WO2016192702A3 - Shaped bodies containing piezo-active calcium titanium oxide, method for the production and excitation thereof and use of piezo-active calcium titanium oxide as piezoelectric molded bodies or a component of piezoelectric molded bodies - Google Patents

Shaped bodies containing piezo-active calcium titanium oxide, method for the production and excitation thereof and use of piezo-active calcium titanium oxide as piezoelectric molded bodies or a component of piezoelectric molded bodies Download PDF

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Publication number
WO2016192702A3
WO2016192702A3 PCT/DE2016/000230 DE2016000230W WO2016192702A3 WO 2016192702 A3 WO2016192702 A3 WO 2016192702A3 DE 2016000230 W DE2016000230 W DE 2016000230W WO 2016192702 A3 WO2016192702 A3 WO 2016192702A3
Authority
WO
WIPO (PCT)
Prior art keywords
titanium oxide
piezo
calcium titanium
molded bodies
active calcium
Prior art date
Application number
PCT/DE2016/000230
Other languages
German (de)
French (fr)
Other versions
WO2016192702A2 (en
Inventor
Eberhard Burkel
Rico SCHNIERER
Original Assignee
Universität Rostock
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Universität Rostock filed Critical Universität Rostock
Publication of WO2016192702A2 publication Critical patent/WO2016192702A2/en
Publication of WO2016192702A3 publication Critical patent/WO2016192702A3/en

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Classifications

    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/46Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates
    • C04B35/462Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates
    • C04B35/465Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates based on alkaline earth metal titanates
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L27/00Materials for grafts or prostheses or for coating grafts or prostheses
    • A61L27/02Inorganic materials
    • A61L27/04Metals or alloys
    • A61L27/06Titanium or titanium alloys
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L27/00Materials for grafts or prostheses or for coating grafts or prostheses
    • A61L27/50Materials characterised by their function or physical properties, e.g. injectable or lubricating compositions, shape-memory materials, surface modified materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/624Sol-gel processing
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/64Burning or sintering processes
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10NELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10N30/00Piezoelectric or electrostrictive devices
    • H10N30/01Manufacture or treatment
    • H10N30/09Forming piezoelectric or electrostrictive materials
    • H10N30/093Forming inorganic materials
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10NELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10N30/00Piezoelectric or electrostrictive devices
    • H10N30/01Manufacture or treatment
    • H10N30/09Forming piezoelectric or electrostrictive materials
    • H10N30/093Forming inorganic materials
    • H10N30/097Forming inorganic materials by sintering
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10NELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10N30/00Piezoelectric or electrostrictive devices
    • H10N30/80Constructional details
    • H10N30/85Piezoelectric or electrostrictive active materials
    • H10N30/853Ceramic compositions
    • H10N30/8536Alkaline earth metal based oxides, e.g. barium titanates
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/66Specific sintering techniques, e.g. centrifugal sintering
    • C04B2235/666Applying a current during sintering, e.g. plasma sintering [SPS], electrical resistance heating or pulse electric current sintering [PECS]
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/74Physical characteristics
    • C04B2235/76Crystal structural characteristics, e.g. symmetry
    • C04B2235/768Perovskite structure ABO3

Abstract

The invention relates to molded bodies, in particular implants, comprising piezo-active calcium titanium oxide, including piezo-active doped calcium titanium oxide, the use of such calcium titanium oxide and a method for the production and for the excitation of the molded bodies by electric fields.
PCT/DE2016/000230 2015-06-03 2016-06-03 Shaped bodies containing piezo-active calcium titanium oxide, method for the production and excitation thereof and use of piezo-active calcium titanium oxide as piezoelectric molded bodies or a component of piezoelectric molded bodies WO2016192702A2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102015108865.7A DE102015108865A1 (en) 2015-06-03 2015-06-03 Moldings containing piezoactive calcium titanium oxide, a process for their preparation and excitation and use of piezoactive calcium titanium oxide as a piezoelectric molded body or component of piezoelectric molded bodies
DE102015108865.7 2015-06-03

Publications (2)

Publication Number Publication Date
WO2016192702A2 WO2016192702A2 (en) 2016-12-08
WO2016192702A3 true WO2016192702A3 (en) 2017-01-26

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/DE2016/000230 WO2016192702A2 (en) 2015-06-03 2016-06-03 Shaped bodies containing piezo-active calcium titanium oxide, method for the production and excitation thereof and use of piezo-active calcium titanium oxide as piezoelectric molded bodies or a component of piezoelectric molded bodies

Country Status (2)

Country Link
DE (1) DE102015108865A1 (en)
WO (1) WO2016192702A2 (en)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0331160A2 (en) * 1988-03-04 1989-09-06 Hitachi, Ltd. Functional ceramic shaped article and process for producing the same
WO2007010512A1 (en) * 2005-07-19 2007-01-25 University Of Limerick Implants
EP2786771A2 (en) * 2013-03-11 2014-10-08 DOT GmbH Method for the preparation of a functionalised implant and functionalised implant
WO2015178196A1 (en) * 2014-05-19 2015-11-26 株式会社村田製作所 Piezoelectric thin film, and piezoelectric thin film element

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3330697A (en) 1963-08-26 1967-07-11 Sprague Electric Co Method of preparing lead and alkaline earth titanates and niobates and coating method using the same to form a capacitor
US4670243A (en) 1986-06-30 1987-06-02 Ferro Corporation Method of precipitating metal titanate powders
FR2617151B1 (en) 1987-06-29 1990-10-12 Solvay PROCESS FOR THE MANUFACTURE OF MIXED METAL OXIDE POWDER, AND MIXED METAL OXIDE POWDERS
US5830270A (en) * 1996-08-05 1998-11-03 Lockheed Martin Energy Systems, Inc. CaTiO3 Interfacial template structure on semiconductor-based material and the growth of electroceramic thin-films in the perovskite class

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0331160A2 (en) * 1988-03-04 1989-09-06 Hitachi, Ltd. Functional ceramic shaped article and process for producing the same
WO2007010512A1 (en) * 2005-07-19 2007-01-25 University Of Limerick Implants
EP2786771A2 (en) * 2013-03-11 2014-10-08 DOT GmbH Method for the preparation of a functionalised implant and functionalised implant
WO2015178196A1 (en) * 2014-05-19 2015-11-26 株式会社村田製作所 Piezoelectric thin film, and piezoelectric thin film element

Non-Patent Citations (7)

* Cited by examiner, † Cited by third party
Title
A. K. DUBEY ET AL: "Multifunctionality of Perovskites BaTiO 3 and CaTiO 3 in a Composite with Hydroxyapatite as Orthopedic Implant Materials", INTEGRATED FERROELECTRICS, vol. 131, no. 1, 1 January 2011 (2011-01-01), US, pages 119 - 126, XP055317469, ISSN: 1058-4587, DOI: 10.1080/10584587.2011.616425 *
AHMED M A ET AL: "Effect of annealing time, weight pressure and Fe doping on the electrical and magnetic behavior of calcium titanate", MATERIALS CHEMISTRY AND PHYSICS, ELSEVIER SA, SWITZERLAND, TAIWAN, REPUBLIC OF CHINA, vol. 114, no. 1, 15 March 2009 (2009-03-15), pages 446 - 450, XP025767815, ISSN: 0254-0584, [retrieved on 20081125], DOI: 10.1016/J.MATCHEMPHYS.2008.09.075 *
BHAVNA C. KESWANI ET AL: "Ferroelectric and piezoelectric properties of Fe doped lead free BaTiO<inf>3</inf>-CaTiO<inf>3</inf> electroceramics", 2015 2ND INTERNATIONAL SYMPOSIUM ON PHYSICS AND TECHNOLOGY OF SENSORS (ISPTS), 1 March 2015 (2015-03-01), pages 102 - 105, XP055317508, ISBN: 978-1-4673-8018-8, DOI: 10.1109/ISPTS.2015.7220092 *
M. KHALID ET AL: "Development of Perovskite Based Ceramics for Ultrasonic Applications", KEY ENGINEERING MATERIALS, vol. 442, 1 June 2010 (2010-06-01), pages 422 - 430, XP055317519, DOI: 10.4028/www.scientific.net/KEM.442.422 *
NAOFUMI OHTSU ET AL: "CaTiO3 coating on titanium for biomaterial application-Optimum thickness and tissue response", JOURNAL OF BIOMEDICAL MATERIALS RESEARCH. PART A, vol. 82A, no. 2, 1 August 2007 (2007-08-01), HOBOKEN, NY, US, pages 304 - 315, XP055317494, ISSN: 1549-3296, DOI: 10.1002/jbm.a.31136 *
PULI VENKATA SREENIVAS ET AL: "Investigations on structure, ferroelectric, piezoelectric and energy storage properties of barium calcium titanate (BCT) ceramics", JOURNAL OF ALLOYS AND COMPOUNDS, vol. 584, 24 September 2013 (2013-09-24), pages 369 - 373, XP028761969, ISSN: 0925-8388, DOI: 10.1016/J.JALLCOM.2013.09.108 *
YANG SANG MO ET AL: "Observation of ferroelectricity induced by defect dipoles in the strain-free epitaxial CaTiO3thin film", CURRENT APPLIED PHYSICS, vol. 14, no. 5, 22 March 2014 (2014-03-22), pages 757 - 760, XP028652382, ISSN: 1567-1739, DOI: 10.1016/J.CAP.2014.03.009 *

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DE102015108865A1 (en) 2016-12-08
WO2016192702A2 (en) 2016-12-08

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