WO2017022955A1 - Completely sealed sample container for gamma spectrometer - Google Patents

Completely sealed sample container for gamma spectrometer Download PDF

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Publication number
WO2017022955A1
WO2017022955A1 PCT/KR2016/007214 KR2016007214W WO2017022955A1 WO 2017022955 A1 WO2017022955 A1 WO 2017022955A1 KR 2016007214 W KR2016007214 W KR 2016007214W WO 2017022955 A1 WO2017022955 A1 WO 2017022955A1
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WIPO (PCT)
Prior art keywords
sample
housing
cover
sample container
coupling portion
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PCT/KR2016/007214
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French (fr)
Korean (ko)
Inventor
오정석
이상한
이민기
윤세원
Original Assignee
한국표준과학연구원
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Publication of WO2017022955A1 publication Critical patent/WO2017022955A1/en

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01TMEASUREMENT OF NUCLEAR OR X-RADIATION
    • G01T1/00Measuring X-radiation, gamma radiation, corpuscular radiation, or cosmic radiation
    • G01T1/16Measuring radiation intensity
    • G01T1/167Measuring radioactive content of objects, e.g. contamination
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01TMEASUREMENT OF NUCLEAR OR X-RADIATION
    • G01T7/00Details of radiation-measuring instruments
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01TMEASUREMENT OF NUCLEAR OR X-RADIATION
    • G01T7/00Details of radiation-measuring instruments
    • G01T7/02Collecting means for receiving or storing samples to be investigated and possibly directly transporting the samples to the measuring arrangement; particularly for investigating radioactive fluids

Definitions

  • the present invention relates to a hermetically sealed sample container for a gamma spectrometer.
  • the present invention includes a housing containing a sample to be measured for radioactivity and a cover for blocking a sample introduced into the housing from the outside, and seaming the housing and the cover to completely block external leakage of the sample.
  • a fully sealed sample container for a spectrometer is a fully sealed.
  • the lower housing 10 in which the sample is located the first cover 20 which primarily isolates the sample located in the housing 10 from the outside, And a marinel beaker composed of a first cover 20 and the second cover 30 to isolate the outside secondary is widely used.
  • the first cover 20 is inserted into the lower housing 10, and the inner wall of the lower housing 10 is connected to the first cover 20.
  • the first cover 20 is pressed into the lower housing 10 by pressing the outer wall formed at the edge. Therefore, the first cover 20 is inserted into the lower housing 10 and the air in the first cover 20 to discharge the air located in the first inner space 11 of the lower housing 10 to the outside.
  • the discharge hole 21 should be formed.
  • the fluid sample when the fluid sample is positioned in the conventional Marinelli beaker, the sample is moved to the second inner space formed between the first cover 20 and the second cover 30 through the discharge hole 21 and outflows to the outside.
  • the biological sample when the biological sample is stored, the biological sample is decayed and the generated gas is not completely blocked by the second cover 30, thereby causing a problem of polluting the surroundings.
  • the performance test of radioactivity meters that measure the radioactivity of samples placed in marineli beakers is not clearly performed if the sample is released directly to the outside or if the nuclide is released through the gas. Therefore, there arises a problem that the reliability of the test for verifying the performance of the radiometer decreases.
  • the combination of the lower housing 10 and the first cover 20 is a method in which the lower housing 10 presses the first cover 20, the lower housing 10 and the first cover 20 are stored in the marineli beaker after the performance test of the radiometer.
  • the process of discarding the sample is difficult because the separation of the first cover 20 and the lower housing 10 is difficult.
  • the present invention has been made in order to solve the above problems, to completely seal the container in which the sample is stored to prevent the discharge of the sample to the outside and can easily perform the operation of discarding the sample, for gamma spectroscopy
  • the purpose is to provide a fully sealed sample container.
  • the sample container is the inlet to which the sample is introduced from the outside, the inner space where the sample introduced through the inlet is located, the sample of the sample located in the inner space
  • a cylindrical housing including a fixing part into which a measuring instrument measuring radioactivity is inserted, and a first coupling part of which an upper end of the inlet is bent outwardly;
  • a cover having a lower surface corresponding to the inlet and including a second coupling portion seaming with the first coupling portion along an edge thereof.
  • the cover may further include a pull tab on the upper surface and a cutting groove provided in the inner side of the second coupling portion such that the cover is separated from the housing by an external force transmitted through the pull tab.
  • the second coupling portion is configured to be inclined inclined from the inner side to the outer side facing the first coupling portion, and the first coupling portion is bent to abut each other in correspondence to the inclination of the opposing surface of the second coupling portion. It may be configured in the form.
  • the housing may be provided with one or more bends on the outer circumferential surface.
  • the cover may be made of a gas permeable material or a gas barrier material.
  • the fixing part may have a cylindrical shape having a constant radius with respect to the vertical longitudinal axis of the housing.
  • the housing and the cover are seamed so that the sample stored in the housing does not leak out.
  • the sample container has a structure in which the respective coupling portions formed in the housing and the cover are fitted to each other, so that the sample and the lid can be easily shimmed.
  • the sample container according to an embodiment of the present invention is provided with a pull tab on the cover so that the sample stored in the housing can be easily disposed.
  • a pull tab on the cover so that the sample stored in the housing can be easily disposed.
  • the durability of the housing against external pressure applied in the vertical direction is improved.
  • FIG. 1 is an exploded perspective view showing a conventional marinel beaker.
  • Figure 2 is a vertical cross-sectional view of a conventional marinel beaker.
  • Figure 3 is a perspective view showing a fully sealed sample container for a gamma spectrometer according to an embodiment of the present invention.
  • Figure 4 is a cross-sectional view showing a fully sealed sample container for the gamma spectrometer according to an embodiment of the present invention.
  • FIG. 5 is a cross-sectional view and a partially enlarged view showing a hermetically sealed sample container for a gamma spectrometer according to an embodiment of the present invention.
  • FIG. 6 is a conceptual diagram illustrating a configuration in which the first coupling portion and the second coupling portion are seamed.
  • FIG. 7 is a cross-sectional view of a sample container provided with a bent portion according to an embodiment of the present invention.
  • FIG. 8 is a view illustrating a shape in which a sample is filled in a sample container according to an embodiment of the present invention.
  • the present invention is a hermetically sealed sample container for a gamma spectrometer according to an embodiment of the present invention, a housing 100 in which a sample used for a radioactivity measurement test is stored, and a housing 100 coupled to the housing 100. It includes a cover 200 for blocking the sample stored inside and the outside.
  • the housing 100 has an inlet 110 through which the sample is introduced from the outside and an inner space in which the sample introduced through the inlet 110 is provided. 120).
  • the fixing unit 130 is inserted into the measuring instrument for measuring the amount of radiation of the sample located in the inner space 120, and the first coupling portion 140, the upper end of the inlet 110 is bent to the outside.
  • the cover 200 has a bottom surface corresponding to the inflow portion 110, and has a second coupling portion 210 at an edge thereof.
  • the first coupling part 140 of the housing 100 and the second coupling part 210 of the lid 200 are seamed.
  • the housing 100 and the cover 200 are separated from each other, and the first coupling part 140 and the cover 200 formed on the upper edge of the housing 100 are separated from each other.
  • the second coupling portion 210 is made of a structure that is easy to combine with each other. After the sample is introduced into the space 120 inside the housing 100, the second coupling part 210 is seated to face the first coupling part 140 as shown in FIG. 5, and then the The second coupling part 210 and the first coupling part 140 are folded or rolled together to couple the housing 100 and the cover 200 to each other.
  • the vertical axis of the housing 100 and the cover 200 is not located on the same line.
  • the second coupling part 210 may be configured such that a surface facing the first coupling part 140 is inclined inclined from the inner side to the outer side. have.
  • the first coupling part 140 may be bent to be in contact with each other in response to the inclination of the facing surface of the second coupling part 210.
  • the ratio of the first coupling part 140 and the second coupling part 210 that are folded together is a planned numerical value. If it is out of the problem, the coupling force is weakened. In other words, when the length of the second coupling portion 210 is insufficient or is formed too long, a problem that the sealing force is lowered may occur.
  • the second coupling portion 210 has a funnel-like structure that opens toward the upper side and the first coupling portion 140 is configured to be fitted to the second coupling portion 210. Accordingly, the ratio of the folding of the first coupling portion 140 and the second coupling portion 210 to each other may be maintained within a predetermined numerical range.
  • the seaming structure of the first coupling portion 140 and the second coupling portion 210 in Figure 6 (b) is a form of bending once, but is not limited to this is optionally stored in the space 120
  • the sample may be banded a plurality of times to prevent the sample from being released to the outside.
  • a fully sealed sample container for a gamma spectrometer may have a pull tap 220 and an edge of the lid 200 on an upper surface of the lid 200 as shown in FIG. 3. It may include a cutting groove 230 provided on the inner side of the second coupling portion (210).
  • the sample container is preferably configured to easily discharge the sample to the outside for disposal of the internal sample.
  • the pull tab 220 pressing the edge of the lid 200 and the cutting groove 230 along the edge of the lid 200 may be provided on the upper surface of the lid 200 using the principle of the lever. .
  • the sample container can be easily discharged to the outside of the sample located in the space 120 by the inner cover of the cover 200 is separated.
  • the fully sealed sample container for the gamma spectrometer may be provided with a single or a plurality of bent portion 150 on the outer peripheral surface of the housing (100).
  • the fully sealed sample container for the gamma spectrometer according to the embodiment of the present invention is mostly used after being used once to prevent the reliability of the performance test of the radiometer by mixing different samples. Discarded.
  • the housing 100 is made of polyethylene (PE) material or polypropylene (PP) material, which is easy to mold and low in cost, but when the housing 100 is made of such a material, the durability becomes weak, Frequently, deformation of the housing 100 occurs.
  • PE polyethylene
  • PP polypropylene
  • the outer peripheral surface of the housing 100 is provided with a bent portion 150 having a polygonal cross section, the housing ( 100) can be configured to improve the durability.
  • the bend 150 may be configured to have a variety of forms of cross-sectional shape of the bend if it can effectively respond to the external force.
  • the fixing part 130 is preferably made of a cylindrical shape having a constant radius (r) with respect to the vertical longitudinal axis of the housing (100).
  • a radiometer is inserted into the fixing part 130 of the sample container, and the inserted radiometer measures radioactivity of a sample present in the housing 100.
  • the radiation emitted from the radionuclides constituting the sample is measured.
  • the amount of self absorption is modified so that an error occurs in the radiation level measured by the inserted radiometer.
  • the fixing part 130 is preferably configured to have a cylindrical shape having a constant radius (r) based on the vertical longitudinal axis of the housing (100).
  • the space in the housing 120 may be configured such that the b and c values of the space 120 in which the sample in the housing 100 is filled are equal to each other.
  • the a value which is a height at which the sample is filled on the upper side of the fixing part 130, is also provided with a scale for visually checking the a value in the housing 100 so that the b value and the same value as the c value can be adjusted. It is preferable.
  • the radioactivity of the sample can be more accurately measured through the radiometer inserted into the fixing part 130. have.
  • the cover 200 may be made of a gas permeable material or a gas barrier line material according to the characteristics of the sample located in the space 120.
  • the biological sample when the biological sample is located in the space 120 of the housing 100, the biological sample may be decayed and gas may be generated, thereby causing an explosion accident. Therefore, when the sample from which a large amount of gas is discharged is located in the space 120, it is preferable that the cover 200 is made of a gas permeable material.
  • the lid 200 may be made of a gas impermeable material.
  • the cover 200 is made of a gas-permeable material to prevent the nuclide from being released to the outside, thereby preventing accidents that may occur in the radioactivity test.

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  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • High Energy & Nuclear Physics (AREA)
  • Molecular Biology (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Measurement Of Radiation (AREA)

Abstract

The present invention relates to a completely sealed sample container for a gamma spectrometer. The sample container according to the present invention comprises: a housing in which a sample, of which the radioactivity is to be measured, is positioned; and a cover for blocking the sample in the housing from the outside, and has a structure for completely blocking the external leakage of the sample by seaming the housing and the cover. Therefore, if a performance test of a radiation detector is carried out using the present invention, more reliable test results can be obtained.

Description

감마분광분석기용 완전 밀폐형 시료 용기Fully sealed sample container for gamma spectroscopy
본 발명은 감마분광분석기용 완전 밀폐형 시료 용기에 관한 것이다. 자세하게, 본 발명은 방사능을 측정하고자 하는 시료를 담는 하우징과 하우징에 유입된 시료를 외부와 차단하는 덮개를 구비하고 상기 하우징과 상기 덮개를 시밍(seaming)하여 시료의 외부 유출을 완전 차단시키는, 감마분광분석기용 완전 밀폐형 시료 용기에 관한 것이다.The present invention relates to a hermetically sealed sample container for a gamma spectrometer. In detail, the present invention includes a housing containing a sample to be measured for radioactivity and a cover for blocking a sample introduced into the housing from the outside, and seaming the housing and the cover to completely block external leakage of the sample. A fully sealed sample container for a spectrometer.
일반적으로, 방사능 측정 성능 시험에 있어서 도 1에 도시된 것과 같이 시료가 위치되는 하부 하우징(10)과, 하우징(10)에 위치된 시료를 외부와 1차적으로 격리 시키는 제1 덮개(20), 및 제1 덮개(20)와 외부를 2차적으로 격리 시키는 제2 덮개(30)로 구성된 마리넬리 비이커가 널리 이용되고 있다.In general, in the radioactivity measurement performance test, as shown in FIG. 1, the lower housing 10 in which the sample is located, the first cover 20 which primarily isolates the sample located in the housing 10 from the outside, And a marinel beaker composed of a first cover 20 and the second cover 30 to isolate the outside secondary is widely used.
그러나, 종래에 사용되던 마리넬리 비이커는 도 2에 도시된 바와 같이 제1 덮개(20)가 하부 하우징(10)의 내부로 삽입되며, 하부 하우징(10)의 내벽이 제1 덮개(20)의 가장자리에 형성된 외벽을 압박하여 제1 덮개(20)가 하부 하우징(10)에 끼움 고정되는 구조로 이루어진다. 때문에, 제1 덮개(20)가 하부 하우징(10)의 내부로 삽입되며 하부 하우징(10)의 제1 내부공간(11)에 위치하고 있는 공기를 외부로 방출하기 위해 제1 덮개(20)에 공기 배출공(21)이 형성되어야 한다.However, in a conventionally used marinel beaker, as shown in FIG. 2, the first cover 20 is inserted into the lower housing 10, and the inner wall of the lower housing 10 is connected to the first cover 20. The first cover 20 is pressed into the lower housing 10 by pressing the outer wall formed at the edge. Therefore, the first cover 20 is inserted into the lower housing 10 and the air in the first cover 20 to discharge the air located in the first inner space 11 of the lower housing 10 to the outside. The discharge hole 21 should be formed.
따라서, 종래 마리넬리 비이커에 유체 시료가 위치 될 경우 그 시료가 배출공(21)을 통해 제1 덮개(20)와 제2 덮개(30) 사이에 형성된 제2 내부공간으로 이동하게 되어 외부로 유출되는 단점이 발생된다. 특히, 생체시료를 보관할 경우 생체시료가 부패되며 발생하는 가스를 제2 덮개(30)에서 완벽하게 차단하지 못해, 주변을 오염시키는 문제점이 발생한다. 시료가 직접적으로 외부로 유출되거나, 가스를 통해 핵종이 외부로 배출될 경우 마리넬리 비이커에 위치하는 시료의 방사능을 측정하는 방사능 측정기의 성능시험(performance test)이 명확히 수행되지 않는다. 따라서, 방사능 측정기의 성능을 검증하는 시험의 신뢰성이 하락하는 문제가 발생한다.Therefore, when the fluid sample is positioned in the conventional Marinelli beaker, the sample is moved to the second inner space formed between the first cover 20 and the second cover 30 through the discharge hole 21 and outflows to the outside. Disadvantages arise. In particular, when the biological sample is stored, the biological sample is decayed and the generated gas is not completely blocked by the second cover 30, thereby causing a problem of polluting the surroundings. The performance test of radioactivity meters that measure the radioactivity of samples placed in marineli beakers is not clearly performed if the sample is released directly to the outside or if the nuclide is released through the gas. Therefore, there arises a problem that the reliability of the test for verifying the performance of the radiometer decreases.
뿐만 아니라, 하부 하우징(10)과 제1 덮개(20)의 결합은 하부 하우징(10)이 제1 덮개(20)를 압박하는 방식이기 때문에, 방사능 측정기의 성능시험이 끝난 후 마리넬리 비이커에 보관되는 시료를 폐기시킬 시, 제1 덮개(20)와 하부 하우징(10)의 분리가 어려워 시료를 폐기 시키는 공정이 어려워지는 단점 또한 존재한다.In addition, since the combination of the lower housing 10 and the first cover 20 is a method in which the lower housing 10 presses the first cover 20, the lower housing 10 and the first cover 20 are stored in the marineli beaker after the performance test of the radiometer. When the sample is to be discarded, there is also a disadvantage that the process of discarding the sample is difficult because the separation of the first cover 20 and the lower housing 10 is difficult.
결국, 시료를 외부와 완벽하게 차단하여 시료의 운반 및 보관 과정에서 시료가 외부로 방출되는 것을 방지하고, 덮개의 개폐가 용이하게 이루어질 수 있는 감마분광분석기용 완전 밀폐형 시료 용기의 필요성이 대두 되고 있다.As a result, there is a need for a completely sealed sample container for a gamma spectrometer that can completely block a sample from the outside to prevent the sample from being released to the outside during transport and storage of the sample, and to easily open and close the cover. .
본 발명은 상기와 같은 문제점을 해결하기 위하여 안출된 것으로서, 시료가 보관되는 용기를 완전 밀폐하여 시료가 외부로 방출되는 것을 방지하고 시료를 폐기하는 작업을 용이하게 수행할 수 있는, 감마분광분석기용 완전 밀폐형 시료 용기를 제공하는데 그 목적이 있다. The present invention has been made in order to solve the above problems, to completely seal the container in which the sample is stored to prevent the discharge of the sample to the outside and can easily perform the operation of discarding the sample, for gamma spectroscopy The purpose is to provide a fully sealed sample container.
상기와 같은 목적을 달성하기 위해서, 본 발명의 일 실시 예에 따른 시료 용기는 외부에서 시료가 유입되는 유입부, 상기 유입부를 통해 유입된 시료가 위치되는 내부 공간, 상기 내부 공간에 위치하는 시료의 방사능을 측정하는 계측기가 삽입되는 고정부, 및 상기 유입부의 상측 단부가 외측으로 구부러진 제1 결합부를 포함하는 원통형 하우징; 및 하면이 상기 유입부에 대응되고, 가장자리를 따라서 상기 제1 결합부와 시밍(seaming)되는 제2 결합부를 포함하는 덮개를 포함한다.In order to achieve the above object, the sample container according to an embodiment of the present invention is the inlet to which the sample is introduced from the outside, the inner space where the sample introduced through the inlet is located, the sample of the sample located in the inner space A cylindrical housing including a fixing part into which a measuring instrument measuring radioactivity is inserted, and a first coupling part of which an upper end of the inlet is bent outwardly; And a cover having a lower surface corresponding to the inlet and including a second coupling portion seaming with the first coupling portion along an edge thereof.
여기서, 상기 덮개는, 상면에 풀탭과, 상기 풀탭을 통해 전달되는 외력에 의해서 상기 덮개가 상기 하우징에서 분리되도록 상기 제2 결합부의 안측에 구비되는 절단홈을 더 포함할 수 있다.Here, the cover may further include a pull tab on the upper surface and a cutting groove provided in the inner side of the second coupling portion such that the cover is separated from the housing by an external force transmitted through the pull tab.
그리고, 상기 제2 결합부는 상기 제1 결합부와 마주보는 면이 내측에서 외측으로 갈수록 경사지게 기울어지도록 구성되고, 상기 제1 결합부는 상기 제2 결합부의 마주보는 면의 경사에 대응하여 서로 맞닿도록 구부러진 형태로 구성될 수 있다.The second coupling portion is configured to be inclined inclined from the inner side to the outer side facing the first coupling portion, and the first coupling portion is bent to abut each other in correspondence to the inclination of the opposing surface of the second coupling portion. It may be configured in the form.
상기 하우징은, 외주면에 단수 또는 복수개의 굴곡부가 구비될 수 있다.The housing may be provided with one or more bends on the outer circumferential surface.
상기 덮개는, 가스 투과성 재질 또는 가스 차단성 재질로 구성될 수 있다.The cover may be made of a gas permeable material or a gas barrier material.
상기 고정부는 상기 하우징의 상하 길이방향 중심축을 기준으로 일정한 반경을 가지는 원통 형상일 수 있다.The fixing part may have a cylindrical shape having a constant radius with respect to the vertical longitudinal axis of the housing.
본 발명의 실시 예에 따른 시료 용기는, 하우징과 덮개가 서로 시밍되어 하우징 내부에 보관되는 시료가 외부로 유출되지 않게 해준다. 그리고, 상기 시료 용기는 하우징과 덮개에 형성된 각각의 결합부가 서로 끼워지는 구조를 가지어, 숙련자가 아니라도 하우징과 덮개의 시밍을 용이하게 수행할 수 있다.In the sample container according to the embodiment of the present invention, the housing and the cover are seamed so that the sample stored in the housing does not leak out. In addition, the sample container has a structure in which the respective coupling portions formed in the housing and the cover are fitted to each other, so that the sample and the lid can be easily shimmed.
본 발명의 실시 예에 따른 상기 시료 용기는 덮개에 풀탭을 구비하여 하우징 내부에 보관되는 시료를 용이하게 폐기시킬 수 있도록 해 준다. 또한, 하우징의 외주면에 굴곡부를 구비하여 상하방향으로 가해지는 외부 압력에 대한 하우징의 내구성이 향상되었다.The sample container according to an embodiment of the present invention is provided with a pull tab on the cover so that the sample stored in the housing can be easily disposed. In addition, by providing a bent portion on the outer circumferential surface of the housing, the durability of the housing against external pressure applied in the vertical direction is improved.
도 1은 종래의 마리넬리 비이커를 나타낸 분해 사시도.1 is an exploded perspective view showing a conventional marinel beaker.
도 2는 종래의 마리넬리 비이커를 나타낸 상하 단면도.Figure 2 is a vertical cross-sectional view of a conventional marinel beaker.
도 3은 본 발명의 실시 예에 따른 감마분광분석기용 완전 밀폐형 시료 용기를 나타낸 사시도.Figure 3 is a perspective view showing a fully sealed sample container for a gamma spectrometer according to an embodiment of the present invention.
도 4는 본 발명의 실시 예에 따른 감마분광분석기용 완전 밀폐형 시료 용기를 나타낸 단면도.Figure 4 is a cross-sectional view showing a fully sealed sample container for the gamma spectrometer according to an embodiment of the present invention.
도 5는 본 발명의 실시 예에 따른 감마분광분석기용 완전 밀폐형 시료 용기를 나타낸 단면도 및 부분 확대도.5 is a cross-sectional view and a partially enlarged view showing a hermetically sealed sample container for a gamma spectrometer according to an embodiment of the present invention.
도 6은 제1 결합부와 제2 결합부가 시밍되는 구성을 도시한 개념도.6 is a conceptual diagram illustrating a configuration in which the first coupling portion and the second coupling portion are seamed.
도 7은 본 발명의 실시 예에 따른 굴곡부가 구비된 시료 용기의 단면도.7 is a cross-sectional view of a sample container provided with a bent portion according to an embodiment of the present invention.
도 8은 본 발명의 실시 예에 따른 시료 용기 내에 시료가 채워진 형상을 도시한 도면.8 is a view illustrating a shape in which a sample is filled in a sample container according to an embodiment of the present invention.
이하, 상기와 같은 본 발명인 감마분광분석기용 완전 밀폐형 시료 용기에 대하여 설명하도록 한다.Hereinafter, the fully-closed sample container for the gamma spectrometer of the present invention as described above will be described.
도 3을 참조하여 설명하면, 본 발명인 감마분광분석기용 완전 밀폐형 시료 용기는, 내부에 방사능 측정 시험에 사용되는 시료가 보관되는 하우징(100)과, 상기 하우징(100)과 결합되어 하우징(100) 내부에 보관되는 시료를 외부와 차단하는 덮개(200)를 포함한다.Referring to FIG. 3, the present invention is a hermetically sealed sample container for a gamma spectrometer according to an embodiment of the present invention, a housing 100 in which a sample used for a radioactivity measurement test is stored, and a housing 100 coupled to the housing 100. It includes a cover 200 for blocking the sample stored inside and the outside.
도 4와 도 5를 참조하여 상세히 설명하면, 상기 하우징(100)은 상측에 외부에서 시료가 유입되는 유입부(110)와, 상기 유입부(110)를 통해 유입된 시료가 구비되는 내부 공간(120)을 가진다. 또한, 내부 공간(120)에 위치하는 시료의 방사선 양을 측정하는 계측기가 삽입되는 고정부(130), 및 유입부(110)의 상측 단부가 외측으로 구부러진 제1 결합부(140)를 포함한다. 상기 덮개(200)는 하면이 상기 유입부(110)에 대응하는 형상을 가지고, 가장자리에 제2 결합부(210)를 구비한다. 그래서, 본 발명의 실시 예에 따른 시료 용기는 상기 하우징(100)의 상기 제1 결합부(140)와 상기 덮개(200)의 상기 제2 결합부(210)가 시밍(seaming)된다.4 and 5, the housing 100 has an inlet 110 through which the sample is introduced from the outside and an inner space in which the sample introduced through the inlet 110 is provided. 120). In addition, the fixing unit 130 is inserted into the measuring instrument for measuring the amount of radiation of the sample located in the inner space 120, and the first coupling portion 140, the upper end of the inlet 110 is bent to the outside. . The cover 200 has a bottom surface corresponding to the inflow portion 110, and has a second coupling portion 210 at an edge thereof. Thus, in the sample container according to the embodiment of the present invention, the first coupling part 140 of the housing 100 and the second coupling part 210 of the lid 200 are seamed.
이하에서는, 도 4 내지 도 6을 참조하여 상기 하우징(100) 및 덮개(200)의 시밍 구조 및 방법을 설명하도록 하겠다.Hereinafter, the seaming structure and method of the housing 100 and the cover 200 will be described with reference to FIGS. 4 to 6.
도 4를 참조하여 설명하면 상기 하우징(100)과 상기 덮개(200)는 서로 분리 되어 있고, 상기 하우징(100)의 상단부 가장자리에 형성된 상기 제1 결합부(140) 및 상기 덮개(200)의 상기 제2 결합부(210)가 서로 결합이 용이한 구조로 이루어진다. 하우징(100) 내부의 공간(120)에 시료를 유입시킨 후, 도 5에 도시된 바와 같이 상기 제2 결합부(210)를 상기 제1 결합부(140)와 서로 마주보게 안착시킨 후, 상기 제2 결합부(210) 및 상기 제1 결합부(140)를 함께 접거나 말아 상기 하우징(100)과 상기 덮개(200)를 서로 결합시킨다.Referring to FIG. 4, the housing 100 and the cover 200 are separated from each other, and the first coupling part 140 and the cover 200 formed on the upper edge of the housing 100 are separated from each other. The second coupling portion 210 is made of a structure that is easy to combine with each other. After the sample is introduced into the space 120 inside the housing 100, the second coupling part 210 is seated to face the first coupling part 140 as shown in FIG. 5, and then the The second coupling part 210 and the first coupling part 140 are folded or rolled together to couple the housing 100 and the cover 200 to each other.
이때, 상기 제1 결합부(140)와 상기 제2 결합부(210)를 서로 마주보게 안착시키는 과정에서, 상기 하우징(100)과 상기 덮개(200)의 상하방향 중심축이 동일선상에 위치되지 않는 것을 방지하기 위해, 도 6의 (a)에 도시된 바와 같이 상기 제2 결합부(210)는 상기 제1 결합부(140)와 마주보는 면이 내측에서 외측으로 갈수록 경사지게 기울어지도록 구성될 수 있다. 그리고, 상기 제1 결합부(140)는 상기 제2 결합부(210)의 마주보는 면의 경사에 대응하여 서로 맞닿도록 구부러지게 구성될 수 있다.At this time, in the process of seating the first coupling portion 140 and the second coupling portion 210 facing each other, the vertical axis of the housing 100 and the cover 200 is not located on the same line. As shown in FIG. 6A, the second coupling part 210 may be configured such that a surface facing the first coupling part 140 is inclined inclined from the inner side to the outer side. have. In addition, the first coupling part 140 may be bent to be in contact with each other in response to the inclination of the facing surface of the second coupling part 210.
상세히 설명하면, 상기 제1 결합부(140)와 상기 제2 결합부(210)를 시밍하는 경우, 함께 접히는 상기 제1 결합부(140)와 상기 제2 결합부(210)의 비율이 계획된 수치에서 벗어나게 되면, 결합력이 약해지는 문제가 발생하게 된다. 다시 말해서, 상기 제2 결합부(210)의 길이가 부족하거나 너무 길게 형성되는 경우 밀폐력이 떨어지는 문제가 발생될 수 있다.In detail, when seaming the first coupling part 140 and the second coupling part 210, the ratio of the first coupling part 140 and the second coupling part 210 that are folded together is a planned numerical value. If it is out of the problem, the coupling force is weakened. In other words, when the length of the second coupling portion 210 is insufficient or is formed too long, a problem that the sealing force is lowered may occur.
이러한 문제를 해결하기 위해서, 상기 제2 결합부(210)는 상측으로 갈수록 벌어지는 깔대기 형 구조를 가지고 상기 제1 결합부(140)는 상기 제2 결합부(210)에 끼워지도록 구성한다. 그에 따라, 상기 제1 결합부(140)와 상기 제2 결합부(210)의 서로 접히는 비율이 일정 수치 범위 내에 유지될 수 있다.In order to solve this problem, the second coupling portion 210 has a funnel-like structure that opens toward the upper side and the first coupling portion 140 is configured to be fitted to the second coupling portion 210. Accordingly, the ratio of the folding of the first coupling portion 140 and the second coupling portion 210 to each other may be maintained within a predetermined numerical range.
아울러, 도 6의 (b)에서 상기 제1 결합부(140)와 상기 제2 결합부(210)의 시밍 구조는 한번 밴딩된 형태이나, 이에 한정되지 아니하고 선택적으로 상기 공간(120)에 보관되는 시료가 외부로 방출되는 것을 방지하기 위해서 복수 번 밴딩된 형태일 수 있다.In addition, the seaming structure of the first coupling portion 140 and the second coupling portion 210 in Figure 6 (b) is a form of bending once, but is not limited to this is optionally stored in the space 120 The sample may be banded a plurality of times to prevent the sample from being released to the outside.
본 발명의 실시 예에 따른 감마분광분석기용 완전 밀폐형 시료 용기는 도 3에 도시된 바와 같이 상기 덮개(200)의 상면에 풀탭(pull tap)(220)과, 상기 덮개(200)의 가장자리를 따라 상기 제2 결합부(210)의 안측에 구비된 절단홈(230)을 포함할 수 있다.A fully sealed sample container for a gamma spectrometer according to an exemplary embodiment of the present invention may have a pull tap 220 and an edge of the lid 200 on an upper surface of the lid 200 as shown in FIG. 3. It may include a cutting groove 230 provided on the inner side of the second coupling portion (210).
도 3을 참조하여 상세히 설명하면. 상기 시료 용기는 내부 시료의 폐기를 위해서 외부로 시료를 배출하기 용이하게 구성되는 것이 바람직하다.Referring to Figure 3 in detail. The sample container is preferably configured to easily discharge the sample to the outside for disposal of the internal sample.
따라서, 상기 덮개(200)의 상면에 지렛대의 원리를 이용해 덮개(200)의 가장자리를 압박하는 상기 풀탭(220)과, 상기 덮개(200)의 가장자리를 따라서 절단홈(230)을 구비할 수 있다. 그래서, 상기 덮개(200)의 중심점에 근접한 상기 풀탭(220)의 내측 끝단을 상측으로 당길 시, 상기 풀탭(220)의 외측 끝단이 상기 절단홈(230)을 압박하여 상기 덮개(200)는 상기 전단홈(230)의 외측에 위치되는 외측 덮개와 절단홈(230)의 내측에 위치되는 내측 덮개로 분리된다. 이로써, 상기 시료 용기는 상기 덮개(200)의 내측 덮개가 분리되어 손쉽게 상기 공간(120)에 위치된 시료를 외부로 배출할 수 있다.Therefore, the pull tab 220 pressing the edge of the lid 200 and the cutting groove 230 along the edge of the lid 200 may be provided on the upper surface of the lid 200 using the principle of the lever. . Thus, when the inner end of the pull tab 220 near the center point of the cover 200 is pulled upward, the outer end of the pull tab 220 presses the cutting groove 230 so that the cover 200 is It is separated into an outer cover which is located outside the shear groove 230 and an inner cover which is located inside the cutting groove 230. Thus, the sample container can be easily discharged to the outside of the sample located in the space 120 by the inner cover of the cover 200 is separated.
또한, 본 발명의 실시 예에 따른 감마분광분석기용 완전 밀폐형 시료 용기는 상기 하우징(100)의 외주면에 단수 또는 복수개의 굴곡부(150)를 구비할 수 있다.In addition, the fully sealed sample container for the gamma spectrometer according to an embodiment of the present invention may be provided with a single or a plurality of bent portion 150 on the outer peripheral surface of the housing (100).
도 7을 참조하여 설명하면, 본 발명의 실시 예에 따른 감마분광분석기용 완전 밀폐형 시료 용기는 서로 다른 시료가 섞이어 방사능 측정기의 성능 테스트의 신뢰성이 떨어지는 것을 방지하기 위하여, 일회 사용된 이후에는 대부분 폐기된다. Referring to FIG. 7, the fully sealed sample container for the gamma spectrometer according to the embodiment of the present invention is mostly used after being used once to prevent the reliability of the performance test of the radiometer by mixing different samples. Discarded.
따라서, 상기 하우징(100)은 단가가 싸며 성형이 쉬운 폴리에틸렌(PE) 재질이나 폴리프로필렌(PP)재질로 제작되나 이런 재질로 얇은 두께의 상기 하우징(100)을 구성하는 경우 내구성이 약해져, 외력에 의해 하우징(100)의 변형이 발생하는 경우가 빈번하다.Therefore, the housing 100 is made of polyethylene (PE) material or polypropylene (PP) material, which is easy to mold and low in cost, but when the housing 100 is made of such a material, the durability becomes weak, Frequently, deformation of the housing 100 occurs.
상기와 같은 단점을 해소하기 위해, 본 발명의 실시 에에 따르면 도 7에 도시된 바와 같이 상기 하우징(100)의 외주면에 다각형의 단면을 가지는 굴곡부(150)를 구비하여, 외부 압력에 대해서 상기 하우징(100)의 내구성이 향상되게 구성할 수 있다.In order to solve the above disadvantages, according to the embodiment of the present invention, as shown in FIG. 7, the outer peripheral surface of the housing 100 is provided with a bent portion 150 having a polygonal cross section, the housing ( 100) can be configured to improve the durability.
이때, 상기 굴곡부(150)는 외력에 효과적으로 대응 가능하다면 그 굴곡의 단면 형상이 다양한 형태를 가지도록 구성될 수 있다. At this time, the bend 150 may be configured to have a variety of forms of cross-sectional shape of the bend if it can effectively respond to the external force.
또한, 본 발명의 실시 예에 따른 감마분광분석기용 완전 밀폐형 시료 용기에서 고정부(130)는 상기 하우징(100)의 상하 길이방향 중심축을 기준으로 일정한 반경(r)을 가지는 원통 형상으로 이루어지는 것이 바람직하다.In addition, in the fully sealed sample container for the gamma spectrometer according to an embodiment of the present invention, the fixing part 130 is preferably made of a cylindrical shape having a constant radius (r) with respect to the vertical longitudinal axis of the housing (100). Do.
도 8을 참조하여 상세히 설명하면, 상기 시료 용기의 상기 고정부(130)에는 방사능 측정기가 삽입되고, 상기 삽입된 방사능 측정기는 상기 하우징(100) 내에 존재하는 시료의 방사능을 측정한다. Referring to FIG. 8, a radiometer is inserted into the fixing part 130 of the sample container, and the inserted radiometer measures radioactivity of a sample present in the housing 100.
여기서, 상기 고정부(130)를 중심으로 그 주변에 시료가 채워지고 상기 시료가 채워지는 공간의 a, b, c 값이 서로 동일하지 않은 경우에는, 시료를 구성하는 방사성 핵종에서 방출된 방사선의 자기흡수(self absorption) 양이 변형되어 상기 삽입된 방사능 측정기에서 측정되는 방사능 수치에 오차가 발생하게 된다.Here, when the sample is filled around the fixing part 130 and the a, b, and c values of the space where the sample is filled are not equal to each other, the radiation emitted from the radionuclides constituting the sample is measured. The amount of self absorption is modified so that an error occurs in the radiation level measured by the inserted radiometer.
그러므로, 이러한 오차를 방지하기 위해서 상기 고정부(130)는 상기 하우징(100)의 상하 길이방향 중심축을 기준으로 일정한 반경(r)을 가지는 원통 형상을 가지도록 구성하는 것이 바람직하다. 상기 고정부(130)가 상기 원통 형상을 가지는 경우, 상기 하우징(100) 내 시료가 채워지는 공간(120)의 b,c 값이 서로 동일해 지도록 상기 하우징 내 공간(120)을 구성할 수 있다. 그리고, 상기 고정부(130)의 상측에 시료가 채워지는 높이인 a 값 역시 상기 b, c 값과 동일하게 조절될 수 있도록 상기 하우징(100)에는 a값을 육안으로 확인할 수 있는 눈금을 구비하는 것이 바람직하다.Therefore, in order to prevent such an error, the fixing part 130 is preferably configured to have a cylindrical shape having a constant radius (r) based on the vertical longitudinal axis of the housing (100). When the fixing part 130 has the cylindrical shape, the space in the housing 120 may be configured such that the b and c values of the space 120 in which the sample in the housing 100 is filled are equal to each other. . In addition, the a value, which is a height at which the sample is filled on the upper side of the fixing part 130, is also provided with a scale for visually checking the a value in the housing 100 so that the b value and the same value as the c value can be adjusted. It is preferable.
이와 같이, 상기 하우징(100) 내에 시료가 채워지는 공간의 a, b, c 값이 서로 일치되도록 해 줌으로써, 상기 고정부(130)에 삽입된 방사능 측정기를 통해 시료의 방사능을 보다 정확하게 측정할 수 있다. As such, by allowing a, b, and c values of the space in which the sample is filled in the housing 100 to coincide with each other, the radioactivity of the sample can be more accurately measured through the radiometer inserted into the fixing part 130. have.
본 발명의 실시 예에 따른 감마분광분석기용 완전 밀폐형 시료 용기에서 상기 덮개(200)는 상기 공간(120)에 위치되는 시료의 특성에 따라 가스 투과성 재질 또는 가스 차단선 재질로 구성할 수 있다.In the completely sealed sample container for the gamma spectrometer according to an embodiment of the present invention, the cover 200 may be made of a gas permeable material or a gas barrier line material according to the characteristics of the sample located in the space 120.
상세히 설명하면, 상기 하우징(100)의 공간(120)에 생체 시료가 위치될 경우 생체 시료가 부패하여 가스가 생성되고 이 가스로 인해서 폭발 사고가 발생될 가능성이 있다. 따라서 다량의 가스가 방출되는 시료가 공간(120)에 위치될 경우 상기 덮개(200)를 가스 투과성 재질로 구성하는 것이 바람직하다.In detail, when the biological sample is located in the space 120 of the housing 100, the biological sample may be decayed and gas may be generated, thereby causing an explosion accident. Therefore, when the sample from which a large amount of gas is discharged is located in the space 120, it is preferable that the cover 200 is made of a gas permeable material.
그리고, 핵종이 가스에 함유되어 외부로 방출될 가능성이 있는 시료가 상기 하우징(100)의 공간(120)에 위치될 경우에는, 덮개(200)를 가스 비투과성 재질로 구성하는 것이 바람직하다. 이 경우, 덮개(200)를 가스 비투과성 재질로 구성하여 핵종이 외부로 방출되지 않도록 해 줌으로써, 방사능 측정 시험에서 발생할 수 있는 사고를 미연에 방지할 수 있다.In addition, when the sample containing the nuclide contained in the gas and is likely to be released to the outside is located in the space 120 of the housing 100, the lid 200 may be made of a gas impermeable material. In this case, the cover 200 is made of a gas-permeable material to prevent the nuclide from being released to the outside, thereby preventing accidents that may occur in the radioactivity test.
본 발명의 상기한 실시 예에 한정하여 기술적 사상을 해석해서는 안 된다. 적용범위가 다양함은 물론이고, 청구범위에서 청구하는 본 발명의 요지를 벗어남이 없이 당업자의 수준에서 다양한 변형 실시가 가능하다. 따라서 이러한 개량 및 변경은 당업자에게 자명한 것인 한 본 발명의 보호범위에 속하게 된다.The technical spirit should not be interpreted as being limited to the above embodiments of the present invention. Various modifications may be made at the level of those skilled in the art without departing from the spirit of the invention as claimed in the claims. Therefore, such improvements and modifications fall within the protection scope of the present invention as long as it will be apparent to those skilled in the art.
[부호의 설명][Description of the code]
100 : 하우징100: housing
110 : 유입부110: inlet
120 : 공간120: space
130 : 고정부130: fixed part
140 : 제1 결합부140: first coupling part
150 : 굴곡부150: bend
200 : 덮개200: cover
210 : 제2 결합부210: second coupling part
220 : 풀탭220: pull tab
230 : 절단홈230: cutting groove

Claims (6)

  1. 외부에서 시료가 유입되는 유입부(110), 상기 유입부(110)를 통해 유입된 시료가 위치되는 내부 공간(120), 상기 공간(120)에 위치하는 시료의 방사능을 측정하는 계측기가 삽입되는 고정부(130), 및 상기 유입부(110)의 상측 단부가 외측으로 구부러진 제1 결합부(140)를 포함하는 원통형 하우징(100); 및An inlet 110 into which the sample is introduced from the outside, an internal space 120 in which the sample introduced through the inlet 110 is located, and a measuring instrument for measuring the radioactivity of the sample located in the space 120 is inserted. A cylindrical housing (100) including a fixing part (130) and a first coupling part (140) having an upper end of the inlet part (110) bent outwardly; And
    하면이 상기 유입부(110)에 대응되고, 가장자리를 따라서 상기 제1 결합부(140)와 시밍(seaming)되는 제2 결합부(210)를 포함하는 덮개(200)를 포함하는, 감마분광분석기용 완전 밀폐형 시료 용기.The lower surface corresponds to the inlet 110, gamma spectroscopic analysis comprising a cover 200 including a second coupling portion 210 seaming with the first coupling portion 140 along an edge Fully enclosed sample vessel.
  2. 제 1항에 있어서, 상기 덮개(200)는,The method of claim 1, wherein the cover 200,
    상면에 풀탭(220)과, 상기 풀탭(220)을 통해 전달되는 외력에 의해서 상기 덮개(200)가 상기 하우징(100)에서 분리되도록 상기 제2 결합부(210)의 안측에 구비된 절단홈(230)을 더 포함하는, 감마분광분석기용 완전 밀폐형 시료 용기.Cutting grooves provided on the inner side of the second coupling portion 210 so that the cover 200 is separated from the housing 100 by the pull tab 220 and the external force transmitted through the pull tab 220 on the upper surface ( 230), further comprising a hermetically sealed sample container for a gamma spectrometer.
  3. 제 1항 또는 제 2항에 있어서, The method according to claim 1 or 2,
    상기 제2 결합부(210)는 상기 제1 결합부(140)와 마주보는 면이 내측에서 외측으로 갈수록 경사지게 기울어지도록 구성되고,The second coupling portion 210 is configured such that the surface facing the first coupling portion 140 is inclined inclined toward the outside from the inside,
    상기 제1 결합부(140)는 상기 제2 결합부(210)의 마주보는 면의 경사에 대응하여 서로 맞닿도록 구부러진 형태로 구성되는 것을 특징으로 하는, 감마분광분석기용 완전 밀폐형 시료 용기.The first coupling part 140 is configured to be bent in contact with each other in response to the inclination of the opposite surface of the second coupling part 210, characterized in that the completely sealed sample container for a gamma spectrometer.
  4. 제 3항에 있어서, 상기 하우징(100)은,The method of claim 3, wherein the housing 100,
    외주면에 단수 또는 복수개의 굴곡부(150)가 구비되는, 감마분광분석기용 완전 밀폐형 시료 용기.A single hermetically sealed sample container for a gamma spectrometer, which is provided with one or more bends 150 on its outer circumferential surface.
  5. 제 3항에 있어서, 상기 덮개(200)는,The method of claim 3, wherein the cover 200,
    가스 투과성 재질 또는 가스 차단성 재질로 구성되는 것을 특징으로 하는, 감마분광분석기용 완전 밀폐형 시료 용기.A hermetically sealed sample container for a gamma spectrometer, characterized in that it is composed of a gas permeable material or a gas barrier material.
  6. 제 1항 또는 제 2항에 있어서, The method according to claim 1 or 2,
    상기 고정부(130)는 상기 하우징(100)의 상하 길이방향 중심축을 기준으로 일정한 반경을 가지는 원통 형상인 것을 특징으로 하는, 감마분광분석기용 완전 밀폐형 시료 용기.The fixing part 130 is characterized in that the cylindrical shape having a constant radius with respect to the vertical longitudinal axis of the housing 100, a completely sealed sample container for the gamma spectrometer.
PCT/KR2016/007214 2015-08-05 2016-07-05 Completely sealed sample container for gamma spectrometer WO2017022955A1 (en)

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KR101987714B1 (en) 2017-11-06 2019-06-11 한국표준과학연구원 Marinelli Beaker for Gamm Spectroscopy with a Screw type Hermetic Cap
KR102211201B1 (en) 2018-11-05 2021-02-03 한국표준과학연구원 Airtight Container for Radioactivity Measurement Such as Radon Using Gamma-ray Spectrometer
KR200491721Y1 (en) 2019-03-14 2020-05-25 (주)한성 Sample container for gamma ray measurement
RU201743U1 (en) * 2020-08-19 2020-12-30 Лаврик Юрий Михайлович SPECTROMETRIC GAS RADIOMETER

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JPH0836094A (en) * 1994-07-23 1996-02-06 Kiriyama Seisakusho:Kk Closed treatment container for radioactive waste
KR200167931Y1 (en) * 1999-08-16 2000-02-15 한국전력공사 Radiation detector protector for gamma-spectrometry
JP2006026638A (en) * 2004-07-12 2006-02-02 Honshu Seikan Kk Square-shaped can
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KR20130086247A (en) * 2010-11-26 2013-07-31 토요세이깐 가부시키가이샤 Container, lid, and seaming method for container

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JPH0836094A (en) * 1994-07-23 1996-02-06 Kiriyama Seisakusho:Kk Closed treatment container for radioactive waste
KR200167931Y1 (en) * 1999-08-16 2000-02-15 한국전력공사 Radiation detector protector for gamma-spectrometry
JP2006026638A (en) * 2004-07-12 2006-02-02 Honshu Seikan Kk Square-shaped can
KR20130086247A (en) * 2010-11-26 2013-07-31 토요세이깐 가부시키가이샤 Container, lid, and seaming method for container
KR20120005372U (en) * 2011-01-17 2012-07-25 김제 Double-sealed cans

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