WO2014146326A1 - 液晶面板、显示装置以及液晶面板的制造方法 - Google Patents
液晶面板、显示装置以及液晶面板的制造方法 Download PDFInfo
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- WO2014146326A1 WO2014146326A1 PCT/CN2013/074964 CN2013074964W WO2014146326A1 WO 2014146326 A1 WO2014146326 A1 WO 2014146326A1 CN 2013074964 W CN2013074964 W CN 2013074964W WO 2014146326 A1 WO2014146326 A1 WO 2014146326A1
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- Prior art keywords
- liquid crystal
- frequency
- crystal panel
- dual
- color filter
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- 238000004519 manufacturing process Methods 0.000 title claims abstract description 13
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- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims description 25
- 229910052731 fluorine Inorganic materials 0.000 claims description 25
- 239000011737 fluorine Substances 0.000 claims description 25
- 239000000203 mixture Substances 0.000 claims description 20
- 210000002858 crystal cell Anatomy 0.000 claims description 12
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- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 2
- 230000008569 process Effects 0.000 description 2
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- PIZHFBODNLEQBL-UHFFFAOYSA-N 2,2-diethoxy-1-phenylethanone Chemical compound CCOC(OCC)C(=O)C1=CC=CC=C1 PIZHFBODNLEQBL-UHFFFAOYSA-N 0.000 description 1
- 239000004986 Cholesteric liquid crystals (ChLC) Substances 0.000 description 1
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
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- 230000004075 alteration Effects 0.000 description 1
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- NIHNNTQXNPWCJQ-UHFFFAOYSA-N o-biphenylenemethane Natural products C1=CC=C2CC3=CC=CC=C3C2=C1 NIHNNTQXNPWCJQ-UHFFFAOYSA-N 0.000 description 1
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
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- C09K19/10—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing at least two benzene rings
- C09K19/20—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing at least two benzene rings linked by a chain containing carbon and oxygen atoms as chain links, e.g. esters or ethers
- C09K19/2007—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing at least two benzene rings linked by a chain containing carbon and oxygen atoms as chain links, e.g. esters or ethers the chain containing -COO- or -OCO- groups
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- G02F1/00—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K19/00—Liquid crystal materials
- C09K19/04—Liquid crystal materials characterised by the chemical structure of the liquid crystal components, e.g. by a specific unit
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- C09K19/30—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing saturated or unsaturated non-aromatic rings, e.g. cyclohexane rings
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- G02F1/1333—Constructional arrangements; Manufacturing methods
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- B32B2457/20—Displays, e.g. liquid crystal displays, plasma displays
- B32B2457/202—LCD, i.e. liquid crystal displays
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K19/00—Liquid crystal materials
- C09K19/04—Liquid crystal materials characterised by the chemical structure of the liquid crystal components, e.g. by a specific unit
- C09K2019/0444—Liquid crystal materials characterised by the chemical structure of the liquid crystal components, e.g. by a specific unit characterized by a linking chain between rings or ring systems, a bridging chain between extensive mesogenic moieties or an end chain group
- C09K2019/0448—Liquid crystal materials characterised by the chemical structure of the liquid crystal components, e.g. by a specific unit characterized by a linking chain between rings or ring systems, a bridging chain between extensive mesogenic moieties or an end chain group the end chain group being a polymerizable end group, e.g. -Sp-P or acrylate
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K19/00—Liquid crystal materials
- C09K19/04—Liquid crystal materials characterised by the chemical structure of the liquid crystal components, e.g. by a specific unit
- C09K19/06—Non-steroidal liquid crystal compounds
- C09K19/08—Non-steroidal liquid crystal compounds containing at least two non-condensed rings
- C09K19/10—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing at least two benzene rings
- C09K19/20—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing at least two benzene rings linked by a chain containing carbon and oxygen atoms as chain links, e.g. esters or ethers
- C09K19/2007—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing at least two benzene rings linked by a chain containing carbon and oxygen atoms as chain links, e.g. esters or ethers the chain containing -COO- or -OCO- groups
- C09K2019/2078—Ph-COO-Ph-COO-Ph
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- G—PHYSICS
- G02—OPTICS
- G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
- G02F1/00—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
- G02F1/01—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour
- G02F1/13—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour based on liquid crystals, e.g. single liquid crystal display cells
- G02F1/133—Constructional arrangements; Operation of liquid crystal cells; Circuit arrangements
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- G02F1/00—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
- G02F1/01—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour
- G02F1/13—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour based on liquid crystals, e.g. single liquid crystal display cells
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- G02F1/00—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
- G02F1/01—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour
- G02F1/13—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour based on liquid crystals, e.g. single liquid crystal display cells
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- G02F1/13775—Polymer-stabilized liquid crystal layers
Definitions
- Liquid crystal panel display device, and manufacturing method of liquid crystal panel
- Embodiments of the present invention relate to a liquid crystal panel, a display device, and a method of manufacturing a liquid crystal panel. Background technique
- TFT-LCD Thin Film Transistor Liquid Crystal Display
- TN Twisted Nematic
- VA Vertical Alignment
- IPS In-Plane Switching
- ADvanced Super Dimension Switch AD-SDS or ADS
- the liquid crystal working efficiency is improved and the light transmission efficiency is increased.
- Advanced super-dimensional field conversion technology improves the picture quality of TFT-LCDs with high resolution, high transmittance, low power consumption, wide viewing angle, high aperture ratio, low chromatic aberration, and no squeeze water ripple ( push Mura ) Etc.
- the liquid crystal can be classified into a nematic liquid crystal, a smectic liquid crystal, and a cholesteric liquid crystal.
- nematic liquid crystal can be classified into a positive nematic liquid crystal, a negative nematic liquid crystal, and a dual frequency liquid crystal.
- the dielectric constant ( ⁇ ) of the liquid crystal is greater than 0, and the liquid crystal is positive; when the electric absorption group is at one end of the short axis of the rod-like liquid crystal molecule, ⁇ is less than 0, and the liquid crystal Negative.
- Positive nematic liquid crystals are mostly used in display modes such as TN, ADS, and IPS, and negative nematic liquid crystals are used in modes such as VA.
- ⁇ is greater than 0, and the liquid crystal is dielectric positive; under the action of high-frequency electric field, ⁇ is less than 0, and the liquid crystal is dielectric negative. Since the dual-frequency liquid crystal exhibits different electrical properties as the electric field frequency changes, the arrangement of the dual-frequency liquid crystal molecules may be abnormal, so it is difficult to apply to the liquid crystal display. Summary of the invention
- An embodiment of the present invention provides a liquid crystal panel including: an array substrate and a color filter substrate, and a liquid crystal layer disposed between the array substrate and the color filter substrate, wherein the liquid crystal layer includes A dual-frequency liquid crystal and a polymer network anchoring the dual-frequency liquid crystal, wherein the polymer network is formed by polymerization of a liquid crystal polymerizable ultraviolet polymerizable monomer.
- Another embodiment of the present invention provides a display device including the above liquid crystal panel.
- Another embodiment of the present invention provides a method for fabricating a liquid crystal panel, comprising: a dual-frequency liquid crystal having a mass percentage of 90% to 98%, and a liquid polymerizable ultraviolet polymerizable monomer having a mass percentage of 1 to 9%.
- a body, and a photoinitiator having a mass percentage of 0.1% to 1% is mixed in the dark to form a mixture; the mixture is defoamed; the defoamed mixture is dropped onto the array substrate, and the sealant is coated Forming a liquid crystal cell on the color filter substrate, and performing vacuum chamber on the array substrate and the color filter substrate; irradiating the liquid crystal cell with ultraviolet light to make the liquid crystal polymerizable ultraviolet polymerizable monomer Polymerization occurs to form a polymer network; and the liquid crystal cell irradiated with ultraviolet light is subjected to heat of the mouth.
- FIG. 1 is a schematic structural view of a liquid crystal panel of an ADS mode in an unpowered state according to an embodiment of the present invention
- FIG. 2 is a schematic diagram showing the structure of an ADS mode liquid crystal panel in an energized state according to an embodiment of the present invention
- FIG. 3 is a polarized light microscope diagram of a liquid crystal layer of an ADS mode liquid crystal panel according to an embodiment of the present invention
- Fig. 4 is a graph showing the relationship between the voltage and the transmittance of the liquid crystal panel of the ADS mode according to the embodiment of the present invention.
- Embodiments of the present invention provide a liquid crystal panel in which a dual-frequency liquid crystal is applied to a liquid crystal display by controlling the arrangement of dual-frequency liquid crystal molecules, thereby optimizing display of the liquid crystal panel.
- Embodiments of the present invention also provide a method of manufacturing the above liquid crystal panel and a display device including the above liquid crystal panel.
- the arrangement of the dual-frequency liquid crystal molecules can be induced, thereby applying the dual-frequency liquid crystal to In the liquid crystal display, the display of the liquid crystal panel is optimized.
- FIG. 1 is a schematic structural view of a liquid crystal panel of an ADS mode in an unpowered state according to an embodiment of the present invention.
- a liquid crystal panel provided by an embodiment of the present invention will be described below with reference to FIG.
- the liquid crystal panel provided by the embodiment of the present invention may include an array substrate 10 and a color filter substrate 1 , and a liquid crystal layer disposed between the array substrate 10 and the color filter substrate 1 .
- the polymer network 4 includes a dual-frequency liquid crystal 3 and an anchor network of a dual-frequency liquid crystal 3, wherein the polymer network 4 is formed by polymerization of a liquid crystal polymerizable ultraviolet polymerizable monomer.
- the polymer network formed by the polymerization reaction of the ultraviolet polymerizable monomer having liquid crystallinity anchors the dual-frequency liquid crystal molecules. Since the polymer network having liquid crystal properties can interact with the dual-frequency liquid crystal by the interaction between molecules, the dual-frequency liquid crystal molecules can be arranged in a parallel orientation structure, and the dual-frequency liquid crystal molecules are defined in the up, down, left and right directions. The sliding, thus making the dual-frequency liquid crystal can be applied to the liquid crystal display.
- the dual-frequency liquid crystal can exhibit dielectric polarity under a low-frequency electric field and the liquid crystal display is usually performed under a low-frequency electric field
- the dual-frequency liquid crystal can be applied to the TN mode, the IPS mode, or the ADS mode under a low-frequency electric field.
- a liquid crystal panel using a positive liquid crystal for example, a dual-frequency liquid crystal can be applied to an ADS mode liquid crystal panel.
- the ADS mode liquid crystal panel the long-axis of the dual-frequency liquid crystal molecules is aligned with the tangential direction of the electric field line. .
- a high-frequency electric field can be applied.
- the dual-frequency liquid crystal exhibits a dielectric negative, and the long-axis of the dual-frequency liquid crystal molecules is aligned perpendicular to the tangential direction of the electric field lines, which helps The dual frequency liquid crystal molecules restore the original parallel oriented structure. Therefore, in the liquid crystal panel provided by the embodiment of the present invention, the arrangement of the dual-frequency liquid crystal molecules can be controlled by changing the frequency of the external electric field, thereby enabling controllable operation of the dual-frequency liquid crystal molecules in the liquid crystal panel, thereby optimizing the liquid crystal panel. Display.
- the dual-frequency liquid crystal is anchored in the polymer network, after applying the low-frequency electric field, the dual-frequency liquid crystal molecules can be rapidly rotated to a desired angle by the electric field, thereby improving the response of the dual-frequency liquid crystal molecules.
- the speed reduces the reaction time of the display device.
- the frequency f of the low frequency electric field is greater than 100 Hz and less than 2000 Hz (ie, 100 Hz ⁇ f ⁇ 2000 Hz), and the frequency f of the high frequency electric field is greater than or equal to 2000 Hz and less than or equal to 30,000 Hz (ie, 2000 Hz ⁇ f ⁇ 30000Hz ).
- the present invention there may be various ultraviolet polymerizable monomers having liquid crystal properties, which can form a polymer network under irradiation of ultraviolet light, for example, a structure in which a molecular terminal is a carbon-carbon double bond, and The monomer needs to have liquid crystallinity so that it can be better dissolved in the liquid crystal molecules.
- the monomer having liquid crystallinity can be the same as the liquid crystal molecule, and the liquid crystal monomer can exhibit different orientations under the action of different alignment agents.
- the ultraviolet polymerizable monomer having liquid crystallinity forms a polymer network, the arrangement of the internal dual-frequency liquid crystal molecules can be fixed by the anchoring force.
- the chemical structure can be employed as:
- n 3, 4, 5, 6, 7, or 8.
- such a monomer can be modified in various structures as long as it does not affect its liquid crystallinity and the characteristics of forming a polymer network.
- the dual-frequency liquid crystal may be a mixed liquid crystal formed by mixing a plurality of fluorine-containing double-frequency liquid crystal molecules.
- the distribution of the long axis of the liquid crystal molecules is a combination of a benzene ring, a cyclohexane, and an ester group (or an ether bond), and the benzene ring in the middle of the molecule may have a hydrogen-absorbing group such as a fluorine functional group and/or a chlorine functional group.
- the liquid crystal molecule of this structure has an electron-withdrawing group on the short axis, thereby exhibiting dual-frequency liquid crystal characteristics.
- a fluorine-based double-frequency liquid crystal molecule may be employed.
- a dual-frequency liquid crystal molecule by mixing a plurality of fluorine-containing groups can be used in the liquid crystal layer of the liquid crystal panel provided by the embodiment of the present invention. The resulting mixed liquid crystal.
- mixing a fluorine-containing double-frequency liquid crystal molecule in a liquid crystal may include:
- n 3, 4, 5, 6, 7, or 8, but embodiments of the present invention are not limited thereto.
- n may be 3, 4, 5, 6, 7, or 8, in the above eight fluorine-containing groups.
- the value of n in each of the fluorine-containing double-frequency liquid crystal molecules may be the same or different, and embodiments of the present invention are not limited thereto.
- the values of n in the two fluorine-containing double-frequency liquid crystal molecules forming the mixed liquid crystal are the same.
- the above eight fluorine-containing double-frequency liquid crystal molecules have a display temperature ranging from -30 °C to 80 °C.
- the mass percentage of each of the fluorine-containing double-frequency liquid crystal molecules in the mixed liquid crystal ranges from 5% to 15%. In the embodiment of the present invention, for example, the mass percentage of each of the fluorine-containing double-frequency liquid crystal molecules in the mixed liquid crystal is 12.5%.
- the mass percentage of each of the fluorine-containing double-frequency liquid crystal molecules in the mixed liquid crystal may range from 5% to 15%, and the mass percentage of each of the fluorine-containing double-frequency liquid crystal molecules may be The same or different, the embodiment of the present invention is not limited thereto.
- the mass percentage of the above two fluorine-containing double-frequency liquid crystal molecules is 15%, respectively. 8%, 10%, 15%, 13%, 14%, 12% and 13%.
- the mass percentage of each of the above eight fluorine-containing double-frequency liquid crystal molecules in the mixed liquid crystal is 12.5%, that is, has the same mass percentage.
- the mixed double-frequency liquid crystal molecules have a reduced melting point and are suitable for use in liquid crystal displays.
- the liquid crystal panel provided by the embodiment of the present invention may further include: a first parallel alignment layer 2 disposed on a side of the color filter substrate 1 facing the liquid crystal layer, and a side surface disposed on the surface of the array substrate 10 facing the liquid crystal layer The second parallel alignment layer 5 on.
- the liquid crystal polymerizable ultraviolet polymerizable monomer and the dual-frequency liquid crystal molecule are provided.
- the long axis directions of the molecules are aligned parallel to the substrate.
- the liquid crystal polymerizable ultraviolet polymerizable monomer is polymerized to form a polymer network 4, and the polymer network 4 can fix the dual-frequency liquid crystal molecules by the anchoring force and still parallel to the substrate according to the molecular long axis direction.
- the ⁇ ij so that the orientation of the dual-frequency liquid crystal molecules is normal, and the display of the liquid crystal panel is optimized.
- the liquid crystal panel provided by the embodiment of the present invention can be applied to a TN mode, a VA mode, an IPS mode, or an ADS mode.
- the liquid crystal panel provided by the embodiment of the present invention can be applied to the ADS mode.
- the liquid crystal panel of the ADS mode provided by the embodiment of the present invention may further include: a pixel electrode 8 formed on the transparent substrate 9; an insulating layer 7 formed on the pixel electrode 8; A slit-shaped common electrode 6 on the insulating layer 7.
- FIG. 1 in the unpowered state, after the action of the parallel alignment layer in the liquid crystal panel, the long axes of the dual-frequency liquid crystal molecules are aligned parallel to the substrate; in addition, since the ultraviolet polymerizable monomer has liquid crystallinity, The molecules of the monomer are also arranged parallel to the substrate. After the photoinitiator is initiated, the ultraviolet polymerizable monomer generates a polymer network, and the polymer network can fix the alignment direction of the long axis of the liquid crystal molecules by the anchoring force.
- FIG. 1 in the unpowered state, after the action of the parallel alignment layer in the liquid crystal panel, the long axes of the dual-frequency liquid crystal molecules are aligned parallel to the substrate; in addition, since the ultraviolet polymerizable monomer has liquid crystallinity, The molecules of the monomer are also arranged parallel to the substrate. After the photoinitiator is initiated, the ultraviolet polymerizable monomer generates a polymer network, and the polymer network can fix the alignment direction of the long axi
- FIG. 2 is a schematic structural diagram of a liquid crystal panel of an ADS mode according to an embodiment of the present invention in an energized state, wherein a dual-frequency liquid crystal molecule exhibits dielectric integrity by using a low frequency electric field.
- a dual-frequency liquid crystal molecule exhibits dielectric integrity by using a low frequency electric field.
- an electric field is generated at the edge of the common electrode 6, and the double-frequency liquid crystal molecules are aligned in the tangential direction of the electric field lines, and the double-frequency liquid crystal molecules are rotated.
- the electric field since the polymer network has an anchoring effect on the liquid crystal molecules, the liquid crystal molecules return to the state before the energization under the action of the polymer network.
- Embodiments of the present invention also provide a display device including any one of the above liquid crystal panels.
- the display device may be: any product or component having a display function such as a liquid crystal panel, an electronic paper, an OLED panel, a liquid crystal television, a liquid crystal display, a digital photo frame, a mobile phone, a tablet computer, or the like.
- the display of the display device can be optimized by employing the above liquid crystal panel in the display device.
- Embodiments of the present invention also provide a method of fabricating a liquid crystal panel, including:
- a dual-frequency liquid crystal having a mass percentage of 90% to 98%, a UV polymerizable monomer having a liquid crystal content of 1 to 9% by mass, and a photoinitiator having a mass percentage of 0.1% to 1% are mixed in the dark Forming a mixture;
- the defoamed mixture is dropped onto the array substrate, the sealant is applied to the color filter substrate, and the liquid crystal cell is formed by vacuum-aligning the array substrate and the color filter substrate;
- the liquid crystal cell is irradiated with ultraviolet light to polymerize the ultraviolet polymerizable monomer having liquid crystallinity to form a polymer network;
- the liquid crystal cell irradiated with ultraviolet light is heated.
- the ultraviolet polymerizable monomer having liquid crystallinity in the liquid crystal layer is polymerized to form a polymer network capable of anchoring the dual-frequency liquid crystal molecules, the arrangement of the dual-frequency liquid crystal molecules can be unified. Therefore, the dual-frequency liquid crystal can be applied to the liquid crystal panel, and the display of the liquid crystal panel is optimized by the dual-frequency liquid crystal display by the low-frequency electric field and the processing of the dual-frequency liquid crystal by the high-frequency electric field.
- the dual-frequency liquid crystal may be a mixed crystal formed by mixing fluorine-containing double-frequency liquid crystal molecules.
- the fluorine-based double-frequency liquid crystal molecules may be selected from the liquid crystal layer of the liquid crystal panel.
- the photoinitiator may be selected from commonly used light.
- An initiator such as ⁇ , ⁇ -diethoxyacetophenone, ⁇ -hydroxyalkylphenone or ⁇ -aminoalkylbenzophenone.
- the photoinitiator is mixed in the dark to form a mixture, for example, it can be mixed by the following mass ratio: a dual-frequency liquid crystal having a mass percentage of 90%, and a liquid crystal violet having a mass percentage of 9%
- the outer polymerizable monomer and the photoinitiator having a mass percentage of 1% are mixed in a light-proof manner to form a mixture; or, a double-frequency liquid crystal having a mass percentage of 95%, a mass percentage of 4.9% of a liquid crystal polymerizable ultraviolet polymerizable a monomer, and a photoinitiator having a mass percentage of 0.1%, are mixed in a light-proof manner to form a mixture; or, a mass percentage of 98% of a dual-frequency liquid crystal, a mass percentage of
- the intensity of ultraviolet light irradiation is 1 to 80 mW/cm 2
- the irradiation time is 5 to 200 minutes.
- the mixture is defoamed, and the defoaming time is 1 to 3 hours.
- the method further includes: performing parallel alignment treatment on the array substrate and the color filter substrate, respectively. .
- Step 101 mixing eight kinds of fluorine-containing double-frequency liquid crystal molecules of the same mass to form a mixed liquid crystal
- Step 102 mixing a mixed liquid crystal, a liquid crystal polymerizable ultraviolet polymerizable monomer and a photoinitiator to form a mixture, wherein: the mass percentage of the mixed liquid crystal is 90 to 98%, and the mass percentage of the ultraviolet polymerizable monomer having liquid crystal property is 1 to 9%, the mass percentage of the photoinitiator is 0.1 to 1%; Step 103, the mixture is placed in a defoamer for defoaming treatment, and the defoaming time is 1 to 3 hours;
- Step 104 dropping the defoamed mixture onto the array substrate, applying the sealant to the color filter substrate, and forming the liquid crystal cell by aligning the array substrate and the color filter substrate under vacuum;
- step 105 Irradiating the liquid crystal cell with ultraviolet light to polymerize the ultraviolet polymerizable monomer having liquid crystallinity to form a polymer network, and also polymerizing the ultraviolet polymerizable monomer in the sealant;
- Step 106 Heating the liquid crystal cell irradiated with ultraviolet light to polymerize the thermal polymerization monomer in the sealant, thereby bonding the array substrate and the color filter substrate.
- the polymer network formed by polymerization of the ultraviolet polymerizable monomer having liquid crystallinity can anchor the arrangement of the dual-frequency liquid crystal molecules, thereby making the dual-frequency liquid crystal applicable.
- the LCD panel It has been found that the liquid crystal panel thus prepared has a display temperature ranging from -30 ° C to 80 ° C, so that the prepared liquid crystal panel can be used for display at a normal temperature.
- FIG. 3 is a polarizing microscope diagram of a liquid crystal layer of an ADS mode liquid crystal panel according to an embodiment of the present invention, and a visible ridge texture can be seen, which is unique to nematic liquid crystal.
- the liquid crystal layer has such a schlieren texture, indicating that the liquid crystal layer can be applied to liquid crystal display.
- 4 is a graph showing a relationship between a voltage and a transmittance of an ADS mode liquid crystal panel according to an embodiment of the present invention, which is a voltage and an ADS mode liquid crystal panel obtained by detecting a liquid crystal panel by a liquid crystal integrated tester. The graph of the over-rate, which is measured at a low frequency state.
- the maximum transmittance of the liquid crystal panel is close to 12%, and the driving voltage at this time is close to 16V; In the process, the transmittance of the liquid crystal panel is small, and as the driving voltage increases, the transmittance of the liquid crystal panel also increases.
- the transmittance of the liquid crystal panel After passing the peak, the transmittance of the liquid crystal panel is slightly reduced, and the power is removed. After the condition, the transmittance of the liquid crystal panel is also close to zero.
- the voltage and transmittance change process conforms to the voltage and transmittance relationship of the liquid crystal panel of the ADS mode, and is also described by the method provided by the embodiment of the present invention.
- the LCD panel can be applied to the ADS mode.
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WO2015122457A1 (ja) * | 2014-02-14 | 2015-08-20 | Dic株式会社 | 液晶表示素子 |
CN104130782B (zh) * | 2014-07-17 | 2016-02-17 | 北京大学 | 一种具有低临界频率的双频液晶材料 |
CN104317093A (zh) * | 2014-11-20 | 2015-01-28 | 京东方科技集团股份有限公司 | 液晶显示装置及其制造方法 |
JP6260747B2 (ja) * | 2015-08-11 | 2018-01-17 | Dic株式会社 | 液晶表示素子 |
CN106886102A (zh) * | 2017-03-24 | 2017-06-23 | 北京大学 | 一种反式电控液晶调光膜及其制备方法 |
CN107272283A (zh) * | 2017-08-20 | 2017-10-20 | 芜湖乐普汽车科技有限公司 | 一种车载显示器的镜面控制液晶盒 |
CN110780503B (zh) * | 2019-11-19 | 2022-07-05 | 华南师范大学 | 一种可变色智能窗 |
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