WO2020163931A1 - Échantillonneur pour la collecte d'échantillons de liquides et de solides - Google Patents

Échantillonneur pour la collecte d'échantillons de liquides et de solides Download PDF

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Publication number
WO2020163931A1
WO2020163931A1 PCT/BR2020/050029 BR2020050029W WO2020163931A1 WO 2020163931 A1 WO2020163931 A1 WO 2020163931A1 BR 2020050029 W BR2020050029 W BR 2020050029W WO 2020163931 A1 WO2020163931 A1 WO 2020163931A1
Authority
WO
WIPO (PCT)
Prior art keywords
sampler
sampling
tank
quick
tube
Prior art date
Application number
PCT/BR2020/050029
Other languages
English (en)
Portuguese (pt)
Inventor
André VIEGAS WENTZ
Rogerio MESQUITA DE CARVALHO
André WEIJH
Original Assignee
Petróleo Brasileiro S.A. - Petrobras
Serviço Nacional De Aprendizagem Industrial - Departamento Regional Do Rio Grande Do Sul
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Petróleo Brasileiro S.A. - Petrobras, Serviço Nacional De Aprendizagem Industrial - Departamento Regional Do Rio Grande Do Sul filed Critical Petróleo Brasileiro S.A. - Petrobras
Publication of WO2020163931A1 publication Critical patent/WO2020163931A1/fr

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Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01FMEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F23/00Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm
    • G01F23/04Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm by dip members, e.g. dip-sticks
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • G01N1/12Dippers; Dredgers

Definitions

  • the present invention is related to inspection technologies, materials, equipment and corrosion. More particularly, the present invention relates to a sludge sampler in oil storage tanks.
  • the invention is related to the activity of collecting sludge samples in oil storage tanks at multiple depths, in homogeneous or not, through accesses to the reservoir roof with conventional and unconventional openings. This activity is necessary for correct characterization and disposal of oil sludge during the tank cleaning process.
  • This activity aims to assess the total sludge volume inside the tank using the same sediment sample collection operation in order to properly estimate the tank maintenance and cleaning procedures.
  • the tool (sampler) that performs this activity must be ergonomic, capable of use and easy and quick assembly by an operator.
  • the tool In addition, due to solvents and hydrocarbons, the tool must have chemical resistance to exposure to oil and its derivatives. The use of the tool must have safety provisions that prevent it from falling into the tank.
  • the sludge level measurement can be performed mechanically by introducing a ruler or measuring tape through access points on the tank's roof or by more sophisticated methods such as ultrasound or acquisition of infrared images of the tank's perimeter. These measurements are used for interpolation of the sludge surface and consequent calculation of the volume of waste included inside the tank.
  • the tools already have ergonomics and chemical resistance to hydrocarbons and solvents necessary for operation, however more than one tool is used for the measurement and characterization of the sludge.
  • US5408890A discloses a portable device for sampling small samples from a large container, in which the device is mounted on the container valve and has the sampler lowered and retrieved, and the sample is transferred to the removable container for the location of the analysis.
  • US20050183520A1 discloses a method and apparatus for manually sampling a fluid source in a well, comprising the act of lowering a tube containing containers and container lids (sampler) into a fluid in the well to allow said fluid pass from the well into the tube to fill at least a portion of the tube, so that the containers and container lids are submerged in the fluid, recover the tube, and close the containers with the container lids while they are still submerged in the fluid.
  • US8429986B2 discloses a device for groundwater sampling using a hydraulic coupler comprising a water sampling tube with an upper end connected to a second socket in a single unit and a lower end connected to a first plug in a single unit and a central casing tube.
  • Document KR896979B1 discloses a water sampler that uses a weight comprising: a control part with a cylinder; a water sampling part in which a sample injection part is formed; a movable part with an end inserted in the control part; a collection part with a water tank in which the sample emitted from the needle is stored; and a weight hanging from a connection ring formed at one end of the collection part.
  • Document US6058790A discloses an accordion-shaped cylindrical liquid sampling tube formed along a predetermined length of its main body so that the sampling tube can be shortened when in storage or transport and returned to its initial length when ready For use.
  • the shortening of the liquid sampling tube allows a larger number of liquid sampling tubes to occupy a certain space in relation to the number of liquid sampling tubes of standard, non-shortened length.
  • US5452620A discloses a sampler valve for use with a sampling device with a sampling tube and a sampling sphere to close one end of the sampler tube that is adapted to enter a tank to obtain a sample of the contents the tank, including a housing and a rotating sphere having a central opening to receive and pass the sampling tube through it; the rotating sphere cooperates with the sampling sphere for its movement away from one end of the sampling tube to allow fluid to escape from it; and an outlet to remove the liquid.
  • the present invention aims to solve the problems of the state of the art described above in a practical and efficient way.
  • the purpose of the present invention is to provide a sampler to collect samples of viscous and solid liquids (lees) that comprise, among other elements, multiple rods with a quick coupling system and enable its assembly quickly and effectively.
  • the present invention provides a sampler for collecting samples of liquids and solids that comprises a plurality of rods interconnected by quick coupling elements and a lower element adapted to carry out a sample collection of liquid.
  • Figure 1 illustrates a schematic view of the sampler for collecting samples of liquids and solids according to a preferred embodiment of the present invention.
  • Figure 1a illustrates a view of the configuration shown in Figure 1 in a disassembled configuration.
  • Figures 2a, 2b, 2c, 2d, and 2e illustrate an assembly sequence of the device of the present invention.
  • Figures 3a and 3b illustrate views and section of the tip sampler according to a particular configuration of the device of the present invention.
  • Figure 4 shows a sectional view of the quick coupling, according to a preferred configuration of the present invention.
  • Figure 5 shows an exploded view of a female type quick coupling according to a particular configuration of the present invention.
  • Figure 1 illustrates a schematic view of the sampler for collecting samples of liquids and solids according to a preferred embodiment of the present invention.
  • Figure 1 a illustrates a view of the configuration shown in Figure 1 in a disassembled configuration.
  • the sampler comprises a plurality of rods 15,13 interconnected by quick coupling elements 1, 3 and a lower element 14 adapted to carry out a liquid sample collection.
  • Figures 2a, 2b, 2c, 2d, and 2e illustrate an assembly sequence of the device of the present invention.
  • Figure 4 shows a sectional view of the quick coupler, according to a preferred configuration of the present invention.
  • Figure 5 shows an exploded view of a female type quick coupling according to a particular configuration of the present invention.
  • quick couplings can be divided into a male 1 and a female 3, where the female coupling it has articulated locks 4 (optionally by screws 5) that are forced into a semi-open position by a counterweight 6.
  • These couplings 1, 3 can be fixed by structural adhesive 10 in carbon fiber pultruded tubes 2, thus forming repetitive segments 15 which are added to achieve the desired depth.
  • These pultruded tubes maximize the longitudinal rigidity of the tool, thus minimizing its own weight.
  • the first stem segment 13 has a variation in the lower coupling, as it has quick couplings of the female type at both ends.
  • Figures 3a and 3b illustrate views and section of the sampling tip according to a particular configuration of the device of the present invention.
  • the coupling serves to fix the other rods 15 and at the bottom end to fix the sampling tip 14.
  • This tip 14 is composed of three parts, a sampling tube 7, made of translucent polymer, which allows visualization of the inside, a sampling valve 9 with flexible petals that allow sediment to enter the interior of the tube, but prevent it from returning, and a male of the quick coupler 8 where it is connected to the rod 13.
  • This male 8 has holes 8a connecting the inside of the sample cup and the outside to allow the fluid to flow out of the tip 14 as it is inserted into the tank.
  • Another intrinsic feature of the tool is its planned buoyancy. Due to its tubular shape 2, the volume of fluid displaced can be balanced with the weight force of each rod to create a safety feature that prevents the tool from falling into the tank, thus ensuring that it floats while being used.
  • the sampling tip 14 connected to the tip transport rod 13 is inserted into the tank.
  • the quick coupling locks themselves are used as a way of fixing the tank jacket allowing the operator to remain hands free to connect the next rod 15. Then the tool is lifted and the quick coupling is locked by moving the locks . In this way the cycle is repeated until the desired depth is reached.
  • the depth can be monitored by a graduation painted on the side of the stem every 10 cm, for example. This graduation, in line with the fact that each stem has exactly one meter, allows the height of the sludge level to be easily measured at the same time as the collection is carried out.
  • the tool of the invention has a reduced diameter to enter the accesses of the support legs of the floating roof of the oil tanks, having several sampling possibilities in the upper part of it.
  • the sludge sampling operation has height control on the rods, with the sampling aiming to acquire information on the chemical characteristics of the sludge as well as its total volume at the bottom of the tank, through the height control of the sampling.
  • the tool is divided into multiple rods of polymeric material and composite material, with low weight and suitable for ergonomic requirements for use by the same operator.
  • the tool also has a flotation system that cancels its weight by thrust when inserted into the tank, making the weight of the rods when removing the equipment to be minimized, facilitating the removal of the equipment from the work place. sampling.
  • a quick coupling system facilitates the assembly and disassembly of the segments.
  • the quick coupling system of the tool in addition to facilitating the operation, allows its locks to be used as support so that it does not fall into the tank when they are in the open position.
  • the locks are forced into a semi-open position by the effect of a metallic counterweight inside the female quick coupler.
  • the locks serve as automatic fixation at the access point for sampling and also serve as a safety lock, preventing the product from falling into the tanks.

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Physics & Mathematics (AREA)
  • Biochemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Fluid Mechanics (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

La présente invention concerne des dispositif de collecte d'échantillons de liquides. À cet effet, la présente invention concerne un échantillonneur pour la collecte d'échantillons de liquides et de solides, comprenant une pluralité de tiges reliées (13, 15) par des éléments de mise en prise rapide (1, 3) et un élément inférieur (14) conçu pour réaliser une collecte d'échantillon de liquide ou de solide.
PCT/BR2020/050029 2019-02-11 2020-02-06 Échantillonneur pour la collecte d'échantillons de liquides et de solides WO2020163931A1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
BR102019002749-5A BR102019002749B1 (pt) 2019-02-11 2019-02-11 Amostrador para coleta de amostras de líquidos e sólidos
BRBR102019002749-5 2019-02-11

Publications (1)

Publication Number Publication Date
WO2020163931A1 true WO2020163931A1 (fr) 2020-08-20

Family

ID=72043781

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/BR2020/050029 WO2020163931A1 (fr) 2019-02-11 2020-02-06 Échantillonneur pour la collecte d'échantillons de liquides et de solides

Country Status (3)

Country Link
AR (1) AR118049A1 (fr)
BR (1) BR102019002749B1 (fr)
WO (1) WO2020163931A1 (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116718420A (zh) * 2023-05-12 2023-09-08 长江生态环保集团有限公司 一种针对排水管网水质采样的装置及方法

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115200944B (zh) * 2022-07-14 2023-07-18 青海省地质环境调查院 一种基于矿泉水基地建设用水文地质智能化取样装置

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1416354A (en) * 1921-04-08 1922-05-16 Charles E Johnson Vacuum sampler for tanks of refined oil and gasoline
US1816726A (en) * 1930-06-11 1931-07-28 Emery G Friedman Oil sampler
FR2423767A1 (fr) * 1978-04-20 1979-11-16 Pipeline Service Sa Procede et dispositif de prise d'un echantillon de liquide dans une cuve de stockage
US4197744A (en) * 1978-08-14 1980-04-15 Overstreet Robbie J Gas safety roof gauging control hatch adapter
US4563896A (en) * 1983-11-09 1986-01-14 Bigheart Pipe Line Corporation Gauger's aid for use in sampling bottom sediment conditions in oil storage tanks
US4790197A (en) * 1987-07-29 1988-12-13 Riginos Kimonides Liquid sampling apparatus
CN202330062U (zh) * 2011-04-02 2012-07-11 上海冠戈实业有限公司 原油储罐采样器的防砂防堵功能结构件
CN203037493U (zh) * 2012-11-30 2013-07-03 中国石油天然气股份有限公司 油罐车含水原油全层取样器

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1416354A (en) * 1921-04-08 1922-05-16 Charles E Johnson Vacuum sampler for tanks of refined oil and gasoline
US1816726A (en) * 1930-06-11 1931-07-28 Emery G Friedman Oil sampler
FR2423767A1 (fr) * 1978-04-20 1979-11-16 Pipeline Service Sa Procede et dispositif de prise d'un echantillon de liquide dans une cuve de stockage
US4197744A (en) * 1978-08-14 1980-04-15 Overstreet Robbie J Gas safety roof gauging control hatch adapter
US4563896A (en) * 1983-11-09 1986-01-14 Bigheart Pipe Line Corporation Gauger's aid for use in sampling bottom sediment conditions in oil storage tanks
US4790197A (en) * 1987-07-29 1988-12-13 Riginos Kimonides Liquid sampling apparatus
CN202330062U (zh) * 2011-04-02 2012-07-11 上海冠戈实业有限公司 原油储罐采样器的防砂防堵功能结构件
CN203037493U (zh) * 2012-11-30 2013-07-03 中国石油天然气股份有限公司 油罐车含水原油全层取样器

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116718420A (zh) * 2023-05-12 2023-09-08 长江生态环保集团有限公司 一种针对排水管网水质采样的装置及方法

Also Published As

Publication number Publication date
BR102019002749A2 (pt) 2020-09-29
BR102019002749B1 (pt) 2024-03-12
AR118049A1 (es) 2021-09-15

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