WO2017156297A3 - Hybrid graphene materials and methods of fabrication - Google Patents

Hybrid graphene materials and methods of fabrication Download PDF

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Publication number
WO2017156297A3
WO2017156297A3 PCT/US2017/021614 US2017021614W WO2017156297A3 WO 2017156297 A3 WO2017156297 A3 WO 2017156297A3 US 2017021614 W US2017021614 W US 2017021614W WO 2017156297 A3 WO2017156297 A3 WO 2017156297A3
Authority
WO
WIPO (PCT)
Prior art keywords
metal substrate
graphene
coated metal
temperature
methods
Prior art date
Application number
PCT/US2017/021614
Other languages
French (fr)
Other versions
WO2017156297A2 (en
Inventor
Robert Terry KENNON
Deepak Varshney
Michael R. Johnson
Scott V. Johnson
Benjamin J. WEINER
Peter J. BORGHETTI
Original Assignee
Advanced Green Innovations, LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US15/068,269 external-priority patent/US20160194205A1/en
Application filed by Advanced Green Innovations, LLC filed Critical Advanced Green Innovations, LLC
Publication of WO2017156297A2 publication Critical patent/WO2017156297A2/en
Publication of WO2017156297A3 publication Critical patent/WO2017156297A3/en

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/182—Graphene
    • C01B32/184—Preparation

Abstract

Methods for fabricating graphene materials may coat a hydrocarbon precursor onto a metal substrate and heat the coated metal substrate to a first temperature. Methods may then maintain the first temperature of the coated metal substrate for a duration which dissociates the hydrocarbon precursor into carbon on the metal substrate, and cool the coated metal substrate to a second temperature that is lower than the first temperature. Heating the coated metal substrate may dissociate the hydrocarbon precursor and cooling the coated metal substrate may allow the dissociated hydrocarbon to arrange itself into graphene on the metal substrate. The present invention comprises a method of fabricating graphene (2D and 3D) structures, doped graphene, graphene-nanoparticle hybrid, graphene nanostructure hybrids using semisolid hydrocarbons in the absence of any gaseous precursors as well as method for forming multiple graphene patterns and transfer of the graphene patterns from the substrate to a transfer strip.
PCT/US2017/021614 2016-03-11 2017-03-09 Hybrid graphene materials and methods of fabrication WO2017156297A2 (en)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US15/068,269 US20160194205A1 (en) 2014-05-30 2016-03-11 Hybrid graphene materials and methods of fabrication
US15/068,269 2016-03-11
US201762453925P 2017-02-02 2017-02-02
US62/453,925 2017-02-02

Publications (2)

Publication Number Publication Date
WO2017156297A2 WO2017156297A2 (en) 2017-09-14
WO2017156297A3 true WO2017156297A3 (en) 2017-11-02

Family

ID=59789879

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2017/021614 WO2017156297A2 (en) 2016-03-11 2017-03-09 Hybrid graphene materials and methods of fabrication

Country Status (1)

Country Link
WO (1) WO2017156297A2 (en)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107893165B (en) * 2017-11-22 2020-01-21 上海紫燕合金应用科技有限公司 Preparation method of graphene-doped magnesium alloy structural member
US20210172905A1 (en) * 2018-01-04 2021-06-10 Lyten, Inc. Sensing device for detecting analytes in batteries
CN108722483B (en) * 2018-05-24 2022-03-18 江西师范大学 Preparation method of AuNPs-ZnONPs @ C/3D-KSC nanocomposite material with porous structure
CN109264706B (en) * 2018-10-16 2020-12-08 李红莉 Method for controllably preparing three-dimensional nano porous graphene powder by chemical vapor deposition method
CN109399623A (en) * 2018-10-23 2019-03-01 江汉大学 A kind of preparation method of two dimension graphitization nano carbon material
DE102018009125A1 (en) * 2018-11-21 2020-05-28 Neutrino Deutschland Gmbh Foil made of metal or a metal alloy
CN111348685B (en) * 2020-03-02 2023-01-10 新奥集团股份有限公司 Graphene-based composite material and preparation method and application thereof
WO2021188044A1 (en) * 2020-03-19 2021-09-23 Panasonic Factory Solutions Asia Pacific A method and an apparatus for manufacturing a porous graphene layer across a precursor material layer on a substrate through thermally localized laser graphitisation
CN113075266B (en) * 2021-03-25 2022-05-17 南京信息工程大学 NGQD/Fe2O3Graphene foam composite film and preparation method and application thereof
CN113328038B (en) * 2021-04-21 2022-08-30 温州大学 Preparation method of graphene-carbon nanotube heterojunction
CN114113238A (en) * 2021-11-17 2022-03-01 中国兵器工业集团第二一四研究所苏州研发中心 Gas sensor based on three-dimensional porous graphene @ quantum dot composite material and preparation method thereof
CN114824333B (en) * 2022-05-16 2023-11-21 北京德泰储能科技有限公司 Graphene modified electrode suitable for various flow battery systems and preparation method

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20140227211A1 (en) * 2011-03-15 2014-08-14 Peerless Worldwide, Llc Facile synthesis of graphene, graphene derivatives and abrasive nanoparticles and their various uses, including as tribologically-beneficial lubricant additives
US20140261998A1 (en) * 2013-03-15 2014-09-18 Guardian Industries Corp. Methods for low-temperature graphene precipitation onto glass, and associated articles/devices
US20150050482A1 (en) * 2013-08-14 2015-02-19 Rodney S. Ruoff Graphene synthesis by suppressing evaporative substrate loss during low pressure chemical vapor deposition
US20150206748A1 (en) * 2012-04-16 2015-07-23 Uchicago Argonne, Llc Graphene layer formation at low substrate temperature on a metal and carbon based substrate
WO2015119618A1 (en) * 2014-02-07 2015-08-13 Empire Technology Development Llc Method of producing graphene from a hydrocarbon gas and liquid metal catalysts
US20150235847A1 (en) * 2012-10-25 2015-08-20 Applied Materials, Inc. Growing graphene on substrates
WO2015184473A1 (en) * 2014-05-30 2015-12-03 Advanced Green Innovations, LLC Hybrid graphene materials and methods of fabrication

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20140227211A1 (en) * 2011-03-15 2014-08-14 Peerless Worldwide, Llc Facile synthesis of graphene, graphene derivatives and abrasive nanoparticles and their various uses, including as tribologically-beneficial lubricant additives
US20150206748A1 (en) * 2012-04-16 2015-07-23 Uchicago Argonne, Llc Graphene layer formation at low substrate temperature on a metal and carbon based substrate
US20150235847A1 (en) * 2012-10-25 2015-08-20 Applied Materials, Inc. Growing graphene on substrates
US20140261998A1 (en) * 2013-03-15 2014-09-18 Guardian Industries Corp. Methods for low-temperature graphene precipitation onto glass, and associated articles/devices
US20150050482A1 (en) * 2013-08-14 2015-02-19 Rodney S. Ruoff Graphene synthesis by suppressing evaporative substrate loss during low pressure chemical vapor deposition
WO2015119618A1 (en) * 2014-02-07 2015-08-13 Empire Technology Development Llc Method of producing graphene from a hydrocarbon gas and liquid metal catalysts
WO2015184473A1 (en) * 2014-05-30 2015-12-03 Advanced Green Innovations, LLC Hybrid graphene materials and methods of fabrication

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Publication number Publication date
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