WO2023184618A1 - Cigarette insertion strip and preparation method therefor - Google Patents

Cigarette insertion strip and preparation method therefor Download PDF

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Publication number
WO2023184618A1
WO2023184618A1 PCT/CN2022/087649 CN2022087649W WO2023184618A1 WO 2023184618 A1 WO2023184618 A1 WO 2023184618A1 CN 2022087649 W CN2022087649 W CN 2022087649W WO 2023184618 A1 WO2023184618 A1 WO 2023184618A1
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WO
WIPO (PCT)
Prior art keywords
cigarette
plant tissue
cuttings
cannabis
base material
Prior art date
Application number
PCT/CN2022/087649
Other languages
French (fr)
Chinese (zh)
Inventor
佟欣洋
熊伟
李涛
刘美洲
Original Assignee
昆明百泓健康产业有限公司
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Filing date
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Publication of WO2023184618A1 publication Critical patent/WO2023184618A1/en

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Classifications

    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00—Cigars; Cigarettes
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00—Cigars; Cigarettes
    • A24D1/18—Selection of materials, other than tobacco, suitable for smoking
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00—Medicinal preparations containing organic active ingredients
    • A61K31/045—Hydroxy compounds, e.g. alcohols; Salts thereof, e.g. alcoholates
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00—Medicinal preparations containing organic active ingredients
    • A61K31/33—Heterocyclic compounds
    • A61K31/335—Heterocyclic compounds having oxygen as the only ring hetero atom, e.g. fungichromin
    • A61K31/35—Heterocyclic compounds having oxygen as the only ring hetero atom, e.g. fungichromin having six-membered rings with one oxygen as the only ring hetero atom
    • A61K31/352—Heterocyclic compounds having oxygen as the only ring hetero atom, e.g. fungichromin having six-membered rings with one oxygen as the only ring hetero atom condensed with carbocyclic rings, e.g. methantheline 
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form

Definitions

  • the present application relates to the field of tobacco technology, and in particular to a cigarette cutting and a preparation method thereof.
  • Cannabidiol (CBD) and other cannabinoids extracted from the flowers and leaves of industrial hemp are the main chemical components of industrial hemp and are also non-addictive components. They have anti-spasmodic, anti-anxiety, and anti-inflammatory pharmacological effects. , not only can be used in the treatment of many difficult diseases.
  • Cannabinoids are also added to cigarettes on the market.
  • the usual method of adding cannabinoids is to grind the flowers and leaves of cannabis and mix them with the shredded tobacco of cigarettes.
  • the flowers and leaves after the grinding process are in the form of small fragments, which cannot be mixed well with conventional cigarette tobacco, and fragments will appear during the blending process. It falls along the gaps in the cut tobacco, and during the use of the finished cigarettes, mosaic and leaf fragments will fall off, which is often referred to as "turning around” and "slag falling".
  • the second is that the small amount of cannabinoids contained in the flowers and leaves is insufficient.
  • this application provides a cigarette insert and a preparation method thereof.
  • the cannabinoids in the cigarette insert are evenly distributed, so that after the cigarette insert and cigarette are lit together, the user can better feel the natural nature of the cannabinoids in the cigarette insert. Release effect.
  • this application provides a cigarette insert, which contains active ingredients and a base material.
  • the active ingredients include cannabinoids; the mass ratio of the cannabinoids in the cigarette inserts is 0.1 % ⁇ 70%.
  • the active ingredient includes cannabis extract and/or cannabis plant tissue, and the cannabis extract and/or cannabis plant tissue contains cannabinoids.
  • the cannabis plant tissue includes cannabis leaves and/or cannabis flowers.
  • the cannabinoid is cannabidiol and/or other isomers.
  • the cigarette insert has at least one of the following characteristics:
  • the mass ratio of the base material to the active ingredient is 10: (1-50);
  • the base material includes green tea plant tissue, black tea plant tissue, mint plant tissue, lotus leaf plant tissue, chrysanthemum plant tissue, licorice plant tissue, kudzu plant tissue, tree moss plant tissue, At least one of Phyllanthus emblica plant tissue, rose plant tissue, and lavender plant tissue.
  • the cigarette insert has at least one of the following characteristics:
  • the cigarette insert is formed by molding and/or screw pressing equipment
  • the cross-sectional shape of the cigarette insert is circular and/or polygonal
  • the length of the cigarette cuttings is 1cm to 7cm;
  • the width of the cigarette insert is 1 mm to 3 mm;
  • the density of the cigarette cuttings is 0.1g/cm 3 to 3.5g/cm 3 ;
  • the hardness of the cigarette cuttings is 38HD to 80HD.
  • the present application provides a method for preparing cigarette inserts.
  • the preparation method includes:
  • the base material raw materials are ground and sieved and then mixed with the active ingredients to obtain mixed powder;
  • the mixed wet materials are shaped to obtain cigarette inserts.
  • the preparation method can also be:
  • the base material raw materials are ground and screened to obtain base material raw material powder
  • the base material is wet-formed and the active ingredients are sprayed to obtain cigarette cuttings.
  • the preparation method has at least one of the following characteristics:
  • the substrate raw materials include green tea plant tissue, black tea plant tissue, mint plant tissue, lotus leaf plant tissue, chrysanthemum plant tissue, licorice plant tissue, kudzu plant tissue, and tree moss plant tissue. , at least one of amla plant tissue, rose plant tissue, and lavender plant tissue;
  • the particle size of the base material raw material after screening is 300 mesh to 500 mesh
  • the active ingredients include cannabis extract and/or cannabis plant tissue, and the cannabis extract and/or cannabis plant tissue contain cannabinoids;
  • the cannabis plant tissue includes cannabis leaves and/or cannabis flowers
  • the cannabinoid is cannabidiol and/or other isomers
  • the binder includes water, ethanol, guar gum, starch gum, chitosan, carboxymethylcellulose, pectin, gum arabic, sodium alginate, gelatin, glucose, polypropylene alcohol and fructose. at least one of;
  • the molding method includes mold molding and/or screw layering equipment press molding
  • the mass proportion of the cannabinoid in the cigarette cuttings is 0.1% to 70%.
  • the preparation method has at least one of the following characteristics:
  • the cross-sectional shape of the cigarette insert is circular and/or polygonal
  • the length of the cigarette cuttings is 1cm to 7cm;
  • the width of the cigarette insert is 1 mm to 3 mm;
  • the density of the cigarette cuttings is 0.1g/cm 3 to 3.5g/cm 3 ;
  • the hardness of the cigarette cuttings is 38HD to 80HD.
  • the cigarette inserts provided by this application can achieve a uniform distribution of cannabinoids in a mass proportion of 0.1% to 70% in the cigarette inserts by adding active ingredients to the base material, so that after the cigarette inserts and cigarettes are ignited together, the user You can better feel the effect of the natural release of cannabinoids in cigarette cuttings and improve the user experience.
  • Cannabidiol (CBD) and other cannabinoids extracted from the flowers and leaves of industrial hemp are the main chemical components of industrial hemp and are also non-addictive components. They have anti-spasmodic, anti-anxiety, and anti-inflammatory pharmacological effects. , not only can be used in the treatment of many difficult diseases.
  • Cannabinoids are also added to cigarettes on the market.
  • the usual method of adding cannabinoids is to grind the flowers and leaves of cannabis and mix them with the shredded tobacco of cigarettes.
  • the flowers and leaves after the grinding process are in the form of small fragments, which cannot be mixed well with conventional cigarette tobacco, and fragments will appear during the blending process. It falls along the gaps in the cut tobacco, and during the use of the finished cigarettes, mosaic and leaf fragments will fall off, which is often referred to as "turning around” and "slag falling".
  • the second is that the small amount of cannabinoids contained in the flowers and leaves is insufficient.
  • this application provides a cigarette insert, which contains active ingredients and a base material.
  • the active ingredients include cannabinoids; the mass proportion of cannabinoids in the cigarette inserts is 0.1% to 70%.
  • the cigarette cuttings can achieve a uniform distribution of cannabinoids in a mass proportion of 0.1% to 70% in the cigarette cuttings, so that after the cigarette cuttings and cigarettes are lit together, the user can Better feel the effect of natural release of cannabinoids in cigarette cuttings and improve user experience.
  • cannabinoids in this application are cannabidiol and/or other isomers, that is, the cannabinoids in cigarette cuttings can all be cannabidiol, or all cannabinoid isomers, or they can also A mixture of cannabidiol and other cannabinoid isomers.
  • the type of cannabinoids can be selected according to actual needs and is not limited here.
  • the active ingredients are at least part of the tissues of the cannabis plant and/or an extract extracted from the cannabis plant.
  • the cannabis plant tissue includes cannabis leaves and/or cannabis flowers, that is, the active ingredients may only include cannabis flowers and leaves. , or may include only cannabis extract, but may also be a mixture of cannabis flowers and leaves with cannabis extract, such that the cannabis extract and/or cannabis plant tissue provides the cannabinoids within the cigarette cutting.
  • hemp flowers and/or hemp leaves of industrial hemp with higher cannabinoid content can be selected, and compared with grinding hemp flowers and/or hemp leaves and mixing them with tobacco , directly using cigarette cuttings made from cannabis flowers and/or cannabis leaves, so that the quality proportion of cannabinoids in the prepared cigarette cuttings can meet the requirements.
  • the active ingredient consists solely of an extract of cannabis
  • the cannabis extract contains higher levels of cannabinoids than if the cannabis flowers and/or leaves were used directly.
  • the active ingredient is a mixture of cannabis flowers and leaves and an extract, if the cannabis flowers and/or leaves contain less cannabinoids, when mixed with the cannabis extract, the cannabinoid content in the cigarette cuttings can be increased.
  • the composition of the active ingredients can be selected according to actual needs and is not limited here.
  • cannabis extracts and/or cannabis plant tissues also contain other components in addition to cannabinoids, in order to ensure that users can better feel the effect of the natural release of cannabinoids in cigarette inserts, cannabinoids are added to the cigarette inserts.
  • the mass proportion of cannabinoids in the cigarette cuttings is 0.1% to 70%.
  • the mass proportion of cannabinoids in the cigarette cuttings can be 0.1%, 10%, 20%, 30%, 40%, 50%, 60%. %, 70%, etc. If the cannabinoid content is too low, when used with cigarettes, the cigarette cuttings will release less cannabinoids and the user experience will be reduced; if the cannabinoid content is too high, the preparation cost will increase accordingly.
  • the mass proportion of cannabinoids in cigarette cuttings can be selected according to actual needs, and is not limited here.
  • the base material is an additive material with a certain flavor. Adding it to the cigarette insert can adjust the taste of the cigarette insert and remove part of the spicy taste of the cigarette tobacco.
  • the substrates used in this application include green tea plant tissue, black tea plant tissue, mint plant tissue, lotus leaf plant tissue, chrysanthemum plant tissue, licorice plant tissue, kudzu plant tissue, tree moss plant tissue, etc. At least one of the plant tissue of Ganzi, the plant tissue of rose, and the plant tissue of lavender, wherein the base plant tissue can be mosaics and leaves, etc.
  • the type of base material can be selected according to actual needs and is not limited here.
  • the mass ratio of the base material and the active ingredient in the cigarette insert is 10: (1-50). Specifically, the mass ratio of the base material and the active ingredient can be 5:1, 10:3, 2:1, 5: 3. 1:1, 1:2, 1:3, 1:4, 1:5, etc.
  • the base material and the active ingredients are combined to prepare cigarette cuttings, and the base material serves as a carrier for the active ingredients to adhere. If the mass ratio of the base material to the active ingredients is too large, that is, the amount of base material used in the cigarette cuttings is large and the amount of active ingredients used is small, the taste of the cigarette cuttings will be improved, but the release amount of cannabinoids will not reach the required level.
  • the mass ratio of the base material to the active ingredients is too small, that is, the amount of base material used in the cigarette inserts becomes smaller and the amount of active ingredients used is large, the release amount of cannabinoids in the cigarette inserts meets the required requirements, but the preparation cost increases, and the taste of cigarette cuttings becomes worse, affecting the user experience.
  • the mass ratio of the base material to the active ingredient can be selected according to actual needs and is not limited here.
  • cigarette inserts of a specific shape can be obtained through mold molding and/or screw pressing equipment.
  • the cross-sectional shape of the cigarette inserts is circular.
  • the cross-sectional shape of the cigarette insert can be selected according to actual needs, and is not limited here.
  • the length of the cigarette inserts is 1cm ⁇ 7cm
  • the width of the cigarette inserts is 1mm ⁇ 3mm.
  • the length of the cigarette inserts can be 1cm, 2cm, 3cm, 4cm, 5cm, 6cm, 7cm, etc.
  • the cigarette The width of the inserts can be 1mm, 1.3mm, 1.6mm, 1.9mm, 2.2mm, 2.5mm, 2.8mm, 3mm, etc.
  • the length or width of the cigarette insert is too long, it will be difficult to match different types of cigarettes, and the preparation cost will increase; if the cigarette If the length or width of the cutting is too short, the volume of the cigarette cutting will become smaller, and if it is used too quickly, the user experience will be reduced.
  • the length and width of the cigarette inserts can be selected according to actual needs and are not limited here.
  • the hardness of cigarette inserts is 38HD ⁇ 80HD.
  • the hardness of cigarette inserts can be 38HD, 40HD, 50HD, 60HD, 65HD, 70HD, 80HD, etc.
  • the cigarette insert needs to have a certain hardness to prevent the cigarette insert from breaking during the insertion process. If the hardness of the cigarette insert is too small, the cigarette insert will easily break during the insertion of shredded tobacco, affecting the user experience; if the hardness of the cigarette insert is too large, the preparation cost will increase.
  • the hardness of the cigarette inserts can be selected according to actual needs and is not limited here.
  • the density of the cigarette inserts needs to be controlled so that the cigarette inserts can better contact with the air and the combustion process is more stable.
  • the density of the cigarette inserts provided in this application is 0.1g/ cm 3 ⁇ 3.5g/cm 3
  • the density of cigarette cuttings can be 0.1g/cm 3 , 0.3g/cm 3 , 0.5g/cm 3 , 1g/cm 3 , 1.5g/cm 3 , 2g/cm 3 , 3.5g/cm 3 etc.
  • the density of the cigarette inserts is too small, that is, the degree of compaction is not enough, the cigarette inserts are easily broken during use; if the density of the cigarette inserts is too high, that is, The density of cigarette cuttings is too high, and the cannabinoids in the cigarette cuttings cannot be fully released during use, which affects the user experience.
  • the density of cigarette cuttings can be selected according to actual needs and is not limited here.
  • this application provides a method for preparing cigarette inserts.
  • the preparation method includes:
  • Step S10 Grind and sieve the base material raw materials and mix them with the active ingredients to obtain mixed powder;
  • Step S20 in a vacuum environment, add a binder to the mixed powder and stir evenly to obtain a mixed wet material;
  • Step S30 mold the mixed wet material to obtain a cigarette insert.
  • the preparation method can also be: grinding and screening the base material raw materials to obtain the base material raw material powder; in a vacuum environment, Add an adhesive to the base material powder and stir evenly to obtain a wet base material; then shape the wet base material and spray the active ingredients to obtain a cigarette insert.
  • the active ingredients are attached to the outer surface of the base material by spraying, and the cigarette cuttings are ignited together with the cigarette, the active ingredients are released more quickly, improving the user experience.
  • This preparation method is suitable for cannabinoids. Cigarette cuttings with an added amount of ⁇ 10%.
  • the active ingredients When the active ingredients are doped into the base material, the active ingredients are evenly distributed in the base material. After the cigarette cuttings are ignited with the cigarette, the active ingredients are released more evenly.
  • This preparation method is suitable for any range of cannabinoids. Added amount of cigarette cuttings.
  • the method of attaching the active ingredients to the base material can be selected according to actual needs, and is not limited here.
  • the active ingredient mixed with the base material is cannabinoids, and the cannabinoids are cannabidiol and/or other isomers. That is, the cannabinoids in the cigarette cuttings can be all cannabidiol, or all cannabinoids. Isomers can also be mixtures of cannabidiol and other cannabinoid isomers. The type of cannabinoids can be selected according to actual needs and is not limited here.
  • the substrate raw materials include green tea plant tissue, black tea plant tissue, mint plant tissue, lotus leaf plant tissue, chrysanthemum plant tissue, licorice plant tissue, kudzu plant tissue, and tree moss plant tissue. , at least one of amla plant tissue, rose plant tissue, and lavender plant tissue. For example, mix two types of green tea and mint, or mix three types of mint, licorice, and lotus leaves, then grind them into powder and sieve.
  • the particle size of the base material powder obtained by screening is 300 mesh to 500 mesh.
  • the particle size can be 300 mesh, 320 mesh, 340 mesh, 360 mesh, 380 mesh, 400 mesh, 420 mesh. mesh, 440 mesh, 460 mesh, 480 mesh, 500 mesh, etc.
  • the particle size of the base material raw materials is within this range, and the base material raw materials can be better mixed with the active ingredients.
  • the particle size of the base material raw material can be specifically selected according to actual needs, and is not limited here.
  • the active ingredients mixed with the base material are at least part of the tissues of the cannabis plant and/or an extract extracted from the cannabis plant.
  • the cannabis plant tissue includes cannabis leaves and/or cannabis flowers, that is, the active ingredients may only include cannabis flowers and leaves. , or may include only cannabis extract, but may also be a mixture of cannabis flowers and leaves with cannabis extract, such that the cannabis extract and/or cannabis plant tissue provides the cannabinoids within the cigarette cutting.
  • hemp flowers and/or hemp leaves of industrial hemp with higher cannabinoid content can be selected, and compared with grinding hemp flowers and/or hemp leaves and mixing them with tobacco , directly using cigarette cuttings made from cannabis flowers and/or cannabis leaves, so that the quality proportion of cannabinoids in the prepared cigarette cuttings can meet the requirements.
  • the active ingredient consists solely of an extract of cannabis
  • the cannabis extract contains higher levels of cannabinoids than if the cannabis flowers and/or leaves were used directly.
  • the active ingredient is a mixture of cannabis flowers and leaves and an extract, if the cannabis flowers and/or leaves contain less cannabinoids, when mixed with the cannabis extract, the cannabinoid content in the cigarette cuttings can be increased.
  • the composition of the active ingredients can be selected according to actual needs and is not limited here.
  • the mass ratio of the base material raw material to the active ingredient is 10: (1-50). Specifically, the mass ratio of the base material raw material to the active ingredient can be 5:1, 10:3, 2:1, 5:3, 1:1, 1:2, 1:3, 1:4, 1:5, etc. Cigarette cuttings are produced after the base material raw material and the active ingredients are combined, and the base material raw material serves as a carrier for the active ingredients to adhere. If the mass ratio of the base material to the active ingredients is too large, that is, the amount of base material used in the cigarette inserts is large and the amount of active ingredients used is small, the taste of the cigarette inserts will be improved, but the release of cannabinoids will not reach the desired level.
  • the required requirements if the mass ratio of the base material to the active ingredient is too small, that is, the amount of base material used in the cigarette cuttings becomes smaller and the amount of active ingredients used is large, the release amount of cannabinoids in the cigarette cuttings meets the required requirements. , but the preparation cost increases, and the taste of cigarette cuttings becomes worse, affecting the user experience.
  • the mass ratio of base material raw materials and active ingredients can be selected according to actual needs, and is not limited here.
  • the base material raw materials and the active ingredients are added into the same container, and a stirring device is used to fully mix the base material raw materials and the active ingredients evenly to obtain a mixed powder.
  • a binder is added to the mixed powder obtained in step S10 in a vacuum equipment, where the binder includes water, ethanol, guar gum, starch gum, chitosan, carboxymethylcellulose, and pectin. , acacia gum, sodium alginate, gelatin, glucose, polypropylene alcohol and at least one fructose.
  • the adhesive used in this application is an aqueous solution containing 1% sodium carboxymethyl cellulose. After the dispersed mixed powder is bonded together by an adhesive, stir it with a stirring device for 25 to 40 minutes to obtain a uniformly mixed wet material.
  • step S30 the wet material obtained in step S20 is pressed and formed through mold forming and/or screw layering equipment.
  • mold forming refers to laying the wet material in the insert mold, and applying vertical pressure to the wet material through hydraulic equipment to obtain a cigarette insert with a certain density, and then taking the cigarette insert from the mold. down and trim the edges.
  • Pressing and forming of screw layering equipment means placing the wet material in a layering container with a specific shape of the outlet.
  • the driving device drives the drive frame to rotate.
  • the drive frame drives the screw to rotate, stirs and passes the wet material through the specific shape of the outlet. Press out to get cigarette cuttings.
  • step S40 is also included, in which the obtained cigarette cuttings are transported to a sterile environment to be naturally dried.
  • the cross-sectional shape of the cigarette insert is circular and/or polygonal, such as square, regular pentagon, etc.
  • the cross-sectional shape of the cigarette insert can be selected according to actual needs, and is not limited here.
  • the length of the cigarette inserts is 1cm ⁇ 7cm
  • the width of the cigarette inserts is 1mm ⁇ 3mm.
  • the length of the cigarette inserts can be 1cm, 2cm, 3cm, 4cm, 5cm, 6cm, 7cm, etc.
  • the cigarette The width of the inserts can be 1mm, 1.3mm, 1.6mm, 1.9mm, 2.2mm, 2.5mm, 2.8mm, 3mm, etc.
  • the length or width of the cigarette insert is too long, it will be difficult to match different types of cigarettes, and the preparation cost will increase; if the cigarette If the length or width of the cutting is too short, the volume of the cigarette cutting will become smaller, and if it is used too quickly, the user experience will be reduced.
  • the length and width of the cigarette inserts can be selected according to actual needs and are not limited here.
  • the hardness of cigarette inserts is 38HD ⁇ 80HD.
  • the hardness of cigarette inserts can be 38HD, 40HD, 50HD, 60HD, 65HD, 70HD, 80HD, etc.
  • the cigarette insert needs to have a certain hardness to prevent the cigarette insert from breaking during the insertion process. If the hardness of the cigarette insert is too small, the cigarette insert will easily break during the insertion of shredded tobacco, affecting the user experience; if the hardness of the cigarette insert is too large, the preparation cost will increase.
  • the hardness of the cigarette inserts can be selected according to actual needs and is not limited here.
  • the density of cigarette cuttings is 0.1g/cm 3 ⁇ 3.5g/cm 3 .
  • the density of cigarette cuttings can be 0.1g/cm 3 , 0.3g/cm 3 , 0.5g/cm 3 , 1g/ cm 3 , 1.5g/cm 3 , 2g/cm 3 , 3.5g/cm 3 etc.
  • the density of the cigarette inserts is too small, that is, the degree of compaction is not enough, the cigarette inserts are easily broken during use; if the density of the cigarette inserts is too high, that is, the cigarette inserts are The density is too high, and the cannabinoids in the cigarette cuttings cannot be fully released during use, affecting the user experience.
  • the density of cigarette cuttings can be selected according to actual needs and is not limited here.
  • the mass proportion of cannabinoids in cigarette cuttings is 0.1% to 70%.
  • the mass proportion of cannabinoids in cigarette cuttings can be 0.1%, 10%, 20%, 30%, 40%. , 50%, 60%, 70%, etc. If the cannabinoid content is too low, when used with cigarettes, the cigarette cuttings will release less cannabinoids and the user experience will be reduced; if the cannabinoid content is too high, the preparation cost will increase accordingly.
  • the mass proportion of cannabinoids in cigarette cuttings can be selected according to actual needs, and is not limited here.
  • the mass proportion of cannabidiol in the cigarette cuttings prepared in Example 1 is 35%, and the density of the cigarette cuttings is 0.64g/cm 3 .
  • the mass proportion of cannabidiol in the cigarette cuttings prepared in Example 2 is 10%, and the density of the cigarette cuttings is 0.77g/cm 3 .
  • the mass proportion of cannabidiol in the cigarette cuttings prepared in Example 3 is 70%, and the density of the cigarette cuttings is 0.55g/cm 3 .
  • the mass proportion of cannabidiol in the cigarette cuttings prepared in Example 4 is 99%, and the density of the cigarette cuttings is 0.43g/cm 3 .
  • the mass proportion of cannabidiol in the cigarette cuttings prepared in Example 5 is 0.35%, and the density of the cigarette cuttings is 1.12g/cm 3 .
  • the mass proportion of cannabidiol in the cigarette cuttings prepared in Example 6 is 1%, and the density of the cigarette cuttings is 0.76g/cm 3 .
  • the mass proportion of cannabidiol in the cigarette cuttings prepared in Example 7 is 35%, and the density of the cigarette cuttings is 0.32g/cm 3 .
  • the mass proportion of cannabidiol in the cigarette cuttings prepared in Example 8 is 35%, and the density of the cigarette cuttings is 1.3g/cm 3 .
  • the mass proportion of cannabidiol in the cigarette cuttings prepared in Example 9 is 10%, and the density of the cigarette cuttings is 0.8g/cm 3 .
  • the cannabis mosaics and leaves are ground and mixed with conventional cut tobacco to prepare cigarettes; the mass proportion of cannabis mosaics and leaves is 33%.
  • the cigarette cuttings prepared in Comparative Example 1 contained a mass content of cannabidiol of 0.33%.
  • Example 1 Comparative Example 1 that when cigarette inserts are used in conjunction with cigarettes, the cigarette inserts contain higher cannabinoid content and can be released evenly, resulting in a better user experience.

Abstract

The present invention relates to a cigarette insertion strip and a preparation method therefor. The cigarette insertion strip comprises effective components and a base material; the effective components contain a cannabinoid; and the mass ratio of the cannabinoid in the cigarette insertion strip is 0.1%-70%. By adding the effective components, such as the cannabinoid, into the base material, the uniform distribution of the cannabinoid having the mass ratio of 0.1%-70% in the cigarette insertion strip can be realized, so that after the cigarette insertion strip and a cigarette are ignited together, a user can better feel the natural release effect of the cannabinoid in the cigarette insertion strip, and the user experience is improved.

Description

卷烟插条及其制备方法Cigarette cuttings and preparation method thereof
本申请要求于2022年03月31日提交中国专利局，申请号为2022103446536，申请名称为“卷烟插条及其制备方法”的中国专利申请的优先权，其全部内容通过引用结合在本申请中。This application claims priority to the Chinese patent application submitted to the China Patent Office on March 31, 2022, with the application number 2022103446536 and the application name "Cigarette Inserts and Preparation Methods", the entire content of which is incorporated into this application by reference. .
技术领域Technical field
本申请涉及烟草技术领域，尤其涉及一种卷烟插条及其制备方法。The present application relates to the field of tobacco technology, and in particular to a cigarette cutting and a preparation method thereof.
背景技术Background technique
利用种植工业***花叶所提取出来的***二酚(Cannabidiol，简称CBD)等***素，是工业***中的主要化学成分，也是非成瘾成分，具有抗痉挛、抗焦虑、抗炎的药理作用，不仅可以作用于多种疑难疾病的治疗。Cannabidiol (CBD) and other cannabinoids extracted from the flowers and leaves of industrial hemp are the main chemical components of industrial hemp and are also non-addictive components. They have anti-spasmodic, anti-anxiety, and anti-inflammatory pharmacological effects. , not only can be used in the treatment of many difficult diseases.
市面上的卷烟中也添加有***素，通常的添加方式为将***的花叶磨碎后与卷烟的烟丝混合。但采用此种添加方式时，因为***花叶的特殊形状和物理特性，经过磨碎工艺后的花叶为细小碎片状，与常规的卷烟烟丝无法很好混合，在掺配过程中会出现碎片顺着烟丝的空隙掉落，并且在成品卷烟使用过程中会存在花叶碎片掉落，也就是常说的“掉头”“落渣”等问题。其次就是少量的花叶所负载的***素含量不足，如果增加***花叶的掺配量又会导致卷烟无法卷接的问题。因此，优化***素的添加工艺，使得卷烟在燃烧过程中***素可均匀释放是本领域技术人员亟待解决的问题。Cannabinoids are also added to cigarettes on the market. The usual method of adding cannabinoids is to grind the flowers and leaves of cannabis and mix them with the shredded tobacco of cigarettes. However, when this addition method is used, due to the special shape and physical properties of cannabis flowers and leaves, the flowers and leaves after the grinding process are in the form of small fragments, which cannot be mixed well with conventional cigarette tobacco, and fragments will appear during the blending process. It falls along the gaps in the cut tobacco, and during the use of the finished cigarettes, mosaic and leaf fragments will fall off, which is often referred to as "turning around" and "slag falling". The second is that the small amount of cannabinoids contained in the flowers and leaves is insufficient. If the blending amount of cannabis flowers and leaves is increased, it will lead to the problem that the cigarette cannot be rolled. Therefore, optimizing the cannabinoid addition process so that cannabinoids can be released evenly during the burning process of cigarettes is an urgent problem that needs to be solved by those skilled in the art.
申请内容Application content
鉴于此，本申请提供一种卷烟插条及其制备方法，卷烟插条中的***素分布均匀，使得卷烟插条与卷烟配合点燃后，使用者可以更好的感受卷烟插条中***素自然释放的效果。In view of this, this application provides a cigarette insert and a preparation method thereof. The cannabinoids in the cigarette insert are evenly distributed, so that after the cigarette insert and cigarette are lit together, the user can better feel the natural nature of the cannabinoids in the cigarette insert. Release effect.
第一方面，本申请提供一种卷烟插条，所述卷烟插条包含有效成分及基材，所述有效成分包含***素；所述***素在所述卷烟插条中的质量占比为0.1％～70％。In a first aspect, this application provides a cigarette insert, which contains active ingredients and a base material. The active ingredients include cannabinoids; the mass ratio of the cannabinoids in the cigarette inserts is 0.1 %~70%.
在可行的实施方式中，所述有效成分包括***提取物和/或***植物体组织，所述***提取物和/或***植物体组织包含***素。In a feasible embodiment, the active ingredient includes cannabis extract and/or cannabis plant tissue, and the cannabis extract and/or cannabis plant tissue contains cannabinoids.
在可行的实施方式中，所述***植物体组织包括***叶和/或***花。In a feasible embodiment, the cannabis plant tissue includes cannabis leaves and/or cannabis flowers.
在可行的实施方式中，所述***素为***二酚和/或其他异构体。In feasible embodiments, the cannabinoid is cannabidiol and/or other isomers.
在可行的实施方式中，所述卷烟插条具有如下特征中的至少一者：In a feasible implementation, the cigarette insert has at least one of the following characteristics:
(1)所述基材与所述有效成分的质量比为10：(1～50)；(1) The mass ratio of the base material to the active ingredient is 10: (1-50);
(2)所述基材包括绿茶植物体组织、红茶植物体组织、薄荷植物体组织、荷叶植物体组织、菊花植物体组织、甘草植物体组织、葛根植物体组织、树苔植物体组织、余甘子植物体组织、玫瑰植物体组织、薰衣草植物体组织中的至少一种。(2) The base material includes green tea plant tissue, black tea plant tissue, mint plant tissue, lotus leaf plant tissue, chrysanthemum plant tissue, licorice plant tissue, kudzu plant tissue, tree moss plant tissue, At least one of Phyllanthus emblica plant tissue, rose plant tissue, and lavender plant tissue.
在可行的实施方式中，所述卷烟插条具有如下特征中的至少一者：In a feasible implementation, the cigarette insert has at least one of the following characteristics:
(1)所述卷烟插条通过模具成型和/或螺杆压条设备压制成型；(1) The cigarette insert is formed by molding and/or screw pressing equipment;
(2)所述卷烟插条的截面形状为圆形和/或多边形；(2) The cross-sectional shape of the cigarette insert is circular and/or polygonal;
(3)所述卷烟插条的长度为1cm～7cm；(3) The length of the cigarette cuttings is 1cm to 7cm;
(4)所述卷烟插条的宽度为1mm～3mm；(4) The width of the cigarette insert is 1 mm to 3 mm;
(5)所述卷烟插条的密度为0.1g/cm 3～3.5g/cm 3； (5) The density of the cigarette cuttings is 0.1g/cm 3 to 3.5g/cm 3 ;
(6)所述卷烟插条的硬度为38HD～80HD。(6) The hardness of the cigarette cuttings is 38HD to 80HD.
第二方面，本申请提供一种卷烟插条的制备方法，所述制备方法包括：In a second aspect, the present application provides a method for preparing cigarette inserts. The preparation method includes:
基材原料研磨并筛分后与有效成分混合，得到混合粉末；The base material raw materials are ground and sieved and then mixed with the active ingredients to obtain mixed powder;
在真空环境中，混合粉末中加入粘合剂并搅拌均匀，得到混合湿料；In a vacuum environment, add binder to the mixed powder and stir evenly to obtain mixed wet material;
将混合湿料成型，得到卷烟插条。The mixed wet materials are shaped to obtain cigarette inserts.
在可行的实施方式中，所述制备方法还可以为：In a feasible implementation, the preparation method can also be:
基材原料研磨并筛分后得到基材原料粉末；The base material raw materials are ground and screened to obtain base material raw material powder;
在真空环境中，在基材原料粉末加入粘合剂并搅拌均匀，得到基材湿料；In a vacuum environment, add adhesive to the base material powder and stir evenly to obtain wet base material;
将基材湿料成型，并喷洒有效成分，得到卷烟插条。The base material is wet-formed and the active ingredients are sprayed to obtain cigarette cuttings.
在可行的实施方式中，所述制备方法具有如下特征中的至少一者：In a feasible implementation, the preparation method has at least one of the following characteristics:
(1)所述基材原料包括绿茶植物体组织、红茶植物体组织、薄荷植物体组织、荷叶植物体组织、菊花植物体组织、甘草植物体组织、葛根植物体组织、树苔植物体组织、余甘子植物体组织、玫瑰植物体组织、薰衣草植物体组织中的至少一种；(1) The substrate raw materials include green tea plant tissue, black tea plant tissue, mint plant tissue, lotus leaf plant tissue, chrysanthemum plant tissue, licorice plant tissue, kudzu plant tissue, and tree moss plant tissue. , at least one of amla plant tissue, rose plant tissue, and lavender plant tissue;
(2)所述基材原料筛分后的粒径大小为300目～500目；(2) The particle size of the base material raw material after screening is 300 mesh to 500 mesh;
(3)所述基材原料与所述有效成分的质量比为10：(1～50)；(3) The mass ratio of the base material raw material to the active ingredient is 10: (1-50);
(4)所述有效成分包括***提取物和/或***植物体组织，所述***提取物和/或***植物体组织包含***素；(4) The active ingredients include cannabis extract and/or cannabis plant tissue, and the cannabis extract and/or cannabis plant tissue contain cannabinoids;
(5)所述***植物体组织包括***叶和/或***花；(5) The cannabis plant tissue includes cannabis leaves and/or cannabis flowers;
(6)所述***素为***二酚和/或其他异构体；(6) The cannabinoid is cannabidiol and/or other isomers;
(7)所述粘合剂包括水、乙醇、瓜尔胶、淀粉胶、壳聚糖、羧甲基纤维素、果胶、***胶、海藻酸钠、明胶、葡萄糖、聚丙烯醇及果糖中的至少一种；(7) The binder includes water, ethanol, guar gum, starch gum, chitosan, carboxymethylcellulose, pectin, gum arabic, sodium alginate, gelatin, glucose, polypropylene alcohol and fructose. at least one of;
(8)所述成型的方式包括模具成型和/或螺杆压条设备压制成型；(8) The molding method includes mold molding and/or screw layering equipment press molding;
(9)所述***素在所述卷烟插条中的质量占比为0.1％～70％。(9) The mass proportion of the cannabinoid in the cigarette cuttings is 0.1% to 70%.
在可行的实施方式中，所述制备方法具有如下特征中的至少一者：In a feasible implementation, the preparation method has at least one of the following characteristics:
(1)所述卷烟插条的截面形状为圆形和/或多边形；(1) The cross-sectional shape of the cigarette insert is circular and/or polygonal;
(2)所述卷烟插条的长度为1cm～7cm；(2) The length of the cigarette cuttings is 1cm to 7cm;
(3)所述卷烟插条的宽度为1mm～3mm；(3) The width of the cigarette insert is 1 mm to 3 mm;
(4)所述卷烟插条的密度为0.1g/cm 3～3.5g/cm 3； (4) The density of the cigarette cuttings is 0.1g/cm 3 to 3.5g/cm 3 ;
(5)所述卷烟插条的硬度为38HD～80HD。(5) The hardness of the cigarette cuttings is 38HD to 80HD.
本申请的技术方案至少具有以下有益的效果：The technical solution of this application has at least the following beneficial effects:
本申请提供的卷烟插条，通过在基材中添加有效成分，可以实现***素在卷烟插条中0.1％～70％质量占比的均匀分布，使得卷烟插条与卷烟配合点燃后，使用者可以更好的感受卷烟插条中***素自然释放的效果，提升用户体验。The cigarette inserts provided by this application can achieve a uniform distribution of cannabinoids in a mass proportion of 0.1% to 70% in the cigarette inserts by adding active ingredients to the base material, so that after the cigarette inserts and cigarettes are ignited together, the user You can better feel the effect of the natural release of cannabinoids in cigarette cuttings and improve the user experience.
具体实施方式Detailed ways
为了更好的理解本申请的技术方案，下面结合附图对本申请实施例进行详细描述。In order to better understand the technical solution of the present application, the embodiments of the present application will be described in detail below with reference to the accompanying drawings.
应当明确，所描述的实施例仅仅是本申请一部分实施例，而不是全部的实施例。基于本申请中的实施例，本领域普通技术人员在没有作出创造性劳动前提下所获得的所有其它实施例，都属于本申请保护的范围。It should be clear that the described embodiments are only some of the embodiments of the present application, rather than all of the embodiments. Based on the embodiments in this application, all other embodiments obtained by those of ordinary skill in the art without making creative efforts fall within the scope of protection of this application.
在本申请实施例中使用的术语是仅仅出于描述特定实施例的目的，而非旨在限制本申请。在本申请实施例和所附权利要求书中所使用的单数形式的“一种”、“所述”和“该”也旨在包括多数形式，除非上下文清楚地表示其它含义。The terminology used in the embodiments of the present application is only for the purpose of describing specific embodiments and is not intended to limit the present application. As used in the embodiments and the appended claims, the singular forms "a," "the" and "the" are intended to include the plural forms as well, unless the context clearly dictates otherwise.
应当理解，本文中使用的术语“和/或”仅仅是一种描述关联对象的关联关系，表示可以存在三种关系，例如，A和/或B，可以表示：单独存在A，同时存在A和B，单独存在B这三种情况。另外，本文中字符“/”，一般表示前后关联对象是一种“或”的关系。It should be understood that the term "and/or" used in this article is only an association relationship describing related objects, indicating that there can be three relationships, for example, A and/or B, which can mean: A alone exists, and A and A exist simultaneously. B, there are three situations of B alone. In addition, the character "/" in this article generally indicates that the related objects are an "or" relationship.
利用种植工业***花叶所提取出来的***二酚(Cannabidiol，简称CBD)等***素，是工业***中的主要化学成分，也是非成瘾成分，具有抗痉挛、抗焦虑、抗炎的药理作用，不仅可以作用于多种疑难疾病的治疗。Cannabidiol (CBD) and other cannabinoids extracted from the flowers and leaves of industrial hemp are the main chemical components of industrial hemp and are also non-addictive components. They have anti-spasmodic, anti-anxiety, and anti-inflammatory pharmacological effects. , not only can be used in the treatment of many difficult diseases.
市面上的卷烟中也添加有***素，通常的添加方式为将***的花叶磨碎后与卷烟的烟丝混合。但采用此种添加方式时，因为***花叶的特殊形状和物理特性，经过磨 碎工艺后的花叶为细小碎片状，与常规的卷烟烟丝无法很好混合，在掺配过程中会出现碎片顺着烟丝的空隙掉落，并且在成品卷烟使用过程中会存在花叶碎片掉落，也就是常说的“掉头”“落渣”等问题。其次就是少量的花叶所负载的***素含量不足，如果增加***花叶的掺配量又会导致卷烟无法卷接的问题。因此，优化***素的添加工艺，使得卷烟在燃烧过程中***素可均匀释放是本领域技术人员亟待解决的问题。Cannabinoids are also added to cigarettes on the market. The usual method of adding cannabinoids is to grind the flowers and leaves of cannabis and mix them with the shredded tobacco of cigarettes. However, when this addition method is used, due to the special shape and physical properties of cannabis flowers and leaves, the flowers and leaves after the grinding process are in the form of small fragments, which cannot be mixed well with conventional cigarette tobacco, and fragments will appear during the blending process. It falls along the gaps in the cut tobacco, and during the use of the finished cigarettes, mosaic and leaf fragments will fall off, which is often referred to as "turning around" and "slag falling". The second is that the small amount of cannabinoids contained in the flowers and leaves is insufficient. If the blending amount of cannabis flowers and leaves is increased, it will lead to the problem that the cigarette cannot be rolled. Therefore, optimizing the cannabinoid addition process so that cannabinoids can be released evenly during the burning process of cigarettes is an urgent problem that needs to be solved by those skilled in the art.
鉴于此，本申请提供一种卷烟插条，卷烟插条包含有效成分及基材，有效成分包含***素；***素在卷烟插条中的质量占比为0.1％～70％。In view of this, this application provides a cigarette insert, which contains active ingredients and a base material. The active ingredients include cannabinoids; the mass proportion of cannabinoids in the cigarette inserts is 0.1% to 70%.
上述方案中，卷烟插条通过在基材中添加有效成分，可以实现***素在卷烟插条中0.1％～70％质量占比的均匀分布，使得卷烟插条与卷烟配合点燃后，使用者可以更好的感受卷烟插条中***素自然释放的效果，提升用户体验。In the above solution, by adding active ingredients to the base material, the cigarette cuttings can achieve a uniform distribution of cannabinoids in a mass proportion of 0.1% to 70% in the cigarette cuttings, so that after the cigarette cuttings and cigarettes are lit together, the user can Better feel the effect of natural release of cannabinoids in cigarette cuttings and improve user experience.
需要说明的是，本申请的***素为***二酚和/或其他异构体，即卷烟插条中的***素可以全部为***二酚，或全部为其他的***素异构体，还可以为***二酚及其他***素异构体的混合物。可根据实际需要选择***素的种类，在此不做限定。It should be noted that the cannabinoids in this application are cannabidiol and/or other isomers, that is, the cannabinoids in cigarette cuttings can all be cannabidiol, or all cannabinoid isomers, or they can also A mixture of cannabidiol and other cannabinoid isomers. The type of cannabinoids can be selected according to actual needs and is not limited here.
在一些实施方式中，有效成分为***植物体的至少部分组织和/或***植物体提炼出来的提取物，***植物体组织包括***叶和/或***花，即有效成分可以仅包括***花叶，或仅包括***提取物，还可以为***花叶与***提取物的混合，使得***提取物和/或***植物体组织提供卷烟插条内的***素。In some embodiments, the active ingredients are at least part of the tissues of the cannabis plant and/or an extract extracted from the cannabis plant. The cannabis plant tissue includes cannabis leaves and/or cannabis flowers, that is, the active ingredients may only include cannabis flowers and leaves. , or may include only cannabis extract, but may also be a mixture of cannabis flowers and leaves with cannabis extract, such that the cannabis extract and/or cannabis plant tissue provides the cannabinoids within the cigarette cutting.
具体的，当有效成分仅包括***花叶时，可选取***素含量较高的工业***的***花和/或***叶，且相比较于将***花和/或***叶磨碎后与烟丝混合，直接使用***花和/或***叶制的卷烟插条，使得制备的卷烟插条内的***素的质量占比可达到需求。当有效成分仅包括***的提取物时，相对于使直接使用***花和/或***叶，***提取物所包含的***素含量较高。当有效成分为***花叶与提取物的混合时，若***花和/或***叶包含的***素较少，与***提取物混合后，可以提高卷烟插条内***素的含量。可根据实际需要选择有效成分的组成，在此不做限定。Specifically, when the active ingredients only include hemp flowers and leaves, hemp flowers and/or hemp leaves of industrial hemp with higher cannabinoid content can be selected, and compared with grinding hemp flowers and/or hemp leaves and mixing them with tobacco , directly using cigarette cuttings made from cannabis flowers and/or cannabis leaves, so that the quality proportion of cannabinoids in the prepared cigarette cuttings can meet the requirements. When the active ingredient consists solely of an extract of cannabis, the cannabis extract contains higher levels of cannabinoids than if the cannabis flowers and/or leaves were used directly. When the active ingredient is a mixture of cannabis flowers and leaves and an extract, if the cannabis flowers and/or leaves contain less cannabinoids, when mixed with the cannabis extract, the cannabinoid content in the cigarette cuttings can be increased. The composition of the active ingredients can be selected according to actual needs and is not limited here.
进一步的，因***提取物和/或***植物体组织除包含***素外，还包含其他成分，为了保证使用者可以更好的感受卷烟插条中***素自然释放的效果，***素在卷烟插条中的质量占比为0.1％～70％，可选的，***素在卷烟插条中的质量占比具体可以为0.1％、10％、20％、30％、40％、50％、60％、70％等。若***素的含量过低，在与卷烟配合使用时，卷烟插条释放的***素少，用户体验感降低；若***素的含量过高，制备成本相应升高。可根据实际需要选择***素在卷烟插条中的质量占比，在此不做限定。Furthermore, since cannabis extracts and/or cannabis plant tissues also contain other components in addition to cannabinoids, in order to ensure that users can better feel the effect of the natural release of cannabinoids in cigarette inserts, cannabinoids are added to the cigarette inserts. The mass proportion of cannabinoids in the cigarette cuttings is 0.1% to 70%. Optionally, the mass proportion of cannabinoids in the cigarette cuttings can be 0.1%, 10%, 20%, 30%, 40%, 50%, 60%. %, 70%, etc. If the cannabinoid content is too low, when used with cigarettes, the cigarette cuttings will release less cannabinoids and the user experience will be reduced; if the cannabinoid content is too high, the preparation cost will increase accordingly. The mass proportion of cannabinoids in cigarette cuttings can be selected according to actual needs, and is not limited here.
在一些实施方式中，基材为具有一定香味的添加材料，添加在卷烟插条内可调整卷烟插条的口感，去除卷烟烟丝的部分辛辣味。本申请使用的基材包括绿茶植物体组织、红茶植物体组织、薄荷植物体组织、荷叶植物体组织、菊花植物体组织、甘草植物体组织、葛根植物体组织、树苔植物体组织、余甘子植物体组织、玫瑰植物体组织、薰衣草植物体组织中的至少一种，其中，基材植物体组织可以为花叶等。可根据实际需要选择基材的种类，在此不做限定。In some embodiments, the base material is an additive material with a certain flavor. Adding it to the cigarette insert can adjust the taste of the cigarette insert and remove part of the spicy taste of the cigarette tobacco. The substrates used in this application include green tea plant tissue, black tea plant tissue, mint plant tissue, lotus leaf plant tissue, chrysanthemum plant tissue, licorice plant tissue, kudzu plant tissue, tree moss plant tissue, etc. At least one of the plant tissue of Ganzi, the plant tissue of rose, and the plant tissue of lavender, wherein the base plant tissue can be mosaics and leaves, etc. The type of base material can be selected according to actual needs and is not limited here.
且卷烟插条中基材与有效成分的质量比为10：(1～50)，具体的，基材与有效成分的质量比具体可以为5：1、10：3、2：1、5：3、1：1、1：2、1：3、1：4、1：5等。基材与有效成分配合后制得卷烟插条，基材作为有效成分附着的载体。若基材与有效成分的质量比过大，即卷烟插条中基材的使用量大，有效成分的使用量小，卷烟插条的口感提升，但***素的释放量达不到所需的要求；若基材与有效成分的质量比过小，即卷烟插条中基材的使用量变小，有效成分的使用量大，卷烟插条的***素的释放量满足所需要求，但制备成本升高，且卷烟插条的口感变差，影响用户体验。可根据实际需要选择基材与有效成分的质量比，在此不做限定。And the mass ratio of the base material and the active ingredient in the cigarette insert is 10: (1-50). Specifically, the mass ratio of the base material and the active ingredient can be 5:1, 10:3, 2:1, 5: 3. 1:1, 1:2, 1:3, 1:4, 1:5, etc. The base material and the active ingredients are combined to prepare cigarette cuttings, and the base material serves as a carrier for the active ingredients to adhere. If the mass ratio of the base material to the active ingredients is too large, that is, the amount of base material used in the cigarette cuttings is large and the amount of active ingredients used is small, the taste of the cigarette cuttings will be improved, but the release amount of cannabinoids will not reach the required level. Requirements; if the mass ratio of the base material to the active ingredients is too small, that is, the amount of base material used in the cigarette inserts becomes smaller and the amount of active ingredients used is large, the release amount of cannabinoids in the cigarette inserts meets the required requirements, but the preparation cost increases, and the taste of cigarette cuttings becomes worse, affecting the user experience. The mass ratio of the base material to the active ingredient can be selected according to actual needs and is not limited here.
进一步的，有效成分与基材的种类及质量比确定后，可通过模具成型和/或螺杆压条设备压制成型的方式得到特定形状的卷烟插条，具体的，卷烟插条的截面形状为圆形和/或多边形，例如正方形、正五边形等，可根据实际需要选择卷烟插条的截面形状，在此不做限定。Further, after the type and mass ratio of the active ingredients and the base material are determined, cigarette inserts of a specific shape can be obtained through mold molding and/or screw pressing equipment. Specifically, the cross-sectional shape of the cigarette inserts is circular. And/or polygon, such as square, regular pentagon, etc., the cross-sectional shape of the cigarette insert can be selected according to actual needs, and is not limited here.
其中，卷烟插条的长度为1cm～7cm，卷烟插条的宽度为1mm～3mm，可选的，卷烟插条的长度具体可以为1cm、2cm、3cm、4cm、5cm、6cm、7cm等，卷烟插条的宽度具体可以为1mm、1.3mm、1.6mm、1.9mm、2.2mm、2.5mm、2.8mm、3mm等。卷烟插条在使用时，将卷烟插条***卷烟的烟丝内，并随烟丝一起点燃，若卷烟插条的长度或宽度过长，难以与不同类型的卷烟配合，且制备成本升高；若卷烟插条的长度或宽度过短，卷烟插条的体积变小，使用过快，使用者体验感降低。可根据实际需要选择卷烟插条的长度及宽度，在此不做限定。Among them, the length of the cigarette inserts is 1cm~7cm, and the width of the cigarette inserts is 1mm~3mm. Optional, the length of the cigarette inserts can be 1cm, 2cm, 3cm, 4cm, 5cm, 6cm, 7cm, etc., the cigarette The width of the inserts can be 1mm, 1.3mm, 1.6mm, 1.9mm, 2.2mm, 2.5mm, 2.8mm, 3mm, etc. When the cigarette insert is used, the cigarette insert is inserted into the shredded tobacco of the cigarette and lit together with the shredded tobacco. If the length or width of the cigarette insert is too long, it will be difficult to match different types of cigarettes, and the preparation cost will increase; if the cigarette If the length or width of the cutting is too short, the volume of the cigarette cutting will become smaller, and if it is used too quickly, the user experience will be reduced. The length and width of the cigarette inserts can be selected according to actual needs and are not limited here.
卷烟插条的硬度为38HD～80HD，可选的，卷烟插条的硬度具体可以为38HD、40HD、50HD、60HD、65HD、70HD、80HD等。卷烟插条在使用时，通过卷烟的一端***卷烟内部，因此卷烟插条需要具备一定的硬度，防止在卷烟插条在***过程中折断。若卷烟插条的硬度过小，在***烟丝的过程中，卷烟插条易发生断裂，影响使用体验；若卷烟插条的硬度过大，制备成本会升高。可根据实际需要选择卷烟插条的硬度，在此不做限定。The hardness of cigarette inserts is 38HD~80HD. Optional, the hardness of cigarette inserts can be 38HD, 40HD, 50HD, 60HD, 65HD, 70HD, 80HD, etc. When the cigarette insert is used, it is inserted into the cigarette through one end of the cigarette. Therefore, the cigarette insert needs to have a certain hardness to prevent the cigarette insert from breaking during the insertion process. If the hardness of the cigarette insert is too small, the cigarette insert will easily break during the insertion of shredded tobacco, affecting the user experience; if the hardness of the cigarette insert is too large, the preparation cost will increase. The hardness of the cigarette inserts can be selected according to actual needs and is not limited here.
为了使得卷烟插条具有更好的燃烧效果，需要控制卷烟插条的密度，使得卷烟插条可以更好的与空气接触，燃烧过程更稳定，本申请提供的卷烟插条的密度为0.1g/cm 3～3.5g/cm 3，可选的，卷烟插条的密度具体可以为0.1g/cm 3、0.3g/cm 3、0.5g/cm 3、1g/cm 3、1.5g/cm 3、2g/cm 3、3.5g/cm 3等。有效成分与基材混合后，通过压制得到卷烟插条，若卷烟插条的密度过小，即压实程度不够，卷烟插条在使用过程中易破碎；若卷烟插条的密度过大，即卷烟插条的密实程度过高，使用过程中，卷烟插条内的***素得不到充分的释放，影响用户体验。可根据实际需要选择卷烟插条的密度，在此不做限定。 In order to make the cigarette inserts have a better burning effect, the density of the cigarette inserts needs to be controlled so that the cigarette inserts can better contact with the air and the combustion process is more stable. The density of the cigarette inserts provided in this application is 0.1g/ cm 3 ~ 3.5g/cm 3 , optional, the density of cigarette cuttings can be 0.1g/cm 3 , 0.3g/cm 3 , 0.5g/cm 3 , 1g/cm 3 , 1.5g/cm 3 , 2g/cm 3 , 3.5g/cm 3 etc. After the active ingredients are mixed with the base material, the cigarette inserts are obtained by pressing. If the density of the cigarette inserts is too small, that is, the degree of compaction is not enough, the cigarette inserts are easily broken during use; if the density of the cigarette inserts is too high, that is, The density of cigarette cuttings is too high, and the cannabinoids in the cigarette cuttings cannot be fully released during use, which affects the user experience. The density of cigarette cuttings can be selected according to actual needs and is not limited here.
第二方面，本申请提供一种卷烟插条的制备方法，制备方法包括：In a second aspect, this application provides a method for preparing cigarette inserts. The preparation method includes:
步骤S10，基材原料研磨并筛分后与有效成分混合，得到混合粉末；Step S10: Grind and sieve the base material raw materials and mix them with the active ingredients to obtain mixed powder;
步骤S20，在真空环境中，混合粉末中加入粘合剂并搅拌均匀，得到混合湿料；Step S20, in a vacuum environment, add a binder to the mixed powder and stir evenly to obtain a mixed wet material;
步骤S30，将混合湿料成型，得到卷烟插条。Step S30: mold the mixed wet material to obtain a cigarette insert.
需要说明的是，除上述制备过程中将基材原料与有效成分混合制备卷烟插条外，制备方法还可以为：将基材原料研磨并筛分后得到基材原料粉末；在真空环境中，在基材原料粉末加入粘合剂并搅拌均匀，得到基材湿料；再将基材湿料成型，并喷洒有效成分，得到卷烟插条。具体的，当有效成分通过喷洒的方式附着在基材原料的外表面时，此种卷烟插条与卷烟配合点燃后，有效成分的释放更快速，提升用户体验，此种制备方法适用于***素添加量≤10％的卷烟插条。有效成分掺杂于基材原料内部时，有效成分在基材原料内的分布均匀，此种卷烟插条与卷烟配合点燃后，有效成分的释放更加均匀，此种制备方法适用于任何范围***素添加量的卷烟插条。可根据实际需要选择有效成分在基材原料上的附着方式，在此不做限定。It should be noted that, in addition to mixing the base material raw materials and active ingredients to prepare cigarette inserts in the above preparation process, the preparation method can also be: grinding and screening the base material raw materials to obtain the base material raw material powder; in a vacuum environment, Add an adhesive to the base material powder and stir evenly to obtain a wet base material; then shape the wet base material and spray the active ingredients to obtain a cigarette insert. Specifically, when the active ingredients are attached to the outer surface of the base material by spraying, and the cigarette cuttings are ignited together with the cigarette, the active ingredients are released more quickly, improving the user experience. This preparation method is suitable for cannabinoids. Cigarette cuttings with an added amount of ≤10%. When the active ingredients are doped into the base material, the active ingredients are evenly distributed in the base material. After the cigarette cuttings are ignited with the cigarette, the active ingredients are released more evenly. This preparation method is suitable for any range of cannabinoids. Added amount of cigarette cuttings. The method of attaching the active ingredients to the base material can be selected according to actual needs, and is not limited here.
同时，与基材原料混合的有效成分为***素，***素为***二酚和/或其他异构体，即卷烟插条中的***素可以全部为***二酚，或全部为其他的***素异构体，还可以为***二酚及其他***素异构体的混合物。可根据实际需要选择***素的种类，在此不做限定。At the same time, the active ingredient mixed with the base material is cannabinoids, and the cannabinoids are cannabidiol and/or other isomers. That is, the cannabinoids in the cigarette cuttings can be all cannabidiol, or all cannabinoids. Isomers can also be mixtures of cannabidiol and other cannabinoid isomers. The type of cannabinoids can be selected according to actual needs and is not limited here.
在步骤S10中，基材原料包括绿茶植物体组织、红茶植物体组织、薄荷植物体组织、荷叶植物体组织、菊花植物体组织、甘草植物体组织、葛根植物体组织、树苔植物体组织、余甘子植物体组织、玫瑰植物体组织、薰衣草植物体组织中的至少一种。例如绿茶、薄荷两种混合或薄荷、甘草、荷叶三种混合后研磨成粉末状并筛分。In step S10, the substrate raw materials include green tea plant tissue, black tea plant tissue, mint plant tissue, lotus leaf plant tissue, chrysanthemum plant tissue, licorice plant tissue, kudzu plant tissue, and tree moss plant tissue. , at least one of amla plant tissue, rose plant tissue, and lavender plant tissue. For example, mix two types of green tea and mint, or mix three types of mint, licorice, and lotus leaves, then grind them into powder and sieve.
其中，筛分得到的基材原料粉末的粒径大小为300目～500目，可选的，粒径大小具体可以为300目、320目、340目、360目、380目、400目、420目、440目、460 目、480目、500目等，基材原料的粒径大小在此范围内，基材原料可以更好的与有效成分进行混合。可根据实际需要具体选择基材原料的粒径大小，在此不做限定。Among them, the particle size of the base material powder obtained by screening is 300 mesh to 500 mesh. Optional, the particle size can be 300 mesh, 320 mesh, 340 mesh, 360 mesh, 380 mesh, 400 mesh, 420 mesh. mesh, 440 mesh, 460 mesh, 480 mesh, 500 mesh, etc. The particle size of the base material raw materials is within this range, and the base material raw materials can be better mixed with the active ingredients. The particle size of the base material raw material can be specifically selected according to actual needs, and is not limited here.
与基材原料混合的有效成分为***植物体的至少部分组织和/或***植物体提炼出来的提取物，***植物体组织包括***叶和/或***花，即有效成分可以仅包括***花叶，或仅包括***提取物，还可以为***花叶与***提取物的混合，使得***提取物和/或***植物体组织提供卷烟插条内的***素。The active ingredients mixed with the base material are at least part of the tissues of the cannabis plant and/or an extract extracted from the cannabis plant. The cannabis plant tissue includes cannabis leaves and/or cannabis flowers, that is, the active ingredients may only include cannabis flowers and leaves. , or may include only cannabis extract, but may also be a mixture of cannabis flowers and leaves with cannabis extract, such that the cannabis extract and/or cannabis plant tissue provides the cannabinoids within the cigarette cutting.
具体的，当有效成分仅包括***花叶时，可选取***素含量较高的工业***的***花和/或***叶，且相比较于将***花和/或***叶磨碎后与烟丝混合，直接使用***花和/或***叶制的卷烟插条，使得制备的卷烟插条内的***素的质量占比可达到需求。当有效成分仅包括***的提取物时，相对于使直接使用***花和/或***叶，***提取物所包含的***素含量较高。当有效成分为***花叶与提取物的混合时，若***花和/或***叶包含的***素较少，与***提取物混合后，可以提高卷烟插条内***素的含量。可根据实际需要选择有效成分的组成，在此不做限定。Specifically, when the active ingredients only include hemp flowers and leaves, hemp flowers and/or hemp leaves of industrial hemp with higher cannabinoid content can be selected, and compared with grinding hemp flowers and/or hemp leaves and mixing them with tobacco , directly using cigarette cuttings made from cannabis flowers and/or cannabis leaves, so that the quality proportion of cannabinoids in the prepared cigarette cuttings can meet the requirements. When the active ingredient consists solely of an extract of cannabis, the cannabis extract contains higher levels of cannabinoids than if the cannabis flowers and/or leaves were used directly. When the active ingredient is a mixture of cannabis flowers and leaves and an extract, if the cannabis flowers and/or leaves contain less cannabinoids, when mixed with the cannabis extract, the cannabinoid content in the cigarette cuttings can be increased. The composition of the active ingredients can be selected according to actual needs and is not limited here.
其中基材原料与有效成分的质量比为10：(1～50)，具体的，基材原料与有效成分的质量比具体可以为5：1、10：3、2：1、5：3、1：1、1：2、1：3、1：4、1：5等。基材原料与有效成分配合后制得卷烟插条，基材原料作为有效成分附着的载体。若基材原料与有效成分的质量比过大，即卷烟插条中基材原料的使用量大，有效成分的使用量小，卷烟插条的口感提升，但***素的释放量达不到所需的要求；若基材原料与有效成分的质量比过小，即卷烟插条中基材原料的使用量变小，有效成分的使用量大，卷烟插条的***素的释放量满足所需要求，但制备成本升高，且卷烟插条的口感变差，影响用户体验。可根据实际需要选择基材原料与有效成分的质量比，在此不做限定。The mass ratio of the base material raw material to the active ingredient is 10: (1-50). Specifically, the mass ratio of the base material raw material to the active ingredient can be 5:1, 10:3, 2:1, 5:3, 1:1, 1:2, 1:3, 1:4, 1:5, etc. Cigarette cuttings are produced after the base material raw material and the active ingredients are combined, and the base material raw material serves as a carrier for the active ingredients to adhere. If the mass ratio of the base material to the active ingredients is too large, that is, the amount of base material used in the cigarette inserts is large and the amount of active ingredients used is small, the taste of the cigarette inserts will be improved, but the release of cannabinoids will not reach the desired level. The required requirements; if the mass ratio of the base material to the active ingredient is too small, that is, the amount of base material used in the cigarette cuttings becomes smaller and the amount of active ingredients used is large, the release amount of cannabinoids in the cigarette cuttings meets the required requirements. , but the preparation cost increases, and the taste of cigarette cuttings becomes worse, affecting the user experience. The mass ratio of base material raw materials and active ingredients can be selected according to actual needs, and is not limited here.
在实际应用过程中，将基材原料与有效成分均加入相同容器内，并使用搅拌装置使得基材原料与有效成分充分混合均匀，得到混合粉末。In the actual application process, the base material raw materials and the active ingredients are added into the same container, and a stirring device is used to fully mix the base material raw materials and the active ingredients evenly to obtain a mixed powder.
在步骤S20中，将步骤S10得到的混合粉末在真空设备中添加粘合剂，其中，粘合剂包括水、乙醇、瓜尔胶、淀粉胶、壳聚糖、羧甲基纤维素、果胶、***胶、海藻酸钠、明胶、葡萄糖、聚丙烯醇及果糖中的至少一种。本申请使用的粘合剂为含有1％羧甲基纤维素钠的水溶液。通过粘合剂将分散的混合粉末粘合在一起后，通过搅拌设备搅拌25min～40min，得到混合均匀的湿料。In step S20, a binder is added to the mixed powder obtained in step S10 in a vacuum equipment, where the binder includes water, ethanol, guar gum, starch gum, chitosan, carboxymethylcellulose, and pectin. , acacia gum, sodium alginate, gelatin, glucose, polypropylene alcohol and at least one fructose. The adhesive used in this application is an aqueous solution containing 1% sodium carboxymethyl cellulose. After the dispersed mixed powder is bonded together by an adhesive, stir it with a stirring device for 25 to 40 minutes to obtain a uniformly mixed wet material.
在步骤S30中，将步骤S20得到的湿料通过模具成型和/或螺杆压条设备压制成型。In step S30, the wet material obtained in step S20 is pressed and formed through mold forming and/or screw layering equipment.
具体的，模具成型是指将湿料铺设于插条模具内，并通过液压设备对湿料施加竖直方向的压力，得到具有一定密实度的卷烟插条，再将卷烟插条从模具上取下，并进 行修边处理。Specifically, mold forming refers to laying the wet material in the insert mold, and applying vertical pressure to the wet material through hydraulic equipment to obtain a cigarette insert with a certain density, and then taking the cigarette insert from the mold. down and trim the edges.
螺杆压条设备压制成型是指将湿料放置于具有特定形状出料口的压条容器内，启驱动装置带动驱动架发生转动，驱动架带动螺杆转动，搅拌并将湿料通过特定形状的出料口压出，得到卷烟插条。Pressing and forming of screw layering equipment means placing the wet material in a layering container with a specific shape of the outlet. The driving device drives the drive frame to rotate. The drive frame drives the screw to rotate, stirs and passes the wet material through the specific shape of the outlet. Press out to get cigarette cuttings.
步骤S30后，还包括步骤S40，将得到的卷烟插条运送至无菌环境中自然晾干。After step S30, step S40 is also included, in which the obtained cigarette cuttings are transported to a sterile environment to be naturally dried.
经过上述步骤S10，步骤S20，步骤S30及步骤S40后，得到具有一定尺寸结构的卷烟插条。After the above steps S10, S20, S30 and S40, a cigarette insert with a certain size structure is obtained.
具体的，卷烟插条的截面形状为圆形和/或多边形，例如正方形、正五边形等，可根据实际需要选择卷烟插条的截面形状，在此不做限定。Specifically, the cross-sectional shape of the cigarette insert is circular and/or polygonal, such as square, regular pentagon, etc. The cross-sectional shape of the cigarette insert can be selected according to actual needs, and is not limited here.
其中，卷烟插条的长度为1cm～7cm，卷烟插条的宽度为1mm～3mm，可选的，卷烟插条的长度具体可以为1cm、2cm、3cm、4cm、5cm、6cm、7cm等，卷烟插条的宽度具体可以为1mm、1.3mm、1.6mm、1.9mm、2.2mm、2.5mm、2.8mm、3mm等。卷烟插条在使用时，将卷烟插条***卷烟的烟丝内，并随烟丝一起点燃，若卷烟插条的长度或宽度过长，难以与不同类型的卷烟配合，且制备成本升高；若卷烟插条的长度或宽度过短，卷烟插条的体积变小，使用过快，使用者体验感降低。可根据实际需要选择卷烟插条的长度及宽度，在此不做限定。Among them, the length of the cigarette inserts is 1cm~7cm, and the width of the cigarette inserts is 1mm~3mm. Optional, the length of the cigarette inserts can be 1cm, 2cm, 3cm, 4cm, 5cm, 6cm, 7cm, etc., the cigarette The width of the inserts can be 1mm, 1.3mm, 1.6mm, 1.9mm, 2.2mm, 2.5mm, 2.8mm, 3mm, etc. When the cigarette insert is used, the cigarette insert is inserted into the shredded tobacco of the cigarette and lit together with the shredded tobacco. If the length or width of the cigarette insert is too long, it will be difficult to match different types of cigarettes, and the preparation cost will increase; if the cigarette If the length or width of the cutting is too short, the volume of the cigarette cutting will become smaller, and if it is used too quickly, the user experience will be reduced. The length and width of the cigarette inserts can be selected according to actual needs and are not limited here.
卷烟插条的硬度为38HD～80HD，可选的，卷烟插条的硬度具体可以为38HD、40HD、50HD、60HD、65HD、70HD、80HD等。卷烟插条在使用时，通过卷烟的一端***卷烟内部，因此卷烟插条需要具备一定的硬度，防止在卷烟插条在***过程中折断。若卷烟插条的硬度过小，在***烟丝的过程中，卷烟插条易发生断裂，影响使用体验；若卷烟插条的硬度过大，制备成本会升高。可根据实际需要选择卷烟插条的硬度，在此不做限定。The hardness of cigarette inserts is 38HD~80HD. Optional, the hardness of cigarette inserts can be 38HD, 40HD, 50HD, 60HD, 65HD, 70HD, 80HD, etc. When the cigarette insert is used, it is inserted into the cigarette through one end of the cigarette. Therefore, the cigarette insert needs to have a certain hardness to prevent the cigarette insert from breaking during the insertion process. If the hardness of the cigarette insert is too small, the cigarette insert will easily break during the insertion of shredded tobacco, affecting the user experience; if the hardness of the cigarette insert is too large, the preparation cost will increase. The hardness of the cigarette inserts can be selected according to actual needs and is not limited here.
卷烟插条的密度为0.1g/cm 3～3.5g/cm 3，可选的，卷烟插条的密度具体可以为0.1g/cm 3、0.3g/cm 3、0.5g/cm 3、1g/cm 3、1.5g/cm 3、2g/cm 3、3.5g/cm 3等。有效成分与基材混合后得到卷烟插条，若卷烟插条的密度过小，即压实程度不够，卷烟插条在使用过程中易破碎；若卷烟插条的密度过大，即卷烟插条的密实程度过高，使用过程中，卷烟插条内的***素得不到充分的释放，影响用户体验。可根据实际需要选择卷烟插条的密度，在此不做限定。 The density of cigarette cuttings is 0.1g/cm 3 ~ 3.5g/cm 3 . Optional, the density of cigarette cuttings can be 0.1g/cm 3 , 0.3g/cm 3 , 0.5g/cm 3 , 1g/ cm 3 , 1.5g/cm 3 , 2g/cm 3 , 3.5g/cm 3 etc. After the active ingredients are mixed with the base material, the cigarette inserts are obtained. If the density of the cigarette inserts is too small, that is, the degree of compaction is not enough, the cigarette inserts are easily broken during use; if the density of the cigarette inserts is too high, that is, the cigarette inserts are The density is too high, and the cannabinoids in the cigarette cuttings cannot be fully released during use, affecting the user experience. The density of cigarette cuttings can be selected according to actual needs and is not limited here.
***素在卷烟插条中的质量占比为0.1％～70％，可选的，***素在卷烟插条中的质量占比具体可以为0.1％、10％、20％、30％、40％、50％、60％、70％等。若***素的含量过低，在与卷烟配合使用时，卷烟插条释放的***素少，用户体验感降低；若 ***素的含量过高，制备成本相应升高。可根据实际需要选择***素在卷烟插条中的质量占比，在此不做限定。The mass proportion of cannabinoids in cigarette cuttings is 0.1% to 70%. Optional, the mass proportion of cannabinoids in cigarette cuttings can be 0.1%, 10%, 20%, 30%, 40%. , 50%, 60%, 70%, etc. If the cannabinoid content is too low, when used with cigarettes, the cigarette cuttings will release less cannabinoids and the user experience will be reduced; if the cannabinoid content is too high, the preparation cost will increase accordingly. The mass proportion of cannabinoids in cigarette cuttings can be selected according to actual needs, and is not limited here.
以下结合实施例具体阐述：The following is explained in detail with reference to the examples:
实施例1：Example 1:
(1)将粒径大小为300目～500目的薄荷粉末与***二酚混合均匀，得到混合粉末；其中，***二酚与薄荷粉末的质量比为7:13；(1) Mix mint powder with a particle size of 300 mesh to 500 mesh and cannabidiol evenly to obtain a mixed powder; wherein, the mass ratio of cannabidiol to mint powder is 7:13;
(2)在真空环境中，混合粉末中加入含有1％羧甲基纤维素钠的水溶液并搅拌35min，得到混合湿料；(2) In a vacuum environment, add an aqueous solution containing 1% sodium carboxymethyl cellulose to the mixed powder and stir for 35 minutes to obtain a mixed wet material;
(3)将混合湿料压制成型并晾干，得到卷烟插条；(3) Press the mixed wet material into shape and dry it to obtain cigarette cuttings;
实施例1制备的卷烟插条中***二酚的质量占比为35％，卷烟插条的密度为0.64g/cm 3。 The mass proportion of cannabidiol in the cigarette cuttings prepared in Example 1 is 35%, and the density of the cigarette cuttings is 0.64g/cm 3 .
实施例2：Example 2:
(1)将粒径大小为300目～500目的薄荷粉末与***二酚混合均匀，得到混合粉末；其中，***二酚与薄荷粉末的质量比为1:9；(1) Mix mint powder with a particle size of 300 mesh to 500 mesh and cannabidiol evenly to obtain a mixed powder; wherein, the mass ratio of cannabidiol to mint powder is 1:9;
(2)在真空环境中，混合粉末中加入含有1％羧甲基纤维素钠的水溶液并搅拌35min，得到混合湿料；(2) In a vacuum environment, add an aqueous solution containing 1% sodium carboxymethyl cellulose to the mixed powder and stir for 35 minutes to obtain a mixed wet material;
(3)将混合湿料压制成型并晾干，得到卷烟插条；(3) Press the mixed wet material into shape and dry it to obtain cigarette cuttings;
实施例2制备的卷烟插条中***二酚的质量占比为10％，卷烟插条的密度为0.77g/cm 3。 The mass proportion of cannabidiol in the cigarette cuttings prepared in Example 2 is 10%, and the density of the cigarette cuttings is 0.77g/cm 3 .
实施例3：Example 3:
(1)将粒径大小为300目～500目的薄荷粉末与***二酚混合均匀，得到混合粉末；其中，***二酚与薄荷粉末的质量比为7:3；(1) Mix mint powder with a particle size of 300 mesh to 500 mesh and cannabidiol evenly to obtain a mixed powder; wherein, the mass ratio of cannabidiol to mint powder is 7:3;
(2)在真空环境中，混合粉末中加入含有1％羧甲基纤维素钠的水溶液并搅拌35min，得到混合湿料；(2) In a vacuum environment, add an aqueous solution containing 1% sodium carboxymethyl cellulose to the mixed powder and stir for 35 minutes to obtain a mixed wet material;
(3)将混合湿料压制成型并晾干，得到卷烟插条；(3) Press the mixed wet material into shape and dry it to obtain cigarette cuttings;
实施例3制备的卷烟插条中***二酚的质量占比为70％，卷烟插条的密度为0.55g/cm 3。 The mass proportion of cannabidiol in the cigarette cuttings prepared in Example 3 is 70%, and the density of the cigarette cuttings is 0.55g/cm 3 .
实施例4：Example 4:
(1)将粒径大小为300目～500目的薄荷粉末与***二酚混合均匀，得到混合粉末；其中，***二酚与薄荷粉末的质量比为99:1；(1) Mix mint powder with a particle size of 300 mesh to 500 mesh and cannabidiol evenly to obtain a mixed powder; wherein, the mass ratio of cannabidiol to mint powder is 99:1;
(2)在真空环境中，混合粉末中加入含有1％羧甲基纤维素钠的水溶液并搅拌35min，得到混合湿料；(2) In a vacuum environment, add an aqueous solution containing 1% sodium carboxymethyl cellulose to the mixed powder and stir for 35 minutes to obtain a mixed wet material;
(3)将混合湿料压制成型并晾干，得到卷烟插条；(3) Press the mixed wet material into shape and dry it to obtain cigarette cuttings;
实施例4制备的卷烟插条中***二酚的质量占比为99％，卷烟插条的密度为0.43g/cm 3。 The mass proportion of cannabidiol in the cigarette cuttings prepared in Example 4 is 99%, and the density of the cigarette cuttings is 0.43g/cm 3 .
实施例5：Example 5:
(1)将粒径大小为300目～500目的薄荷粉末与***花叶粉末混合均匀，得到混合粉末；其中，***花叶粉末与薄荷粉末的质量比为7:13；(1) Mix mint powder with a particle size of 300 to 500 mesh and cannabis mosaic and leaf powder evenly to obtain a mixed powder; wherein, the mass ratio of cannabis mosaic and leaf powder to mint powder is 7:13;
(2)在真空环境中，混合粉末中加入含有1％羧甲基纤维素钠的水溶液并搅拌35min，得到混合湿料；(2) In a vacuum environment, add an aqueous solution containing 1% sodium carboxymethyl cellulose to the mixed powder and stir for 35 minutes to obtain a mixed wet material;
(3)将混合湿料压制成型并晾干，得到卷烟插条；(3) Press the mixed wet material into shape and dry it to obtain cigarette cuttings;
实施例5制备的卷烟插条中***二酚的质量占比为0.35％，卷烟插条的密度为1.12g/cm 3。 The mass proportion of cannabidiol in the cigarette cuttings prepared in Example 5 is 0.35%, and the density of the cigarette cuttings is 1.12g/cm 3 .
实施例6：Example 6:
(1)将粒径大小为300目～500目的薄荷粉末与***二酚及***花叶粉末的混合物混合均匀，得到混合粉末；其中，混合物与薄荷粉末的质量比为7:13；(1) Mix mint powder with a particle size of 300 to 500 mesh, cannabidiol and cannabis mosaic and leaf powder evenly to obtain a mixed powder; wherein, the mass ratio of the mixture to mint powder is 7:13;
(2)在真空环境中，混合粉末中加入含有1％羧甲基纤维素钠的水溶液并搅拌35min，得到混合湿料；(2) In a vacuum environment, add an aqueous solution containing 1% sodium carboxymethyl cellulose to the mixed powder and stir for 35 minutes to obtain a mixed wet material;
(3)将混合湿料压制成型并晾干，得到卷烟插条；(3) Press the mixed wet material into shape and dry it to obtain cigarette cuttings;
实施例6制备的卷烟插条中***二酚的质量占比为1％，卷烟插条的密度为0.76g/cm 3。 The mass proportion of cannabidiol in the cigarette cuttings prepared in Example 6 is 1%, and the density of the cigarette cuttings is 0.76g/cm 3 .
实施例7：Example 7:
(1)将粒径大小为300目～500目的薄荷粉末与***二酚混合均匀，得到混合粉末；其中，***二酚与薄荷粉末的质量比为7:13；(1) Mix mint powder with a particle size of 300 mesh to 500 mesh and cannabidiol evenly to obtain a mixed powder; wherein, the mass ratio of cannabidiol to mint powder is 7:13;
(2)在真空环境中，混合粉末中加入含有1％羧甲基纤维素钠的水溶液并搅拌35min， 得到混合湿料；(2) In a vacuum environment, add an aqueous solution containing 1% sodium carboxymethylcellulose to the mixed powder and stir for 35 minutes to obtain a wet mixed material;
(3)将混合湿料压制成型并晾干，得到卷烟插条；(3) Press the mixed wet material into shape and dry it to obtain cigarette cuttings;
实施例7制备的卷烟插条中***二酚的质量占比为35％，卷烟插条的密度为0.32g/cm 3。 The mass proportion of cannabidiol in the cigarette cuttings prepared in Example 7 is 35%, and the density of the cigarette cuttings is 0.32g/cm 3 .
实施例8：Example 8:
(1)将粒径大小为300目～500目的薄荷粉末与***二酚混合均匀，得到混合粉末；其中，***二酚与薄荷粉末的质量比为7:13；(1) Mix mint powder with a particle size of 300 mesh to 500 mesh and cannabidiol evenly to obtain a mixed powder; wherein, the mass ratio of cannabidiol to mint powder is 7:13;
(2)在真空环境中，混合粉末中加入含有1％羧甲基纤维素钠的水溶液并搅拌35min，得到混合湿料；(2) In a vacuum environment, add an aqueous solution containing 1% sodium carboxymethyl cellulose to the mixed powder and stir for 35 minutes to obtain a mixed wet material;
(3)将混合湿料压制成型并晾干，得到卷烟插条；(3) Press the mixed wet material into shape and dry it to obtain cigarette cuttings;
实施例8制备的卷烟插条中***二酚的质量占比为35％，卷烟插条的密度为1.3g/cm 3。 The mass proportion of cannabidiol in the cigarette cuttings prepared in Example 8 is 35%, and the density of the cigarette cuttings is 1.3g/cm 3 .
实施例9：Example 9:
(1)将薄荷植物体组织研磨成粒径大小为300目～500目的薄荷粉末；(1) Grind mint plant tissue into mint powder with a particle size of 300 to 500 mesh;
(2)在真空环境中，薄荷粉末中加入含有1％羧甲基纤维素钠的水溶液并搅拌35min，得到基材湿料；(2) In a vacuum environment, add an aqueous solution containing 1% sodium carboxymethyl cellulose to the mint powder and stir for 35 minutes to obtain a wet base material;
(3)将基材湿料压制成型并喷洒***二酚，晾干得到卷烟插条，其中，***二酚与薄荷粉末的质量比为7:13。(3) Press the wet base material into shape, spray cannabidiol, and dry to obtain cigarette cuttings, in which the mass ratio of cannabidiol to mint powder is 7:13.
实施例9制备的卷烟插条中***二酚的质量占比为10％，卷烟插条的密度为0.8g/cm 3。 The mass proportion of cannabidiol in the cigarette cuttings prepared in Example 9 is 10%, and the density of the cigarette cuttings is 0.8g/cm 3 .
对比例1：Comparative example 1:
将***花叶磨碎后与常规烟丝混合，制得卷烟；其中，***花叶质量占比为33％。The cannabis mosaics and leaves are ground and mixed with conventional cut tobacco to prepare cigarettes; the mass proportion of cannabis mosaics and leaves is 33%.
对比例1制备的卷烟插条包含的***二酚的质量含量为0.33％。The cigarette cuttings prepared in Comparative Example 1 contained a mass content of cannabidiol of 0.33%.
测试：将实施例1～9制备的卷烟插条与卷烟配合点燃。Test: The cigarette cuttings prepared in Examples 1 to 9 are combined with cigarettes and ignited.
Figure PCTCN2022087649-appb-000001
Figure PCTCN2022087649-appb-000001
Figure PCTCN2022087649-appb-000002
Figure PCTCN2022087649-appb-000002
由实施例1与对比例1可知，采用卷烟插条与卷烟配合使用，卷烟插条包含的***素含量较高且可以均匀释放，用户体验感更好。It can be seen from Example 1 and Comparative Example 1 that when cigarette inserts are used in conjunction with cigarettes, the cigarette inserts contain higher cannabinoid content and can be released evenly, resulting in a better user experience.
最后应说明的是，以上各实施例仅用以说明本申请的技术方案，而非对其限制。尽管参照前述各实施例对本申请进行了详细的说明，本领域的普通技术人员应当理解，其依然可以对前述各实施例所记载的技术方案进行修改，或者对其中部分或者全部技术特征进行等同替换。而这些修改或者替换，并不使相应技术方案的本质脱离本申请各实施例技术方案的范围。Finally, it should be noted that the above embodiments are only used to illustrate the technical solution of the present application, but not to limit it. Although the present application has been described in detail with reference to the foregoing embodiments, those of ordinary skill in the art will understand that they can still modify the technical solutions described in the foregoing embodiments, or make equivalent substitutions for some or all of the technical features. . However, these modifications or substitutions do not cause the essence of the corresponding technical solutions to depart from the scope of the technical solutions of the embodiments of this application.

Claims (10)

  1. 一种卷烟插条，其特征在于，所述卷烟插条包含有效成分及基材，所述有效成分包含***素；所述***素在所述卷烟插条中的质量占比为0.1％～70％。A cigarette insert, characterized in that the cigarette insert contains active ingredients and a base material, and the active ingredients include cannabinoids; the mass proportion of the cannabinoids in the cigarette inserts is 0.1% to 70% %.
  2. 根据权利要求1所述卷烟插条，其特征在于，所述有效成分包括***提取物和/或***植物体组织，所述***提取物和/或***植物体组织包含***素。The cigarette cutting according to claim 1, characterized in that the active ingredients include cannabis extract and/or cannabis plant tissue, and the cannabis extract and/or cannabis plant tissue contain cannabinoids.
  3. 根据权利要求2所述卷烟插条，其特征在于，所述***植物体组织包括***叶和/或***花。The cigarette cutting according to claim 2, wherein the cannabis plant tissue includes cannabis leaves and/or cannabis flowers.
  4. 根据权利要求2所述卷烟插条，其特征在于，所述***素为***二酚和/或其他异构体。The cigarette insert according to claim 2, wherein the cannabinoid is cannabidiol and/or other isomers.
  5. 根据权利要求1所述卷烟插条，其特征在于，所述卷烟插条具有如下特征中的至少一者：The cigarette insert according to claim 1, characterized in that the cigarette insert has at least one of the following characteristics:
    (1)所述基材与所述有效成分的质量比为10：(1～50)；(1) The mass ratio of the base material to the active ingredient is 10: (1-50);
    (2)所述基材包括绿茶植物体组织、红茶植物体组织、薄荷植物体组织、荷叶植物体组织、菊花植物体组织、甘草植物体组织、葛根植物体组织、树苔植物体组织、余甘子植物体组织、玫瑰植物体组织、薰衣草植物体组织中的至少一种。(2) The base material includes green tea plant tissue, black tea plant tissue, mint plant tissue, lotus leaf plant tissue, chrysanthemum plant tissue, licorice plant tissue, kudzu plant tissue, tree moss plant tissue, At least one of Phyllanthus emblica plant tissue, rose plant tissue, and lavender plant tissue.
  6. 根据权利要求1所述卷烟插条，其特征在于，所述卷烟插条具有如下特征中的至少一者：The cigarette insert according to claim 1, characterized in that the cigarette insert has at least one of the following characteristics:
    (1)所述卷烟插条通过模具成型和/或螺杆压条设备压制成型；(1) The cigarette insert is formed by molding and/or screw pressing equipment;
    (2)所述卷烟插条的截面形状为圆形和/或多边形；(2) The cross-sectional shape of the cigarette insert is circular and/or polygonal;
    (3)所述卷烟插条的长度为1cm～7cm；(3) The length of the cigarette cuttings is 1cm to 7cm;
    (4)所述卷烟插条的宽度为1mm～3mm；(4) The width of the cigarette insert is 1 mm to 3 mm;
    (5)所述卷烟插条的密度为0.1g/cm 3～3.5g/cm 3； (5) The density of the cigarette cuttings is 0.1g/cm 3 to 3.5g/cm 3 ;
    (6)所述卷烟插条的硬度为38HD～80HD。(6) The hardness of the cigarette cuttings is 38HD to 80HD.
  7. 一种卷烟插条的制备方法，其特征在于，所述制备方法包括：A method for preparing cigarette cuttings, characterized in that the preparation method includes:
    基材原料研磨并筛分后与有效成分混合，得到混合粉末；The base material raw materials are ground and sieved and then mixed with the active ingredients to obtain mixed powder;
    在真空环境中，混合粉末中加入粘合剂并搅拌均匀，得到混合湿料；In a vacuum environment, add binder to the mixed powder and stir evenly to obtain mixed wet material;
    将混合湿料成型，得到卷烟插条。The mixed wet materials are shaped to obtain cigarette inserts.
  8. 根据权利要求7所述制备方法，其特征在于，所述制备方法还可以为：The preparation method according to claim 7, characterized in that, the preparation method can also be:
    基材原料研磨并筛分后得到基材原料粉末；The base material raw materials are ground and screened to obtain base material raw material powder;
    在真空环境中，在基材原料粉末加入粘合剂并搅拌均匀，得到基材湿料；In a vacuum environment, add adhesive to the base material powder and stir evenly to obtain wet base material;
    将基材湿料成型，并喷洒有效成分，得到卷烟插条。The base material is wet-formed and the active ingredients are sprayed to obtain cigarette cuttings.
  9. 根据权利要求7所述制备方法，其特征在于，所述制备方法具有如下特征中 的至少一者：The preparation method according to claim 7, characterized in that the preparation method has at least one of the following characteristics:
    (1)所述基材原料包括绿茶植物体组织、红茶植物体组织、薄荷植物体组织、荷叶植物体组织、菊花植物体组织、甘草植物体组织、葛根植物体组织、树苔植物体组织、余甘子植物体组织、玫瑰植物体组织、薰衣草植物体组织中的至少一种；(1) The substrate raw materials include green tea plant tissue, black tea plant tissue, mint plant tissue, lotus leaf plant tissue, chrysanthemum plant tissue, licorice plant tissue, kudzu plant tissue, and tree moss plant tissue. , at least one of amla plant tissue, rose plant tissue, and lavender plant tissue;
    (2)所述基材原料筛分后的粒径大小为300目～500目；(2) The particle size of the base material raw material after screening is 300 mesh to 500 mesh;
    (3)所述基材原料与所述有效成分的质量比为10：(1～50)；(3) The mass ratio of the base material raw material to the active ingredient is 10: (1-50);
    (4)所述有效成分包括***提取物和/或***植物体组织，所述***提取物和/或***植物体组织包含***素；(4) The active ingredients include cannabis extract and/or cannabis plant tissue, and the cannabis extract and/or cannabis plant tissue contain cannabinoids;
    (5)所述***植物体组织包括***叶和/或***花；(5) The cannabis plant tissue includes cannabis leaves and/or cannabis flowers;
    (6)所述***素为***二酚和/或其他异构体；(6) The cannabinoid is cannabidiol and/or other isomers;
    (7)所述粘合剂包括水、乙醇、瓜尔胶、淀粉胶、壳聚糖、羧甲基纤维素、果胶、***胶、海藻酸钠、明胶、葡萄糖、聚丙烯醇及果糖中的至少一种；(7) The binder includes water, ethanol, guar gum, starch gum, chitosan, carboxymethylcellulose, pectin, gum arabic, sodium alginate, gelatin, glucose, polypropylene alcohol and fructose. at least one of;
    (8)所述成型的方式包括模具成型和/或螺杆压条设备压制成型；(8) The molding method includes mold molding and/or screw layering equipment press molding;
    (9)所述***素在所述卷烟插条中的质量占比为0.1％～70％。(9) The mass proportion of the cannabinoid in the cigarette cuttings is 0.1% to 70%.
  10. 根据权利要求7所述制备方法，其特征在于，所述制备方法具有如下特征中的至少一者：The preparation method according to claim 7, characterized in that the preparation method has at least one of the following characteristics:
    (1)所述卷烟插条的截面形状为圆形和/或多边形；(1) The cross-sectional shape of the cigarette insert is circular and/or polygonal;
    (2)所述卷烟插条的长度为1cm～7cm；(2) The length of the cigarette cuttings is 1cm to 7cm;
    (3)所述卷烟插条的宽度为1mm～3mm；(3) The width of the cigarette insert is 1 mm to 3 mm;
    (4)所述卷烟插条的密度为0.1g/cm 3～3.5g/cm 3； (4) The density of the cigarette cuttings is 0.1g/cm 3 to 3.5g/cm 3 ;
    (5)所述卷烟插条的硬度为38HD～80HD。(5) The hardness of the cigarette cuttings is 38HD to 80HD.
PCT/CN2022/087649 2022-03-31 2022-04-19 Cigarette insertion strip and preparation method therefor WO2023184618A1 (en)

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