D1 (en) * | 2001-06-21 | 2006-07-06 | Habasit Ag | Monolithischer riemen mit ethylen-alpha olefin-copolymeren |
| US7906586B2 (en) * | 2003-12-09 | 2011-03-15 | Dow Global Technologies Llc | Thermoplastic olefinic compositions |
| US20050209403A1 (en) * | 2003-12-09 | 2005-09-22 | Walton Kim L | Thermoplastic olefinic compositions |
| ES2341977T3 (es) * | 2004-06-28 | 2010-06-30 | Dow Global Technologies Inc. | Promotores de adhesion para materiales estratificados multiestructurales. |
| JP5318567B2 (ja) * | 2005-05-12 | 2013-10-16 | ダウ グローバル テクノロジーズ エルエルシー | 光沢の少ない熱成形押出しシート材 |
| JP5225845B2 (ja) | 2005-09-12 | 2013-07-03 | ダウ グローバル テクノロジーズ エルエルシー | エチレン／α−オレフィン組成物から調製された自動車部品 |
| BRPI0520599A2 (pt) | 2005-10-07 | 2009-10-06 | Pirelli & C Spa | poste de serviço, material compósito termoplástico, e, processo para a produção de um poste de serviço |
| BRPI0709467A2 (pt) * | 2006-04-06 | 2011-07-19 | Dow Global Technologies Inc | método para aplicar uma composição termicamente expansìvel e composição poliolefìnica termicamente expansìvel |
| RU2450026C2 (ru) * | 2006-05-17 | 2012-05-10 | ДАУ ГЛОБАЛ ТЕКНОЛОДЖИЗ ЭлЭлСи | Способ полимеризации полиолефинов в растворе |
| DE602007005398D1 (de) * | 2006-11-01 | 2010-04-29 | Dow Global Technologies Inc | Polyurethanzusammensetzungen und daraus hergestellte gegenstände und herstellungsverfahren dafür |
| MX2009006749A (es) | 2006-12-21 | 2009-08-20 | Dow Global Technologies Inc | Composiciones de poliolefina y articulos preparados a partir de las mismas, y metodos para su elaboracion. |
| JP5100342B2 (ja) * | 2007-12-05 | 2012-12-19 | 三井化学株式会社 | ゴム組成物およびその用途 |
| EP2352769B1 (de) * | 2008-11-21 | 2013-05-01 | Dow Global Technologies LLC | Ummantelung mit einem olefinbasiertem polymer für ein mittelspannungskabel |
| CN102482465B (zh) | 2009-07-02 | 2014-04-30 | 陶氏环球技术有限责任公司 | Tpo组合物，制品，和所述组合物制备方法 |
| JP5357643B2 (ja) * | 2009-07-08 | 2013-12-04 | 三井化学株式会社 | ゴム組成物およびその用途 |
| KR101657733B1 (ko) | 2009-07-09 | 2016-09-20 | 어드밴스드 테크놀러지 머티리얼즈, 인코포레이티드 | 라이너 베이스의 저장 시스템, 라이너 및 반도체 공정에 고순도 재료를 공급하는 방법 |
| EP2454317B1 (de) | 2009-07-14 | 2013-05-01 | Dow Global Technologies LLC | Vakuumthermogeformte, extrudierte folie mit verbesserter glanzreduktion |
| BR112012011058B1 (pt) | 2009-11-23 | 2021-06-08 | Dow Global Technologies Llc | composição, filme e artigo |
| US20130203939A1 (en) | 2010-05-21 | 2013-08-08 | Shuwen Peng | Thermoplastic compositions and articles formed from the same |
| EP2576688B1 (de) | 2010-05-27 | 2017-01-18 | Dow Global Technologies LLC | Polymerzusammensetzungen auf ethylenbasis, verfahren zu ihrer herstellung und artikel daraus |
| JP5955839B2 (ja) | 2010-06-22 | 2016-07-20 | ダウ グローバル テクノロジーズ エルエルシー | 架橋組成物およびそれから製造される物品 |
| IT1400743B1 (it) | 2010-06-30 | 2013-07-02 | Dow Global Technologies Inc | Composizioni polimeriche |
| EP2643094A4 (de) | 2010-11-23 | 2017-05-24 | Advanced Technology Materials, Inc. | Spender mit einem inneren behälter |
| US20130252005A1 (en) | 2010-12-10 | 2013-09-26 | Dow Global Technologies Llc | Films with improved coefficient of friction |
| KR101861399B1 (ko) | 2010-12-21 | 2018-05-28 | 다우 글로벌 테크놀로지스 엘엘씨 | 올레핀 기재 중합체 및 분산 중합 |
| BR112013022316A2 (pt) | 2011-03-01 | 2017-05-30 | Advanced Tech Materials | sistema baseado em revestimento interno, e, método para prover um sistema baseado em revestimento interno |
| US9023906B2 (en) | 2011-05-18 | 2015-05-05 | Mitsui Chemicals, Inc. | Propylene-based copolymer, propylene-based copolymer composition, molded product thereof and foamed product thereof, and production process therefor |
| KR101248423B1 (ko) * | 2011-06-09 | 2013-04-02 | 에스케이종합화학 주식회사 | 에틸렌 - α-올레핀 - 디엔 공중합체의 제조방법 |
| BR112014006802B1 (pt) | 2011-09-23 | 2020-11-24 | Dow Global Technologies Llc | composição e artigo |
| EP2751198B1 (de) | 2011-10-10 | 2017-09-13 | Dow Global Technologies LLC | Polymerzusammensetzungen mit verbessertem zurückhalten der eigenschaften unter mechanischen und thermischen spannungen |
| JP6104277B2 (ja) | 2011-12-13 | 2017-03-29 | ダウ グローバル テクノロジーズ エルエルシー | エチレン−プロピレン−ジエン共重合体組成物 |
| JP6153537B2 (ja) * | 2011-12-19 | 2017-06-28 | ダウ グローバル テクノロジーズ エルエルシー | 分散重合で調製したエチレン系ポリマー |
| MX365252B (es) | 2012-05-09 | 2019-05-28 | Sasol Tech Pty Ltd | Separación de componentes de una corriente de hidrocarburo de multicomponente. |
| WO2014046777A1 (en) * | 2012-09-20 | 2014-03-27 | Exxonmobil Chemical Patents Inc. | Modified polyethylene compositions for films |
| US8901236B2 (en) * | 2012-10-09 | 2014-12-02 | Lion Copolymer Geismar, Llc | Process for creating an ethylene elastomer |
| BR112015010919B1 (pt) | 2012-11-30 | 2021-08-17 | Dow Global Technologies Llc | Composição, composição reticulada e artigo |
| SG11201504578XA (en) | 2013-01-18 | 2015-08-28 | Dow Global Technologies Llc | Polymerization processes for high molecular weight polyolefins |
| US9493593B2 (en) | 2013-06-28 | 2016-11-15 | Lg Chem, Ltd. | Elastic diene terpolymer and preparation method thereof |
| KR101585206B1 (ko) * | 2013-07-22 | 2016-01-13 | 주식회사 엘지화학 | 디엔을 포함하는 3원계 탄성 공중합체 및 이의 제조 방법 |
| KR101585204B1 (ko) | 2013-06-28 | 2016-01-13 | 주식회사 엘지화학 | 디엔을 포함하는 3원계 탄성 공중합체 및 이의 제조 방법 |
| US9650460B2 (en) | 2013-06-28 | 2017-05-16 | Lg Chem, Ltd. | Elastic diene terpolymer and preparation method thereof |
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| BR112018077391B1 (pt) | 2016-06-30 | 2023-01-03 | Dow Global Technologies Llc. | Composição, composição reticulada e artigo |
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| JP7381449B2 (ja) | 2017-08-24 | 2023-11-15 | ダウ グローバル テクノロジーズ エルエルシー | エチレン／ｃ５－ｃ１０アルファ－オレフィン／ポリエチレンインターポリマー |
| CN111492004A (zh) | 2017-08-30 | 2020-08-04 | 陶氏环球技术有限责任公司 | 用于未铺地毯地板的热塑性聚烯烃 |
| KR20200120688A (ko) | 2018-02-14 | 2020-10-21 | 다우 글로벌 테크놀로지스 엘엘씨 | 지속적 고온 내성이 개선된 에틸렌/알파-올레핀 혼성중합체 조성물 |
| US11970602B2 (en) | 2018-02-14 | 2024-04-30 | Dow Global Technologies Llc | Ethylene/alpha-olefin interpolymer compositions with improved long term heat aging performance |
| KR102520418B1 (ko) | 2018-02-14 | 2023-04-11 | 다우 글로벌 테크놀로지스 엘엘씨 | 지속적 고온 내열성이 개선된 에틸렌/알파-올레핀 혼성중합체 조성물 |
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1999
- 1999-11-02 JP JP2000579651A patent/JP5276757B2/ja not_active Expired - Lifetime
- 1999-11-02 CN CNB99815105XA patent/CN1134467C/zh not_active Expired - Lifetime
- 1999-11-02 EP EP10184006.4A patent/EP2277928B1/de not_active Expired - Lifetime
- 1999-11-02 EP EP99971431A patent/EP1159320B1/de not_active Expired - Lifetime
- 1999-11-02 DE DE69943133T patent/DE69943133D1/de not_active Expired - Lifetime
- 1999-11-02 MX MXPA01004337A patent/MXPA01004337A/es active IP Right Grant
- 1999-11-02 AU AU12416/00A patent/AU1241600A/en not_active Abandoned
- 1999-11-02 ES ES10184006.4T patent/ES2666708T3/es not_active Expired - Lifetime
- 1999-11-02 WO PCT/US1999/025637 patent/WO2000026268A1/en active IP Right Grant
- 1999-11-02 ES ES99971431T patent/ES2356612T3/es not_active Expired - Lifetime
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- 1999-11-02 AT AT99971431T patent/ATE495205T1/de not_active IP Right Cessation
- 1999-11-02 KR KR1020017005415A patent/KR100623106B1/ko active IP Right Grant
- 1999-11-02 BR BRPI9915199-5A patent/BR9915199B1/pt not_active IP Right Cessation
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Also Published As
| Publication number | Publication date |
|---|---|
| ES2666708T3 (es) | 2018-05-07 |
| US20070203314A1 (en) | 2007-08-30 |
| CN1134467C (zh) | 2004-01-14 |
| CA2347501A1 (en) | 2000-05-11 |
| BR9915199B1 (pt) | 2010-09-08 |
| JP2014145082A (ja) | 2014-08-14 |
| EP2277928A1 (de) | 2011-01-26 |
| EP1159320A1 (de) | 2001-12-05 |
| KR20010080925A (ko) | 2001-08-25 |
| JP2012136706A (ja) | 2012-07-19 |
| BR9915199A (pt) | 2001-12-04 |
| CN1332755A (zh) | 2002-01-23 |
| KR100623106B1 (ko) | 2006-09-13 |
| CA2347501C (en) | 2010-03-23 |
| EP2277928B1 (de) | 2018-02-21 |
| MXPA01004337A (es) | 2002-04-24 |
| JP2002528610A (ja) | 2002-09-03 |
| ES2356612T3 (es) | 2011-04-11 |
| JP5276757B2 (ja) | 2013-08-28 |
| AU1241600A (en) | 2000-05-22 |
| EP1159320B1 (de) | 2011-01-12 |
| WO2000026268A1 (en) | 2000-05-11 |
| JP6117143B2 (ja) | 2017-04-19 |
| JP6039906B2 (ja) | 2016-12-07 |
| DE69943133D1 (de) | 2011-02-24 |
| US7750104B2 (en) | 2010-07-06 |
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